Figure 4
Plots for the compound TIBCAJ. (a) The variation of Friedifstat with sin θ/λ for the radiations Cr Kα, Cu Kα and Mo Kα. The polynomial representation of Friedifstat for Mo Kα is Friedifstat = 2072.2(sin θ/λ)3 − 434.19(sin θ/λ)2 − 23.951 sin θ/λ + 1269.1. (b) A scatter plot of normalized log Aobs versus (sin θ/λ)2. (c) A scatter plot of Dobs versus (sin θ/λ)2. (d) A similar scatter plot of Dobs values normalized according to the procedure applied to the values of Aobs. (e) The scatter plot of Dobs values further adjusted to allow for the variation of Friedifstat with sin θ/λ. |