Acta Crystallographica Section B

Structural Science

Volume 53, Part 4 (August 1997)

research papers

Acta Cryst. (1997). B53, 719-725    [doi:10.1107/S0108768197004874]

Conformation-Related Reaction Efficiency of Glutarimides with Phenyllithium. Structures of 3,3,5,5-Tetramethylglutarimide and 2-Hydroxy-2-phenyl-3,3,5,5-tetramethyl-6-piperidone. X-ray and Theoretical Study

J. K. Maurin, Z. Czarnocki, B. Paluchowska and M. Winnicka-Maurin

Synopsis: Crystallographic and ab initio studies have clarified the reason for yield variations in the reaction of differently substituted glutarimides with phenyllithium. It has been shown that conformational changes in glutarimide, introduced by substitution, resulted in electron charge distribution changes.

	Structure factor file (CIF format) (92.6 kbytes) Contains datablock 8
	Structure factor file (CIF format) (109.1 kbytes) Contains datablock 9

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