Acta Crystallographica Section B

Structural Science

Volume 54, Part 2 (April 1998)

research papers

Acta Cryst. (1998). B54, 139-150    [doi:10.1107/S0108768197010136]

Crystal Engineering Using Bis- and Tris-phenols. Adducts with 1,4,8,11-Tetraazacyclotetradecane (Cyclam): Isolated Ladders in the Adduct with 4,4'-Thiodiphenol, Tethered Ladders in the Adduct with 4,4'-Sulfonyldiphenol and Two Interwoven Three-Dimensional Networks in the Adduct with 1,1,1-Tris(4-hydroxyphenyl)ethane

G. Ferguson, C. Glidewell, R. M. Gregson and P. R. Meehan

Synopsis: The 2:1 adducts formed between 4,4'-thiodiphenol or 4,4'-sulfonyldiphenol with cyclam take the form of supramolecular ladders, with chains of diphenol anions forming the uprights and [cyclamH₂]²⁺ cations the rungs; with CH₃C(C₆H₄OH)₃, cyclam forms a three-dimensional interwoven structure without void spaces.

	Structure factor file (CIF format) (183.4 kbytes) Contains datablock 1
	Structure factor file (CIF format) (288.6 kbytes) Contains datablock 2
	Structure factor file (CIF format) (396.6 kbytes) Contains datablock 3

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