# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_1 _shelx_title ' 04src0430 in Pnma' _shelx_refln_list_code 4 _shelx_F_calc_maximum 212.27 _exptl_crystal_F_000 672.00 _reflns_d_resolution_high 0.7698 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' _cell_length_a 13.8572 _cell_length_b 12.8086 _cell_length_c 6.0801 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5643.75 4800.63 268.05 o 4 0 0 25195.58 11265.10 806.80 o 6 0 0 4117.27 3511.07 46.97 o 8 0 0 13871.09 14625.56 266.65 o 10 0 0 21527.63 23393.80 329.62 o 12 0 0 11563.30 11978.13 199.90 o 14 0 0 2815.89 3002.69 70.48 o 16 0 0 14.72 12.49 3.33 o 18 0 0 383.61 392.03 34.38 o 2 1 0 1136.07 1092.13 38.85 o 4 1 0 214.62 197.63 2.50 o 6 1 0 3995.05 4115.34 35.92 o 8 1 0 1566.93 1584.80 17.13 o 10 1 0 216.08 199.16 3.62 o 12 1 0 112.87 121.12 3.13 o 14 1 0 3667.63 3729.35 56.48 o 16 1 0 187.51 167.34 7.48 o 2 2 0 2793.75 2668.01 57.48 o 4 2 0 261.56 248.49 3.21 o 6 2 0 702.24 637.16 6.61 o 8 2 0 682.21 670.77 7.13 o 10 2 0 50.85 58.94 2.15 o 12 2 0 834.00 876.25 13.06 o 14 2 0 21.11 20.42 3.23 o 16 2 0 27.39 30.17 3.42 o 4 3 0 2845.60 2636.37 22.18 o 6 3 0 2888.22 2901.83 25.21 o 8 3 0 12083.65 12528.83 157.92 o 10 3 0 15179.29 15940.32 188.19 o 12 3 0 6943.44 7206.78 92.10 o 14 3 0 31.32 29.12 2.38 o 16 3 0 222.47 201.92 7.22 o 0 4 0 4118.23 3874.16 81.49 o 2 4 0 7636.80 8470.33 107.28 o 4 4 0 465.65 639.51 7.81 o 6 4 0 3046.23 2983.59 29.57 o 8 4 0 6994.91 7103.30 83.15 o 10 4 0 2152.19 2103.58 27.21 o 12 4 0 1124.80 1119.29 17.85 o 14 4 0 313.84 306.87 15.90 o 16 4 0 3239.73 3528.45 155.32 o 2 5 0 541.02 446.99 7.16 o 4 5 0 9046.68 9855.58 101.84 o 6 5 0 1119.82 1048.82 10.60 o 8 5 0 4797.28 4859.95 46.96 o 10 5 0 418.92 409.21 7.80 o 12 5 0 135.19 118.04 4.42 o 14 5 0 89.06 85.26 6.12 o 16 5 0 826.38 876.16 36.91 o 0 6 0 24975.62 29283.07 501.69 o 2 6 0 178.87 245.77 5.77 o 4 6 0 3319.42 3725.45 37.52 o 6 6 0 1026.38 1046.71 13.02 o 8 6 0 8386.40 8550.84 69.69 o 10 6 0 43.92 53.46 4.34 o 12 6 0 123.33 120.82 4.98 o 14 6 0 20.87 19.31 3.54 o 16 6 0 910.33 900.30 72.27 o 2 7 0 12982.30 13278.30 172.08 o 4 7 0 793.49 807.96 14.46 o 6 7 0 3084.34 3181.84 32.64 o 8 7 0 266.24 265.97 5.31 o 10 7 0 4348.66 4472.94 65.53 o 12 7 0 2612.27 2642.20 58.19 o 14 7 0 861.68 844.89 40.97 o 16 7 0 805.88 818.99 57.27 o 0 8 0 2001.28 1946.25 35.83 o 2 8 0 1449.71 1454.16 17.31 o 4 8 0 142.06 169.87 4.38 o 6 8 0 341.92 377.13 6.90 o 8 8 0 699.38 664.06 11.97 o 10 8 0 17.81 20.91 2.88 o 12 8 0 185.37 165.51 9.93 o 14 8 0 6.26 2.67 5.25 o 2 9 0 578.33 633.37 10.40 o 4 9 0 1295.12 1225.43 15.08 o 6 9 0 1776.70 1683.14 23.12 o 8 9 0 63.94 63.02 3.95 o 10 9 0 223.24 217.29 8.84 o 12 9 0 105.64 107.57 16.30 o 14 9 0 775.08 831.68 47.52 o 0 10 0 45058.75 55888.99 1371.96 o 2 10 0 136.80 150.08 4.63 o 4 10 0 3136.16 3086.68 48.13 o 6 10 0 124.54 130.12 5.00 o 8 10 0 4009.70 4308.88 77.08 o 10 10 0 5320.25 5665.86 131.25 o 12 10 0 2395.80 2462.01 111.26 o 14 10 0 1459.40 1509.56 107.62 o 2 11 0 488.23 456.50 10.62 o 4 11 0 364.57 378.97 9.44 o 6 11 0 753.12 698.10 16.69 o 8 11 0 1253.52 1213.85 37.22 o 10 11 0 171.43 165.12 10.03 o 12 11 0 57.11 51.28 10.04 o 0 12 0 1656.12 1708.18 58.15 o 2 12 0 1077.49 1084.76 21.98 o 4 12 0 356.05 346.75 10.70 o 6 12 0 2256.53 2347.68 81.54 o 8 12 0 55.26 45.52 6.28 o 10 12 0 6.86 5.60 11.98 o 12 12 0 14.27 4.50 8.14 o 2 13 0 10300.42 11536.03 362.78 o 4 13 0 451.62 491.19 18.58 o 6 13 0 445.16 432.41 19.23 o 8 13 0 2848.32 3029.79 134.40 o 10 13 0 3262.46 3433.85 167.11 o 0 14 0 250.81 234.46 20.37 o 2 14 0 1717.15 1873.62 81.97 o 4 14 0 243.96 219.61 14.77 o 6 14 0 2989.78 3201.56 166.81 o 8 14 0 1047.24 1038.24 51.04 o 2 15 0 1388.41 1479.94 79.36 o 4 15 0 4040.43 4428.08 262.07 o 6 15 0 194.98 174.05 14.27 o 0 16 0 2941.18 3135.60 220.61 o 2 16 0 4.94 2.07 7.42 o 4 16 0 230.51 187.63 35.23 o 1 0 1 19132.49 7686.50 576.19 o 2 0 1 13110.10 4923.41 494.43 o 3 0 1 8677.33 8912.35 124.64 o 6 0 1 2673.57 2650.69 24.43 o 7 0 1 12.57 -0.37 0.67 o 8 0 1 7729.82 7944.87 99.82 o 9 0 1 1847.10 1809.78 21.82 o 10 0 1 73.61 63.28 3.12 o 11 0 1 4626.30 4498.16 58.91 o 12 0 1 464.86 451.37 8.26 o 13 0 1 934.31 1010.35 19.26 o 14 0 1 2236.39 2308.48 34.97 o 15 0 1 142.15 136.96 4.64 o 16 0 1 465.80 457.92 15.18 o 17 0 1 1055.04 1029.55 68.16 o 0 1 1 25.99 13.61 1.03 o 1 1 1 995.93 966.16 8.13 o 2 1 1 204.24 198.18 2.17 o 3 1 1 4173.16 4131.74 44.92 o 4 1 1 1255.92 1299.29 11.82 o 5 1 1 2123.31 2122.56 18.71 o 6 1 1 475.65 482.96 4.72 o 7 1 1 9247.85 9699.45 81.12 o 8 1 1 16.65 19.64 0.78 o 9 1 1 83.21 76.45 1.63 o 10 1 1 322.10 345.63 3.56 o 11 1 1 862.58 849.81 7.49 o 12 1 1 366.43 369.67 4.10 o 13 1 1 2703.59 2733.30 31.23 o 14 1 1 1.08 0.88 1.43 o 15 1 1 427.79 405.06 9.80 o 16 1 1 717.14 734.12 17.38 o 17 1 1 2411.49 2529.72 85.01 o 1 2 1 3743.72 3772.04 25.53 o 2 2 1 2090.68 2083.03 14.93 o 3 2 1 1157.63 1091.76 9.15 o 4 2 1 1431.32 1421.80 12.16 o 5 2 1 290.51 248.18 2.89 o 6 2 1 195.55 169.80 3.07 o 7 2 1 1101.34 1008.55 9.75 o 8 2 1 774.82 756.15 6.83 o 9 2 1 510.16 488.31 4.43 o 10 2 1 41.58 40.92 1.23 o 11 2 1 84.73 88.94 2.06 o 12 2 1 35.29 35.81 1.86 o 13 2 1 763.92 751.21 9.70 o 14 2 1 396.03 412.74 6.37 o 15 2 1 860.33 830.97 15.78 o 16 2 1 605.05 573.33 18.87 o 17 2 1 64.05 54.08 6.46 o 0 3 1 4514.39 4303.64 40.08 o 1 3 1 4762.91 4638.63 33.18 o 2 3 1 12880.09 14243.85 100.38 o 3 3 1 5234.22 5526.40 37.74 o 4 3 1 3008.40 2919.92 23.46 o 5 3 1 302.60 306.46 3.13 o 6 3 1 21255.88 24418.49 199.14 o 7 3 1 11511.37 12175.69 72.94 o 8 3 1 10.19 5.99 0.88 o 9 3 1 2158.85 2136.95 19.32 o 10 3 1 252.54 244.82 5.90 o 11 3 1 4.82 3.52 1.23 o 12 3 1 596.72 617.87 8.24 o 13 3 1 9.44 13.46 1.40 o 14 3 1 546.33 526.43 8.99 o 15 3 1 3682.72 3777.44 75.63 o 16 3 1 968.93 1001.55 35.26 o 17 3 1 690.00 727.49 32.47 o 1 4 1 2070.02 2065.89 16.24 o 2 4 1 191.36 153.08 2.04 o 3 4 1 3952.98 4269.29 31.46 o 4 4 1 862.78 778.28 6.12 o 5 4 1 10382.50 10513.36 65.13 o 6 4 1 21.08 24.08 1.06 o 7 4 1 274.12 267.37 3.08 o 8 4 1 215.60 217.38 2.74 o 9 4 1 11990.63 12420.32 105.93 o 10 4 1 306.72 317.65 4.18 o 11 4 1 1550.09 1490.45 15.51 o 12 4 1 1346.37 1397.69 15.99 o 13 4 1 288.90 285.87 5.13 o 14 4 1 360.16 367.30 8.77 o 15 4 1 2604.69 2719.11 62.52 o 16 4 1 11.02 12.15 3.37 o 17 4 1 1230.54 1225.89 56.09 o 0 5 1 1305.19 1186.42 13.56 o 1 5 1 166.57 125.84 2.88 o 2 5 1 802.03 805.89 6.70 o 3 5 1 8330.81 8457.43 56.52 o 4 5 1 194.08 201.67 3.05 o 5 5 1 4856.23 4972.37 32.53 o 6 5 1 162.87 136.16 2.16 o 7 5 1 3027.93 2954.54 22.11 o 8 5 1 885.98 898.93 7.86 o 9 5 1 3467.72 3500.25 26.99 o 10 5 1 30.27 33.35 1.82 o 11 5 1 318.88 327.36 4.75 o 12 5 1 106.02 99.05 2.90 o 13 5 1 0.02 0.39 1.45 o 14 5 1 1341.48 1309.46 22.83 o 15 5 1 354.30 368.03 8.26 o 16 5 1 209.42 212.47 9.34 o 17 5 1 43.83 47.90 7.60 o 1 6 1 3426.81 3537.54 25.89 o 2 6 1 2840.63 2926.04 21.33 o 3 6 1 1643.73 1870.38 14.28 o 4 6 1 6107.82 6317.32 42.30 o 5 6 1 12785.68 13286.88 82.24 o 6 6 1 126.20 126.18 3.21 o 7 6 1 38.23 54.74 2.44 o 8 6 1 802.71 813.85 8.33 o 9 6 1 7542.83 7587.05 64.23 o 10 6 1 310.49 313.71 4.37 o 11 6 1 2293.40 2282.10 28.77 o 12 6 1 695.09 665.93 12.05 o 13 6 1 887.43 887.64 15.17 o 14 6 1 189.42 180.14 5.45 o 15 6 1 2486.60 2573.10 54.23 o 16 6 1 71.34 59.27 6.00 o 0 7 1 176.19 190.99 6.24 o 1 7 1 2954.22 2879.29 22.00 o 2 7 1 2631.78 2538.64 18.39 o 3 7 1 954.12 932.84 7.54 o 4 7 1 6.24 7.70 1.73 o 5 7 1 8.43 6.75 1.26 o 6 7 1 3597.65 3598.70 29.63 o 7 7 1 7508.27 7726.37 56.28 o 8 7 1 298.72 314.97 4.34 o 9 7 1 1910.33 1963.75 20.59 o 10 7 1 98.72 102.38 2.80 o 11 7 1 190.81 183.53 4.47 o 12 7 1 99.58 91.63 4.04 o 13 7 1 2.49 7.41 2.65 o 14 7 1 331.94 309.38 14.14 o 15 7 1 1977.65 1899.76 64.66 o 16 7 1 69.80 67.58 8.06 o 1 8 1 4923.33 4984.54 33.75 o 2 8 1 413.16 426.86 5.16 o 3 8 1 421.85 410.11 4.62 o 4 8 1 631.98 631.90 6.86 o 5 8 1 1449.70 1472.87 12.58 o 6 8 1 115.81 116.09 2.65 o 7 8 1 1279.65 1359.90 12.27 o 8 8 1 417.85 400.65 6.96 o 9 8 1 14.16 16.83 2.18 o 10 8 1 0.44 1.20 1.75 o 11 8 1 317.90 327.94 7.34 o 12 8 1 68.63 60.09 3.65 o 13 8 1 1007.14 978.26 28.21 o 14 8 1 355.79 358.43 18.08 o 15 8 1 114.56 93.99 8.95 o 0 9 1 2230.37 2258.86 27.59 o 1 9 1 1763.22 1716.53 16.95 o 2 9 1 867.27 869.60 8.83 o 3 9 1 6191.76 6435.47 49.64 o 4 9 1 28.82 35.48 2.15 o 5 9 1 190.12 147.63 4.01 o 6 9 1 539.84 556.89 6.95 o 7 9 1 7131.67 7352.26 75.10 o 8 9 1 387.73 388.52 6.13 o 9 9 1 1607.62 1651.92 22.46 o 10 9 1 0.75 1.81 2.62 o 11 9 1 120.96 125.64 6.39 o 12 9 1 242.84 233.54 8.88 o 13 9 1 3617.92 3877.55 109.48 o 14 9 1 51.53 38.81 6.57 o 1 10 1 5685.08 5913.29 53.84 o 2 10 1 555.00 524.40 8.77 o 3 10 1 2008.97 1993.34 25.26 o 4 10 1 5852.01 6062.47 61.28 o 5 10 1 1522.77 1557.86 18.18 o 6 10 1 528.95 530.74 8.21 o 7 10 1 509.50 559.59 8.68 o 8 10 1 1013.49 1007.59 16.06 o 9 10 1 589.40 595.47 11.52 o 10 10 1 72.70 66.26 6.38 o 11 10 1 3072.21 3283.23 74.70 o 12 10 1 363.03 344.27 13.39 o 13 10 1 175.37 163.99 11.05 o 14 10 1 335.09 331.52 31.95 o 0 11 1 363.66 371.71 8.13 o 1 11 1 18.39 20.78 2.22 o 2 11 1 19.29 13.49 2.33 o 3 11 1 2.54 4.56 2.29 o 4 11 1 532.89 513.97 12.59 o 5 11 1 682.33 671.19 10.73 o 6 11 1 485.06 484.09 11.37 o 7 11 1 1240.89 1173.51 22.62 o 8 11 1 0.27 2.36 2.83 o 9 11 1 154.52 157.68 6.18 o 10 11 1 244.08 229.70 8.22 o 11 11 1 571.06 594.39 19.13 o 12 11 1 588.98 556.55 21.55 o 13 11 1 282.51 259.28 12.88 o 1 12 1 337.23 352.26 6.84 o 2 12 1 2005.81 2079.10 29.23 o 3 12 1 295.83 279.44 6.28 o 4 12 1 135.34 135.37 4.83 o 5 12 1 448.89 446.54 11.62 o 6 12 1 61.13 54.60 4.42 o 7 12 1 7.13 4.68 3.17 o 8 12 1 34.95 36.10 4.30 o 9 12 1 523.90 525.02 20.04 o 10 12 1 606.36 577.99 20.48 o 11 12 1 1432.87 1433.40 49.02 o 12 12 1 4.91 -1.43 4.98 o 0 13 1 313.55 326.32 11.80 o 1 13 1 1656.45 1700.31 35.82 o 2 13 1 1352.39 1457.42 30.12 o 3 13 1 23.32 32.08 3.73 o 4 13 1 374.96 398.08 11.74 o 5 13 1 4.71 4.34 3.59 o 6 13 1 3161.35 3383.50 97.11 o 7 13 1 755.89 706.95 21.32 o 8 13 1 8.63 12.57 4.42 o 9 13 1 1814.57 1871.79 58.41 o 10 13 1 5.10 16.50 5.87 o 11 13 1 0.74 -1.50 7.65 o 1 14 1 43.14 30.75 6.00 o 2 14 1 764.46 782.71 26.43 o 3 14 1 375.26 382.30 13.98 o 4 14 1 39.16 33.62 4.89 o 5 14 1 1174.88 1221.41 56.94 o 6 14 1 18.78 11.88 6.52 o 7 14 1 178.74 179.65 10.18 o 8 14 1 534.71 533.90 21.41 o 9 14 1 3131.59 3259.25 142.44 o 0 15 1 1753.77 1806.27 104.78 o 1 15 1 9.78 8.96 5.06 o 2 15 1 15.16 20.40 5.43 o 3 15 1 408.38 403.18 17.36 o 4 15 1 303.10 278.76 17.59 o 5 15 1 438.66 442.57 26.28 o 6 15 1 271.04 243.94 13.18 o 7 15 1 235.50 207.26 16.64 o 1 16 1 24.22 18.76 6.36 o 2 16 1 316.67 308.80 17.19 o 3 16 1 100.33 80.52 10.15 o 4 16 1 753.40 682.80 40.27 o 1 0 2 15707.75 17374.86 174.72 o 2 0 2 19.15 21.27 1.92 o 3 0 2 61.44 37.27 1.96 o 4 0 2 688.55 560.79 7.56 o 5 0 2 2541.26 2519.99 39.93 o 6 0 2 246.39 325.03 20.04 o 7 0 2 1227.36 1284.48 19.21 o 8 0 2 166.46 130.61 6.43 o 9 0 2 8593.70 9067.79 186.82 o 10 0 2 4626.52 4600.89 68.78 o 11 0 2 325.45 316.79 23.94 o 12 0 2 450.40 392.11 15.11 o 13 0 2 3873.02 3976.07 124.14 o 14 0 2 1271.08 1359.30 42.89 o 15 0 2 767.57 789.87 24.57 o 16 0 2 10.90 9.08 5.29 o 17 0 2 741.52 690.78 47.90 o 1 1 2 135.33 142.39 1.94 o 2 1 2 316.34 325.82 2.97 o 3 1 2 4524.18 4829.06 39.57 o 4 1 2 420.38 388.97 4.79 o 5 1 2 2069.21 2221.41 29.97 o 6 1 2 1293.02 1277.71 16.20 o 7 1 2 477.76 473.36 7.01 o 8 1 2 147.34 141.84 4.25 o 9 1 2 2764.48 2855.90 33.13 o 10 1 2 93.33 92.29 6.96 o 11 1 2 589.35 631.50 11.25 o 12 1 2 74.78 77.53 4.79 o 13 1 2 587.37 612.26 11.67 o 14 1 2 480.11 490.23 20.65 o 15 1 2 2019.04 2090.24 39.04 o 16 1 2 22.77 14.49 4.45 o 17 1 2 879.56 845.94 32.81 o 0 2 2 11321.37 12785.22 102.14 o 1 2 2 7071.92 7496.64 48.15 o 2 2 2 291.35 343.91 3.19 o 3 2 2 3269.23 3171.89 23.69 o 4 2 2 1193.88 1164.13 18.48 o 5 2 2 421.85 383.57 4.81 o 6 2 2 679.66 644.38 6.18 o 7 2 2 2313.38 2309.23 32.83 o 8 2 2 288.60 274.95 4.09 o 9 2 2 1951.27 1951.92 21.48 o 10 2 2 1154.98 1145.58 16.59 o 11 2 2 2533.27 2563.19 30.21 o 12 2 2 300.16 275.97 6.81 o 13 2 2 0.18 6.79 2.80 o 14 2 2 82.21 81.33 5.53 o 15 2 2 1.83 -0.11 4.07 o 16 2 2 4.32 6.13 6.09 o 17 2 2 336.98 342.57 16.89 o 1 3 2 10481.83 11652.82 64.70 o 2 3 2 3005.13 2806.37 17.59 o 3 3 2 13095.00 14380.78 81.98 o 4 3 2 910.77 969.56 7.79 o 5 3 2 186.52 174.60 2.68 o 6 3 2 215.32 217.49 5.14 o 7 3 2 267.18 248.36 3.26 o 8 3 2 427.21 385.53 3.97 o 9 3 2 79.75 76.91 1.49 o 10 3 2 387.85 342.23 4.55 o 11 3 2 9326.58 9899.42 101.33 o 12 3 2 1703.04 1733.05 29.07 o 13 3 2 189.67 187.31 8.14 o 14 3 2 253.08 260.15 9.16 o 15 3 2 392.69 408.92 17.01 o 16 3 2 273.95 267.65 10.46 o 17 3 2 103.12 110.25 9.26 o 0 4 2 110.75 95.00 3.20 o 1 4 2 3455.38 3193.56 18.91 o 2 4 2 2775.08 2916.05 18.59 o 3 4 2 109.89 107.90 1.76 o 4 4 2 37.79 49.50 1.45 o 5 4 2 1492.42 1439.05 10.35 o 6 4 2 793.05 756.21 6.63 o 7 4 2 690.82 674.13 6.17 o 8 4 2 1977.24 1932.46 15.69 o 9 4 2 2325.02 2361.90 19.80 o 10 4 2 292.23 269.58 4.42 o 11 4 2 2749.28 2849.72 32.40 o 12 4 2 331.63 321.85 5.08 o 13 4 2 5652.35 5861.01 135.06 o 14 4 2 80.54 76.37 3.33 o 15 4 2 76.00 71.50 7.83 o 16 4 2 832.73 843.90 26.69 o 1 5 2 8159.08 8191.99 47.46 o 2 5 2 8421.16 8753.12 48.53 o 3 5 2 1636.16 1627.76 10.67 o 4 5 2 2593.11 2641.73 17.44 o 5 5 2 1756.74 1762.19 14.16 o 6 5 2 308.06 282.43 3.39 o 7 5 2 9008.41 9533.84 64.61 o 8 5 2 5478.10 5473.81 44.25 o 9 5 2 2199.37 2189.68 18.40 o 10 5 2 1142.22 1099.80 12.52 o 11 5 2 3344.80 3497.31 38.75 o 12 5 2 1374.65 1401.60 18.16 o 13 5 2 56.32 56.10 2.58 o 14 5 2 359.55 326.43 9.57 o 15 5 2 71.21 70.35 6.08 o 16 5 2 55.31 62.49 7.55 o 0 6 2 3.33 16.42 2.23 o 1 6 2 5894.90 5982.32 32.27 o 2 6 2 1955.75 2095.85 13.13 o 3 6 2 3828.74 3858.65 24.72 o 4 6 2 20.73 15.13 1.17 o 5 6 2 44.50 42.55 1.50 o 6 6 2 1250.59 1284.11 10.53 o 7 6 2 2533.01 2485.53 17.71 o 8 6 2 805.32 737.49 7.40 o 9 6 2 7056.16 7213.38 65.13 o 10 6 2 185.49 163.91 3.18 o 11 6 2 1480.98 1497.74 18.16 o 12 6 2 533.27 508.87 9.48 o 13 6 2 6027.89 6382.15 122.70 o 14 6 2 123.37 113.19 5.68 o 15 6 2 184.24 177.30 10.23 o 16 6 2 682.15 683.76 33.82 o 1 7 2 882.84 895.92 8.27 o 2 7 2 1578.70 1576.91 11.78 o 3 7 2 7982.51 8187.80 54.09 o 4 7 2 409.06 405.27 5.31 o 5 7 2 1317.14 1361.61 10.50 o 6 7 2 346.85 339.29 4.25 o 7 7 2 184.25 179.92 3.09 o 8 7 2 111.24 115.94 2.76 o 9 7 2 12.69 9.96 1.87 o 10 7 2 405.92 394.16 5.77 o 11 7 2 3812.83 3899.00 60.53 o 12 7 2 818.38 796.10 16.06 o 13 7 2 824.24 838.85 19.37 o 14 7 2 205.09 194.02 6.50 o 15 7 2 594.48 564.20 19.89 o 0 8 2 8310.93 8684.98 77.05 o 1 8 2 4581.81 4680.69 26.42 o 2 8 2 579.49 573.57 5.77 o 3 8 2 4655.27 4721.70 34.25 o 4 8 2 1091.85 1094.79 9.70 o 5 8 2 805.13 829.91 7.87 o 6 8 2 1084.26 1053.01 12.11 o 7 8 2 232.49 240.55 6.11 o 8 8 2 134.49 133.62 2.89 o 9 8 2 3126.35 3279.31 38.69 o 10 8 2 1720.77 1746.64 27.29 o 11 8 2 1249.65 1275.10 23.49 o 12 8 2 743.66 737.65 16.05 o 13 8 2 165.40 170.26 7.11 o 14 8 2 79.37 74.10 6.41 o 15 8 2 132.38 110.57 12.78 o 1 9 2 1982.92 2047.18 15.52 o 2 9 2 422.54 413.57 6.42 o 3 9 2 1460.91 1395.73 12.18 o 4 9 2 1027.52 1112.92 10.89 o 5 9 2 6523.54 6770.57 57.89 o 6 9 2 785.12 729.20 8.87 o 7 9 2 902.96 931.18 12.88 o 8 9 2 910.76 923.34 13.10 o 9 9 2 2520.56 2600.42 41.26 o 10 9 2 64.89 69.60 3.27 o 11 9 2 2702.15 2735.56 66.56 o 12 9 2 3.82 -0.59 3.77 o 13 9 2 2.48 0.68 5.56 o 14 9 2 809.89 818.63 38.37 o 0 10 2 7180.29 7516.15 92.09 o 1 10 2 1534.44 1544.60 16.09 o 2 10 2 27.19 26.89 2.35 o 3 10 2 1750.53 1801.64 17.68 o 4 10 2 474.87 463.00 6.95 o 5 10 2 1871.57 1927.19 24.80 o 6 10 2 11.06 7.41 2.25 o 7 10 2 1501.62 1527.81 21.13 o 8 10 2 144.91 153.51 4.72 o 9 10 2 1146.74 1102.90 20.72 o 10 10 2 2074.22 2142.06 60.94 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991.45 979.23 10.36 o 8 5 3 1811.88 1800.50 17.07 o 9 5 3 60.50 60.76 2.58 o 10 5 3 1582.45 1632.85 19.74 o 11 5 3 645.75 642.45 11.36 o 12 5 3 290.34 281.66 8.11 o 13 5 3 388.17 358.76 11.49 o 14 5 3 2050.54 2034.54 60.03 o 15 5 3 1146.80 1178.45 37.50 o 1 6 3 184.30 178.06 3.96 o 2 6 3 101.98 92.01 2.30 o 3 6 3 236.30 245.88 3.58 o 4 6 3 3402.93 3343.30 21.66 o 5 6 3 286.94 285.90 4.10 o 6 6 3 240.57 235.10 3.60 o 7 6 3 670.32 623.54 7.48 o 8 6 3 0.51 3.32 1.32 o 9 6 3 0.11 2.56 2.00 o 10 6 3 41.50 41.37 1.84 o 11 6 3 590.49 609.34 11.25 o 12 6 3 2142.79 2172.93 43.01 o 13 6 3 63.11 62.17 6.09 o 14 6 3 4.01 3.54 6.11 o 15 6 3 1.16 5.41 6.14 o 0 7 3 444.08 430.31 8.66 o 1 7 3 13.13 11.63 1.51 o 2 7 3 4396.17 4474.79 28.31 o 3 7 3 88.20 89.47 2.59 o 4 7 3 62.85 70.36 2.36 o 5 7 3 36.04 32.09 1.97 o 6 7 3 6404.88 6659.01 66.14 o 7 7 3 76.43 74.96 2.50 o 8 7 3 1126.44 1154.03 13.26 o 9 7 3 0.47 2.69 1.63 o 10 7 3 191.60 198.88 4.39 o 11 7 3 153.39 153.35 4.87 o 12 7 3 188.47 176.60 6.75 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67.80 3.65 o 8 10 3 1998.88 2068.22 46.59 o 9 10 3 808.23 790.19 24.00 o 10 10 3 376.30 339.02 14.21 o 11 10 3 475.85 477.90 21.42 o 12 10 3 284.35 284.91 16.71 o 0 11 3 14.45 10.90 3.57 o 1 11 3 96.53 96.18 4.10 o 2 11 3 336.23 325.14 7.76 o 3 11 3 3363.82 3589.77 57.50 o 4 11 3 201.37 175.48 5.96 o 5 11 3 925.19 988.89 21.02 o 6 11 3 40.20 41.09 4.41 o 7 11 3 1296.24 1317.48 34.79 o 8 11 3 4.01 7.19 4.23 o 9 11 3 512.46 523.98 16.94 o 10 11 3 70.99 70.43 7.86 o 11 11 3 323.66 280.13 15.18 o 1 12 3 139.23 137.18 5.42 o 2 12 3 1748.46 1762.90 32.47 o 3 12 3 599.12 591.98 15.26 o 4 12 3 77.36 72.20 4.73 o 5 12 3 79.56 68.00 4.73 o 6 12 3 43.58 45.76 6.11 o 7 12 3 70.89 63.47 7.10 o 8 12 3 1.10 0.17 4.62 o 9 12 3 18.62 23.87 9.99 o 10 12 3 384.35 350.28 24.43 o 0 13 3 167.68 140.24 11.65 o 1 13 3 105.01 93.79 7.73 o 2 13 3 1896.95 1948.90 49.79 o 3 13 3 417.01 384.64 14.81 o 4 13 3 831.74 820.43 26.00 o 5 13 3 6.49 7.49 4.85 o 6 13 3 5151.19 5712.95 175.40 o 7 13 3 579.68 550.16 19.73 o 8 13 3 166.68 157.20 10.44 o 1 14 3 2048.26 2140.75 73.09 o 2 14 3 612.51 609.13 25.62 o 3 14 3 33.79 32.24 6.32 o 4 14 3 117.66 115.73 8.06 o 5 14 3 1565.21 1645.66 51.47 o 6 14 3 4.21 -4.00 7.64 o 0 15 3 2823.60 2928.47 146.24 o 1 15 3 614.50 592.45 22.61 o 2 15 3 62.54 66.02 8.81 o 3 15 3 26.98 14.70 8.27 o 0 0 4 17104.01 18447.49 267.15 o 1 0 4 5.56 5.19 2.24 o 2 0 4 129.62 124.62 3.75 o 3 0 4 10155.00 10951.30 123.00 o 4 0 4 2102.84 2065.98 20.77 o 5 0 4 2965.67 3006.85 33.94 o 6 0 4 648.53 622.89 8.55 o 7 0 4 4867.66 4874.62 112.32 o 8 0 4 3886.38 3922.50 113.89 o 9 0 4 170.61 133.86 8.75 o 10 0 4 130.68 136.47 9.63 o 11 0 4 651.58 637.90 34.05 o 12 0 4 1224.13 1175.14 55.46 o 13 0 4 199.26 215.85 19.10 o 14 0 4 73.36 66.40 10.81 o 15 0 4 3514.98 3781.88 208.36 o 1 1 4 3643.75 3677.70 26.55 o 2 1 4 85.87 85.94 2.26 o 3 1 4 3799.44 3903.49 23.97 o 4 1 4 2084.96 2100.10 16.20 o 5 1 4 4847.02 4936.84 37.69 o 6 1 4 23.34 22.13 1.24 o 7 1 4 1457.12 1417.52 15.31 o 8 1 4 15.92 0.78 3.70 o 9 1 4 1033.22 1072.73 20.39 o 10 1 4 181.55 169.57 9.41 o 11 1 4 3699.96 3872.49 75.66 o 12 1 4 492.21 504.53 21.93 o 13 1 4 225.02 218.51 12.14 o 14 1 4 154.98 149.49 12.91 o 15 1 4 1859.57 1891.81 58.76 o 0 2 4 1558.34 1560.89 14.02 o 1 2 4 383.68 368.80 4.13 o 2 2 4 1703.28 1689.18 11.85 o 3 2 4 464.05 440.35 4.69 o 4 2 4 33.86 38.52 1.95 o 5 2 4 0.04 1.83 1.06 o 6 2 4 1026.92 991.94 12.90 o 7 2 4 634.39 613.90 7.63 o 8 2 4 1170.83 1201.73 18.86 o 9 2 4 767.55 763.48 14.15 o 10 2 4 1673.64 1644.97 26.73 o 11 2 4 267.41 269.08 9.95 o 12 2 4 767.80 815.69 26.19 o 13 2 4 454.80 461.28 18.50 o 14 2 4 622.65 659.94 21.84 o 15 2 4 0.72 -4.51 6.28 o 1 3 4 185.35 179.91 2.74 o 2 3 4 7132.17 7256.59 50.95 o 3 3 4 2141.32 2230.87 14.85 o 4 3 4 1464.70 1461.59 11.18 o 5 3 4 5496.53 5530.29 46.69 o 6 3 4 574.96 583.44 6.41 o 7 3 4 1254.73 1217.22 19.29 o 8 3 4 835.18 835.31 10.63 o 9 3 4 2.83 8.15 3.23 o 10 3 4 2686.86 2691.28 48.36 o 11 3 4 126.51 121.82 7.32 o 12 3 4 196.33 184.58 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10.10 12.24 1.78 o 4 6 4 1018.11 995.22 11.28 o 5 6 4 446.78 438.94 6.45 o 6 6 4 1968.26 2000.69 23.52 o 7 6 4 117.61 124.82 3.32 o 8 6 4 613.68 615.80 9.26 o 9 6 4 630.58 622.22 11.56 o 10 6 4 77.88 75.00 3.74 o 11 6 4 1872.73 1913.35 45.80 o 12 6 4 395.20 367.83 22.61 o 13 6 4 1519.80 1563.74 49.95 o 14 6 4 23.36 5.01 10.76 o 1 7 4 479.65 440.07 5.73 o 2 7 4 1622.08 1691.73 17.96 o 3 7 4 2351.98 2353.77 27.24 o 4 7 4 15.66 16.13 2.01 o 5 7 4 409.72 437.84 6.96 o 6 7 4 441.80 437.67 7.84 o 7 7 4 0.23 6.05 1.91 o 8 7 4 3.80 6.93 1.80 o 9 7 4 21.21 18.75 4.25 o 10 7 4 789.05 809.21 19.37 o 11 7 4 1335.96 1354.03 37.52 o 12 7 4 55.89 43.04 6.81 o 13 7 4 619.11 648.35 23.43 o 0 8 4 1611.54 1686.84 31.78 o 1 8 4 72.23 70.65 3.38 o 2 8 4 657.79 660.55 9.29 o 3 8 4 20.41 21.48 2.29 o 4 8 4 84.13 78.43 3.05 o 5 8 4 5.29 5.51 1.84 o 6 8 4 218.51 216.14 4.70 o 7 8 4 65.30 61.90 3.07 o 8 8 4 768.58 767.43 17.95 o 9 8 4 258.42 240.53 7.67 o 10 8 4 1657.83 1735.74 44.71 o 11 8 4 22.58 32.82 4.06 o 12 8 4 648.16 647.39 19.32 o 1 9 4 388.43 408.51 7.65 o 2 9 4 783.57 800.18 12.22 o 3 9 4 1582.66 1650.81 20.62 o 4 9 4 3941.53 4149.85 57.63 o 5 9 4 1321.14 1328.29 19.70 o 6 9 4 15.96 11.60 2.39 o 7 9 4 174.34 162.18 5.48 o 8 9 4 1182.05 1142.57 27.22 o 9 9 4 691.47 698.34 23.30 o 10 9 4 88.14 80.80 6.28 o 11 9 4 836.90 847.79 28.40 o 12 9 4 123.89 104.81 19.00 o 0 10 4 3358.34 3536.51 69.77 o 1 10 4 48.22 40.16 3.39 o 2 10 4 7.81 9.89 2.84 o 3 10 4 2527.91 2674.39 37.55 o 4 10 4 228.28 219.63 6.43 o 5 10 4 806.62 803.72 18.42 o 6 10 4 17.19 18.26 3.71 o 7 10 4 1492.73 1560.75 40.36 o 8 10 4 1303.20 1346.81 35.57 o 9 10 4 3.40 -7.87 5.42 o 10 10 4 10.91 13.68 5.28 o 11 10 4 174.09 159.13 12.80 o 1 11 4 1526.05 1581.15 29.28 o 2 11 4 276.58 268.51 8.83 o 3 11 4 1023.66 1007.42 22.04 o 4 11 4 232.97 208.35 7.53 o 5 11 4 1376.61 1397.78 37.70 o 6 11 4 1.38 -1.49 4.03 o 7 11 4 517.90 538.62 16.46 o 8 11 4 156.37 156.76 9.81 o 9 11 4 206.91 188.46 11.64 o 0 12 4 146.40 131.83 10.64 o 1 12 4 9.54 13.75 4.14 o 2 12 4 1430.62 1479.59 37.88 o 3 12 4 2.11 -0.64 3.89 o 4 12 4 121.85 117.09 7.82 o 5 12 4 29.64 30.58 5.82 o 6 12 4 2077.16 2169.77 62.00 o 7 12 4 190.61 173.46 10.47 o 8 12 4 89.98 85.00 8.59 o 1 13 4 177.08 148.78 9.51 o 2 13 4 883.77 836.97 28.90 o 3 13 4 245.15 228.22 11.85 o 4 13 4 85.48 79.07 8.08 o 5 13 4 2200.31 2258.06 87.45 o 6 13 4 311.95 287.13 15.30 o 0 14 4 66.69 75.35 11.14 o 1 14 4 1691.51 1784.73 79.51 o 2 14 4 1.90 20.53 12.71 o 3 14 4 1717.91 1763.06 74.66 o 1 0 5 1930.72 1949.84 24.89 o 2 0 5 11.83 19.21 2.87 o 3 0 5 877.81 851.67 14.62 o 4 0 5 51.07 49.84 3.37 o 5 0 5 1093.03 1120.51 16.35 o 6 0 5 1248.44 1282.50 36.07 o 7 0 5 571.83 585.64 12.30 o 8 0 5 49.09 62.72 15.34 o 9 0 5 2594.41 2671.19 109.95 o 10 0 5 691.78 704.50 30.51 o 11 0 5 498.98 527.04 26.99 o 12 0 5 642.55 613.44 36.09 o 13 0 5 9.20 19.03 12.33 o 0 1 5 546.59 522.35 8.48 o 1 1 5 917.76 916.67 11.02 o 2 1 5 753.00 771.16 8.59 o 3 1 5 43.50 36.49 2.05 o 4 1 5 167.41 158.31 3.70 o 5 1 5 962.20 1000.51 11.16 o 6 1 5 87.36 95.76 2.49 o 7 1 5 444.50 458.20 6.80 o 8 1 5 815.92 815.03 13.62 o 9 1 5 275.41 247.25 23.73 o 10 1 5 85.23 98.78 10.28 o 11 1 5 708.12 716.10 24.72 o 12 1 5 18.46 7.79 7.24 o 13 1 5 1253.15 1384.62 89.84 o 1 2 5 63.38 56.66 2.37 o 2 2 5 635.94 683.47 8.28 o 3 2 5 2248.55 2323.14 19.83 o 4 2 5 4330.73 4597.52 41.55 o 5 2 5 322.94 325.71 5.00 o 6 2 5 1211.86 1260.92 13.39 o 7 2 5 1.45 3.03 1.98 o 8 2 5 2155.02 2144.79 32.71 o 9 2 5 265.64 266.48 8.40 o 10 2 5 6.07 9.64 6.09 o 11 2 5 2085.18 2151.94 58.62 o 12 2 5 0.44 6.69 6.40 o 13 2 5 826.55 906.70 25.42 o 0 3 5 1478.36 1491.66 20.17 o 1 3 5 724.91 701.33 7.30 o 2 3 5 78.47 79.95 2.54 o 3 3 5 0.08 1.25 2.06 o 4 3 5 49.88 52.88 2.58 o 5 3 5 205.14 217.11 3.95 o 6 3 5 24.22 21.23 2.12 o 7 3 5 2351.20 2406.92 30.88 o 8 3 5 1053.03 1085.11 17.85 o 9 3 5 785.19 807.77 18.97 o 10 3 5 21.92 26.15 6.82 o 11 3 5 493.04 501.71 15.16 o 12 3 5 177.67 163.49 9.72 o 13 3 5 18.01 28.52 8.77 o 1 4 5 15.56 20.16 1.77 o 2 4 5 1050.94 1051.13 11.20 o 3 4 5 0.84 1.78 1.62 o 4 4 5 2.80 1.51 1.67 o 5 4 5 760.97 787.86 9.58 o 6 4 5 149.60 147.65 3.60 o 7 4 5 29.71 34.54 3.09 o 8 4 5 182.60 181.27 4.93 o 9 4 5 2313.08 2413.70 37.61 o 10 4 5 134.89 128.06 9.26 o 11 4 5 387.09 364.62 19.35 o 12 4 5 743.08 706.84 24.17 o 13 4 5 44.49 24.18 12.81 o 0 5 5 1888.71 2040.06 29.41 o 1 5 5 1833.26 1903.67 18.65 o 2 5 5 1900.58 1992.46 20.98 o 3 5 5 416.97 405.09 5.80 o 4 5 5 4277.10 4429.33 46.51 o 5 5 5 2069.88 2098.19 26.47 o 6 5 5 11112.40 12042.00 143.92 o 7 5 5 323.92 308.52 9.05 o 8 5 5 254.41 258.23 7.78 o 9 5 5 440.58 427.24 12.44 o 10 5 5 1573.17 1559.31 41.05 o 11 5 5 424.68 418.91 14.06 o 12 5 5 866.98 871.77 29.01 o 1 6 5 38.09 37.01 2.20 o 2 6 5 3493.52 3670.75 44.94 o 3 6 5 3.97 5.96 2.06 o 4 6 5 947.50 966.15 14.37 o 5 6 5 452.14 443.66 7.99 o 6 6 5 76.29 76.96 3.07 o 7 6 5 112.82 106.44 4.43 o 8 6 5 1396.51 1408.85 28.85 o 9 6 5 1534.22 1560.28 37.74 o 10 6 5 1010.10 1021.17 28.36 o 11 6 5 299.13 290.89 13.10 o 12 6 5 463.00 389.74 28.42 o 0 7 5 65.39 54.68 3.62 o 1 7 5 496.83 505.47 7.76 o 2 7 5 71.40 72.20 3.08 o 3 7 5 8.64 9.22 2.47 o 4 7 5 122.52 120.20 3.82 o 5 7 5 77.70 74.81 3.80 o 6 7 5 152.11 149.10 5.33 o 7 7 5 2005.27 2037.27 48.72 o 8 7 5 369.14 352.52 11.27 o 9 7 5 440.23 426.35 13.67 o 10 7 5 2.22 3.74 3.95 o 11 7 5 441.23 387.35 15.69 o 1 8 5 1.75 2.65 2.45 o 2 8 5 1730.97 1777.63 27.44 o 3 8 5 1204.35 1246.96 19.33 o 4 8 5 4958.02 5187.14 77.04 o 5 8 5 297.65 281.05 7.69 o 6 8 5 1102.46 1095.50 23.81 o 7 8 5 0.42 4.22 3.92 o 8 8 5 3055.52 3188.35 85.51 o 9 8 5 165.80 153.95 8.02 o 10 8 5 38.35 39.80 5.43 o 0 9 5 4160.55 4445.89 114.04 o 1 9 5 516.79 500.24 9.97 o 2 9 5 21.31 22.33 3.22 o 3 9 5 22.56 18.84 3.10 o 4 9 5 1548.10 1553.20 37.58 o 5 9 5 665.50 673.91 17.15 o 6 9 5 1646.61 1693.11 38.74 o 7 9 5 180.72 179.34 8.65 o 8 9 5 1016.73 1064.97 32.84 o 9 9 5 126.95 103.39 7.42 o 1 10 5 1017.31 989.06 21.55 o 2 10 5 500.20 483.63 21.88 o 3 10 5 399.16 406.53 15.82 o 4 10 5 449.98 431.49 13.73 o 5 10 5 374.14 361.61 11.46 o 6 10 5 603.70 607.76 18.54 o 7 10 5 308.42 311.15 12.63 o 8 10 5 410.98 397.74 15.01 o 0 11 5 42.21 39.94 6.40 o 1 11 5 230.53 222.41 11.25 o 2 11 5 659.24 634.93 20.78 o 3 11 5 0.70 6.75 6.29 o 4 11 5 56.35 50.98 7.18 o 5 11 5 287.07 249.03 11.40 o 6 11 5 814.63 794.73 33.85 o 7 11 5 175.41 156.34 10.69 o 1 12 5 27.33 21.12 6.33 o 2 12 5 684.15 710.45 26.65 o 3 12 5 782.00 782.42 28.73 o 4 12 5 0.08 -3.96 6.17 o 5 12 5 99.55 86.82 12.33 o 0 0 6 3356.39 3539.10 111.08 o 1 0 6 963.72 1005.30 19.35 o 2 0 6 64.32 54.21 4.06 o 3 0 6 1176.34 1240.23 23.69 o 4 0 6 266.13 261.33 6.62 o 5 0 6 71.69 64.98 3.42 o 6 0 6 231.39 218.98 6.87 o 7 0 6 776.96 817.72 19.05 o 8 0 6 74.87 71.66 11.72 o 9 0 6 946.59 947.14 44.59 o 10 0 6 493.39 528.97 29.99 o 11 0 6 125.11 103.33 14.82 o 1 1 6 2373.32 2516.58 36.63 o 2 1 6 452.27 467.87 7.85 o 3 1 6 896.09 871.56 11.75 o 4 1 6 816.04 820.83 12.07 o 5 1 6 350.56 338.24 6.54 o 6 1 6 3.27 2.06 2.00 o 7 1 6 2001.20 2042.60 34.44 o 8 1 6 182.60 181.30 6.98 o 9 1 6 153.23 130.73 12.59 o 10 1 6 56.92 57.73 9.63 o 11 1 6 1240.83 1243.50 47.13 o 0 2 6 2942.35 3147.62 47.79 o 1 2 6 2458.77 2543.08 30.47 o 2 2 6 1466.45 1507.43 19.67 o 3 2 6 73.48 71.10 3.07 o 4 2 6 1165.48 1219.38 15.26 o 5 2 6 6.79 1.19 1.97 o 6 2 6 2885.44 3056.47 48.32 o 7 2 6 1590.99 1641.22 34.92 o 8 2 6 4.02 4.38 1.75 o 9 2 6 1330.26 1345.73 39.04 o 10 2 6 171.82 160.94 10.77 o 11 2 6 136.68 129.80 10.05 o 1 3 6 172.19 183.65 5.79 o 2 3 6 411.46 399.80 6.49 o 3 3 6 438.96 439.37 6.87 o 4 3 6 235.67 226.78 5.39 o 5 3 6 550.55 553.68 10.47 o 6 3 6 68.52 73.14 3.95 o 7 3 6 8.93 8.38 3.28 o 8 3 6 0.02 0.36 2.18 o 9 3 6 135.18 105.96 8.19 o 10 3 6 6.21 14.49 7.97 o 11 3 6 663.67 633.60 20.28 o 0 4 6 902.43 924.00 16.22 o 1 4 6 1232.48 1249.94 15.97 o 2 4 6 9.33 6.54 2.53 o 3 4 6 1880.53 1942.33 25.02 o 4 4 6 177.78 161.39 4.21 o 5 4 6 342.12 341.55 7.42 o 6 4 6 0.72 3.93 3.43 o 7 4 6 89.92 91.98 9.19 o 8 4 6 318.12 325.31 16.97 o 9 4 6 959.99 960.92 28.71 o 10 4 6 46.03 37.81 8.17 o 1 5 6 757.93 732.50 10.22 o 2 5 6 3028.17 3167.01 45.82 o 3 5 6 430.36 436.49 7.56 o 4 5 6 5784.12 6123.24 91.32 o 5 5 6 2686.73 2719.39 51.81 o 6 5 6 447.48 424.40 11.55 o 7 5 6 200.48 195.64 7.63 o 8 5 6 3175.46 3251.64 87.51 o 9 5 6 1515.66 1544.24 45.51 o 10 5 6 276.90 231.26 12.74 o 0 6 6 5.07 8.72 3.71 o 1 6 6 246.35 242.63 5.55 o 2 6 6 185.10 166.86 4.53 o 3 6 6 153.51 149.02 5.65 o 4 6 6 10.04 11.96 3.60 o 5 6 6 35.56 35.86 4.14 o 6 6 6 411.09 412.41 13.30 o 7 6 6 55.03 51.61 5.22 o 8 6 6 13.01 15.49 5.99 o 9 6 6 32.15 36.96 8.86 o 1 7 6 144.00 129.79 4.55 o 2 7 6 1086.28 1111.59 20.45 o 3 7 6 154.29 135.10 6.02 o 4 7 6 0.10 1.78 3.44 o 5 7 6 63.76 57.70 4.62 o 6 7 6 80.04 79.31 5.58 o 7 7 6 346.63 337.79 11.70 o 8 7 6 92.22 82.39 7.53 o 0 8 6 3671.41 3878.83 120.51 o 1 8 6 1230.05 1230.21 42.97 o 2 8 6 1372.74 1457.46 39.32 o 3 8 6 0.00 0.07 3.92 o 4 8 6 1244.63 1237.38 31.79 o 5 8 6 2.38 3.16 3.81 o 6 8 6 2777.22 2879.65 76.06 o 7 8 6 1357.65 1348.31 40.73 o 1 9 6 467.84 496.75 16.59 o 2 9 6 315.43 309.96 10.12 o 3 9 6 493.03 465.42 14.78 o 4 9 6 10.13 9.07 4.86 o 5 9 6 26.37 18.57 5.09 o 6 9 6 30.37 15.19 6.93 o 0 10 6 2793.95 2929.86 114.91 o 1 10 6 202.44 182.99 9.47 o 2 10 6 2.74 2.81 6.34 o 3 10 6 78.58 66.83 6.58 o 4 10 6 302.69 276.85 14.88 o 1 0 7 1953.87 1975.14 62.15 o 2 0 7 435.13 426.47 13.61 o 3 0 7 18.42 23.13 4.66 o 4 0 7 84.89 75.89 6.43 o 5 0 7 587.24 574.70 26.48 o 6 0 7 24.15 13.96 5.99 o 7 0 7 781.54 809.05 35.15 o 8 0 7 207.84 224.87 25.15 o 0 1 7 3511.38 3663.81 98.70 o 1 1 7 507.77 487.19 11.31 o 2 1 7 7.87 9.72 3.75 o 3 1 7 2602.24 2665.33 66.13 o 4 1 7 391.06 363.74 11.61 o 5 1 7 111.69 111.46 7.08 o 6 1 7 388.36 372.64 12.49 o 7 1 7 1865.47 1980.96 64.98 o 8 1 7 1087.43 1036.18 42.55 o 1 2 7 378.24 352.01 8.70 o 2 2 7 2786.95 2842.30 54.24 o 3 2 7 11.18 6.94 3.28 o 4 2 7 148.64 133.21 8.57 o 5 2 7 1040.50 1038.01 29.56 o 6 2 7 679.44 697.22 19.57 o 7 2 7 272.00 257.90 8.86 o 8 2 7 1.25 -6.12 8.55 o 0 3 7 72.77 68.89 7.16 o 1 3 7 268.21 261.64 10.44 o 2 3 7 159.95 144.48 7.40 o 3 3 7 470.51 465.18 14.77 o 4 3 7 170.15 146.70 7.21 o 5 3 7 185.73 190.73 13.28 o 6 3 7 26.52 32.45 6.71 o 7 3 7 37.04 33.05 4.12 o 1 4 7 1419.90 1401.55 30.10 o 2 4 7 1296.45 1305.59 27.81 o 3 4 7 9.46 13.59 4.42 o 4 4 7 572.32 553.61 15.93 o 5 4 7 1932.42 1965.77 55.25 o 6 4 7 14.85 7.90 4.44 o 7 4 7 178.68 163.25 11.37 o 0 5 7 3523.52 3665.41 112.13 o 1 5 7 0.81 0.47 3.66 o 2 5 7 71.14 65.03 5.12 o 3 5 7 189.26 182.46 7.89 o 4 5 7 8.98 18.08 7.88 o 5 5 7 80.33 70.81 7.14 o 6 5 7 315.80 290.15 13.62 o 1 6 7 10.83 12.45 4.76 o 2 6 7 461.03 431.62 21.36 o 3 6 7 4.80 -0.17 4.82 o 4 6 7 95.85 89.47 8.32 o 5 6 7 60.87 50.26 7.02 o 0 7 7 17.87 14.62 7.18 o 1 7 7 7.43 5.62 4.87 o 2 7 7 253.52 239.21 11.90 o 3 7 7 226.20 215.40 11.40 o # # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_2 _shelx_title ' 04src0369 in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 378.89 _exptl_crystal_F_000 1536.00 _reflns_d_resolution_high 0.7696 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 13.8045 _cell_length_b 10.7964 _cell_length_c 20.7719 _cell_angle_alpha 90.000 _cell_angle_beta 104.132 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 78771.47 29811.07 4173.06 o 3 0 0 3359.34 3153.97 59.80 o 4 0 0 36147.48 35522.57 598.34 o 5 0 0 112280.29 118706.57 1792.67 o 6 0 0 2627.42 2332.40 42.96 o 7 0 0 3815.16 4210.48 68.90 o 8 0 0 4196.85 4090.37 74.38 o 9 0 0 15.46 22.92 15.47 o 10 0 0 6189.35 6326.71 123.56 o 11 0 0 9510.22 9648.05 193.16 o 12 0 0 5390.64 5444.75 147.41 o 13 0 0 65.38 12.87 26.86 o 14 0 0 4312.45 4704.28 256.96 o 15 0 0 1767.98 1722.32 186.92 o 16 0 0 2188.52 1726.47 374.02 o 17 0 0 2058.17 1568.32 221.49 o 2 1 0 1961.94 1913.74 33.12 o 3 1 0 64.11 78.28 6.36 o 4 1 0 6964.43 6499.41 82.15 o 5 1 0 3313.48 3290.03 43.79 o 6 1 0 4260.55 3938.54 55.02 o 7 1 0 640.80 665.99 18.66 o 8 1 0 5683.74 5607.78 73.53 o 9 1 0 81.82 79.59 14.74 o 10 1 0 4645.82 4699.79 70.35 o 11 1 0 323.77 314.49 21.10 o 12 1 0 164.20 159.92 21.45 o 13 1 0 228.90 216.96 27.21 o 14 1 0 1615.89 1655.92 66.50 o 15 1 0 24.21 -20.24 37.38 o 16 1 0 3.94 -22.68 53.13 o 17 1 0 2.29 21.89 47.03 o 0 2 0 52477.15 53133.53 1117.19 o 1 2 0 3479.83 3424.09 46.13 o 2 2 0 1467.05 1458.07 20.50 o 3 2 0 1858.19 1781.08 32.49 o 4 2 0 5153.60 4831.03 72.24 o 5 2 0 56.87 5.82 6.61 o 6 2 0 1801.76 1844.79 27.34 o 7 2 0 7625.88 7517.67 93.47 o 8 2 0 4800.52 4785.51 88.87 o 9 2 0 842.69 826.72 27.45 o 10 2 0 0.91 -0.75 14.16 o 11 2 0 272.25 229.31 21.87 o 12 2 0 2196.37 2202.08 58.16 o 13 2 0 86.39 85.96 22.29 o 14 2 0 2053.46 2067.34 75.26 o 15 2 0 209.42 194.58 34.69 o 16 2 0 240.10 177.26 47.89 o 17 2 0 0.97 108.58 62.51 o 1 3 0 1585.52 1612.64 35.67 o 2 3 0 2.26 8.95 7.36 o 3 3 0 7843.05 7753.93 88.63 o 4 3 0 4286.88 4721.93 66.51 o 5 3 0 1537.95 1603.61 34.80 o 6 3 0 27.58 27.99 9.76 o 7 3 0 3.98 9.35 12.58 o 8 3 0 1815.02 1904.68 32.99 o 9 3 0 4068.50 4257.29 64.46 o 10 3 0 2537.98 2589.32 57.85 o 11 3 0 237.76 189.68 20.96 o 12 3 0 1113.29 1165.74 41.31 o 13 3 0 3284.63 3473.45 112.01 o 14 3 0 1903.69 1862.41 75.04 o 15 3 0 318.02 245.32 33.70 o 16 3 0 120.04 26.68 43.58 o 0 4 0 5978.45 6065.98 99.69 o 1 4 0 260.21 239.25 11.81 o 2 4 0 7937.35 7720.41 90.88 o 3 4 0 13285.75 13510.59 162.14 o 4 4 0 1786.33 1722.45 28.78 o 5 4 0 8914.03 8399.12 101.15 o 6 4 0 1958.69 1908.37 49.01 o 7 4 0 2055.53 2105.35 54.60 o 8 4 0 644.93 653.01 24.12 o 9 4 0 6914.67 7285.88 102.59 o 10 4 0 27.51 13.70 15.59 o 11 4 0 2981.00 2978.36 66.21 o 12 4 0 1747.76 1823.11 56.58 o 13 4 0 112.60 91.01 30.55 o 14 4 0 138.37 108.06 35.75 o 15 4 0 1750.03 1535.16 112.84 o 16 4 0 1466.76 1398.02 129.56 o 1 5 0 23961.26 24804.49 275.94 o 2 5 0 273.33 281.83 14.56 o 3 5 0 3549.09 3465.16 51.98 o 4 5 0 200.66 119.73 15.01 o 5 5 0 39.50 58.12 12.70 o 6 5 0 487.23 476.73 20.31 o 7 5 0 421.21 484.20 22.17 o 8 5 0 4310.64 4352.76 69.30 o 9 5 0 538.16 465.58 24.51 o 10 5 0 754.24 798.40 30.30 o 11 5 0 177.50 185.18 25.69 o 12 5 0 653.30 621.26 37.00 o 13 5 0 3940.57 4170.20 164.26 o 14 5 0 213.89 69.03 40.46 o 15 5 0 41.79 16.59 49.26 o 16 5 0 196.62 141.62 70.60 o 0 6 0 15087.36 15046.64 258.80 o 1 6 0 1223.59 1230.68 26.86 o 2 6 0 995.10 1052.93 25.93 o 3 6 0 205.58 181.06 16.18 o 4 6 0 561.37 550.99 20.37 o 5 6 0 1690.83 1708.36 43.98 o 6 6 0 1442.21 1381.42 32.88 o 7 6 0 269.68 262.18 18.41 o 8 6 0 8.10 -19.92 19.33 o 9 6 0 780.92 718.46 29.61 o 10 6 0 8.90 -8.17 18.26 o 11 6 0 165.85 130.81 31.02 o 12 6 0 82.42 63.15 24.61 o 13 6 0 385.91 345.16 34.38 o 14 6 0 777.22 710.56 63.79 o 15 6 0 532.10 504.37 74.38 o 1 7 0 1061.85 1046.64 27.88 o 2 7 0 831.10 840.27 35.42 o 3 7 0 1422.97 1413.48 42.51 o 4 7 0 8044.29 8264.71 145.70 o 5 7 0 7246.16 7264.07 122.87 o 6 7 0 1715.88 1611.24 45.06 o 7 7 0 411.39 330.07 25.36 o 8 7 0 1290.57 1210.55 44.93 o 9 7 0 589.16 623.21 36.81 o 10 7 0 1396.68 1289.25 54.25 o 11 7 0 207.23 188.61 31.52 o 12 7 0 790.00 725.82 48.92 o 13 7 0 654.82 607.08 71.48 o 14 7 0 776.84 752.27 69.83 o 15 7 0 42.35 75.07 149.87 o 0 8 0 3.85 29.23 25.87 o 1 8 0 237.66 257.01 19.41 o 2 8 0 7165.37 7374.82 120.41 o 3 8 0 2100.95 2150.42 51.03 o 4 8 0 3948.00 3913.88 89.14 o 5 8 0 49.53 68.43 26.16 o 6 8 0 5.43 9.91 18.42 o 7 8 0 788.34 750.39 35.54 o 8 8 0 43.41 35.30 20.88 o 9 8 0 312.14 289.89 32.89 o 10 8 0 11.52 17.61 29.56 o 11 8 0 5875.48 6067.54 258.77 o 12 8 0 681.12 611.02 54.35 o 13 8 0 2.28 5.89 44.29 o 14 8 0 2010.63 1803.79 159.80 o 1 9 0 585.71 581.25 29.28 o 2 9 0 1142.23 1078.79 41.41 o 3 9 0 459.05 472.82 33.89 o 4 9 0 69.02 34.98 23.27 o 5 9 0 1081.21 1075.72 40.13 o 6 9 0 790.79 862.42 43.57 o 7 9 0 1351.66 1257.16 53.88 o 8 9 0 0.07 1.35 35.85 o 9 9 0 163.01 134.23 32.19 o 10 9 0 13.84 47.79 34.11 o 11 9 0 549.34 548.58 62.10 o 12 9 0 915.51 819.69 75.38 o 13 9 0 476.63 479.45 68.05 o 0 10 0 189.21 240.41 42.33 o 1 10 0 37.17 31.38 23.05 o 2 10 0 1334.13 1470.23 71.19 o 3 10 0 3999.52 4281.62 116.70 o 4 10 0 205.03 182.52 24.81 o 5 10 0 1.74 10.67 25.15 o 6 10 0 52.73 69.44 30.20 o 7 10 0 5404.37 5857.64 180.14 o 8 10 0 1570.79 1681.62 91.51 o 9 10 0 11586.61 13466.79 462.50 o 10 10 0 565.61 583.29 72.27 o 11 10 0 1071.16 1010.96 85.50 o 12 10 0 1569.15 1365.15 153.19 o 1 11 0 9190.96 10232.65 312.82 o 2 11 0 4.81 -24.35 28.99 o 3 11 0 34.95 73.40 36.61 o 4 11 0 22.92 50.78 38.69 o 5 11 0 432.47 442.25 49.80 o 6 11 0 212.34 147.54 41.56 o 7 11 0 13.73 27.00 50.71 o 8 11 0 147.61 109.56 50.80 o 9 11 0 223.92 243.60 59.57 o 10 11 0 310.48 326.11 62.81 o 0 12 0 10778.90 12327.47 711.69 o 1 12 0 202.67 185.76 42.12 o 2 12 0 913.63 809.20 69.89 o 3 12 0 761.14 635.24 64.17 o 4 12 0 1577.60 1592.83 90.41 o 5 12 0 8819.13 9237.03 488.71 o 6 12 0 0.32 -19.32 64.64 o 7 12 0 1407.86 1336.42 148.62 o 8 12 0 157.31 86.47 62.40 o 9 12 0 35.12 -89.25 96.56 o 1 13 0 1009.32 1079.70 89.32 o 2 13 0 191.43 100.68 58.38 o 3 13 0 1205.52 1265.99 102.42 o 4 13 0 1852.29 1777.88 129.81 o 5 13 0 370.00 354.43 79.26 o 6 13 0 1619.25 1647.69 129.12 o 0 14 0 240.74 111.88 70.98 o 1 14 0 89.81 143.98 87.29 o -17 1 1 25.59 75.68 58.59 o -16 1 1 2714.28 2549.61 130.86 o -15 1 1 776.84 734.86 75.88 o -14 1 1 113.20 98.65 28.48 o -13 1 1 1595.49 1644.17 52.10 o -12 1 1 5.52 27.53 18.42 o -11 1 1 3360.85 3348.43 63.92 o -10 1 1 17658.51 18425.61 268.67 o -9 1 1 108.96 93.72 12.18 o -8 1 1 8.23 -1.52 13.91 o -7 1 1 4875.93 4621.46 55.57 o -6 1 1 313.09 279.33 13.75 o -5 1 1 3355.47 3371.31 42.79 o -4 1 1 39685.95 38881.05 500.36 o -3 1 1 4155.65 3855.84 51.02 o -2 1 1 3732.68 3567.85 50.88 o 2 1 1 19113.02 18292.29 234.94 o 3 1 1 6937.13 6756.37 86.24 o 4 1 1 3986.27 3926.56 47.69 o 5 1 1 5849.20 5961.86 77.35 o 6 1 1 555.28 471.62 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59.76 o 4 0 22 90.59 124.70 51.66 o 5 0 22 271.91 289.50 115.61 o 6 0 22 30.57 17.06 66.36 o -13 1 22 901.59 1079.92 208.99 o -12 1 22 20.10 183.55 101.00 o -11 1 22 35.96 111.09 60.42 o -10 1 22 726.47 903.87 90.81 o -9 1 22 0.29 -58.85 53.40 o -8 1 22 102.53 142.55 50.95 o -7 1 22 111.86 61.91 52.01 o -6 1 22 25.58 -25.33 61.06 o -5 1 22 92.25 3.10 56.30 o -4 1 22 1026.00 1078.51 33.77 o -3 1 22 397.52 380.58 18.64 o -2 1 22 36.20 20.47 12.26 o -1 1 22 844.89 924.49 49.20 o 0 1 22 40.51 45.84 25.44 o 1 1 22 536.02 537.28 42.78 o 2 1 22 42.28 59.81 31.53 o 3 1 22 606.14 707.44 86.68 o 4 1 22 319.55 229.85 77.65 o 5 1 22 285.82 290.53 49.81 o 6 1 22 256.51 160.35 79.52 o -13 2 22 229.29 268.88 127.20 o -12 2 22 240.13 220.00 92.54 o -11 2 22 6.34 -18.38 80.67 o -10 2 22 206.64 162.52 107.65 o -9 2 22 96.24 6.78 92.53 o -8 2 22 158.42 159.39 76.89 o -7 2 22 38.98 163.29 75.33 o -6 2 22 49.09 38.84 68.29 o -5 2 22 21.23 25.06 9.35 o -4 2 22 3760.38 3892.99 110.57 o -3 2 22 205.74 193.37 14.35 o -2 2 22 227.25 228.91 21.02 o -1 2 22 577.00 587.48 32.92 o 0 2 22 431.36 451.63 33.40 o 1 2 22 3066.92 3371.26 157.99 o 2 2 22 24.54 -0.21 25.45 o 3 2 22 269.23 178.28 57.97 o 4 2 22 2499.12 2572.68 160.49 o 5 2 22 629.71 640.89 124.45 o 6 2 22 678.05 599.87 73.17 o -12 3 22 8.64 -33.88 103.47 o -11 3 22 91.45 91.88 108.95 o -10 3 22 27.48 -122.76 81.84 o -9 3 22 64.30 136.84 92.14 o -8 3 22 3138.30 3506.29 335.06 o -7 3 22 127.88 234.33 114.69 o -6 3 22 1464.10 1479.93 78.09 o -5 3 22 596.50 557.56 32.36 o -4 3 22 462.36 400.96 17.57 o -3 3 22 1734.64 1789.53 70.47 o -2 3 22 2225.75 2455.23 94.94 o -1 3 22 1764.52 1738.05 76.32 o 0 3 22 397.34 434.06 34.31 o 1 3 22 32.54 20.52 27.45 o 2 3 22 361.35 309.20 41.73 o 3 3 22 1432.84 1484.85 81.88 o 4 3 22 416.10 351.04 53.01 o 5 3 22 786.32 652.71 97.51 o -12 4 22 750.78 1207.69 202.98 o -11 4 22 306.40 410.04 128.38 o -10 4 22 35.81 89.79 120.55 o -9 4 22 734.94 800.97 142.49 o -8 4 22 302.89 333.41 106.62 o -7 4 22 37.09 97.74 241.22 o -6 4 22 1547.26 1647.10 125.24 o -5 4 22 611.52 599.05 41.83 o -4 4 22 413.30 402.15 34.04 o -3 4 22 618.27 620.01 35.23 o -2 4 22 290.64 249.76 21.29 o -1 4 22 136.74 123.40 23.98 o 0 4 22 1544.83 1377.62 66.90 o 1 4 22 254.99 211.12 32.67 o 2 4 22 316.55 314.06 42.09 o 3 4 22 174.24 111.31 40.89 o 4 4 22 1741.31 1757.39 192.45 o 5 4 22 473.24 397.25 78.61 o -11 5 22 92.16 -48.35 108.04 o -10 5 22 1968.17 2025.33 270.14 o -9 5 22 356.65 430.78 117.96 o -8 5 22 184.33 248.28 42.36 o -7 5 22 80.93 48.67 39.37 o -6 5 22 514.39 521.07 114.58 o -5 5 22 2601.70 2667.50 146.71 o -4 5 22 2281.94 2281.63 111.89 o -3 5 22 262.09 279.58 49.63 o -2 5 22 692.34 642.38 60.59 o -1 5 22 1945.41 1957.76 95.96 o 0 5 22 441.47 354.37 51.75 o 1 5 22 45.10 1.10 32.04 o 2 5 22 198.15 173.63 49.93 o 3 5 22 0.29 35.30 48.60 o 4 5 22 4025.98 4232.91 303.18 o -9 6 22 148.95 100.09 72.46 o -8 6 22 326.66 233.44 48.49 o -7 6 22 92.76 82.50 38.71 o -6 6 22 23.24 106.34 74.93 o -5 6 22 2713.08 3108.46 371.11 o -4 6 22 0.02 3.56 22.49 o -3 6 22 1432.96 1511.30 100.41 o -2 6 22 54.40 26.81 52.65 o -1 6 22 0.26 -21.34 44.60 o 0 6 22 411.70 398.19 63.33 o 1 6 22 311.79 318.27 90.85 o 2 6 22 307.78 190.86 63.98 o 3 6 22 651.60 470.34 103.24 o -8 7 22 234.22 241.90 78.98 o -7 7 22 4.71 -8.99 59.03 o -6 7 22 3.22 -89.53 82.10 o -5 7 22 1204.15 1417.28 105.96 o -4 7 22 155.39 220.62 101.59 o -3 7 22 478.49 2107.86 796.30 o -2 7 22 72.29 59.80 47.50 o -1 7 22 1297.53 1470.09 160.06 o 0 7 22 12.70 -27.98 71.02 o 1 7 22 213.52 151.89 58.08 o -5 8 22 74.41 -21.60 63.73 o -4 8 22 30.60 115.68 60.00 o -3 8 22 80.97 36.47 40.74 o -2 8 22 1746.59 1883.48 153.85 o -12 1 23 457.04 236.46 80.11 o -11 1 23 1825.98 1876.99 131.80 o -10 1 23 160.53 214.83 82.88 o -9 1 23 6619.56 7711.57 429.88 o -8 1 23 0.27 -33.21 54.49 o -7 1 23 1467.93 1744.35 132.97 o -6 1 23 662.91 505.82 127.63 o -5 1 23 914.43 875.11 143.55 o -4 1 23 143.19 104.30 9.73 o -3 1 23 34.38 34.24 11.17 o -2 1 23 1064.68 1028.07 45.81 o -1 1 23 1062.64 916.09 43.24 o 0 1 23 108.86 134.56 27.68 o 1 1 23 70.62 61.39 29.12 o 2 1 23 28.29 19.63 31.89 o 3 1 23 1019.94 1026.74 84.12 o 4 1 23 420.91 250.79 54.76 o 5 1 23 429.60 471.89 82.96 o -12 2 23 316.78 337.58 120.69 o -11 2 23 2207.52 2633.35 233.51 o -10 2 23 2602.73 3007.08 297.63 o -9 2 23 80.00 86.27 93.70 o -8 2 23 921.58 732.47 131.29 o -7 2 23 1721.37 1660.13 183.52 o -6 2 23 1526.45 1299.76 157.81 o -5 2 23 4083.59 4127.54 245.14 o -4 2 23 522.23 436.45 26.83 o -3 2 23 1058.46 997.23 49.47 o -2 2 23 1806.64 1792.23 84.72 o -1 2 23 1153.45 1144.65 57.52 o 0 2 23 25.68 13.32 23.36 o 1 2 23 245.10 210.18 34.15 o 2 2 23 548.73 596.23 78.01 o 3 2 23 1916.13 1853.92 139.15 o 4 2 23 208.31 161.27 73.22 o 5 2 23 3121.77 3158.26 272.82 o -12 3 23 1418.18 1762.66 195.47 o -11 3 23 60.34 131.50 146.87 o -10 3 23 484.77 546.94 114.32 o -9 3 23 966.36 971.07 129.86 o -8 3 23 13.52 -25.28 123.80 o -7 3 23 453.82 645.22 128.13 o -6 3 23 2627.52 1246.57 116.53 o -5 3 23 818.69 885.01 58.55 o -4 3 23 2033.84 1986.20 109.24 o -3 3 23 1074.64 1058.99 51.73 o -2 3 23 5.38 35.20 24.39 o -1 3 23 61.09 94.09 32.86 o 0 3 23 70.41 12.89 25.67 o 1 3 23 561.11 495.73 63.07 o 2 3 23 77.86 68.92 77.77 o 3 3 23 105.72 188.48 62.52 o 4 3 23 569.68 611.76 87.64 o -11 4 23 40.33 138.40 132.15 o -10 4 23 718.68 717.13 138.18 o -9 4 23 1141.15 1051.98 138.21 o -8 4 23 522.06 653.45 107.80 o -7 4 23 271.92 467.39 142.98 o -6 4 23 1176.95 1210.51 93.52 o -5 4 23 1025.94 1115.95 112.21 o -4 4 23 132.83 92.91 23.24 o -3 4 23 363.51 336.37 32.36 o -2 4 23 381.56 402.43 39.64 o -1 4 23 496.98 496.77 41.24 o 0 4 23 784.48 823.40 68.03 o 1 4 23 386.97 303.42 45.36 o 2 4 23 665.75 557.04 60.95 o 3 4 23 542.99 492.29 76.25 o -10 5 23 557.79 629.47 183.80 o -9 5 23 2890.86 3314.04 277.43 o -8 5 23 950.86 657.49 169.49 o -7 5 23 755.40 719.10 84.74 o -6 5 23 0.12 48.35 44.83 o -5 5 23 4.69 -36.62 34.84 o -4 5 23 355.84 301.75 44.79 o -3 5 23 16.52 3.27 21.51 o -2 5 23 939.52 957.97 142.39 o -1 5 23 106.00 63.97 38.98 o 0 5 23 421.05 383.60 77.30 o 1 5 23 40.45 7.76 39.83 o 2 5 23 35.62 45.79 74.48 o -7 6 23 1245.26 1425.87 156.08 o -6 6 23 20.28 60.47 44.05 o -5 6 23 338.87 660.17 768.48 o -4 6 23 279.43 244.12 43.56 o -3 6 23 168.55 235.31 65.75 o -2 6 23 659.76 634.65 402.16 o -1 6 23 36.35 56.61 52.42 o 0 6 23 0.05 9.23 57.44 o 1 6 23 2.34 29.43 41.22 o -6 7 23 382.64 266.68 63.22 o -5 7 23 48.54 199.13 92.66 o -4 7 23 1428.83 1466.42 143.05 o -3 7 23 2072.34 2168.87 141.49 o -2 7 23 26.71 28.27 43.98 o -1 7 23 51.12 -6.32 45.15 o -11 0 24 169.46 182.33 100.87 o -10 0 24 2550.28 2526.54 248.43 o -9 0 24 904.01 1147.70 147.32 o -8 0 24 188.27 188.20 97.36 o -7 0 24 2940.67 3377.93 261.28 o -6 0 24 305.10 317.11 109.88 o -5 0 24 577.22 409.45 100.77 o -4 0 24 894.64 754.48 160.95 o -3 0 24 30.89 44.02 23.83 o -2 0 24 2037.12 2193.64 229.85 o -1 0 24 1607.39 1611.34 157.09 o 0 0 24 1315.63 1372.49 212.95 o 1 0 24 8454.40 9453.17 987.65 o 2 0 24 2108.36 2038.01 226.33 o 3 0 24 3367.31 3535.36 352.41 o 4 0 24 823.01 644.67 139.49 o -11 1 24 837.10 870.88 113.11 o -10 1 24 11.81 168.13 81.30 o -9 1 24 286.77 360.79 126.75 o -8 1 24 89.09 -42.69 56.01 o -7 1 24 105.07 28.28 79.50 o -6 1 24 358.69 363.26 125.39 o -5 1 24 42.82 -61.25 61.64 o -4 1 24 996.85 1105.53 102.86 o -3 1 24 493.54 520.74 49.69 o -2 1 24 2925.43 2898.64 126.89 o -1 1 24 330.67 320.87 35.19 o 0 1 24 128.95 57.72 51.80 o 1 1 24 8.90 25.50 45.81 o 2 1 24 685.27 650.18 83.94 o 3 1 24 358.57 255.10 76.89 o -11 2 24 0.03 40.66 118.59 o -10 2 24 2042.45 2368.60 243.67 o -9 2 24 771.70 674.39 159.70 o -8 2 24 641.30 769.25 156.17 o -7 2 24 693.81 819.46 137.92 o -6 2 24 298.21 319.20 113.65 o -5 2 24 37.66 121.33 74.54 o -4 2 24 7.53 17.67 22.83 o -3 2 24 360.91 305.65 27.07 o -2 2 24 600.27 602.13 51.26 o -1 2 24 1931.62 1977.78 93.60 o 0 2 24 276.71 227.71 77.30 o 1 2 24 2328.46 2270.29 145.95 o 2 2 24 330.59 250.20 85.54 o 3 2 24 0.23 -50.29 56.04 o -10 3 24 42.42 -24.89 101.65 o -9 3 24 243.74 49.40 129.16 o -8 3 24 10.21 104.26 96.96 o -7 3 24 69.71 161.34 92.14 o -6 3 24 259.10 215.05 108.57 o -5 3 24 355.38 374.62 47.18 o -4 3 24 6.73 51.47 34.25 o -3 3 24 53.56 123.55 31.81 o -2 3 24 24.42 39.62 23.31 o -1 3 24 16.72 44.70 28.19 o 0 3 24 1224.43 1351.41 105.79 o 1 3 24 46.27 -11.24 30.83 o 2 3 24 235.24 155.35 56.20 o 3 3 24 67.19 71.39 72.13 o -10 4 24 0.64 -87.83 101.26 o -9 4 24 485.56 700.23 134.78 o -8 4 24 25.69 94.35 153.65 o -7 4 24 2.76 -4.56 87.31 o -6 4 24 621.00 551.67 112.63 o -5 4 24 2291.11 2332.64 158.24 o -4 4 24 1475.92 1507.86 105.34 o -3 4 24 2362.11 2210.00 129.85 o -2 4 24 6.03 -41.68 27.79 o -1 4 24 227.35 308.01 51.34 o 0 4 24 273.91 315.78 60.13 o 1 4 24 264.61 269.64 51.80 o 2 4 24 325.21 196.85 64.76 o -8 5 24 204.50 189.24 107.26 o -7 5 24 137.84 -13.81 126.03 o -6 5 24 285.97 324.89 51.99 o -5 5 24 2070.32 2434.83 191.86 o -4 5 24 912.97 1014.88 88.65 o -3 5 24 27.63 66.19 33.76 o -2 5 24 491.07 430.31 52.68 o -1 5 24 718.06 660.86 57.26 o 0 5 24 92.90 22.62 39.82 o 1 5 24 264.28 299.37 53.11 o -6 6 24 2586.85 2947.66 275.30 o -5 6 24 225.59 176.08 52.91 o -4 6 24 50.34 71.42 99.44 o -3 6 24 134.17 160.10 42.81 o -2 6 24 20.83 13.09 39.58 o -10 1 25 1571.68 1842.09 170.32 o -9 1 25 620.16 481.74 90.97 o -8 1 25 524.86 460.53 128.92 o -7 1 25 307.73 241.13 128.12 o -6 1 25 998.08 837.96 153.85 o -5 1 25 687.04 545.70 94.12 o -4 1 25 36.19 30.76 67.77 o -3 1 25 75.56 78.84 26.04 o -2 1 25 310.43 249.78 51.13 o -1 1 25 0.17 17.00 35.15 o 0 1 25 785.14 712.72 66.17 o 1 1 25 238.77 255.98 54.58 o 2 1 25 823.29 798.59 145.03 o -10 2 25 1345.41 997.55 159.87 o -9 2 25 522.44 446.58 134.65 o -8 2 25 77.89 129.41 117.03 o -7 2 25 763.42 825.61 139.10 o -6 2 25 3313.86 3758.07 343.67 o -5 2 25 2094.50 1800.34 200.11 o -4 2 25 4340.68 4466.75 318.31 o -3 2 25 1920.98 1823.75 136.24 o -2 2 25 121.71 124.11 28.38 o -1 2 25 1001.70 1007.54 111.61 o 0 2 25 890.76 789.18 79.87 o 1 2 25 5666.82 5819.58 630.50 o 2 2 25 118.85 198.60 66.21 o -9 3 25 151.17 230.16 89.27 o -8 3 25 4.58 -6.78 87.18 o -7 3 25 254.99 339.39 118.60 o -6 3 25 127.85 77.94 74.94 o -5 3 25 741.22 882.44 146.53 o -4 3 25 165.66 222.79 43.68 o -3 3 25 93.82 60.61 28.47 o -2 3 25 332.43 207.31 35.67 o -1 3 25 96.89 35.90 30.68 o 0 3 25 790.36 710.47 68.58 o 1 3 25 104.35 48.74 61.81 o -8 4 25 510.90 512.40 154.07 o -7 4 25 18.19 -49.52 103.08 o -6 4 25 666.68 937.28 252.25 o -5 4 25 28.79 153.26 125.24 o -4 4 25 2.81 6.17 47.70 o -3 4 25 558.55 600.94 71.31 o -2 4 25 23.18 69.49 27.09 o -1 4 25 45.60 76.10 39.37 o 0 4 25 31.02 62.52 57.65 o -6 5 25 69.35 69.20 132.41 o -5 5 25 892.39 808.43 87.96 o -4 5 25 304.30 194.50 51.82 o -3 5 25 147.11 81.89 47.46 o -2 5 25 361.24 322.25 52.61 o -8 0 26 5622.95 6205.28 661.65 o -7 0 26 1446.24 1615.74 180.48 o -6 0 26 3070.48 3064.67 291.55 o -2 0 26 186.58 203.32 41.58 o -1 0 26 801.70 996.66 106.25 o 0 0 26 1552.75 1590.11 184.40 o -8 1 26 172.76 388.25 128.37 o -7 1 26 767.93 545.58 134.02 o -6 1 26 1.05 155.34 112.73 o -5 1 26 40.33 4.95 110.77 o -4 1 26 565.31 648.12 125.40 o -3 1 26 664.87 730.53 126.32 o -2 1 26 5.16 -10.79 27.49 o -1 1 26 46.64 -38.68 44.86 o 0 1 26 547.99 449.28 60.51 o -8 2 26 336.32 405.48 104.14 o -7 2 26 529.88 509.54 136.09 o -6 2 26 8.73 45.35 114.68 o -5 2 26 655.27 411.02 120.19 o -4 2 26 1018.52 960.78 145.50 o -3 2 26 339.29 317.23 53.05 o -2 2 26 1.75 49.20 26.75 o -1 2 26 358.72 350.89 41.86 o -7 3 26 503.67 371.89 110.41 o -6 3 26 104.45 33.88 94.62 o -5 3 26 42.42 70.89 119.11 o -4 3 26 453.43 570.66 98.67 o -3 3 26 2471.80 2360.95 171.59 o -2 3 26 15.63 6.23 47.87 o # # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_3 _shelx_title ' 03swb002 in Pna2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 259.99 _exptl_crystal_F_000 1728.00 _reflns_d_resolution_high 0.7704 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' _cell_length_a 20.3441 _cell_length_b 11.9481 _cell_length_c 15.9661 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 3 -20 3.46 27.70 66.69 o 2 3 -20 44.42 166.81 83.53 o 3 3 -20 151.98 344.80 92.47 o 4 3 -20 31.88 27.70 139.07 o 0 4 -20 186.93 166.82 138.83 o 1 4 -20 165.44 94.40 92.48 o 9 2 -19 11.23 0.00 83.38 o 0 3 -19 55.82 111.37 83.39 o 1 3 -19 119.24 83.51 69.68 o 2 3 -19 55.98 -27.84 58.97 o 3 3 -19 294.58 190.86 66.78 o 4 3 -19 106.49 305.99 66.76 o 5 3 -19 83.55 119.38 111.38 o 6 3 -19 121.90 361.70 71.53 o 7 3 -19 13.85 95.26 66.69 o 8 3 -19 47.39 27.70 83.39 o 9 3 -19 13.07 83.38 83.38 o 1 4 -19 297.30 575.61 152.99 o 2 4 -19 146.64 111.11 58.97 o 3 4 -19 36.43 79.28 69.40 o 4 4 -19 57.60 47.63 66.69 o 5 4 -19 165.04 169.76 86.75 o 6 4 -19 44.21 46.34 49.78 o 7 4 -19 48.85 69.40 78.55 o 8 4 -19 45.75 83.20 58.87 o 0 5 -19 32.59 -83.11 83.11 o 1 5 -19 24.67 -39.56 66.55 o 2 5 -19 78.27 145.48 83.25 o 3 5 -19 175.31 208.05 78.47 o 4 5 -19 74.73 0.00 97.11 o 5 5 -19 60.16 13.88 69.40 o 6 5 -19 31.49 -24.66 86.66 o 1 6 -19 149.16 290.94 97.96 o 2 6 -19 6.57 36.94 49.55 o 10 2 -18 77.52 55.69 55.69 o 12 2 -18 10.17 27.70 83.38 o 4 3 -18 398.19 473.48 83.72 o 5 3 -18 237.08 180.88 78.68 o 6 3 -18 184.37 236.42 78.67 o 7 3 -18 65.56 0.00 83.39 o 8 3 -18 41.91 117.32 86.86 o 9 3 -18 2.95 -13.99 41.69 o 10 3 -18 1.26 97.23 58.96 o 11 3 -18 40.60 55.41 111.09 o 12 3 -18 22.04 111.09 83.11 o 0 4 -18 248.41 138.85 111.13 o 1 4 -18 173.25 250.08 78.57 o 2 4 -18 43.83 138.95 66.69 o 3 4 -18 92.33 111.10 83.40 o 4 4 -18 3.26 -38.87 46.15 o 5 4 -18 136.44 63.47 66.70 o 6 4 -18 3.61 0.00 39.27 o 7 4 -18 157.44 166.53 78.57 o 8 4 -18 101.16 128.40 97.11 o 9 4 -18 8.00 46.19 69.39 o 10 4 -18 131.85 277.08 110.83 o 11 4 -18 22.79 138.51 110.81 o 1 5 -18 307.86 213.99 66.52 o 2 5 -18 37.76 83.11 58.77 o 3 5 -18 348.63 403.72 98.10 o 4 5 -18 33.25 114.80 69.40 o 5 5 -18 49.79 55.50 58.87 o 6 5 -18 74.15 79.24 69.26 o 7 5 -18 240.35 261.33 66.51 o 8 5 -18 35.96 13.85 58.77 o 9 5 -18 47.26 27.70 55.41 o 0 6 -18 34.60 -55.41 55.41 o 1 6 -18 9.52 11.87 66.49 o 2 6 -18 12.26 67.28 66.49 o 3 6 -18 47.25 41.56 58.77 o 4 6 -18 8.21 13.71 124.52 o 5 6 -18 48.30 18.47 49.56 o 6 6 -18 12.87 97.07 235.19 o 7 6 -18 85.03 36.91 55.27 o 8 6 -18 67.19 246.32 165.81 o 1 7 -18 62.54 -27.47 124.39 o 2 7 -18 49.79 86.96 66.35 o 3 7 -18 19.97 82.97 58.67 o 4 7 -18 28.53 162.06 66.35 o 5 7 -18 77.94 152.12 124.26 o 9 2 -17 169.88 166.26 55.42 o 11 2 -17 84.55 55.69 83.39 o 12 2 -17 1.94 27.70 55.68 o 13 2 -17 63.91 277.88 111.10 o 14 2 -17 147.96 333.33 111.11 o 5 3 -17 107.43 -27.98 55.69 o 6 3 -17 12.64 27.98 83.66 o 7 3 -17 344.53 412.65 124.87 o 8 3 -17 38.93 31.34 40.17 o 9 3 -17 68.98 101.71 55.55 o 10 3 -17 93.53 36.93 49.59 o 11 3 -17 38.25 92.38 49.58 o 12 3 -17 97.56 110.83 55.41 o 13 3 -17 100.01 110.83 110.83 o 14 3 -17 6.42 110.81 138.51 o 1 4 -17 254.07 305.84 78.59 o 2 4 -17 28.95 11.88 66.69 o 3 4 -17 144.48 129.76 69.41 o 4 4 -17 173.81 254.33 110.84 o 5 4 -17 305.99 284.44 69.71 o 6 4 -17 193.60 182.41 83.13 o 7 4 -17 118.77 101.53 32.05 o 8 4 -17 130.09 194.08 97.12 o 9 4 -17 87.04 79.24 40.32 o 10 4 -17 19.00 33.24 46.10 o 11 4 -17 1.12 -27.70 83.11 o 12 4 -17 37.98 -27.70 83.11 o 13 4 -17 15.93 27.70 110.53 o 0 5 -17 40.11 0.00 55.41 o 1 5 -17 79.80 36.94 55.41 o 2 5 -17 92.79 72.04 46.11 o 3 5 -17 50.96 64.58 138.66 o 4 5 -17 53.27 66.60 83.25 o 5 5 -17 24.48 27.70 46.10 o 6 5 -17 6.55 15.85 66.54 o 7 5 -17 48.82 0.00 83.11 o 8 5 -17 92.18 152.25 96.83 o 9 5 -17 168.24 229.41 66.44 o 10 5 -17 1.42 82.87 58.67 o 11 5 -17 126.23 331.66 110.55 o 12 5 -17 96.95 55.14 82.84 o 1 6 -17 12.62 110.81 83.11 o 2 6 -17 20.09 -38.78 46.10 o 3 6 -17 106.04 225.22 69.27 o 4 6 -17 163.23 181.54 82.85 o 5 6 -17 430.05 452.45 111.31 o 6 6 -17 169.92 138.45 138.27 o 7 6 -17 43.86 64.57 69.26 o 8 6 -17 75.37 27.71 82.84 o 9 6 -17 36.09 96.68 58.57 o 10 6 -17 11.46 110.53 110.53 o 11 6 -17 43.74 110.54 82.83 o 0 7 -17 217.00 442.29 138.28 o 1 7 -17 123.44 193.40 110.55 o 2 7 -17 217.88 193.57 58.59 o 3 7 -17 13.78 127.13 46.05 o 4 7 -17 19.34 -27.70 78.16 o 5 7 -17 13.37 27.67 78.26 o 6 7 -17 37.58 67.18 66.43 o 7 7 -17 23.76 27.60 78.26 o 8 7 -17 6.75 -16.60 55.27 o 9 7 -17 133.10 110.55 55.14 o 1 8 -17 27.31 0.00 49.33 o 2 8 -17 55.36 63.19 66.29 o 3 8 -17 90.53 79.03 66.29 o 4 8 -17 26.27 96.68 78.16 o 5 8 -17 123.49 -23.66 66.44 o 6 8 -17 22.25 147.58 86.39 o 10 0 -16 332.67 83.43 111.15 o 12 0 -16 234.52 222.26 194.55 o 7 1 -16 111.17 111.11 222.22 o 8 1 -16 289.07 333.43 83.43 o 9 1 -16 33.08 55.68 83.39 o 10 1 -16 15.16 63.14 97.24 o 11 1 -16 97.41 111.10 111.10 o 12 1 -16 69.69 0.00 111.10 o 16 1 -16 109.74 83.40 55.69 o 9 2 -16 77.47 27.71 83.39 o 10 2 -16 49.50 223.30 83.67 o 11 2 -16 226.44 250.96 96.86 o 12 2 -16 216.29 277.68 83.14 o 13 2 -16 75.96 27.71 55.41 o 14 2 -16 17.62 0.00 55.41 o 15 2 -16 57.67 221.91 111.09 o 16 2 -16 10.18 -27.70 55.40 o 6 3 -16 62.22 55.69 55.69 o 7 3 -16 373.18 524.16 98.40 o 8 3 -16 27.41 37.14 32.04 o 9 3 -16 47.39 34.20 44.37 o 10 3 -16 77.54 77.64 46.15 o 11 3 -16 60.67 59.59 40.38 o 12 3 -16 170.01 110.84 83.13 o 13 3 -16 18.45 27.70 83.11 o 14 3 -16 67.24 110.82 83.11 o 15 3 -16 213.12 387.68 110.85 o 0 4 -16 528.43 389.05 138.93 o 1 4 -16 210.83 210.38 83.42 o 2 4 -16 103.80 115.05 69.55 o 3 4 -16 36.84 -38.80 46.31 o 4 4 -16 116.87 206.27 110.97 o 5 4 -16 50.04 110.98 97.10 o 6 4 -16 93.32 83.26 83.40 o 7 4 -16 130.96 182.09 56.05 o 8 4 -16 108.40 130.72 40.35 o 9 4 -16 285.46 248.25 51.97 o 10 4 -16 175.80 130.71 40.32 o 11 4 -16 48.07 155.03 55.27 o 12 4 -16 12.50 83.11 83.11 o 13 4 -16 108.85 165.96 110.55 o 14 4 -16 19.73 110.53 110.53 o 15 4 -16 36.80 110.54 110.54 o 1 5 -16 43.49 44.33 46.10 o 2 5 -16 52.33 0.00 83.11 o 3 5 -16 243.73 383.98 78.39 o 4 5 -16 108.07 273.08 66.50 o 5 5 -16 958.00 943.15 89.51 o 6 5 -16 190.78 201.83 56.85 o 7 5 -16 183.29 178.70 42.45 o 8 5 -16 49.70 67.89 51.82 o 9 5 -16 220.99 162.33 66.12 o 10 5 -16 1.09 23.73 124.38 o 11 5 -16 65.02 36.79 138.11 o 12 5 -16 34.99 27.70 82.83 o 13 5 -16 91.21 165.68 110.55 o 14 5 -16 41.57 27.70 82.83 o 0 6 -16 456.77 636.57 166.07 o 1 6 -16 113.05 138.35 83.12 o 2 6 -16 142.06 99.64 55.28 o 3 6 -16 234.59 207.41 58.69 o 4 6 -16 337.62 315.67 71.27 o 5 6 -16 32.72 11.08 83.11 o 6 6 -16 95.15 46.12 49.54 o 7 6 -16 215.34 315.73 193.29 o 8 6 -16 154.68 142.08 66.30 o 9 6 -16 32.12 -3.97 66.29 o 10 6 -16 75.97 193.38 78.17 o 11 6 -16 26.54 0.00 82.83 o 12 6 -16 5.36 27.70 82.83 o 13 6 -16 40.98 -82.83 110.54 o 1 7 -16 47.22 165.67 110.54 o 2 7 -16 117.10 183.00 96.56 o 3 7 -16 270.78 307.31 110.31 o 4 7 -16 240.27 193.58 83.00 o 5 7 -16 56.95 138.15 82.84 o 6 7 -16 76.46 43.27 82.84 o 7 7 -16 304.99 390.07 110.45 o 8 7 -16 47.49 -23.62 66.29 o 9 7 -16 101.68 165.82 49.34 o 10 7 -16 34.11 55.13 110.54 o 11 7 -16 87.96 303.93 82.84 o 0 8 -16 295.87 303.77 82.87 o 1 8 -16 10.36 0.00 82.83 o 2 8 -16 166.94 186.39 71.03 o 3 8 -16 111.74 102.61 66.30 o 4 8 -16 61.14 209.10 82.70 o 5 8 -16 28.77 -44.30 124.39 o 6 8 -16 89.78 47.35 66.29 o 7 8 -16 258.36 340.64 66.45 o 8 8 -16 45.87 -43.54 110.54 o 9 8 -16 9.85 82.83 138.23 o 1 9 -16 36.74 41.42 38.98 o 2 9 -16 29.41 153.92 66.29 o 3 9 -16 91.41 39.57 66.29 o 4 9 -16 91.97 151.99 58.68 o 5 9 -16 93.61 86.96 124.40 o 6 9 -16 70.01 96.85 58.67 o 2 0 -15 196.43 167.61 46.42 o 4 0 -15 740.04 603.29 72.01 o 6 0 -15 763.41 668.38 139.28 o 8 0 -15 352.30 222.60 55.72 o 10 0 -15 125.64 83.40 83.40 o 12 0 -15 36.88 55.68 55.68 o 14 0 -15 57.37 0.00 55.69 o 0 1 -15 1246.93 912.60 107.50 o 1 1 -15 112.85 61.32 44.31 o 2 1 -15 93.62 176.53 60.39 o 3 1 -15 30.59 13.87 32.87 o 4 1 -15 224.16 152.63 44.37 o 5 1 -15 21.74 12.74 30.04 o 6 1 -15 62.99 152.93 58.97 o 7 1 -15 68.23 97.25 58.97 o 8 1 -15 178.46 123.12 111.26 o 9 1 -15 8.88 -11.28 111.22 o 10 1 -15 859.25 925.66 118.77 o 11 1 -15 114.43 148.69 48.26 o 12 1 -15 118.98 133.24 43.00 o 13 1 -15 216.86 247.65 138.98 o 14 1 -15 5.41 16.61 46.31 o 16 1 -15 51.53 111.09 55.69 o 17 1 -15 42.11 0.00 83.39 o 18 1 -15 60.02 0.00 83.39 o 1 2 -15 540.83 460.87 51.15 o 2 2 -15 46.02 13.89 27.91 o 3 2 -15 250.64 155.57 46.46 o 4 2 -15 395.92 425.11 60.83 o 5 2 -15 172.00 155.78 55.42 o 6 2 -15 328.89 186.03 97.44 o 7 2 -15 72.61 150.01 46.31 o 8 2 -15 104.42 27.71 58.97 o 9 2 -15 20.63 17.42 35.60 o 10 2 -15 65.62 22.28 37.20 o 11 2 -15 25.28 -2.75 32.80 o 12 2 -15 164.74 163.68 222.38 o 13 2 -15 24.06 38.93 32.74 o 14 2 -15 542.42 521.13 73.24 o 15 2 -15 2.82 27.70 83.11 o 16 2 -15 16.02 -27.70 55.40 o 17 2 -15 188.65 221.96 110.84 o 0 3 -15 388.22 222.90 46.39 o 1 3 -15 397.48 307.77 46.36 o 2 3 -15 61.95 5.52 46.31 o 3 3 -15 643.22 590.09 59.04 o 4 3 -15 235.99 144.54 46.33 o 5 3 -15 481.98 504.10 69.46 o 6 3 -15 65.53 80.05 72.95 o 7 3 -15 59.07 94.13 42.75 o 8 3 -15 5.86 37.15 30.39 o 9 3 -15 206.65 199.01 58.86 o 10 3 -15 194.00 123.11 26.37 o 11 3 -15 102.44 91.25 31.43 o 12 3 -15 43.62 -6.91 30.40 o 13 3 -15 41.44 23.10 30.34 o 14 3 -15 7.99 38.98 46.26 o 15 3 -15 9.61 55.40 110.81 o 16 3 -15 29.60 221.35 110.81 o 17 3 -15 58.58 55.41 55.41 o 1 4 -15 481.08 417.66 98.23 o 2 4 -15 251.91 219.57 52.90 o 3 4 -15 55.33 34.63 40.88 o 4 4 -15 38.08 44.61 48.38 o 5 4 -15 148.44 120.28 48.10 o 6 4 -15 36.99 67.40 40.45 o 7 4 -15 747.65 814.94 75.42 o 8 4 -15 3.74 -11.89 24.20 o 9 4 -15 112.23 111.00 44.08 o 10 4 -15 35.92 57.96 29.88 o 11 4 -15 65.13 62.46 41.59 o 12 4 -15 65.11 49.81 32.60 o 13 4 -15 248.62 164.26 42.59 o 14 4 -15 61.60 138.25 110.54 o 15 4 -15 5.83 -55.40 55.40 o 16 4 -15 111.18 138.26 82.84 o 0 5 -15 173.62 277.11 83.13 o 1 5 -15 218.13 263.86 58.79 o 2 5 -15 788.37 793.24 106.57 o 3 5 -15 436.02 325.72 71.32 o 4 5 -15 116.30 124.55 124.55 o 5 5 -15 155.86 160.53 66.73 o 6 5 -15 20.72 43.38 40.21 o 7 5 -15 247.62 170.16 42.44 o 8 5 -15 127.11 161.84 46.69 o 9 5 -15 61.79 75.64 35.07 o 10 5 -15 108.68 90.93 63.83 o 11 5 -15 85.16 48.43 50.34 o 12 5 -15 97.71 75.89 73.21 o 13 5 -15 67.19 110.54 82.84 o 15 5 -15 35.72 55.13 82.83 o 16 5 -15 4.22 138.23 110.53 o 1 6 -15 71.82 121.45 82.98 o 2 6 -15 27.40 86.92 165.80 o 3 6 -15 41.74 80.12 38.47 o 4 6 -15 501.73 607.73 98.77 o 5 6 -15 766.06 982.66 99.02 o 6 6 -15 466.06 502.13 65.23 o 7 6 -15 416.87 373.36 43.68 o 8 6 -15 130.49 91.98 31.94 o 9 6 -15 8.27 96.78 52.32 o 10 6 -15 21.26 -27.52 82.97 o 11 6 -15 97.58 55.30 46.06 o 12 6 -15 14.93 27.70 110.53 o 13 6 -15 55.91 82.84 82.84 o 14 6 -15 100.68 110.23 66.15 o 15 6 -15 190.05 102.37 66.16 o 0 7 -15 376.65 358.99 110.61 o 1 7 -15 310.49 412.16 78.10 o 2 7 -15 324.29 215.71 110.46 o 3 7 -15 42.31 68.97 78.06 o 4 7 -15 31.35 -55.27 110.40 o 5 7 -15 57.89 82.84 45.90 o 6 7 -15 66.46 122.29 66.29 o 7 7 -15 41.97 55.27 49.33 o 8 7 -15 56.71 88.33 46.06 o 9 7 -15 900.98 927.78 193.11 o 10 7 -15 212.56 186.16 40.16 o 11 7 -15 16.25 -27.70 55.40 o 12 7 -15 21.25 55.41 110.81 o 13 7 -15 32.39 27.70 55.41 o 1 8 -15 238.27 223.76 58.59 o 2 8 -15 25.88 18.35 49.33 o 3 8 -15 26.16 41.42 41.42 o 4 8 -15 19.46 33.10 45.89 o 5 8 -15 496.99 580.70 151.80 o 6 8 -15 124.86 193.40 58.58 o 7 8 -15 60.07 41.56 124.39 o 8 8 -15 66.51 165.81 78.17 o 9 8 -15 58.82 46.02 49.36 o 10 8 -15 25.30 27.70 83.11 o 11 8 -15 28.86 83.11 83.11 o 12 8 -15 18.17 110.81 110.81 o 0 9 -15 16.99 110.53 110.53 o 1 9 -15 48.33 -11.07 45.90 o 2 9 -15 330.04 330.92 66.32 o 3 9 -15 161.03 201.35 66.30 o 4 9 -15 8.67 35.48 66.28 o 5 9 -15 2.53 -27.70 39.18 o 6 9 -15 2.40 -43.54 66.28 o 7 9 -15 42.55 -138.38 110.68 o 8 9 -15 229.37 166.03 83.28 o 9 9 -15 108.05 27.71 55.41 o 1 10 -15 84.09 27.71 78.17 o 2 10 -15 75.79 122.53 110.68 o 3 10 -15 176.55 179.81 58.68 o 4 10 -15 86.16 86.84 69.13 o 5 10 -15 116.98 162.17 66.50 o 6 10 -15 20.26 35.62 66.49 o 0 0 -14 689.30 783.24 167.86 o 2 0 -14 2930.74 2817.37 256.04 o 4 0 -14 89.80 50.24 46.47 o 6 0 -14 79.01 66.87 153.36 o 8 0 -14 1101.82 1022.34 113.38 o 10 0 -14 370.40 240.67 55.58 o 12 0 -14 1342.47 1506.09 159.58 o 14 0 -14 305.10 278.28 111.42 o 16 0 -14 114.37 139.09 111.11 o 1 1 -14 414.77 407.49 48.47 o 2 1 -14 27.18 16.64 32.83 o 3 1 -14 746.80 608.12 54.32 o 4 1 -14 338.32 349.89 33.99 o 5 1 -14 86.00 94.73 32.80 o 6 1 -14 187.55 170.18 33.99 o 7 1 -14 2.07 -32.48 21.65 o 8 1 -14 319.42 215.75 41.75 o 9 1 -14 196.34 163.92 36.04 o 10 1 -14 55.88 23.59 28.26 o 11 1 -14 76.05 66.47 28.26 o 12 1 -14 127.17 108.51 36.70 o 13 1 -14 596.02 568.79 71.36 o 14 1 -14 64.42 27.70 39.38 o 15 1 -14 60.81 -13.85 58.97 o 16 1 -14 131.50 137.56 111.11 o 17 1 -14 61.52 166.78 83.39 o 18 1 -14 103.16 111.10 83.40 o 19 1 -14 9.89 -27.70 83.38 o 0 2 -14 573.12 749.23 87.30 o 1 2 -14 504.43 449.50 51.15 o 2 2 -14 1275.11 1097.69 82.07 o 3 2 -14 79.00 38.10 36.27 o 4 2 -14 170.04 117.48 35.96 o 5 2 -14 141.79 108.76 32.86 o 6 2 -14 101.64 108.94 30.09 o 7 2 -14 8.33 -12.48 27.67 o 8 2 -14 132.57 123.81 40.31 o 9 2 -14 421.76 297.96 60.27 o 10 2 -14 128.22 68.33 37.59 o 11 2 -14 101.10 41.80 29.81 o 12 2 -14 260.95 188.98 48.27 o 13 2 -14 41.95 75.43 28.61 o 14 2 -14 3.88 23.86 26.34 o 15 2 -14 51.11 39.66 40.42 o 16 2 -14 64.52 -27.70 55.41 o 17 2 -14 19.71 -27.70 55.41 o 18 2 -14 73.85 166.23 55.41 o 19 2 -14 122.26 83.12 55.41 o 1 3 -14 105.40 130.49 33.97 o 2 3 -14 382.77 328.69 50.96 o 3 3 -14 77.49 132.87 56.15 o 4 3 -14 346.22 378.11 44.33 o 5 3 -14 757.47 686.90 61.68 o 6 3 -14 382.33 464.85 39.12 o 7 3 -14 364.38 305.69 36.09 o 8 3 -14 78.02 115.59 30.03 o 9 3 -14 111.85 103.90 26.73 o 10 3 -14 26.97 9.23 26.92 o 11 3 -14 106.71 97.23 26.35 o 12 3 -14 33.83 56.75 31.32 o 13 3 -14 53.90 9.75 20.42 o 14 3 -14 557.77 527.83 53.64 o 15 3 -14 279.06 320.53 80.29 o 16 3 -14 30.95 83.11 83.11 o 17 3 -14 22.54 83.11 83.11 o 18 3 -14 0.30 27.70 55.40 o 0 4 -14 219.15 178.61 56.35 o 1 4 -14 453.69 466.19 34.87 o 2 4 -14 78.26 52.14 28.99 o 3 4 -14 455.94 406.49 45.23 o 4 4 -14 89.18 44.89 25.68 o 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1015.37 o 3 2 1 887.57 882.01 40.35 o 4 2 1 8281.69 8320.60 271.62 o 5 2 1 22693.45 23487.31 946.96 o 6 2 1 33615.32 36840.93 1332.03 o 7 2 1 9379.75 9986.58 297.59 o 8 2 1 7065.29 7165.07 226.87 o 9 2 1 217.67 168.76 19.81 o 10 2 1 376.65 319.68 21.25 o 11 2 1 1195.41 1471.80 57.55 o 12 2 1 732.03 676.24 47.21 o 13 2 1 1065.28 1010.57 47.17 o 14 2 1 2828.30 2476.60 371.87 o 15 2 1 3718.48 3874.45 156.11 o 16 2 1 627.34 792.19 74.52 o 17 2 1 127.55 97.67 49.47 o 18 2 1 140.08 120.78 81.47 o 19 2 1 472.62 527.51 166.79 o 20 2 1 487.70 467.87 77.45 o 21 2 1 88.46 32.93 45.71 o 22 2 1 154.29 98.48 55.14 o 23 2 1 113.05 38.48 150.73 o 24 2 1 513.83 713.96 164.70 o 25 2 1 40.24 109.71 82.28 o 26 2 1 284.94 -54.88 164.35 o 0 3 1 19946.63 20385.30 1088.79 o 1 3 1 25082.40 25905.80 1250.24 o 2 3 1 12681.10 12742.49 426.07 o 3 3 1 1862.33 1994.76 68.54 o 4 3 1 4195.14 4152.66 124.63 o 5 3 1 4597.02 4585.32 147.69 o 6 3 1 946.53 1002.08 34.82 o 7 3 1 2300.30 2057.10 72.14 o 8 3 1 9300.13 9392.59 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56.17 o 3 7 2 1699.09 1650.43 59.94 o 4 7 2 2924.36 2907.45 90.56 o 5 7 2 6499.54 6669.13 212.52 o 6 7 2 1290.71 1258.79 51.96 o 7 7 2 2485.21 2610.39 97.44 o 8 7 2 1274.69 1301.28 49.63 o 9 7 2 472.03 362.51 48.24 o 10 7 2 53.94 99.01 19.71 o 11 7 2 539.18 543.21 39.15 o 12 7 2 161.31 222.19 36.10 o 13 7 2 742.22 638.93 61.26 o 14 7 2 164.35 210.98 31.72 o 15 7 2 637.02 730.69 52.59 o 16 7 2 120.29 111.61 39.69 o 17 7 2 66.76 81.29 32.24 o 18 7 2 296.12 136.20 65.02 o 19 7 2 61.38 43.87 22.57 o 20 7 2 273.93 294.49 53.28 o 21 7 2 87.18 37.40 55.27 o 22 7 2 60.61 78.98 27.38 o 23 7 2 118.30 151.91 47.00 o 0 8 2 8177.47 8545.28 398.45 o 1 8 2 2009.42 2121.36 90.52 o 2 8 2 1755.54 1880.88 73.71 o 3 8 2 1069.99 1076.99 47.97 o 4 8 2 3954.27 4039.59 152.20 o 5 8 2 21.68 46.43 20.46 o 6 8 2 1947.23 1755.04 110.23 o 7 8 2 304.44 349.50 30.48 o 8 8 2 956.09 984.77 49.56 o 9 8 2 4660.50 5010.40 214.24 o 10 8 2 445.02 403.87 30.55 o 11 8 2 106.61 74.15 19.65 o 12 8 2 912.25 905.98 55.11 o 13 8 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49.85 o 4 14 2 93.62 97.62 59.16 o 5 14 2 16.43 22.32 46.40 o 6 14 2 101.66 93.09 55.41 o 7 14 2 67.78 0.00 39.38 o 8 14 2 3.40 47.73 66.81 o 9 14 2 111.18 97.50 59.07 o 10 14 2 230.49 315.66 70.53 o 11 14 2 36.79 97.58 125.50 o 1 15 2 5.14 35.84 66.95 o 2 15 2 71.04 -11.18 46.36 o 3 15 2 61.38 -74.12 55.55 o 4 15 2 77.87 229.21 87.13 o 5 15 2 99.39 108.07 180.51 o 6 15 2 55.59 0.00 49.98 o 2 0 3 11685.21 11745.66 657.65 o 4 0 3 38580.48 43532.22 2246.92 o 6 0 3 9286.43 8760.32 509.79 o 8 0 3 12356.09 12026.35 488.65 o 10 0 3 240.80 270.88 36.18 o 12 0 3 2166.53 1966.58 117.49 o 14 0 3 693.25 487.03 49.42 o 16 0 3 96.85 81.46 54.31 o 18 0 3 158.15 217.53 81.47 o 20 0 3 49.00 -108.88 81.73 o 22 0 3 150.53 244.95 81.74 o 0 1 3 29775.74 33772.50 1786.63 o 1 1 3 14396.80 13452.15 549.89 o 2 1 3 12801.67 12861.03 441.50 o 3 1 3 2053.12 1938.52 73.60 o 4 1 3 7321.90 7028.13 255.08 o 5 1 3 1752.56 1580.94 59.02 o 6 1 3 3616.04 3338.98 114.45 o 7 1 3 2377.06 2205.00 75.88 o 8 1 3 1986.21 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5204.95 5305.89 198.44 o 2 4 3 176.80 203.92 29.15 o 3 4 3 2654.81 2745.02 81.00 o 4 4 3 1492.65 1381.16 65.92 o 5 4 3 9040.88 8792.72 241.25 o 6 4 3 7646.98 7421.39 218.25 o 7 4 3 9326.05 9820.38 288.53 o 8 4 3 65.94 55.41 22.00 o 9 4 3 1964.56 1966.05 67.95 o 10 4 3 521.48 506.07 35.72 o 11 4 3 1881.77 1951.55 79.51 o 12 4 3 321.33 342.01 35.71 o 13 4 3 879.75 898.80 57.39 o 14 4 3 739.46 632.08 47.78 o 15 4 3 842.12 861.34 54.44 o 16 4 3 297.62 322.77 35.63 o 17 4 3 79.94 96.21 29.60 o 18 4 3 44.09 64.82 54.72 o 19 4 3 55.41 55.98 15.98 o 20 4 3 268.58 305.71 31.06 o 21 4 3 42.78 57.84 23.73 o 22 4 3 16.12 109.98 109.98 o 23 4 3 64.19 109.71 109.71 o 24 4 3 18.03 0.00 82.28 o 25 4 3 1.37 82.27 136.85 o 0 5 3 17185.20 17668.48 1047.66 o 1 5 3 4352.37 4411.77 143.56 o 2 5 3 636.42 612.71 33.37 o 3 5 3 667.73 677.66 40.53 o 4 5 3 799.30 722.98 60.60 o 5 5 3 1126.43 1117.85 66.07 o 6 5 3 65.01 104.15 19.54 o 7 5 3 3873.28 3802.48 116.76 o 8 5 3 227.06 308.25 36.12 o 9 5 3 2025.27 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4812.61 172.57 o 7 8 3 1923.24 1863.69 100.91 o 8 8 3 550.32 611.41 35.82 o 9 8 3 408.38 399.34 51.22 o 10 8 3 297.90 311.07 30.43 o 11 8 3 122.99 159.33 24.88 o 12 8 3 233.19 252.85 33.65 o 13 8 3 79.75 118.40 22.94 o 14 8 3 370.27 390.83 33.80 o 15 8 3 132.83 102.84 39.68 o 16 8 3 613.26 731.15 58.16 o 17 8 3 157.14 145.59 29.76 o 18 8 3 112.04 65.79 35.49 o 19 8 3 58.68 -66.80 82.84 o 20 8 3 25.35 16.83 55.41 o 21 8 3 56.32 0.00 50.29 o 22 8 3 30.18 22.47 46.79 o 0 9 3 9127.98 9938.75 616.35 o 1 9 3 1803.20 1763.32 77.43 o 2 9 3 5106.79 5557.91 206.48 o 3 9 3 1027.87 1071.05 67.86 o 4 9 3 251.35 274.30 36.48 o 5 9 3 280.69 345.49 28.30 o 6 9 3 557.00 530.73 37.53 o 7 9 3 1532.34 1573.94 95.29 o 8 9 3 344.35 406.43 34.59 o 9 9 3 249.52 273.95 26.97 o 10 9 3 1430.40 1551.96 107.28 o 11 9 3 160.23 164.81 29.92 o 12 9 3 366.98 385.27 39.11 o 13 9 3 408.60 415.94 44.42 o 14 9 3 203.12 141.65 32.68 o 15 9 3 10.06 -6.97 27.74 o 16 9 3 199.78 104.12 35.57 o 17 9 3 7.20 6.98 22.73 o 18 9 3 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1182.84 127.17 o 7 12 4 166.91 150.26 32.86 o 8 12 4 131.58 130.96 32.31 o 9 12 4 100.88 131.36 52.67 o 10 12 4 21.37 0.00 32.70 o 11 12 4 46.90 52.00 67.09 o 12 12 4 151.46 176.23 42.75 o 13 12 4 0.82 -16.79 55.96 o 14 12 4 22.54 69.81 59.16 o 15 12 4 1.37 111.64 83.66 o 1 13 4 88.82 9.34 50.03 o 2 13 4 24.88 111.55 83.94 o 3 13 4 371.94 471.39 107.34 o 4 13 4 19.38 44.71 42.09 o 5 13 4 42.24 21.43 42.85 o 6 13 4 117.31 241.85 116.43 o 7 13 4 375.88 318.58 68.60 o 8 13 4 132.86 -4.26 42.87 o 9 13 4 48.45 100.60 46.52 o 10 13 4 136.20 167.54 49.86 o 11 13 4 121.00 199.96 126.07 o 12 13 4 16.59 23.90 67.09 o 13 13 4 91.36 251.02 111.65 o 0 14 4 23.17 27.98 55.68 o 1 14 4 18.03 18.53 111.50 o 2 14 4 109.98 69.77 78.86 o 3 14 4 9.30 97.65 59.16 o 4 14 4 115.29 122.77 46.52 o 5 14 4 4.46 37.01 69.67 o 6 14 4 134.84 139.46 59.07 o 7 14 4 50.74 43.84 66.89 o 8 14 4 83.09 139.39 125.09 o 9 14 4 231.88 296.26 66.91 o 10 14 4 219.43 272.78 87.09 o 1 15 4 44.86 135.34 66.95 o 2 15 4 33.06 -31.80 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6854.37 229.83 o 4 2 5 2522.09 2545.59 100.45 o 5 2 5 10155.27 10009.82 344.73 o 6 2 5 3083.71 3262.42 112.81 o 7 2 5 7332.71 7413.93 254.63 o 8 2 5 1833.96 1582.55 71.82 o 9 2 5 1304.69 1373.53 64.74 o 10 2 5 1456.56 1411.80 71.72 o 11 2 5 1184.63 1197.14 52.46 o 12 2 5 311.88 293.14 39.41 o 13 2 5 4273.06 4064.23 248.39 o 14 2 5 688.97 641.45 39.44 o 15 2 5 993.03 956.04 74.98 o 16 2 5 253.37 277.73 27.72 o 17 2 5 373.19 222.90 55.73 o 18 2 5 849.58 918.85 167.06 o 0 3 5 14852.81 14468.42 634.16 o 1 3 5 5811.14 5651.51 208.49 o 2 3 5 5266.28 4935.82 199.91 o 3 3 5 1037.39 860.83 52.43 o 4 3 5 940.83 925.04 64.61 o 5 3 5 2607.99 2380.47 92.78 o 6 3 5 2574.78 2243.32 128.52 o 7 3 5 872.36 785.11 59.44 o 8 3 5 11553.66 11827.78 520.73 o 9 3 5 3514.55 3409.88 140.99 o 10 3 5 1571.38 1583.75 79.42 o 11 3 5 808.77 779.81 57.76 o 12 3 5 1108.09 1128.32 68.38 o 13 3 5 1210.72 1192.45 77.02 o 14 3 5 358.10 370.27 37.05 o 15 3 5 698.46 667.08 42.83 o 16 3 5 363.03 389.63 35.48 o 17 3 5 252.18 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5 84.65 -27.43 82.01 o 0 7 5 5314.02 5077.04 259.66 o 1 7 5 210.74 183.31 30.03 o 2 7 5 436.02 437.21 36.57 o 3 7 5 545.81 544.48 44.25 o 4 7 5 485.43 480.20 50.53 o 5 7 5 178.47 211.13 32.73 o 6 7 5 991.40 972.95 55.82 o 7 7 5 26.96 36.84 23.10 o 8 7 5 2203.77 2206.40 93.74 o 9 7 5 55.55 49.31 13.44 o 10 7 5 462.52 512.80 37.28 o 11 7 5 528.60 633.23 44.08 o 12 7 5 50.29 27.68 20.85 o 13 7 5 1548.73 1662.39 108.37 o 14 7 5 7.19 13.87 29.44 o 15 7 5 538.59 634.15 57.17 o 16 7 5 91.56 110.87 31.99 o 17 7 5 3.63 46.17 31.98 o 18 7 5 185.50 235.38 40.40 o 19 7 5 20.00 27.76 68.84 o 20 7 5 62.68 18.65 25.12 o 21 7 5 46.43 33.46 97.52 o 22 7 5 3.69 28.09 68.42 o 1 8 5 967.44 1184.23 89.83 o 2 8 5 147.87 139.29 32.77 o 3 8 5 1585.64 1715.34 78.89 o 4 8 5 2972.09 3116.42 137.34 o 5 8 5 1361.79 1326.74 90.07 o 6 8 5 152.43 141.86 30.07 o 7 8 5 8.20 40.17 17.12 o 8 8 5 552.49 591.33 37.94 o 9 8 5 178.79 147.88 19.53 o 10 8 5 84.21 131.31 25.52 o 11 8 5 60.85 62.64 27.81 o 12 8 5 268.02 227.27 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10109.14 10497.30 309.24 o 8 2 7 2043.63 2032.11 72.91 o 9 2 7 1342.03 1154.05 51.13 o 10 2 7 1056.28 1048.87 51.00 o 11 2 7 176.06 164.50 33.41 o 12 2 7 454.17 384.51 32.24 o 13 2 7 629.73 587.72 42.84 o 14 2 7 1236.80 1324.01 75.08 o 15 2 7 1279.95 1247.15 113.60 o 16 2 7 76.61 83.39 19.69 o 17 2 7 534.93 560.97 49.68 o 18 2 7 89.16 55.51 41.56 o 19 2 7 15.23 55.68 27.98 o 20 2 7 325.20 389.72 83.43 o 0 3 7 2054.16 2008.25 87.40 o 1 3 7 3287.08 3176.94 113.99 o 2 3 7 5179.56 5116.55 163.33 o 3 3 7 2734.02 2783.67 92.72 o 4 3 7 3027.92 2756.17 97.92 o 5 3 7 1073.44 905.18 48.94 o 6 3 7 4676.67 5008.90 174.52 o 7 3 7 680.75 601.47 36.41 o 8 3 7 6414.48 6474.50 216.32 o 9 3 7 1498.61 1461.06 74.32 o 10 3 7 2669.39 2577.83 114.31 o 11 3 7 1355.26 1455.11 71.62 o 12 3 7 1938.44 1763.89 143.23 o 13 3 7 641.83 632.52 49.90 o 14 3 7 149.06 199.20 39.39 o 15 3 7 51.66 41.83 41.83 o 16 3 7 21.08 0.00 19.69 o 17 3 7 45.79 46.33 24.83 o 18 3 7 67.35 37.06 24.83 o 19 3 7 107.40 73.82 28.40 o 20 3 7 39.09 -27.98 55.96 o 1 4 7 6978.26 6743.61 301.34 o 2 4 7 879.10 835.59 52.36 o 3 4 7 1535.58 1452.96 87.71 o 4 4 7 84.11 111.85 55.70 o 5 4 7 2550.39 2497.35 128.33 o 6 4 7 599.90 532.80 59.27 o 7 4 7 158.77 169.61 39.49 o 8 4 7 461.05 416.65 69.07 o 9 4 7 851.94 709.04 81.91 o 10 4 7 485.29 526.63 67.96 o 11 4 7 74.11 97.56 39.48 o 12 4 7 775.82 825.08 79.19 o 13 4 7 348.01 337.32 39.50 o 14 4 7 732.26 754.87 79.07 o 15 4 7 26.05 18.62 27.84 o 16 4 7 35.26 18.65 25.03 o 17 4 7 142.83 187.54 41.70 o 18 4 7 35.43 18.65 25.03 o 19 4 7 7.04 37.12 24.85 o 20 4 7 45.98 55.13 27.43 o 21 4 7 20.19 27.43 27.43 o 0 5 7 2429.17 2592.59 197.37 o 1 5 7 321.28 251.93 39.61 o 2 5 7 365.03 462.32 59.32 o 3 5 7 1677.87 1363.14 87.78 o 4 5 7 921.37 869.83 79.26 o 5 5 7 1163.50 1139.14 93.28 o 6 5 7 2457.71 2448.21 128.24 o 7 5 7 2325.51 2259.48 128.21 o 8 5 7 3302.39 3210.80 196.41 o 9 5 7 2649.64 2848.83 161.15 o 10 5 7 1211.02 1314.16 187.00 o 11 5 7 745.97 644.34 59.36 o 12 5 7 766.87 704.89 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371.68 59.29 o 14 10 7 398.71 544.02 221.91 o 15 10 7 71.73 128.12 46.36 o 16 10 7 103.00 27.71 55.69 o 17 10 7 12.20 83.66 83.66 o 18 10 7 2.48 55.96 55.96 o 0 11 7 220.76 322.31 78.88 o 1 11 7 144.35 197.11 47.31 o 2 11 7 946.93 878.53 108.84 o 3 11 7 187.62 308.09 57.38 o 4 11 7 86.61 130.88 48.30 o 5 11 7 184.33 167.66 52.30 o 6 11 7 153.08 200.45 52.31 o 7 11 7 78.64 123.66 40.66 o 8 11 7 416.64 460.79 83.37 o 9 11 7 371.31 303.56 57.51 o 10 11 7 286.03 353.55 52.44 o 11 11 7 190.89 247.90 67.09 o 12 11 7 545.86 744.07 99.01 o 13 11 7 52.24 97.73 59.26 o 14 11 7 76.95 134.51 83.53 o 15 11 7 16.13 27.70 83.38 o 16 11 7 13.59 0.00 83.38 o 1 12 7 141.10 167.50 59.17 o 2 12 7 202.34 184.01 82.95 o 3 12 7 111.58 83.72 64.47 o 4 12 7 39.75 0.03 78.94 o 5 12 7 346.13 365.97 71.41 o 6 12 7 112.33 91.36 52.24 o 7 12 7 58.04 25.76 42.85 o 8 12 7 224.91 223.30 52.32 o 9 12 7 3.51 -13.99 59.35 o 10 12 7 103.56 37.31 55.97 o 11 12 7 46.23 179.80 67.07 o 12 12 7 17.98 127.63 84.22 o 13 12 7 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12 4 8 802.66 895.70 79.09 o 13 4 8 289.43 271.73 41.16 o 14 4 8 154.26 83.76 39.48 o 15 4 8 240.67 215.10 56.26 o 16 4 8 57.67 69.82 39.57 o 17 4 8 403.94 599.00 84.70 o 18 4 8 90.43 69.79 39.48 o 19 4 8 508.12 429.76 51.57 o 20 4 8 129.64 137.43 55.14 o 21 4 8 581.04 466.42 82.36 o 1 5 8 1781.33 1602.53 127.41 o 2 5 8 2470.40 2636.41 139.40 o 3 5 8 966.20 773.13 67.28 o 4 5 8 1056.17 1171.68 99.75 o 5 5 8 1683.53 1813.59 166.58 o 6 5 8 3083.77 3347.88 280.18 o 7 5 8 2474.97 2381.25 140.50 o 8 5 8 739.97 859.56 93.20 o 9 5 8 21.62 46.63 27.98 o 10 5 8 382.80 433.56 59.21 o 11 5 8 210.41 175.65 56.54 o 12 5 8 162.80 125.64 39.48 o 13 5 8 8.69 69.91 70.09 o 14 5 8 5.10 37.06 24.83 o 15 5 8 9.48 -18.65 25.03 o 16 5 8 425.10 399.84 59.40 o 17 5 8 449.83 499.96 79.20 o 18 5 8 109.84 97.95 39.58 o 19 5 8 104.45 111.94 39.58 o 20 5 8 13.48 0.00 27.70 o 21 5 8 5.87 82.83 55.13 o 22 5 8 62.22 0.00 27.43 o 0 6 8 4725.96 5103.70 453.74 o 1 6 8 966.78 828.06 59.51 o 2 6 8 2369.72 2471.34 128.36 o 3 6 8 1063.96 838.39 197.94 o 4 6 8 616.02 606.85 67.34 o 5 6 8 647.36 757.64 155.11 o 6 6 8 877.94 784.61 79.31 o 7 6 8 2032.81 1653.05 125.99 o 8 6 8 473.52 465.32 59.32 o 9 6 8 1323.70 1256.69 185.49 o 10 6 8 837.39 764.73 67.05 o 11 6 8 328.88 294.10 82.47 o 12 6 8 538.41 582.09 87.35 o 13 6 8 19.95 55.82 55.54 o 14 6 8 196.53 271.51 46.48 o 15 6 8 13.01 -9.45 69.81 o 16 6 8 8.04 0.00 41.83 o 17 6 8 55.45 97.80 39.57 o 18 6 8 220.77 185.83 46.69 o 19 6 8 170.35 112.50 56.25 o 20 6 8 66.59 56.24 56.24 o 21 6 8 69.45 111.93 55.96 o 22 6 8 64.93 110.82 55.41 o 1 7 8 1373.52 1546.04 113.56 o 2 7 8 669.20 789.43 79.37 o 3 7 8 2218.25 2319.25 193.46 o 4 7 8 25.67 18.65 27.98 o 5 7 8 3106.66 3181.20 248.72 o 6 7 8 244.87 349.86 97.71 o 7 7 8 1258.34 1222.51 140.17 o 8 7 8 34.12 153.76 39.57 o 9 7 8 327.78 204.94 46.43 o 10 7 8 75.67 13.89 39.48 o 11 7 8 136.62 164.71 46.46 o 12 7 8 261.23 321.25 57.65 o 13 7 8 454.87 402.06 81.38 o 14 7 8 31.45 27.84 55.55 o 15 7 8 834.84 940.39 107.14 o 16 7 8 64.62 69.68 41.70 o 17 7 8 551.15 596.10 67.01 o 18 7 8 57.20 50.40 46.47 o 19 7 8 7.88 0.00 56.24 o 20 7 8 31.52 84.77 56.51 o 21 7 8 7.22 56.51 56.51 o 0 8 8 421.30 392.37 84.02 o 1 8 8 1502.16 1486.07 169.58 o 2 8 8 2171.92 2335.78 208.25 o 3 8 8 1183.12 1245.00 93.54 o 4 8 8 199.33 140.05 59.48 o 5 8 8 572.56 437.45 84.74 o 6 8 8 80.73 55.97 39.58 o 7 8 8 42.62 27.98 55.96 o 8 8 8 315.36 199.41 69.86 o 9 8 8 1125.45 1143.90 128.43 o 10 8 8 101.81 106.05 97.39 o 11 8 8 483.09 573.22 59.31 o 12 8 8 203.36 122.76 83.14 o 13 8 8 187.40 218.80 98.79 o 14 8 8 75.95 156.41 42.53 o 15 8 8 126.24 111.33 46.20 o 16 8 8 9.76 -55.68 39.37 o 17 8 8 35.74 14.03 69.54 o 18 8 8 58.40 0.00 55.96 o 19 8 8 115.94 168.74 56.25 o 20 8 8 76.86 84.78 56.52 o 1 9 8 394.78 368.34 45.38 o 2 9 8 260.65 213.07 42.71 o 3 9 8 110.83 117.53 46.62 o 4 9 8 259.60 326.41 84.54 o 5 9 8 766.90 734.09 99.34 o 6 9 8 95.61 139.70 97.81 o 7 9 8 222.20 210.10 59.38 o 8 9 8 44.95 -44.77 46.56 o 9 9 8 150.61 243.91 46.53 o 10 9 8 12.32 72.78 84.08 o 11 9 8 107.05 72.59 46.46 o 12 9 8 596.32 729.57 92.84 o 13 9 8 208.44 165.16 46.48 o 14 9 8 159.08 184.12 54.87 o 15 9 8 2.68 33.33 46.19 o 16 9 8 352.13 363.83 78.69 o 17 9 8 26.72 167.05 83.66 o 18 9 8 3.61 0.00 55.96 o 0 10 8 11.51 -69.36 46.24 o 1 10 8 382.17 305.90 47.28 o 2 10 8 119.60 76.06 30.03 o 3 10 8 297.19 259.44 64.93 o 4 10 8 293.96 224.97 105.14 o 5 10 8 49.48 43.86 40.50 o 6 10 8 8.42 69.81 69.81 o 7 10 8 458.74 452.81 70.15 o 8 10 8 70.88 83.95 59.36 o 9 10 8 148.08 261.12 168.20 o 10 10 8 133.36 41.87 39.48 o 11 10 8 172.47 102.83 69.41 o 12 10 8 46.55 69.74 59.26 o 13 10 8 148.48 231.14 66.94 o 14 10 8 82.25 33.49 46.47 o 15 10 8 6.67 33.43 46.35 o 16 10 8 1.97 0.00 83.38 o 17 10 8 58.08 83.67 83.67 o 1 11 8 451.61 309.50 47.30 o 2 11 8 157.32 142.88 35.76 o 3 11 8 18.03 34.34 42.91 o 4 11 8 220.98 93.80 76.53 o 5 11 8 497.54 442.57 132.73 o 6 11 8 72.85 55.74 42.85 o 7 11 8 342.48 286.74 84.32 o 8 11 8 203.13 153.94 59.37 o 9 11 8 474.58 457.93 93.25 o 10 11 8 7.14 50.26 46.61 o 11 11 8 367.05 344.94 83.02 o 12 11 8 1.72 46.85 111.50 o 13 11 8 31.86 0.00 83.66 o 14 11 8 30.49 38.97 46.40 o 15 11 8 112.72 83.40 111.38 o 0 12 8 1440.44 1791.77 279.97 o 1 12 8 238.17 386.66 209.66 o 2 12 8 31.03 -3.96 67.09 o 3 12 8 7.46 51.89 40.58 o 4 12 8 191.67 223.28 57.47 o 5 12 8 29.96 -6.86 54.25 o 6 12 8 195.06 182.77 52.29 o 7 12 8 113.33 79.80 40.66 o 8 12 8 76.73 2.75 57.51 o 9 12 8 62.24 -13.99 59.36 o 10 12 8 768.63 812.59 183.35 o 11 12 8 104.99 211.72 67.08 o 12 12 8 132.13 129.22 98.36 o 13 12 8 54.37 41.95 79.04 o 1 13 8 28.21 103.51 66.95 o 2 13 8 13.55 55.80 66.95 o 3 13 8 212.77 321.17 125.81 o 4 13 8 228.24 223.25 97.55 o 5 13 8 23.60 139.62 46.40 o 6 13 8 108.97 67.05 83.81 o 7 13 8 135.35 315.01 67.10 o 8 13 8 73.24 223.58 125.78 o 9 13 8 10.21 -27.98 50.03 o 10 13 8 16.38 -6.17 111.78 o 0 14 8 69.83 111.37 83.67 o 1 14 8 57.99 72.49 46.36 o 2 14 8 115.76 161.05 87.14 o 3 14 8 65.62 39.85 66.95 o 4 14 8 8.07 10.50 125.49 o 5 14 8 1.79 -39.85 66.95 o 2 0 9 612.86 563.55 59.18 o 4 0 9 126.09 167.11 39.39 o 6 0 9 420.34 430.82 55.34 o 8 0 9 0.01 -13.85 39.37 o 10 0 9 7.11 46.51 27.70 o 12 0 9 965.56 1056.23 71.85 o 14 0 9 1539.69 1635.85 113.56 o 16 0 9 0.76 -18.50 24.80 o 18 0 9 158.27 27.71 83.41 o 20 0 9 33.80 55.41 55.41 o 0 1 9 16413.07 16230.83 773.05 o 1 1 9 1761.07 1692.60 72.64 o 2 1 9 420.75 580.49 56.22 o 3 1 9 162.00 163.66 22.01 o 4 1 9 108.50 203.54 30.01 o 5 1 9 302.94 287.38 27.87 o 6 1 9 1354.87 1214.03 76.20 o 7 1 9 927.27 916.56 51.14 o 8 1 9 236.71 255.94 30.02 o 9 1 9 687.13 665.36 47.33 o 10 1 9 1545.20 1750.19 92.53 o 11 1 9 603.98 662.19 45.61 o 12 1 9 205.05 209.78 30.01 o 13 1 9 781.08 829.28 55.71 o 14 1 9 18.37 52.10 51.59 o 15 1 9 84.05 102.56 19.96 o 16 1 9 107.51 138.71 32.94 o 17 1 9 31.59 62.44 34.50 o 18 1 9 170.95 194.57 58.98 o 19 1 9 152.52 197.80 70.24 o 20 1 9 104.14 -27.98 55.69 o 1 2 9 2806.98 2701.83 92.80 o 2 2 9 4447.93 4651.15 154.28 o 3 2 9 2683.29 2579.26 99.58 o 4 2 9 4231.09 4002.68 124.57 o 5 2 9 3434.70 3483.16 113.30 o 6 2 9 7842.26 7943.28 277.92 o 7 2 9 643.33 610.38 88.33 o 8 2 9 885.67 997.01 60.15 o 9 2 9 536.70 565.36 33.97 o 10 2 9 496.59 377.14 32.74 o 11 2 9 483.90 463.81 44.64 o 12 2 9 93.84 77.70 20.99 o 13 2 9 269.32 293.49 40.54 o 14 2 9 637.69 712.35 68.65 o 15 2 9 661.95 736.29 64.33 o 16 2 9 83.34 97.23 22.64 o 17 2 9 368.68 335.16 83.72 o 18 2 9 68.99 46.33 24.83 o 19 2 9 149.17 150.17 41.29 o 20 2 9 187.28 167.93 55.98 o 0 3 9 615.09 697.49 55.79 o 1 3 9 1834.47 1699.69 85.36 o 2 3 9 3755.08 3634.87 137.89 o 3 3 9 601.58 628.89 38.05 o 4 3 9 1970.87 1902.79 98.74 o 5 3 9 233.58 262.87 40.79 o 6 3 9 1953.83 2060.71 91.31 o 7 3 9 851.37 902.98 58.44 o 8 3 9 1842.34 1825.14 86.65 o 9 3 9 1978.67 2008.67 92.31 o 10 3 9 3424.97 3569.52 207.55 o 11 3 9 58.07 74.28 32.20 o 12 3 9 1383.27 1437.46 110.69 o 13 3 9 178.60 189.88 32.21 o 14 3 9 333.25 290.24 55.30 o 15 3 9 80.32 133.74 46.36 o 16 3 9 68.24 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3266.19 3399.75 407.22 o 2 7 9 1173.85 1190.04 119.14 o 3 7 9 1094.53 1167.83 138.73 o 4 7 9 422.13 429.48 46.61 o 5 7 9 314.89 398.33 46.59 o 6 7 9 751.68 655.56 84.50 o 7 7 9 233.74 217.18 111.84 o 8 7 9 30.86 41.94 39.47 o 9 7 9 1328.69 1216.41 127.72 o 10 7 9 75.33 177.06 70.37 o 11 7 9 1342.23 1430.53 154.47 o 12 7 9 206.84 223.64 46.44 o 13 7 9 194.84 205.05 46.30 o 14 7 9 122.94 27.85 39.38 o 15 7 9 73.90 44.64 46.41 o 16 7 9 14.64 27.84 39.37 o 17 7 9 71.44 55.83 55.96 o 18 7 9 7.21 27.98 56.24 o 19 7 9 43.72 84.50 56.24 o 20 7 9 3.09 28.26 56.51 o 1 8 9 245.59 375.72 112.25 o 2 8 9 42.10 -13.92 59.46 o 3 8 9 705.72 600.91 83.38 o 4 8 9 28.66 100.90 46.56 o 5 8 9 1022.31 1087.94 107.84 o 6 8 9 233.82 140.13 39.59 o 7 8 9 1032.05 1052.10 125.90 o 8 8 9 126.31 100.75 55.97 o 9 8 9 379.73 506.85 68.62 o 10 8 9 93.85 153.61 39.48 o 11 8 9 133.18 306.29 155.03 o 12 8 9 30.64 0.00 46.29 o 13 8 9 444.24 438.99 114.23 o 14 8 9 135.79 94.77 46.43 o 15 8 9 357.49 321.04 59.19 o 16 8 9 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191.96 67.21 o 3 8 17 89.69 -8.00 67.16 o 4 8 17 26.67 9.33 50.05 o 5 8 17 123.40 99.81 67.02 o 6 8 17 22.15 -4.01 125.63 o 0 0 18 699.31 1087.02 223.01 o 2 0 18 1292.33 1558.74 197.32 o 4 0 18 546.86 592.62 87.08 o 6 0 18 318.04 452.93 78.79 o 8 0 18 16.56 186.73 49.83 o 10 0 18 1.90 27.84 55.82 o 12 0 18 253.67 320.52 78.88 o 1 1 18 22.49 -27.93 35.22 o 2 1 18 206.45 217.31 68.28 o 3 1 18 66.82 74.22 36.44 o 4 1 18 32.29 20.30 30.00 o 5 1 18 94.45 102.08 44.24 o 6 1 18 134.57 133.70 44.28 o 7 1 18 9.36 34.85 41.80 o 8 1 18 62.36 105.06 50.98 o 9 1 18 8.93 -5.16 30.01 o 10 1 18 38.31 85.19 38.10 o 11 1 18 17.59 57.63 52.34 o 12 1 18 29.81 12.66 30.05 o 0 2 18 595.24 706.34 84.30 o 1 2 18 238.13 137.52 39.94 o 2 2 18 77.90 34.76 39.93 o 3 2 18 62.41 24.72 36.47 o 4 2 18 6.56 -9.24 48.19 o 5 2 18 43.30 118.23 39.92 o 6 2 18 62.81 71.80 33.92 o 7 2 18 74.03 34.34 38.05 o 8 2 18 39.98 91.48 47.25 o 9 2 18 132.35 173.97 41.74 o 10 2 18 73.93 85.18 38.06 o 11 2 18 149.91 137.62 45.55 o 12 2 18 10.21 63.78 38.07 o 1 3 18 54.97 -25.79 47.16 o 2 3 18 18.88 36.43 39.90 o 3 3 18 300.59 359.27 61.45 o 4 3 18 397.60 440.94 65.65 o 5 3 18 236.76 357.30 50.88 o 6 3 18 180.78 214.54 47.19 o 7 3 18 67.99 15.20 29.96 o 8 3 18 42.20 16.67 63.41 o 9 3 18 2.63 -18.51 36.44 o 10 3 18 1.19 74.15 48.26 o 11 3 18 41.37 -15.11 52.15 o 12 3 18 22.60 47.02 43.73 o 0 4 18 244.81 186.77 66.71 o 1 4 18 174.72 274.01 40.87 o 2 4 18 44.24 19.20 39.91 o 3 4 18 92.49 143.89 52.89 o 4 4 18 3.16 57.28 39.89 o 5 4 18 135.04 109.32 44.18 o 6 4 18 3.58 25.34 48.06 o 7 4 18 157.05 102.89 48.78 o 8 4 18 103.17 102.50 56.15 o 9 4 18 8.15 39.14 37.91 o 10 4 18 131.02 87.01 59.19 o 11 4 18 22.69 -46.39 64.19 o 1 5 18 307.78 302.90 52.17 o 2 5 18 38.47 27.81 44.15 o 3 5 18 348.96 306.30 55.85 o 4 5 18 32.03 72.88 39.87 o 5 5 18 50.08 106.18 44.23 o 6 5 18 75.57 15.15 52.05 o 7 5 18 239.22 129.70 64.16 o 8 5 18 35.62 5.59 57.18 o 9 5 18 47.39 10.46 36.78 o 0 6 18 33.61 0.00 111.64 o 1 6 18 9.97 -55.77 49.83 o 2 6 18 12.76 13.85 59.16 o 3 6 18 47.24 55.68 49.83 o 4 6 18 8.30 -95.65 66.95 o 5 6 18 47.52 135.53 125.36 o 6 6 18 12.62 69.56 69.67 o 7 6 18 86.43 191.36 71.56 o 8 6 18 66.00 158.90 66.75 o 1 7 18 61.87 83.94 67.16 o 2 7 18 48.61 175.76 139.77 o 3 7 18 20.38 -67.06 55.96 o 4 7 18 30.99 -22.32 46.51 o 5 7 18 77.57 55.96 97.66 o 2 0 19 36.26 43.36 111.37 o 4 0 19 93.19 236.75 78.76 o 6 0 19 63.14 83.53 59.16 o 8 0 19 100.46 239.08 59.17 o 10 0 19 13.84 19.84 66.95 o 0 1 19 238.11 167.11 78.78 o 1 1 19 80.50 184.59 58.39 o 2 1 19 187.98 238.84 58.38 o 3 1 19 51.07 36.37 50.98 o 4 1 19 224.09 263.18 60.20 o 5 1 19 21.97 91.64 40.19 o 6 1 19 141.39 57.31 48.27 o 7 1 19 7.57 5.65 50.67 o 8 1 19 4.55 -3.10 56.30 o 9 1 19 79.80 85.32 39.96 o 10 1 19 91.88 226.37 68.46 o 1 2 19 153.41 182.39 61.46 o 2 2 19 47.90 -76.34 50.89 o 3 2 19 25.21 70.49 44.21 o 4 2 19 25.03 27.86 36.42 o 5 2 19 75.26 81.36 42.75 o 6 2 19 9.13 68.52 52.22 o 7 2 19 89.78 76.92 38.05 o 8 2 19 118.63 160.76 47.26 o 9 2 19 11.73 -45.01 30.01 o 0 3 19 54.96 139.08 49.78 o 1 3 19 118.43 216.76 52.92 o 2 3 19 56.21 52.62 49.03 o 3 3 19 297.08 229.10 55.22 o 4 3 19 106.79 283.97 68.40 o 5 3 19 85.49 94.81 38.04 o 6 3 19 120.67 144.35 39.91 o 7 3 19 15.11 -23.64 42.74 o 8 3 19 45.76 107.25 47.18 o 9 3 19 12.70 24.98 32.76 o 1 4 19 302.73 316.69 52.05 o 2 4 19 145.02 92.19 39.91 o 3 4 19 37.71 9.27 44.19 o 4 4 19 57.51 51.58 47.18 o 5 4 19 163.45 199.39 39.91 o 6 4 19 44.73 101.94 44.17 o 7 4 19 49.66 14.91 50.87 o 8 4 19 45.40 99.60 39.35 o 0 5 19 31.15 51.62 66.61 o 1 5 19 24.32 89.89 48.22 o 2 5 19 78.23 63.57 47.18 o 3 5 19 177.49 121.88 50.85 o 4 5 19 72.88 128.87 60.14 o 5 5 19 62.34 188.96 76.38 o 6 5 19 30.75 177.91 76.99 o 1 6 19 150.78 223.33 87.21 o 2 6 19 6.24 27.98 46.35 o 0 0 20 47.26 -83.39 55.68 o 2 0 20 121.00 133.57 46.31 o 4 0 20 168.85 180.94 78.77 o 6 0 20 324.11 348.82 78.79 o 1 1 20 14.30 -46.46 36.42 o 2 1 20 64.39 92.72 48.15 o 3 1 20 12.35 -13.85 41.69 o 4 1 20 87.31 34.31 50.92 o 5 1 20 37.32 175.59 57.76 o 6 1 20 27.18 -51.16 56.26 o 0 2 20 10.15 37.23 97.23 o 1 2 20 14.23 55.64 39.90 o 2 2 20 71.16 184.11 56.46 o 3 2 20 10.26 17.85 52.18 o 4 2 20 103.59 105.95 68.26 o 5 2 20 9.05 19.87 66.56 o 6 2 20 106.78 73.90 44.19 o 1 3 20 3.33 0.00 47.20 o 2 3 20 43.95 3.76 68.26 o 3 3 20 153.89 189.12 42.09 o 4 3 20 32.14 40.98 68.46 o 0 4 20 188.66 182.78 66.77 o 1 4 20 166.09 250.69 56.19 o # # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_4 _shelx_title ' 03swb001' _shelx_refln_list_code 4 _shelx_F_calc_maximum 152.36 _exptl_crystal_F_000 1320.00 _reflns_d_resolution_high 0.7701 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 12.5207 _cell_length_b 16.1282 _cell_length_c 13.1311 _cell_angle_alpha 90.000 _cell_angle_beta 95.903 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6790.29 5642.12 806.91 o 4 0 0 7672.66 6627.36 151.63 o 6 0 0 325.84 224.23 8.54 o 8 0 0 0.75 5.00 2.58 o 10 0 0 5898.93 5612.82 160.43 o 12 0 0 2259.99 2461.83 98.22 o 14 0 0 44.58 41.67 6.94 o 2 1 0 6264.41 5745.60 108.23 o 3 1 0 8054.21 7679.67 119.94 o 4 1 0 3045.30 2955.75 47.42 o 5 1 0 3327.88 3129.99 47.00 o 6 1 0 5327.13 4894.61 73.09 o 7 1 0 2206.11 2046.71 33.02 o 8 1 0 10.80 20.11 3.38 o 9 1 0 246.39 227.41 9.10 o 10 1 0 1913.57 1809.81 33.59 o 11 1 0 556.04 544.07 18.63 o 12 1 0 394.84 367.96 9.17 o 13 1 0 199.65 194.31 6.52 o 14 1 0 4.66 5.55 2.31 o 1 2 0 23214.74 7621.51 2476.05 o 2 2 0 135.64 153.38 2.74 o 3 2 0 9073.28 8901.05 134.56 o 4 2 0 1193.27 1272.40 19.85 o 5 2 0 67.00 97.27 2.99 o 6 2 0 123.90 91.55 3.51 o 7 2 0 9.78 18.06 1.46 o 8 2 0 724.33 720.55 13.02 o 9 2 0 741.82 733.46 13.23 o 10 2 0 1.89 2.57 1.64 o 11 2 0 145.41 154.21 5.62 o 12 2 0 323.92 334.13 17.25 o 13 2 0 1274.94 1254.57 31.07 o 14 2 0 8.28 8.29 2.30 o 15 2 0 215.47 223.58 14.01 o 1 3 0 190.60 173.66 3.68 o 2 3 0 12020.51 12571.03 182.69 o 3 3 0 12227.67 12474.78 200.46 o 4 3 0 4054.88 3884.36 68.43 o 5 3 0 1338.17 1245.65 26.17 o 6 3 0 2220.08 2150.73 33.96 o 7 3 0 2519.01 2389.47 36.73 o 8 3 0 789.89 726.46 14.84 o 9 3 0 553.57 531.41 9.90 o 10 3 0 56.10 60.26 3.89 o 11 3 0 21.93 18.96 2.60 o 12 3 0 8.06 10.42 1.65 o 13 3 0 739.96 729.36 19.75 o 14 3 0 26.47 17.86 2.01 o 15 3 0 25.67 27.42 6.85 o 1 4 0 6918.59 6893.94 112.61 o 2 4 0 7379.06 7087.94 120.54 o 3 4 0 2012.03 1915.96 30.25 o 4 4 0 58.82 63.57 2.38 o 5 4 0 943.39 919.56 20.02 o 6 4 0 178.43 224.39 4.65 o 7 4 0 248.82 279.94 6.20 o 8 4 0 366.26 395.47 8.00 o 9 4 0 73.95 87.17 3.54 o 10 4 0 617.51 637.54 12.95 o 11 4 0 205.05 213.76 6.10 o 12 4 0 471.67 460.90 11.75 o 13 4 0 78.22 79.35 4.39 o 14 4 0 21.56 14.79 3.48 o 15 4 0 134.87 123.49 13.73 o 1 5 0 634.08 598.54 9.83 o 2 5 0 1384.64 1262.36 26.38 o 3 5 0 5696.39 5947.06 82.63 o 4 5 0 2.59 4.20 1.47 o 5 5 0 1019.72 970.34 17.40 o 6 5 0 2125.57 1987.48 40.23 o 7 5 0 3812.05 3967.47 75.20 o 8 5 0 9.17 9.17 2.47 o 9 5 0 0.26 -1.80 1.59 o 10 5 0 54.99 49.79 3.35 o 11 5 0 27.45 37.82 2.81 o 12 5 0 2.47 5.96 1.97 o 13 5 0 401.91 410.93 14.66 o 14 5 0 168.39 156.35 10.27 o 15 5 0 141.01 144.10 13.73 o 0 6 0 785.88 691.81 17.55 o 1 6 0 4646.91 5047.56 79.22 o 2 6 0 160.71 150.62 4.76 o 3 6 0 1185.95 1190.47 19.90 o 4 6 0 0.19 2.77 1.80 o 5 6 0 284.80 313.13 5.80 o 6 6 0 706.23 741.52 14.53 o 7 6 0 475.64 511.38 8.89 o 8 6 0 669.56 673.29 13.13 o 9 6 0 720.46 766.16 15.87 o 10 6 0 86.23 73.97 3.54 o 11 6 0 2040.68 2044.32 45.44 o 12 6 0 291.05 280.34 9.09 o 13 6 0 91.71 80.88 7.05 o 14 6 0 34.13 30.82 3.86 o 15 6 0 10.42 3.42 6.85 o 1 7 0 1682.78 1572.80 23.67 o 2 7 0 2714.63 2783.04 44.26 o 3 7 0 114.31 172.35 5.96 o 4 7 0 228.53 187.02 5.47 o 5 7 0 677.27 684.93 22.98 o 6 7 0 2102.70 2210.00 43.76 o 7 7 0 1228.64 1245.94 28.31 o 8 7 0 77.82 68.51 3.11 o 9 7 0 197.51 178.40 6.94 o 10 7 0 207.76 224.47 6.18 o 11 7 0 1180.88 1197.60 28.55 o 12 7 0 2.76 5.14 2.59 o 13 7 0 1.13 -1.85 2.98 o 14 7 0 109.94 103.28 7.96 o 15 7 0 31.97 20.89 5.81 o 0 8 0 387.99 260.62 10.00 o 1 8 0 296.67 277.25 9.64 o 2 8 0 2868.51 2863.43 51.20 o 3 8 0 572.29 546.26 12.86 o 4 8 0 1524.48 1429.40 28.94 o 5 8 0 46.34 62.53 2.88 o 6 8 0 2008.94 1911.51 37.93 o 7 8 0 180.16 176.74 5.13 o 8 8 0 423.19 457.22 10.00 o 9 8 0 13.12 6.57 2.76 o 10 8 0 253.45 260.91 7.51 o 11 8 0 118.09 118.66 5.18 o 12 8 0 309.19 326.35 13.46 o 13 8 0 4.42 -1.98 3.58 o 14 8 0 4.46 10.89 4.45 o 1 9 0 2975.73 3083.52 61.54 o 2 9 0 601.06 539.76 9.40 o 3 9 0 335.87 350.90 7.32 o 4 9 0 1232.79 1218.00 26.75 o 5 9 0 17.16 13.47 3.28 o 6 9 0 3986.00 3964.11 53.71 o 7 9 0 0.09 4.34 3.36 o 8 9 0 644.44 680.49 13.86 o 9 9 0 1120.55 1179.73 24.43 o 10 9 0 796.20 827.51 19.81 o 11 9 0 168.27 153.22 9.84 o 12 9 0 206.54 207.52 16.26 o 13 9 0 1.07 6.97 4.95 o 14 9 0 154.49 172.53 27.27 o 0 10 0 2099.22 2044.46 52.83 o 1 10 0 71.80 59.80 5.65 o 2 10 0 265.95 277.77 6.37 o 3 10 0 817.72 857.23 26.16 o 4 10 0 4161.98 4216.78 74.49 o 5 10 0 3363.46 3437.49 68.03 o 6 10 0 1167.56 1201.02 19.80 o 7 10 0 32.66 30.22 4.18 o 8 10 0 134.36 141.98 4.85 o 9 10 0 329.27 342.15 9.88 o 10 10 0 11.73 16.37 3.78 o 11 10 0 236.00 219.49 10.58 o 12 10 0 45.62 52.36 7.70 o 13 10 0 815.89 902.15 56.98 o 14 10 0 165.67 154.04 14.32 o 1 11 0 1164.58 1207.34 24.76 o 2 11 0 422.90 406.47 16.01 o 3 11 0 192.38 191.00 10.75 o 4 11 0 2216.88 2219.13 53.40 o 5 11 0 826.48 822.71 19.02 o 6 11 0 2.49 -2.78 2.47 o 7 11 0 1002.25 1034.19 20.35 o 8 11 0 104.64 96.89 4.19 o 9 11 0 33.79 30.74 3.06 o 10 11 0 26.76 26.98 3.03 o 11 11 0 818.93 864.25 32.32 o 12 11 0 1.10 4.17 5.55 o 13 11 0 5.62 -6.01 9.56 o 0 12 0 39.11 50.86 6.48 o 1 12 0 1278.46 1286.13 22.45 o 2 12 0 586.77 633.77 12.74 o 3 12 0 263.97 227.86 7.08 o 4 12 0 42.02 53.25 3.67 o 5 12 0 89.44 81.96 4.32 o 6 12 0 93.04 87.56 4.00 o 7 12 0 15.57 16.60 3.66 o 8 12 0 118.48 127.01 5.08 o 9 12 0 6.06 5.34 2.89 o 10 12 0 18.05 18.48 4.95 o 11 12 0 216.30 223.43 11.85 o 12 12 0 626.91 706.00 50.02 o 13 12 0 155.92 134.13 11.71 o 1 13 0 1167.22 1155.84 22.77 o 2 13 0 1683.24 1695.29 35.08 o 3 13 0 978.55 968.98 20.59 o 4 13 0 24.90 14.23 3.09 o 5 13 0 962.63 924.37 19.62 o 6 13 0 143.16 146.96 5.22 o 7 13 0 81.61 78.83 6.11 o 8 13 0 101.30 108.93 6.21 o 9 13 0 617.28 629.14 19.46 o 10 13 0 335.84 325.39 14.32 o 11 13 0 64.93 70.11 7.94 o 12 13 0 68.09 72.79 15.69 o 0 14 0 180.11 208.84 10.14 o 1 14 0 139.19 133.00 5.98 o 2 14 0 226.91 203.77 6.79 o 3 14 0 71.61 66.40 5.55 o 4 14 0 28.70 30.93 4.57 o 5 14 0 58.65 54.41 4.27 o 6 14 0 9.69 11.28 3.89 o 7 14 0 22.62 23.48 4.39 o 8 14 0 25.16 19.22 5.67 o 9 14 0 360.33 365.71 12.70 o 10 14 0 39.65 43.53 8.04 o 11 14 0 87.97 107.15 12.89 o 12 14 0 108.16 98.92 9.23 o 1 15 0 103.76 82.44 7.18 o 2 15 0 361.33 357.53 14.03 o 3 15 0 18.00 26.50 5.17 o 4 15 0 52.40 47.89 6.32 o 5 15 0 86.04 63.25 5.33 o 6 15 0 29.29 27.01 3.92 o 7 15 0 151.30 171.17 7.57 o 8 15 0 112.34 118.61 11.68 o 9 15 0 61.78 64.36 5.82 o 10 15 0 7.10 11.78 10.02 o 11 15 0 52.38 50.48 8.58 o 0 16 0 56.08 45.21 6.89 o 1 16 0 0.71 5.10 3.97 o 2 16 0 234.27 230.20 9.54 o 3 16 0 4.31 10.54 8.76 o 4 16 0 8.10 4.10 4.59 o 5 16 0 9.37 4.79 4.91 o 6 16 0 2.29 4.48 3.95 o 7 16 0 37.15 25.09 4.46 o 8 16 0 21.25 18.56 6.11 o 9 16 0 5.73 15.09 4.56 o 10 16 0 73.38 60.22 9.02 o 1 17 0 31.84 28.55 7.46 o 2 17 0 3.28 5.99 6.28 o 3 17 0 252.96 295.64 17.43 o 4 17 0 75.78 62.00 7.19 o 5 17 0 1.52 -2.85 4.17 o 6 17 0 533.20 521.14 28.96 o 7 17 0 211.85 194.05 18.66 o 8 17 0 12.05 9.06 7.17 o 9 17 0 22.98 38.84 8.56 o 0 18 0 310.42 285.11 20.62 o 1 18 0 258.78 253.62 19.91 o 2 18 0 262.18 254.92 13.91 o 3 18 0 3.72 6.64 6.32 o 4 18 0 505.98 543.83 21.63 o 5 18 0 133.15 148.76 12.52 o 6 18 0 153.71 154.63 12.99 o 7 18 0 26.86 32.53 6.95 o 8 18 0 73.17 83.50 14.13 o 1 19 0 59.49 87.47 10.82 o 2 19 0 59.84 41.68 7.62 o 3 19 0 44.05 44.34 7.98 o 4 19 0 2.28 11.90 7.01 o 5 19 0 187.87 181.17 14.52 o 6 19 0 380.57 385.19 37.62 o 0 20 0 73.57 65.15 13.22 o 1 20 0 753.33 825.38 40.58 o 2 20 0 11.73 11.02 9.95 o 3 20 0 24.90 21.92 9.82 o 4 20 0 5.95 13.83 12.00 o -15 0 1 93.48 80.10 10.46 o -13 0 1 538.53 513.19 27.45 o -11 0 1 1241.42 1230.98 32.39 o -9 0 1 1525.13 1569.30 61.33 o -7 0 1 6084.16 5918.71 145.99 o -5 0 1 8252.40 7638.34 215.59 o -3 0 1 2876.37 2737.55 86.45 o 3 0 1 972.62 910.48 21.90 o 5 0 1 5872.33 5837.56 148.76 o 7 0 1 1614.13 1579.56 39.98 o 9 0 1 474.70 444.32 14.04 o 11 0 1 320.83 321.31 12.59 o 13 0 1 216.34 232.47 14.00 o 15 0 1 293.92 226.71 24.07 o -15 1 1 60.67 45.26 4.93 o -14 1 1 26.18 28.39 1.51 o -13 1 1 573.57 626.45 17.72 o -12 1 1 399.49 428.62 30.29 o -11 1 1 81.36 78.92 3.71 o -10 1 1 253.16 254.52 19.24 o -9 1 1 1425.51 1381.64 40.72 o -8 1 1 888.89 899.59 19.79 o -7 1 1 1584.88 1466.03 38.07 o -6 1 1 470.35 490.04 10.02 o -5 1 1 3474.16 3652.09 116.02 o -4 1 1 0.96 4.92 2.00 o -3 1 1 3.62 9.82 2.34 o -2 1 1 1665.10 1552.80 38.21 o 2 1 1 11699.73 11712.19 227.49 o 4 1 1 39.14 41.46 1.71 o 5 1 1 73.59 43.15 2.57 o 6 1 1 64.00 49.56 2.67 o 7 1 1 867.64 853.84 14.41 o 8 1 1 70.91 95.67 3.38 o 9 1 1 1795.17 1742.07 33.50 o 10 1 1 1153.53 1133.80 22.52 o 11 1 1 206.39 202.64 5.53 o 12 1 1 148.74 154.35 5.47 o 13 1 1 687.37 711.02 25.57 o 14 1 1 29.30 17.36 4.48 o 15 1 1 361.91 347.81 23.97 o 16 1 1 63.75 41.21 10.30 o -15 2 1 23.96 27.69 3.45 o -14 2 1 307.14 277.08 14.12 o -13 2 1 285.89 275.10 10.56 o -12 2 1 19.73 12.82 4.07 o -11 2 1 1.12 0.82 2.16 o -10 2 1 259.02 258.29 8.06 o -9 2 1 130.07 126.99 4.68 o -8 2 1 191.19 207.06 4.21 o -7 2 1 304.18 264.80 4.80 o -6 2 1 2031.86 1860.97 28.48 o -5 2 1 1127.54 1029.33 21.97 o -4 2 1 1879.70 1873.85 29.12 o -3 2 1 1435.50 1387.90 26.65 o -2 2 1 9658.11 9721.01 230.12 o -1 2 1 2910.34 2743.37 71.29 o 0 2 1 975.57 856.18 125.05 o 1 2 1 516.83 404.49 12.83 o 2 2 1 16211.32 16660.15 655.06 o 3 2 1 4670.09 4479.56 84.35 o 4 2 1 1857.31 1966.37 29.87 o 5 2 1 32.26 38.52 3.29 o 7 2 1 260.93 260.15 8.88 o 8 2 1 69.69 74.89 3.02 o 9 2 1 1018.61 981.78 18.72 o 10 2 1 7.37 3.79 2.24 o 11 2 1 2.17 4.11 1.66 o 12 2 1 1258.97 1327.00 25.03 o 13 2 1 9.60 3.92 2.01 o 14 2 1 20.12 9.70 2.61 o 15 2 1 39.03 60.38 10.59 o -15 3 1 42.95 35.09 3.52 o -14 3 1 63.08 55.15 5.59 o -13 3 1 37.97 40.45 3.79 o -12 3 1 714.32 720.05 19.07 o -11 3 1 494.45 522.59 19.20 o -10 3 1 211.50 185.35 6.04 o -9 3 1 1117.69 1144.50 20.23 o -8 3 1 1.51 3.59 2.84 o -7 3 1 433.46 423.23 8.65 o -6 3 1 136.01 168.12 5.55 o -5 3 1 450.04 473.05 9.89 o -4 3 1 29.48 67.94 2.41 o -3 3 1 10540.11 10927.31 153.51 o -2 3 1 1914.38 1790.79 28.15 o 0 3 1 3092.32 2976.32 50.62 o 1 3 1 519.44 442.12 7.15 o 2 3 1 94.64 94.60 2.91 o 3 3 1 1238.50 1325.84 19.97 o 4 3 1 237.58 246.08 5.04 o 5 3 1 183.11 136.82 6.39 o 6 3 1 603.92 778.48 16.83 o 7 3 1 6.05 9.72 1.87 o 8 3 1 792.17 740.54 13.09 o 9 3 1 15.26 10.43 2.15 o 10 3 1 515.80 536.69 12.47 o 11 3 1 107.13 110.82 4.21 o 12 3 1 1353.34 1360.70 38.13 o 13 3 1 195.99 199.92 7.84 o 14 3 1 182.53 183.34 7.71 o 15 3 1 56.18 59.12 6.97 o -15 4 1 3.39 2.32 2.43 o -14 4 1 1007.70 973.87 39.89 o -13 4 1 6.02 8.79 1.90 o -12 4 1 487.19 487.53 15.30 o -11 4 1 39.22 51.46 3.17 o -10 4 1 501.52 513.62 12.35 o -9 4 1 756.05 768.28 15.15 o -8 4 1 1068.46 1110.65 22.46 o -7 4 1 81.91 53.00 2.51 o -6 4 1 4431.97 4465.15 98.54 o -5 4 1 5948.67 6302.57 84.61 o -4 4 1 5260.81 5183.37 70.63 o -3 4 1 4934.56 4864.88 86.28 o -2 4 1 1640.71 1548.87 31.62 o -1 4 1 59.59 105.91 5.99 o 0 4 1 5305.16 5232.15 99.79 o 1 4 1 4091.85 4284.99 99.01 o 2 4 1 613.08 618.72 12.88 o 3 4 1 1026.83 841.36 17.91 o 4 4 1 584.05 467.04 11.05 o 5 4 1 8696.34 9626.84 134.55 o 6 4 1 9860.35 9932.08 141.97 o 7 4 1 175.52 181.05 5.36 o 8 4 1 722.47 761.90 16.06 o 9 4 1 273.84 310.10 9.13 o 10 4 1 420.16 401.96 9.10 o 11 4 1 13.84 8.93 2.55 o 12 4 1 16.74 17.77 3.25 o 13 4 1 82.54 75.66 6.19 o 14 4 1 121.29 109.15 9.61 o 15 4 1 387.91 349.24 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