Figure 3
Scattered X-ray intensities of [gamma]-Sb2O3 under ambient conditions as a function of diffraction angle 2[theta]. The observed pattern (diamonds) measured in Debye-Scherrer geometry, the best Rietveld fit profiles (line) and the difference curve between the observed and the calculated profiles (below) are shown. The high-angle part starting at 9.5° 2[theta] is enlarged for clarity. The second phase is included as a LeBail fit.  [article HTML]

© International Union of Crystallography 2012