Acta Cryst. (2012). B68, 89-90 [ doi:10.1107/S0108768111054371 ]
Abstract: A revision is presented of the restrained Rietveld analysis of the crystal structure of magnesium perchlorate tetrahydrate, Mg(ClO4)2·4H2O, recently published by Robertson & Bish [(2010), Acta Cryst. B66, 579-584 ]. The actual symmetry of the material is shown to be C2/m. The corrected structure model is refined by the derivative difference method [Solovyov (2004). J. Appl. Cryst. 37, 743-749], anisotropically for all non-H atoms and isotropically for two independent H atoms without restraints.
Keywords: X-ray powder diffraction; crystal structure revision; derivative difference minimization.
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