Structural phase transition to disorder low-temperature phase in [Fe(ptz)6](BF4)2 spin-crossover compounds

Kusz, J.; Zubko, M.; Neder, R.B.; Gütlich, P.

doi:10.1107/S0108768111053298

Acta Crystallographica Section B
Acta Crystallographica
Section B STRUCTURAL SCIENCE, CRYSTAL ENGINEERING AND MATERIALS

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Figure 4
A time-dependent sequence of (a) q-scans of the 113 Bragg reflection at constant temperature after quick cooling to 100 K. This figure shows the slow structural phase transition from the LS supercooled phase (LS-ord) to the LS disordered phase (LS-dis). Time dependence of (b) FWHM and (c) peak intensity. Fig. 4

(a) shows selected q-scans from the full time series shown in (b) and (c).

STRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS

ISSN: 2052-5206

Volume 68| Part 1| February 2012| Pages 40-56

https://doi.org/10.1107/S0108768111053298

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