Acta Crystallographica Section C

Crystal Structure Communications

Volume 39, Part 2 (February 1983)



research papers (inorganic compounds)



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Acta Cryst. (1983). C39, 143-145    [ doi:10.1107/S0108270183003911 ]

Dipotassium ditellurium(IV) pentaoxide trihydrate, K2Te2O5.3H2O

L. Andersen and J. Moret



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Acta Cryst. (1983). C39, 145-148    [ doi:10.1107/S0108270183003923 ]

Structure of an oxonium antimony(III) sulphate, (H3O)2Sb2(SO4)4

R. Mercier, J. Douglade, P. G. Jones and G. M. Sheldrick



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Acta Cryst. (1983). C39, 148-151    [ doi:10.1107/S0108270183003935 ]

Eisen(II,III)germaniumoxid Fe3,2Ge1,8O8

K. Kato, E. Takayama and N. Kimizuka



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Acta Cryst. (1983). C39, 151-154    [ doi:10.1107/S0108270183003947 ]

Eisen(II,III)germaniumoxid Fe15Ge8O36

K. Kato, E. Takayama, N. Kimizuka, H. Haneda and H. Yamamura



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Acta Cryst. (1983). C39, 154-159    [ doi:10.1107/S0108270183003959 ]

Untersuchungen an Polyhalogeniden. 6. Hexaamminocobalt(III)heptaiodid, [Co(NH3)6]I3I4

K.-F. Tebbe



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Acta Cryst. (1983). C39, 159-162    [ doi:10.1107/S0108270183003960 ]

The room-temperature structure of DUO2AsO4.4D2O by powder neutron diffraction

A. N. Fitch, L. Bernard, A. T. Howe, A. F. Wright and B. E. F. Fender



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Acta Cryst. (1983). C39, 162-166    [ doi:10.1107/S0108270183003972 ]

The structure of deuterated ammonium uranyl phosphate trihydrate, ND4UO2PO4.3D2O, by powder neutron diffraction

A. N. Fitch and B. E. F. Fender



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Acta Cryst. (1983). C39, 166-169    [ doi:10.1107/S0108270183003984 ]

A glaserite-type structure: calcium tripotassium hydrogenbis(phosphate), CaK3H(PO4)2

S. Takagi, M. Mathew and W. E. Brown


research papers (metal-organic compounds)



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Acta Cryst. (1983). C39, 170-173    [ doi:10.1107/S0108270183003996 ]

The structure of promaziniumyl free radical cation tetrachlorocuprate salt, (C17H21N2S)[CuCl4]

R. B. Von Dreele and J. Harris



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Acta Cryst. (1983). C39, 174-176    [ doi:10.1107/S010827018300400X ]

Structure of polymeric [mu]-(oxalato-O1,O2:O1',O2')-bis[diaqua(oxalato-O1,O2)indium] dihydrate, [In2(C2O4)3(H2O)4\].2H2O

N. Bulc and L. Golic



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Acta Cryst. (1983). C39, 176-178    [ doi:10.1107/S0108270183004011 ]

Structure of ammonium and sodium bis(oxalato)indate(III) dihydrate, NH4[In(C2O4)2].2H2O and Na[In(C2O4)2].2H2O

N. Bulc, L. Golic and J. Siftar



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Acta Cryst. (1983). C39, 178-180    [ doi:10.1107/S0108270183004023 ]

Structure of tris[2(1H)-pyridinethione-S]copper(I) nitrate (TPTCN), [Cu(C5H5NS)3]NO3

S. C. Kokkou, S. Fortier, P. J. Rentzeperis and P. Karagiannidis



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Acta Cryst. (1983). C39, 181-184    [ doi:10.1107/S0108270183004035 ]

Structures of the tetramethylammonium salts of the bromide, chloride and azide adducts of uranyl bis(hexafluoroacetylacetonate), [UO2{(CF3CO)2CH}2X]-.[N(CH3)4]+

L. Prasad, E. J. Gabe, B. Glavincevski and S. Brownstein



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Acta Cryst. (1983). C39, 184-186    [ doi:10.1107/S0108270183004047 ]

Structure of 1,2-ethanedithiolatobis(triphenylphosphine)platinum(II), C38H34P2PtS2

S. A. Bryan and D. M. Roundhill



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Acta Cryst. (1983). C39, 186-188    [ doi:10.1107/S0108270183004059 ]

Structure of trans-dichlorobis(1-methylimidazole)palladium(II), [Pd(C4H6N2)2Cl2]

M. C. Navarro-Ranninger, S. Martínez-Carrera and S. García-Blanco



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Acta Cryst. (1983). C39, 188-190    [ doi:10.1107/S0108270183004060 ]

Structure of trans-dichlorobis(2-methylimidazole)palladium(II), [Pd(C4H6N2)2Cl2]

M. C. Navarro-Ranninger, S. Martínez-Carrera and S. García-Blanco



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Acta Cryst. (1983). C39, 190-192    [ doi:10.1107/S0108270183004072 ]

Structure of a cubic form of tetraethylammonium octakis(thiocyanato-N)thorate(IV), [N(C2H5)4]4[Th(NCS)8]

P. Charpin, M. Lance and A. Navaza



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Acta Cryst. (1983). C39, 192-194    [ doi:10.1107/S0108270183004084 ]

([eta]-Allyl)bromodicarbonyl(N,N'-di-tert-butylethanediimine)molybdenum(II), MoBr(C3H5)(C10H20N2)(CO)2

A. J. Graham, D. Akrigg and B. Sheldrick



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Acta Cryst. (1983). C39, 194-199    [ doi:10.1107/S0108270183004096 ]

The structure of dicholoro(2,2':6',2''-terpyridyl)copper(II) monohydrate, [Cu(C15H11N3)Cl2].H2O

T. Rojo, M. Vlasse and D. Beltran-Porter



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Acta Cryst. (1983). C39, 199-200    [ doi:10.1107/S0108270183004102 ]

Bis(N-cyclohexylsalicylideneaminato)nickel(II), [Ni(C13H16NO)2]

S. C. Bhatia, V. K. Syal, R. P. Kashyap, P. C. Jain and C. J. Brown



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Acta Cryst. (1983). C39, 201-203    [ doi:10.1107/S0108270183004114 ]

Bis(3-allylacetylacetonato)copper(II), C16H22CuO4

A. A. Aruffo, L. D. Anderson, E. C. Lingafelter and V. Schomaker



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Acta Cryst. (1983). C39, 203-205    [ doi:10.1107/S0108270183004126 ]

Structure of catena-[mu]-aqua-bis(benzimidazole)diformatocopper(II), [Cu(C7H6N2)2(CHO2)2(H2O)]

M. Bukowska-Strzyzewska and A. Tosik



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Acta Cryst. (1983). C39, 206-208    [ doi:10.1107/S0108270183004138 ]

Structure of dichloro(5,6,8,9,11,12,14,15-octahydro-2,3-benzo-1,4,7,10,13-pentaoxacyclopentadec-2-ene)copper(II) chloroform solvate, [Cu(C14H20O5)Cl2].CHCl3, a CuII-crown-ether complex with pentagonal-bipyramidal geometry

T. Sakurai, K. Kobayashi, S. Tsuboyama, Y. Kohno, N. Azuma and K. Ishizu



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Acta Cryst. (1983). C39, 208-211    [ doi:10.1107/S010827018300414X ]

Structure of cis-bis(acetylacetonato)diaquacalcium monohydrate, [Ca(C5H7O2)2(H2O)2].H2O

J. J. Sahbari and M. M. Olmstead



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Acta Cryst. (1983). C39, 211-213    [ doi:10.1107/S0108270183004151 ]

Bis[bis(diethylamino)glyoximato]nickel(II), C20H42N8NiO4

L. A. Nuvan, J. L. Briansó, X. Solans, M. Font-Altaba and M. de Matheus


research papers (organic compounds)



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Acta Cryst. (1983). C39, 214-216    [ doi:10.1107/S0108270183004163 ]

Structure of trimethyl[(cis-2-methyl-1,3-oxathiolan-5-yl)methyl]ammonium iodide, C8H18NOS+.I-

R. Bardi, A. M. Piazzesi, A. Del Pra and L. Villa



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Acta Cryst. (1983). C39, 216-219    [ doi:10.1107/S0108270183004175 ]

Tetramethylammonium benzotriazolide, C4H12N+.C6H4N3-

S. Capasso, F. Giordano and A. Zagari



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Acta Cryst. (1983). C39, 219-222    [ doi:10.1107/S0108270183004187 ]

(2S,4S,5R)-2-Chloro-3,4-dimethyl-5-phenyl-1,3,2-oxazaphospholidine 2-sulphide, C10H13ClNOPS

T. J. Bartczak and Z. Galdecki



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Acta Cryst. (1983). C39, 222-224    [ doi:10.1107/S0108270183004199 ]

(2R,4S,5R)-2-Chloro-3,4-dimethyl-5-phenyl-1,3,2-oxazaphospholidine 2-sulphide, C10H13ClNOPS

T. J. Bartczak, Z. Galdecki and M. Rutkowska



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Acta Cryst. (1983). C39, 224-227    [ doi:10.1107/S0108270183004205 ]

Structure of 2-[(3,5-dichlorophenyl)amino]-5,5-dimethyl-1,3,2-dioxaphosphorinane 2-selenide, C11H14Cl2NO2PSe

T. J. Bartczak and W. Wolf



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Acta Cryst. (1983). C39, 227-230    [ doi:10.1107/S0108270183004217 ]

(3R,6R)-3-Benzyl-8-thia-1,4-diazabicyclo[4.3.0]nonane-2,5-dione, C13H14N2O2S

M. Van Poucke, H. J. Geise and A. T. H. Lenstra



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Acta Cryst. (1983). C39, 230-232    [ doi:10.1107/S0108270183004229 ]

4-Methyl-N-8-quinolybenzenesulphonamide, C16H14N2O2S. The active component of LIX 34

G. Germain, J.-P. Declercq, J. M. Castresana, M. P. Elizalde and J. M. Arrieta



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Acta Cryst. (1983). C39, 232-234    [ doi:10.1107/S0108270183004230 ]

Nicotinic acid, C6H5NO2: refinement

A. Kutoglu and C. Scheringer



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Acta Cryst. (1983). C39, 234-237    [ doi:10.1107/S0108270183004242 ]

Structural studies of radical reaction products. I. The structure of an asymmetrically substituted diazene: 3-(p-chlorophenyl)-4-(p-chlorophenylazo)-4-methyl-2-pentanone, C18H18Cl2N2O

A. Albinati, F. Ganazzoli and A. Citterio



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Acta Cryst. (1983). C39, 237-240    [ doi:10.1107/S0108270183004254 ]

Studies of monoclinic hen egg white lysozyme. II. The refinement at 2.5 Å resolution - conformational variability between the two independent molecules

S. T. Rao, J. Hogle and M. Sundaralingam

PDB reference: 1lym



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Acta Cryst. (1983). C39, 240-245    [ doi:10.1107/S0108270183004266 ]

Structure of 3-(2-pyridyl)-2-(2-tolyl)-1,3-thiazolidin-4-one, C15H14N2OS

D. Hickel, J.-M. Léger, A. Carpy, M. G. Vigorita, A. Chimirri and S. Grasso



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Acta Cryst. (1983). C39, 246-248    [ doi:10.1107/S0108270183004278 ]

[(Chloro-6 méthoxy-2 acridinyl-9)aminopentyl]-1 thymine-méthanol (1:2), C24H25ClN4O3.2CH4O

R. El Couhen, C. Courseille, G. Précigoux, J. F. Constant et J. Lhomme



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Acta Cryst. (1983). C39, 248-250    [ doi:10.1107/S010827018300428X ]

Structure of 2,2-dimethyl-4,6,6-triphenyl-1-thia-4-azaspiro[2.3]hexan-5-one, C24H21NOS

K. Fukuyama, S. Fujii, Y. Katsube and I. Yamamoto



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Acta Cryst. (1983). C39, 250-253    [ doi:10.1107/S0108270183004291 ]

Tetrafluorophthalic acid (TFAC), C8H2F4O4

D. S. Sake Gowda and R. Rudman



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Acta Cryst. (1983). C39, 253-255    [ doi:10.1107/S0108270183004308 ]

Structure of morpholinium 4-morpholinecarboxylate, C4H10NO+.C5H8NO3-

R. B. Von Dreele, R. L. Bradshaw and W. J. Burke



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Acta Cryst. (1983). C39, 255-257    [ doi:10.1107/S010827018300431X ]

Structure of plaunolide, a new furanoid diterpene from Croton sublyratus, C20H20O5

H. Haruyama, T. Hata, A. Ogiso, C. Tamura and E. Kitazawa



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Acta Cryst. (1983). C39, 258-259    [ doi:10.1107/S0108270183004321 ]

Hydroxy-17[beta] diméthyl-7[alpha],17[alpha] estrène-4 one-3, C20H30O2

J.-P. Mornon, J. Delettré et E. Surcouf



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Acta Cryst. (1983). C39, 260-265    [ doi:10.1107/S0108270183004333 ]

Structure cristallographique du clathrate triclinique tri-o-thymotide-benzène (2:2,5), 2C33H36O6.2,5C6H6

J. Allemand and R. Gerdil



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Acta Cryst. (1983). C39, 266-268    [ doi:10.1107/S0108270183004345 ]

3-Thioxo-2-pyridinecarboxylic acid, C6H5NO2S. Redetermination of the structure

P. E. Bourne and M. R. Taylor



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Acta Cryst. (1983). C39, 268-270    [ doi:10.1107/S0108270183004357 ]

Structure of funicin, antimicrobial substance from Aspergillus funiculosus, C17H18O5

M. Nakamura, K. Fukuyama, T. Tsukihara, Y. Katsube and T. Hamasaki



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Acta Cryst. (1983). C39, 270-273    [ doi:10.1107/S0108270183004369 ]

Cyclohexylammonium [mu]-disulfido-bis(trioxophosphate)(4-) monohydrate, 4C6H14N4+.O6P2S24-.H2O

Ch. Betzel, D. Loewus and W. Saenger



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Acta Cryst. (1983). C39, 273-275    [ doi:10.1107/S0108270183004370 ]

Methyldigitoxigenin, C24H36O4

L. Prasad and E. J. Gabe



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Acta Cryst. (1983). C39, 275-278    [ doi:10.1107/S0108270183004382 ]

Structures of polycyclic polyamines: 1,5,9,13-tetraazatricyclo[11.3.1.15,9]octadecane, C14H28N4

E. J. Gabe, L. Prasad, G. R. Weisman and V. B. Johnson



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Acta Cryst. (1983). C39, 278-280    [ doi:10.1107/S0108270183004394 ]

Structure of 1-(4-chlorobenzylidene)-5,5-dimethyl-3-pyrazolidone betaine, C12H13ClN2O

S. Kulpe, I. Seidel, P. Leibnitz and G. Geissler



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Acta Cryst. (1983). C39, 281-283    [ doi:10.1107/S0108270183004400 ]

L-Lysine sulphate, C6H16N2O22+.SO42-: a novel conformation of the L-lysine side chain

S. Capasso, C. A. Mattia, L. Mazzarella and A. Zagari



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Acta Cryst. (1983). C39, 283-287    [ doi:10.1107/S0108270183004412 ]

Dithiin tautomers: dimethyl 2,4-diphenyl-2H,4H-1,3-dithiin-5,6-dicarboxylate (I), C20H18O4S2, and dimethyl 2,6-diphenyl-2H,4H-1,3-dithiin-4,5-dicarboxylate (II), C20H18O4S2

I. L. Karle and J. Karle



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Acta Cryst. (1983). C39, 287-289    [ doi:10.1107/S0108270183004424 ]

Methyl (±)-5[alpha]-acetoxymethyl-4[beta]-methoxy-1-oxo-1,2,3,4,4a[beta],5,6,7,8,8a[alpha]-decahydronaphthalene-4a[beta]-carboxylate, C16H24O6

B. Rubin, J. Epstein and L. Brooks



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Acta Cryst. (1983). C39, 289-291    [ doi:10.1107/S0108270183004436 ]

Structure of 5H,8H-dibenzo[d,f][1,2]oxathiocin 7,7-dioxide, C14H12O3S

F. Brisse, M. J. Olivier, D. N. Harpp and K. Steliou



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Acta Cryst. (1983). C39, 292-294    [ doi:10.1107/S0108270183004448 ]

Structure of 3,3'-(ethylenediimino)bis(3-methyl-2-butanone oxime), C12H26N4O2

M. S. Hussain and Mazhar-ul-Haque



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Acta Cryst. (1983). C39, 295-297    [ doi:10.1107/S010827018300445X ]

Structure of cytovaricin-acetonitrile (1:1), C47H80O16.C2H3N

T. Sakurai, T. Kihara and K. Isono



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Acta Cryst. (1983). C39, 297-300    [ doi:10.1107/S0108270183004461 ]

The structure of tetrazole steroid analogues. III. Structure of 4,6-diaza-A,B-bishomocholest-4a-eno[4,3-d][6,7-d]bistetrazole (HS-649), C27H42N8

J. Husain, I. J. Tickle, R. A. Palmer, H. Singh and K. K. Bhutani



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Acta Cryst. (1983). C39, 300-302    [ doi:10.1107/S0108270183004473 ]

1,8-Dinitro-4,5-dihydroxyanthraquinone, C14H6N2O8

C. J. Brown and M. L. Colclough



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Acta Cryst. (1983). C39, 302-303    [ doi:10.1107/S0108270183004485 ]

2,5-Bis(1,1,3,3-tetramethylbutyl)-1,4-benzoquinone, C22H36O2

C. J. Brown and J. E. Channing



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Acta Cryst. (1983). C39, 304-306    [ doi:10.1107/S0108270183004497 ]

Structure of 2-benzyl-6-exo-[2,3-dimethyl-4-(2,6-diiodo-4-methylphenoxy)phenoxy]-2-azabicyclo[2.2.1]heptan-3-one, C28H27I2NO3

H. L. Ammon, S. K. Bhattacharjee, P. S. Ravi and S. J. Potlock



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Acta Cryst. (1983). C39, 307-309    [ doi:10.1107/S0108270183004503 ]

Ajugareptansone B, C24H30O8, a disordered structure

X. Solans, C. Miravitlles, J. P. Declercq and G. Germain



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Acta Cryst. (1983). C39, 310-312    [ doi:10.1107/S0108270183004515 ]

Structure of quinidine, C20H24N2O2

S. Kashino and M. Haisa



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Acta Cryst. (1983). C39, 312-314    [ doi:10.1107/S0108270183004527 ]

[alpha]-(p-Bromobenzoyloxy)-[beta]-phenylazostilbene, C27H19BrN2O2

D. D. Bray, J. Minadeo and C. S. Russell



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Acta Cryst. (1983). C39, 315-316    [ doi:10.1107/S0108270183004539 ]

3-0-Methyl-[alpha]-D-glucopyranose, C7H14O6

B. Sheldrick and D. Akrigg


short communications



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Acta Cryst. (1983). C39, 316    [ doi:10.1107/S0108270183004540 ]

Elementary patterns in protein-nucleic acid interactions. VI. Structure of 3-(7-adeninyl)propionamide monohydrate: addendum

M. Takimoto, A. Takenaka and Y. Sasada


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