Acta Crystallographica Section C

Crystal Structure Communications

Volume 39, Part 6 (June 1983)

• research papers
  • inorganic compounds
  • metal-organic compounds
  • organic compounds
• short communications

research papers

inorganic compounds

Acta Cryst. (1983). C39, 651-655    [doi:10.1107/S0108270183005806]

The structure of the low-temperature phase V of ammonium nitrate, ND₄NO₃

M. Ahtee, K. J. Smolander, B. W. Lucas and A. W. Hewat

Acta Cryst. (1983). C39, 656-658    [doi:10.1107/S0108270183005818]

Structure du trimétaphosphate-tellurate d'ammonium, 2(NH₄)₃P₃O₉.Te(OH)₆

N. Boudjada, A. Boudjada et J. C. Guitel

Acta Cryst. (1983). C39, 658-661    [doi:10.1107/S010827018300582X]

Preparation and structure of sodium octatungstotetraphosphate(12-) icosahydrate, Na₁₂P₄W₈O₄₀.20H₂O, a 1:2(X:M) heteropolyanion

B. M. Gatehouse and A. J. Jozsa

Acta Cryst. (1983). C39, 662-664    [doi:10.1107/S0108270183005831]

The dierbium dipalladium silicide, Er₂Pd₂Si, structure, a periodic intergrowth of CeCu₂ and MnP structure-type segments

K. Klepp, E. Hovestreydt and E. Parthé

Acta Cryst. (1983). C39, 664-667    [doi:10.1107/S0108270183005843]

Structure de l'orthophosphate double NaCuPO₄-

M. Quarton and A. W. Kolsi

Acta Cryst. (1983). C39, 667-668    [doi:10.1107/S0108270183005855]

Re-examination of the UZr₆FO₁₄ crystal structure

R. Papiernik, D. Mercurio, B. Frit and H. Bärnighausen

Acta Cryst. (1983). C39, 668-670    [doi:10.1107/S0108270183005867]

Single-crystal structure of copper lanthanum telluride Cu₀.₂₈LaTe₂: a disordered tunnel structure

Nguyen-Huy Dung, M.-P. Pardo and P. Boy

Acta Cryst. (1983). C39, 670-673    [doi:10.1107/S0108270183005879]

Polymorphisme de LaYbS₃. Affinement des structures des deux variétés

N. Rodier, R. Julien et V. Tien

Acta Cryst. (1983). C39, 673-675    [doi:10.1107/S0108270183005880]

Affinement de la structure de NdAlO₃ par diffraction de neutrons selon la méthode du temps de vol

G. Roult, R. Pastuszak, R. Marchand et Y. Laurent

Acta Cryst. (1983). C39, 675-677    [doi:10.1107/S0108270183005892]

Structures of five large-period polytypes of cadmium iodide

S. K. Chaudhary, G. K. Chadha and G. C. Trigunayat

Acta Cryst. (1983). C39, 678-680    [doi:10.1107/S0108270183005909]

The average structure of K₂MoO₄ in the incommensurate phase at 633 K

A. J. van den Berg, H. Overeijnder and F. Tuinstra

Acta Cryst. (1983). C39, 680-683    [doi:10.1107/S0108270183005910]

Reinvestigation of the structure of tetracadmium sodium orthovanadate, Cd₄Na(VO₄)₃

S. C. Abrahams, P. Marsh and J. Ravez

Acta Cryst. (1983). C39, 683-685    [doi:10.1107/S0108270183005922]

Structure refinement of hafnium phosphide, Hf₃P

V. Pathanasin, S. Thanomkul and S. Pramatus

Acta Cryst. (1983). C39, 685-689    [doi:10.1107/S0108270183005934]

Structure de l'hydroxyborate de thallium hydraté, Tl[B₃O₄(OH)₂].0,5H₂O

M. Touboul, C. Bois, D. Mangin et D. Amoussou

metal-organic compounds

Acta Cryst. (1983). C39, 690-694    [doi:10.1107/S0108270183005946]

Structures of two forms of sodium acetate, Na⁺.C₂H₃O₂^-

Leh-Yeh Hsu and C. E. Nordman

Acta Cryst. (1983). C39, 694-698    [doi:10.1107/S0108270183005958]

Sodium-hydrogen and boron-hydrogen interactions in the cubane structure of tetrasodium tetra-₃-hydrido-tetrakis(trimethylborate) diethyl ether solvate, [NaB(CH₃)₃H]₄.(C₂H₅)₂O

N. A. Bell, H. M. M. Shearer and C. B. Spencer

Acta Cryst. (1983). C39, 698-701    [doi:10.1107/S010827018300596X]

[1,9-Bis(diphenylphosphino)-3,7-dithianonane]monobromonickel(II) tetraphenylborate, C₃₁H₃₄BrNiP₂S₂⁺.C₂₄H₂₀B^-, at 295K, and [1,9-bis(diphenylphosphino)-3,7-dithianonane]monoiodonickel(II) tetraphenylborate, C₃₁H₃₄INiP₂S₂⁺.C₂₄H₂₀B^-, at 120K

G.-I. Bertinsson

Acta Cryst. (1983). C39, 701-703    [doi:10.1107/S0108270183005971]

The catena structure and EPR properties of bis(oxamide oximato)copper(II)-oxamide oxime, [Cu(C₂H₅N₄O₂)₂].C₂H₆N₄O₂

H. Endres, N. Genc and D. Nöthe

Acta Cryst. (1983). C39, 704-705    [doi:10.1107/S0108270183005983]

Structure of trans-dinitratobis(oxamide oxime)copper(II),[Cu(C₂H₆N₄O₂)₂(NO₃)₂]

H. Endres and N. Genc

Acta Cryst. (1983). C39, 705-707    [doi:10.1107/S0108270183005995]

Structure of trans-aquabromobis[ethanedial dioximato(1-)-N,N']cobalt(III), [CoBr(C₂H₃N₂O₂)₂H₂O]

M. Mégnamisi-Bélombé, H. Endres and E. Rossato

Acta Cryst. (1983). C39, 707-709    [doi:10.1107/S0108270183006009]

Structure of di--chloro-bis[chloro(1,2-cyclohexanedione dioxime-N,N')copper(II)], [Cu₂(C₆H₁₀N₂O₂)₂Cl₄]

M. Mégnamisi-Bélombé and H. Endres

Acta Cryst. (1983). C39, 709-711    [doi:10.1107/S0108270183006010]

10-Chlorophenothiantimonin, C₁₂H₈ClSSb

W. T. Pennington, A. W. Cordes, J. C. Graham and Y. W. Jung

Acta Cryst. (1983). C39, 712-714    [doi:10.1107/S0108270183006022]

Structure of 10,10-dimethylphenothiastannin,C₁₄H₁₄SSn

W. T. Pennington, A. W. Cordes, J. C. Graham and Y. W. Jung

Acta Cryst. (1983). C39, 714-717    [doi:10.1107/S0108270183006034]

(N,N-Dimethylformamide)tetrakis(8-quinolinolato)thorium(IV), [Th(C₃H₇NO)(C₉H₆NO)₄]

R. J. Barton, R. W. Dabeka, H. Shengzhi, L. M. Mihichuk, M. Pizzey, B. E. Robertson and W. J. Wallace

Acta Cryst. (1983). C39, 718-720    [doi:10.1107/S0108270183006046]

Poly{aquadichloro[3,6-di(2-pyridyl)pyridazine]--hydroxo-dicopper(II) chloride dihydrate},{[Cu₂(C₁₄H₁₀N₄)Cl₂(H₂O)(OH)]Cl}_n.2nH₂O

P. Dapporto, G. De Munno, G. Bruno and M. Romeo

Acta Cryst. (1983). C39, 720-723    [doi:10.1107/S0108270183006058]

Aquabis(2,2'-bipyridyl)bis(thiocyanato-N)calcium, [Ca(C₁₀H₈N₂)₂(SCN)₂(H₂O)], and catena-bis(2,2'-bipyridyl)-bis--(thiocyanato-S,N)-barium, [Ba(C₁₀H₈N₂)₂(SCN)₂\]

W. H. Watson, D. A. Grossie, F. Vögtle and W. M. Müller

Acta Cryst. (1983). C39, 723-725    [doi:10.1107/S010827018300606X]

Tris(3-hydroxy-4H-pyran-4-onato)iron(III), C₁₅H₉FeO₉

B. F. Anderson, D. A. Buckingham, G. B. Robertson and J. Webb

Acta Cryst. (1983). C39, 726-728    [doi:10.1107/S0108270183006071]

trans-Azido(dimethylglyoximato-N,N')(dimethylglyoxime-N,N')(pyridine)cobalt(III), [Co(C₅H₅N)(C₄H₈N₂O₂)(C₄H₈N₂O₂)N₃\]

M. N. Ponnuswamy and J. Trotter

Acta Cryst. (1983). C39, 729-730    [doi:10.1107/S0108270183006083]

Structure of caesium fluoride-succinic acid (1:1), CsF.C₄H₆O₄

J. Emsley, D. J. Jones and R. Kuroda

Acta Cryst. (1983). C39, 731-732    [doi:10.1107/S0108270183006095]

Structure of 5,5-dimethyl-2-phenylamino-1,3,2-dioxaphosphorinane 2-selenide, C₁₁H₁₆NO₂PSe

T. J. Bartczak, Z. Galdecki, H. B. Trzezwinska and W. Wolf

organic compounds

Acta Cryst. (1983). C39, 733-734    [doi:10.1107/S0108270183006101]

Structure of 1,2-di(4-pyridyl)ethylene-7,7,8,8-tetracyano-p-quinodimethane (1:1), C₁₂H₁₀N₂.C₁₂H₄N₄

G. J. Ashwell, D. A. Kennedy and I. W. Nowell

Acta Cryst. (1983). C39, 735-737    [doi:10.1107/S0108270183006113]

Structure of a -lactam, 2,6a-di-p-tolyl-6,6a-dihydro-3H,5H-azeto[2,1-b]imidazol-5-one, C₁₉H₁₈N₂O

F. R. Ahmed

Acta Cryst. (1983). C39, 737-738    [doi:10.1107/S0108270183006125]

Structure of 3-bromo-⁵-thietane 1,1-dioxide, C₃H₅BrO₂S

J. F. Chiang

Acta Cryst. (1983). C39, 738-740    [doi:10.1107/S0108270183006137]

3-Hydroxy-1,2,3-benzotriazin-4(3H)-one, C₇H₅N₃O₂

W. E. Hunt, C. H. Schwalbe and K. Vaughan

Acta Cryst. (1983). C39, 741-742    [doi:10.1107/S0108270183006149]

7-Hydroxy-4'-methoxyisoflavanquinone (claussequinone), C₁₆H₁₄O₅

M. T. P. Gambardella, Y. P. Mascarenhas and R. H. A. Santos

Acta Cryst. (1983). C39, 743-745    [doi:10.1107/S0108270183006150]

Ethyl 3-[4,5-dimethoxy-2-(4-methyl-2-pyridylsulphamoyl)phenyl]propionate, C₁₉H₂₄O₆S

E. Eliopoulos, B. Sheldrick and S. Hamodrakas

Acta Cryst. (1983). C39, 745-747    [doi:10.1107/S0108270183006162]

Structure of 8,5'-anhydro-8-hydroxy-9--D-ribofuranosyladenine (8,5'-O-cyclo-A) monohydrate, C₁₀H₁₁N₅O₄.H₂O

S. Sugio, H. Mizuno, K. Kitamura, K. Hamada, M. Ikehara and K.-i. Tomita

Acta Cryst. (1983). C39, 748-750    [doi:10.1107/S0108270183006174]

Structure of the nematogenic compound 5,8-dihydro-6,7-dimethyl-1,4-naphthalenediyl bis(4-ethoxybenzoate), C₃₀H₃₀O₆

I. Rapthel, H. Hartung and M. Jaskólski

Acta Cryst. (1983). C39, 750-753    [doi:10.1107/S0108270183006186]

Méthyl-4 diphényl-2,3 hexahydro-1,3,3a,4,5,9b naphto[1,2-c]pyrroletricarboxylate-1,1,3a triméthylique et méthyl-5 diphényl-2,3 hexahydro-1,3,3a,4,5,9b naphto[1,2-c]pyrroletricarboxylate-1,1,3a triméthylique, C₃₁H₃₁NO₆: deux pyrrolidines obtenues par cycloaddition dipolaire-1,3

L. Toupet et J.-C. Messager

Acta Cryst. (1983). C39, 753-756    [doi:10.1107/S0108270183006198]

Méthyl-4 tétrahydro-3a,4,5,9b 1H-benzo[e]indazolecarboxylate-3a méthylique et méthyl-5 tétrahydro-3a,4,5,9b 1H-benzo[e]indazolecarboxylate-3a méthylique, C₁₄H₁₆N₂O₂: etude stéréochimique de la cycloaddition dipolaire-1,3

L. Toupet

Acta Cryst. (1983). C39, 756-758    [doi:10.1107/S0108270183006204]

1,5-Bis(-isopropyl-2,4-dimethoxybenzyl)-2,4-dimethoxybenzene, C₃₂H₄₂O₆

G. Bruno, G. Bombieri, G. Rizzardi, G. Polizzotti and M. C. Natoli

Acta Cryst. (1983). C39, 758-761    [doi:10.1107/S0108270183006216]

The structure of tanacetols A, C₁₇H₂₆O₄, and B, C₁₉H₃₀O₅, two new sesquiterpene alcohols from Tanacetum vulgare L.

M. Calleri, G. Chiari and D. Viterbo

Acta Cryst. (1983). C39, 762-764    [doi:10.1107/S0108270183006228]

Structure of trimethyl[(cis-5-methyl-1-oxolan-2-yl)methyl]ammonium iodide, C₉H₂₀NO⁺.I^-

R. Bardi, A. M. Piazzesi, A. Del Pra and L. Villa

Acta Cryst. (1983). C39, 764-766    [doi:10.1107/S010827018300623X]

Structures of substituted perfluoropolyphenyls. III. Structure of 1-bromo-4,5,6-trifluoro-2,3-bis(pentafluorophenyl)benzene, C₁₈BrF₁₃

J. B. Jones and D. S. Brown

Acta Cryst. (1983). C39, 766-768    [doi:10.1107/S0108270183006241]

Structure of N,N'-di-n-hexyl-4-oxoheptanediamide, C₁₉H₃₆N₂O₃

D. R. Rueda and J. Fayos

Acta Cryst. (1983). C39, 768-770    [doi:10.1107/S0108270183006253]

12-Phenyl-5,12-dihydrodibenz[b,g]azocin-5-one, C₂₁H₁₅NO

H. Preut, M. Thimme, T. Eicher and C. Krüger

Acta Cryst. (1983). C39, 770-771    [doi:10.1107/S0108270183006265]

Structure of syn-1,6:8,13-bismethano-2-aza[14]annulene, C₁₅H₁₃N

J. Lex, E. Vogel and M. Simonetta

Acta Cryst. (1983). C39, 772-775    [doi:10.1107/S0108270183006277]

Structure of ammonium 5-fluoro-2'-deoxyuridine cyclic 3',5'-monophosphate trihydrate, C₉H₉FN₂O₇P^-. NH₄⁺.3H₂O

T. Koritsánszky, A. Kálmán, J. Béres, K. Kömives and L. Ötvös

Acta Cryst. (1983). C39, 776-778    [doi:10.1107/S0108270183006289]

Structure of the 3₁₀-helical pentapeptide Boc-Aib-L-Ala-Aib-L-Ala-Aib-OMe dihydrate, C₂₄H₄₃N₅O₈.2H₂O

R. Bosch, G. Jung and W. Winter

Acta Cryst. (1983). C39, 778-780    [doi:10.1107/S0108270183006290]

Structure of the monoclinic form of 2,6-di-tert-butyl-4-methylphenol (DBMP), C₁₅H₂₄O

Y. Iimura, T. Sakurai, Y. Ohno, K.-I. Asahi and K. Isono

Acta Cryst. (1983). C39, 780-782    [doi:10.1107/S0108270183006307]

Structure of (2R,3S)-3,5-dimethyl-2-{(S)-1-[(3S,5R,6R)-3,5-dimethyl-2-oxo-tetrahydro-2H-pyran-6-yl]ethyl}-2,3-dihydro-4-pyranone, C₁₆H₂₄O₄

R. D. Adams and B. E. Segmuller

Acta Cryst. (1983). C39, 782-784    [doi:10.1107/S0108270183006319]

7-Hydroxy-1,2,3,5,6,8-hexamethyltetracyclo[4.2.1.1²,⁵.0³,⁷]dec-4-y methanesulphonate, C₁₇H₂₈O₄S

A. S. Secco and J. Trotter

Acta Cryst. (1983). C39, 785-788    [doi:10.1107/S0108270183006320]

Lycopsamine and intermedine, C₁₅H₂₅NO₅: diastereoisomeric pyrrolizidine alkaloids

M. F. Mackay, M. Sadek and C. C. J. Culvenor

Acta Cryst. (1983). C39, 789-790    [doi:10.1107/S0108270183006332]

Structure of trimethyl[(cis-3-methylcyclopentyl)methyl]ammonium iodide, C₁₀H₂₂N⁺.I^-

R. Bardi, A. M. Piazzesi, A. Del Pra and L. Villa

Acta Cryst. (1983). C39, 790-792    [doi:10.1107/S0108270183006344]

Structure of [2-(ethylideneaminooxy)ethyl]trimethylammonium iodide, C₇H₁₇N₂O⁺.I^-

R. Bardi, A. M. Piazzesi and A. Del Pra

Acta Cryst. (1983). C39, 793-794    [doi:10.1107/S0108270183006356]

Structure of -(diphenylmethyleneamino)--phenyldeoxybenzoin, C₃₃H₂₅NO

C. Ruiz-Valero, E. Gutiérrez-Puebla and A. Monge

Acta Cryst. (1983). C39, 795-796    [doi:10.1107/S0108270183006368]

Structure of 2-[-(diphenylmethylimino)benzyl]benzophenone, C₃₃H₂₅NO

C. Ruiz-Valero, A. Monge and E. Gutiérrez-Puebla

Acta Cryst. (1983). C39, 796-798    [doi:10.1107/S010827018300637X]

Structure of 3',5'-di-O-acetyl-5-bromo-2'-deoxyuridine, C₁₃H₁₅BrN₂O₇

J. N. Low

Acta Cryst. (1983). C39, 798-801    [doi:10.1107/S0108270183006381]

Structure of (Z)-1,3,4,5,6-penta-O-acetyl-keto-D-fructose (2,4-dinitrophenyl)hydrazone, C₂₂H₂₆N₄O₁₄

B. Kojic-Prodic, Z. Ruzic-Toros and K. Linek

Acta Cryst. (1983). C39, 801-806    [doi:10.1107/S0108270183006393]

Structures of 3-hydroxy-5-bufa-14,20,22-trienolide, C₂₄H₃₂O₃, and 3-acetoxy-15-(o-nitrobenzoyloxy)-7-oxo-5,14-bufa-8,20,22-trienolide, C₃₃H₃₅NO₉

L. R. Nassimbeni, M. L. Niven, G. M. Sheldrick, G. R. Pettit, M. Inoue and Y. Kamano

short communications

Acta Cryst. (1983). C39, 807    [doi:10.1107/S010827018300640X]

The crystal structure of (+)₅₈₉-tris[(-)-trans-1,2-diaminocyclohexane]cobalt(III) chloride monohydrate ('ob' isomer): errata

A. Kobayashi, F. Marumo and Y. Saito

Acta Cryst. (1983). C39, 808    [doi:10.1107/S0108270183006411]

Manganese bromide tetrahydrate

E. D. Crozier, N. Alberding and B. R. Sundheim

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