Acta Crystallographica Section C

Crystal Structure Communications

Volume 39, Part 7 (July 1983)

• research papers
  • inorganic compounds
  • metal-organic compounds
  • organic compounds
• short communications

research papers

inorganic compounds

Acta Cryst. (1983). C39, 809-810    [doi:10.1107/S0108270183006423]

Structure d'un trimétaphosphate acide de sodium: Na₂HP₃O₉

M. T. Averbuch-Pouchot, J. C. Guitel et A. Durif

Acta Cryst. (1983). C39, 811-812    [doi:10.1107/S0108270183006435]

Structure d'un tétramétaphosphate de sodium-strontium: SrNa₂P₄O₁₂

M. T. Averbuch-Pouchot et A. Durif

Acta Cryst. (1983). C39, 812-813    [doi:10.1107/S0108270183006447]

Structure of disodium strontium tetrametaphosphate hexahydrate, SrNa₂P₄O₁₂.6H₂O

A. Durif, M. T. Averbuch-Pouchot and J. C. Guitel

Acta Cryst. (1983). C39, 814-816    [doi:10.1107/S0108270183006459]

Structure du pentasulfure de digallium et de diétain, Ga₂Sn₂S₅

A. Mazurier, F. Thevet et S. Jaulmes

Acta Cryst. (1983). C39, 817-819    [doi:10.1107/S0108270183006460]

Structure of pentasodium trihydrogenhexatungstoplatinate(IV) icosahydrate, Na₅[H₃PtW₆O₂₄].20H₂O

U. Lee, A. Kobayashi and Y. Sasaki

Acta Cryst. (1983). C39, 819-822    [doi:10.1107/S0108270183006472]

Pentapotassium disulfite tris(hydrogensulfite), K₅(HSO₃)₃(S₂O₅)

A. Magnusson, L.-G. Johansson and O. Lindqvist

Acta Cryst. (1983). C39, 822-824    [doi:10.1107/S0108270183006484]

Structure de l'octasulfure de pentaindium et de potassium, In₅KS₈

D. Carré et M.-P. Pardo

Acta Cryst. (1983). C39, 824-827    [doi:10.1107/S0108270183006496]

Structure de la demesmaekerite, Pb₂Cu₅(SeO₃)₆(UO₂)₂(OH)₆.2H₂O

D. Ginderow and F. Cesbron

Acta Cryst. (1983). C39, 827-829    [doi:10.1107/S0108270183006502]

Redetermination of the structure of tetrasulphurtetranitrogen dioxide, S₄N₄O₂

P. G. Jones, W. Pinkert and G. M. Sheldrick

Acta Cryst. (1983). C39, 829-832    [doi:10.1107/S0108270183006514]

Barium strontium niobate and barium strontium tantalate, Ba₃SrNb₂O₉ and Ba₃SrTa₂O₉, a Rietveld refinement of neutron powder diffraction data

H. W. Zandbergen and D. J. W. IJdo

metal-organic compounds

Acta Cryst. (1983). C39, 833-835    [doi:10.1107/S0108270183006526]

Structure d'un complexe de métal de transition smectique: le bis{[(octyl-4 phényl)-1 éthylènedithiolato-1,2](2-)-S,S'}nickel, C₃₂H₄₄NiS₄

M. Cotrait, J. Gaultier, C. Polycarpe, A. M. Giroud et U. T. Mueller-Westerhoff

Acta Cryst. (1983). C39, 835-838    [doi:10.1107/S0108270183006538]

Structure of bis(tetraethylammonium) tetrathiomolybdate(VI), 2C₈H₂₀N⁺.MoS₄^2-

M. G. Kanatzidis and D. Coucouvanis

Acta Cryst. (1983). C39, 838-841    [doi:10.1107/S010827018300654X]

Structure of disodium nitronitrosylbis[2,4,5,6-(1H,3H)-pyrimidinetetrone 5-oximato(2-)]ruthenate(II) heptahydrate, Na₂[Ru(C₄HN₃O₄)₂(NO)(NO₂)].7H₂O

F. Abraham, G. Nowogrocki, S. Sueur and C. Brémard

Acta Cryst. (1983). C39, 841-843    [doi:10.1107/S0108270183006551]

Bis{-chloro-[N,N'-ethanediylidenebis(1-isopropyl-2-methylpropylamine)]copper(I)}, [Cu₂(C₁₆H₃₂N₂)₂Cl₂]

H. tom Dieck and L. Stamp

Acta Cryst. (1983). C39, 843-845    [doi:10.1107/S0108270183006563]

Structure of -oxo-(pyrimidine)--sulphido-bis{[(O,O'-diisopropylphosphorodithioato)-S,S']oxomolybdenum(V)}, Mo₂(C₄H₄N₂)(C₆H₁₄O₂PS₂)₂O₃S

P. J. Baricelli, M. G. B. Drew and P. C. H. Mitchell

Acta Cryst. (1983). C39, 846-849    [doi:10.1107/S0108270183006575]

Analysis of disorder by force-field calculation: the structure of 1,4,7,11-tetraazacyclotetradecane (isocyclam)-nickel perchlorate, C₁₀H₂₄N₄-Ni(ClO₄)₂

J. C. A. Boeyens

Acta Cryst. (1983). C39, 850-852    [doi:10.1107/S0108270183006587]

Structures of disodium malonate trihydrate, Na₂C₃H₂O₄.3H₂O, and dilithium malonate, Li₂C₃H₂O₄

M. Soriano-Garcia and S. N. Rao

Acta Cryst. (1983). C39, 852-854    [doi:10.1107/S0108270183006599]

Bis{3-[2-(2-pyridyl)ethyl]imino-2-butanone oximato}cobalt(III) perchlorate, C₂₂H₂₈CoN₆O₂⁺.ClO₄^-

A. Pajunen and S. Pajunen

Acta Cryst. (1983). C39, 854-856    [doi:10.1107/S0108270183006605]

Thiaminium tetrachlorocobaltate(II) monohydrate, C₁₂H₁₈N₄OS²⁺.CoCl₄^2-.H₂O

C. L. MacLaurin and M. F. Richardson

Acta Cryst. (1983). C39, 856-858    [doi:10.1107/S0108270183006617]

Structural characterization of 3--cyclopentadienyl-1,2-dimethyl-1,2-dicarba-3-cobalta-closo-octaborane, 1,2-(CH₃)₂-3,1,2,-(-C₅H₅)CoC₂B₅H₅

G. J. Zimmerman and L. G. Sneddon

Acta Cryst. (1983). C39, 858-860    [doi:10.1107/S0108270183006629]

Carbonatobis(triisopropylphosphine)platinum(II), C₁₉H₄₂O₃P₂Pt

G. B. Robertson and P. A. Tucker

Acta Cryst. (1983). C39, 861-863    [doi:10.1107/S0108270183006630]

Structure of a complex between sodium perchlorate and 6,7,9,10,12,13,15,16,23,24,26,27-dodecahydrodibenzo[b,k][1,4,7,10,13,16,19,22]octaoxacyclotetracosin (asymmetric dibenzo-24-crown-8), C₂₄H₃₂O₈.NaClO₄

J. D. Owen

Acta Cryst. (1983). C39, 863-865    [doi:10.1107/S0108270183006642]

[N,N'-Ethylenebis(salicylideneiminato)]nickel(II), [Ni(C₁₆H₁₄N₂O₂)]. A redetermination

A. Gaetani Manfredotti and C. Guastini

Acta Cryst. (1983). C39, 865-868    [doi:10.1107/S0108270183006654]

Structure of ³-allyl[1,2-bis(dimethylphosphino)ethane]-⁶-toluenetungsten hexafluorophosphate, [W(C₃H₅)(C₇H₈)(C₆H₁₆P₂)]PF₆

A. Gourdon and K. Prout

Acta Cryst. (1983). C39, 868-871    [doi:10.1107/S0108270183006666]

Structures of N-(4-cyanophenyl)acetohydroxamic acid, C₉H₈N₂O₂ (I), and tris[N-(4-cyanophenyl)acetohydroxamato]iron(III) hydrate, [Fe(C₉H₇N₂O₂)₃].0.1H₂O (II)

R. R. Mocherla, D. R. Powell, C. L. Barnes and D. van der Helm

Acta Cryst. (1983). C39, 872-874    [doi:10.1107/S0108270183006678]

Structure of (3,5,5,13,13,15-hexamethyl-1,2,6,9,12-pentaazacyclopentadeca-2,15-diene)nickel(II) perchlorate, C₁₆H₃₃N₅Ni²⁺.2ClO₄^-

F. W. B. Einstein and T. Jones

Acta Cryst. (1983). C39, 874-877    [doi:10.1107/S010827018300668X]

Structure of sodium diisopropyldithiocarbamate pentahydrate, Na[C₇H₁₄NS₂].5H₂O

I. Ymén

Acta Cryst. (1983). C39, 877-879    [doi:10.1107/S0108270183006691]

Structure of diiodo[1,2-bis(phenylthio)benzene]palladium(II) diiodine (1/1), [Pd(C₁₈H₁₄S₂)I₂]I₂

L. R. Gray, D. J. Gulliver, W. Levason and M. Webster

organic compounds

Acta Cryst. (1983). C39, 880-882    [doi:10.1107/S0108270183006708]

Structure of bis(triphenylphosphoranediyl)ammonium chloride-boric acid adduct (1:1), C₃₆H₃₀NP₂⁺.Cl^-.BH₃O₃

S. J. Andrews, D. A. Robb and A. J. Welch

Acta Cryst. (1983). C39, 882-887    [doi:10.1107/S010827018300671X]

Structural studies of intermediates in antibiotic synthesis. I. The structures of penicillin sulfoxide rearrangement products: 2,3,5,6-tetrahydro-5-hydroxymethyl-6,6-dimethyl-1,3-dioxo-8-[(phenylacetyl)amino]-1H-imidazo[5,1-c][1,4]thiazine (I) , C₁₇H₁₉N₃O₄S, and 2,3,5,6-tetrahydro-6,6-dimethyl-1,3-dioxo-8-[(phenylacetyl)amino]-1H-imidazo[5,1-c][1,4]thiazine-5-carboxylic acid (II), C₁₇H₁₇N₃O₅S

T. E. Haran, A. Nudelman and Z. Shakked

Acta Cryst. (1983). C39, 887-888    [doi:10.1107/S0108270183006721]

1-Methyl-5-thia-1-thioniacyclooctane iodide, C₇H₁₅S₂⁺.I^-

W. K. Musker, M. M. Olmstead and M. H. Goodrow

Acta Cryst. (1983). C39, 889-890    [doi:10.1107/S0108270183006733]

exo-2-Chloro-anti-[7](4-chlorophenylthio)benzo[8,9,10]trinorbornene, C₁₇H₁₄Cl₂S

G. H. Schmid, B. Toyonaga, PikYuen Siew and S. C. Nyburg

Acta Cryst. (1983). C39, 891-893    [doi:10.1107/S0108270183006745]

Structures of 2-amino-3,5-dibromo-N-cyclohexyl-N-methylbenzenemethanamine-salicylic acid (1:1)(ABCMBMA-SALA), C₁₄H₂₀Br₂N₂.C₇H₆O₃

N. Shimizu, S. Nishigaki, Y. Nakai and K. Osaki

Acta Cryst. (1983). C39, 894-896    [doi:10.1107/S0108270183006757]

tert-Butyloxycarbonyl--aminoisobutyryl--aminoisobutyrate benzyl ester, C₂₀H₃₀N₂O₅

P. Van Roey, G. D. Smith, T. M. Balasubramanian and G. R. Marshall

Acta Cryst. (1983). C39, 896-899    [doi:10.1107/S0108270183006769]

Structure of a 1:2 adduct between 1,4,7,10,13,16-hexaoxacyclooctadecane and N,N'-dimethylthiourea, C₁₂H₂₄O₆.2C₃H₈N₂S

G. Weber

Acta Cryst. (1983). C39, 899-901    [doi:10.1107/S0108270183006770]

The structure of gentiogenal: (±)-6-methyl-1-oxo-3,4-dihydro-1H,6H-pyrano[3,4-c]pyran-5-carbaldehyde, C₁₀H₁₀O₄

A. L. Spek, A. J. M. Duisenberg, W. G. van der Sluis, J. M. van der Nat and R. P. Labadie

Acta Cryst. (1983). C39, 901-903    [doi:10.1107/S0108270183006782]

Structure of 1,1,3,3-tetraisopropyl-1,3-disiloxanediol, C₁₂H₃₀O₃Si₂

W. Clegg

Acta Cryst. (1983). C39, 903-905    [doi:10.1107/S0108270183006794]

Tétrahydro-5,6,7,7a benzo[3,4]cyclobuta[1,2-b]benzazocine[1], C₁₇H₁₅N

B. Viossat, N. Rodier, G. Adam, J. Andrieux et M. Plat

Acta Cryst. (1983). C39, 905-907    [doi:10.1107/S0108270183006800]

(6S)-1,4-Diazabicyclo[4.4.0]dec-8-ene-2,5-dione monohydrate, C₈H₁₀N₂O₂.H₂O

J. Dillen and A. T. H. Lenstra

Acta Cryst. (1983). C39, 908-909    [doi:10.1107/S0108270183006812]

The structure of hexamethylenediammonium bis(monohydrogen oxalate) monohydrate, C₆H₁₈N₂²⁺.2C₂HO₄^-.H₂O

J. Vijayalakshmi and R. Srinivasan

Acta Cryst. (1983). C39, 910-912    [doi:10.1107/S0108270183006824]

-(2,3-Dimethylphenyl)--butyrolactone, C₁₂H₁₄O₂

A. S. Secco and J. Trotter

Acta Cryst. (1983). C39, 912-914    [doi:10.1107/S0108270183006836]

Structure of piperazinium succinate, C₄H₄O₄^2-.C₄H₁₂N₂²⁺

M. Vanier and F. Brisse

Acta Cryst. (1983). C39, 914-915    [doi:10.1107/S0108270183006848]

Structure of piperazinium adipate, C₆H₈O₄^2-.C₄H₁₂N₂²⁺

M. Vanier and F. Brisse

Acta Cryst. (1983). C39, 916-917    [doi:10.1107/S010827018300685X]

Structure of piperazinium suberate monohydrate, C₈H₁₂O₄^2-.C₄H₁₂N₂²⁺.H₂O

M. Vanier, F. Bélanger-Gariépy and F. Brisse

Acta Cryst. (1983). C39, 918-920    [doi:10.1107/S0108270183006861]

Structure of N-cyano-N',N''-dimethyl-N'-nitrosoguanidine, C₄H₇N₅O

W. V. Cruz and K. Seff

short communications

Acta Cryst. (1983). C39, 920    [doi:10.1107/S0108270183006873]

The low-temperature X-ray diffraction studies of the heptahydridobis(tertiaryphosphine)rhenium complexes, [ReH₇{P(C₃H₇)₂(C₆H₅)}₂] and [ReH₇{P(C₆H₅)₃}₂]:erratum

J. A. K. Howard, K. A. Mead and J. L. Spencer

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