Acta Crystallographica Section C

Crystal Structure Communications

Volume 39, Part 8 (August 1983)



research papers


inorganic compounds



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Acta Cryst. (1983). C39, 921-925    [doi:10.1107/S0108270183006885]

Structures of Pb3GeGa10O20 and Ba3SnFe10O20

M. C. Cadée, G. C. Verschoor and D. J. W. IJdo



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Acta Cryst. (1983). C39, 925-930    [doi:10.1107/S0108270183006897]

A neutron diffraction determination of the structure of deuterated aluminium nitrate nonahydrate, A1(NO3)3.9D2O

K. Hermansson



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Acta Cryst. (1983). C39, 930-936    [doi:10.1107/S0108270183006903]

Structure and electron deformation density of LiNO2.H2O at 295 K

K. Hermansson and J. O. Thomas



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Acta Cryst. (1983). C39, 936-939    [doi:10.1107/S0108270183006915]

Structure de l'orthophosphate triple de magnésium et de sodium, NaMg4(PO4)3

M. Ben Amara, M. Vlasse, R. Olazcuaga, G. Le Flem et P. Hagenmuller



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Acta Cryst. (1983). C39, 939-941    [doi:10.1107/S0108270183006927]

Tetraaquatrinitratoneodymium(III) dihydrate, [Nd(NO3)3(H2O)4].2H2O

D. J. Rogers, N. J. Taylor and G. E. Toogood



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Acta Cryst. (1983). C39, 941-943    [doi:10.1107/S0108270183006939]

Calcium cesium triazide monohydrate, CaCs(N3)3.H2O

H. Krischner, F. A. Mautner and Ch. Kratky



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Acta Cryst. (1983). C39, 943-946    [doi:10.1107/S0108270183006940]

Structures of Ba8Ga7, Sr8Ga7 and Sr8Al7

M. L. Fornasini



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Acta Cryst. (1983). C39, 946-947    [doi:10.1107/S0108270183006952]

Structural redermination of the ThNi phase

M. L. Fornasini



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Acta Cryst. (1983). C39, 947-952    [doi:10.1107/S0108270183006964]

Structure de l'octachlorure de tricadmium et de calcium 8,5-hydraté, 2[Ca(H2O)7].[Cd6Cl16(H2O)2][infinity].H2O

H. Leligny et J. C. Monier



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Acta Cryst. (1983). C39, 952-956    [doi:10.1107/S0108270183006976]

Structure refinement of strontium nitrate, Sr(NO3)2, and barium nitrate, Ba(NO3)2

H. Nowotny and G. Heger



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Acta Cryst. (1983). C39, 956-958    [doi:10.1107/S0108270183006988]

Calcium sulfat subhydrat, CaSO4.0,8H2O

W. Abriel



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Acta Cryst. (1983). C39, 959-960    [doi:10.1107/S010827018300699X]

Dithalliumtrischwefeltrinitrid-tetraschwefelpentanitrid, Tl2S7N8

H. Martan and J. Weiss



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Acta Cryst. (1983). C39, 961-962    [doi:10.1107/S0108270183007003]

Structure of cesium fac-trichlorotrioxorhenate(VII), Cs2[ReCl3O3]

T. Lis



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Acta Cryst. (1983). C39, 963-965    [doi:10.1107/S0108270183007015]

Structure of solid carbon diselenide (CSe2) at 17.5, 50 and 200K

B. M. Powell and B. H. Torrie



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Acta Cryst. (1983). C39, 966-968    [doi:10.1107/S0108270183007027]

Structure of monoclinic nickel sulphate hexadeuterate, NiSO4.6D2O

H. Ptasiewicz-Bak, G. J. McIntyre and I. Olovsson



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Acta Cryst. (1983). C39, 968-971    [doi:10.1107/S0108270183007039]

Structure de la phase ordonnée du sesquiséléniure de gallium, Ga2Se3

G. Ghémard, S. Jaulmes, J. Etienne et J. Flahaut



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Acta Cryst. (1983). C39, 971-974    [doi:10.1107/S0108270183007040]

Sur les composés III-V-VI: étude structurale du disulfure d'antimoine et de thallium, TlSbS2

N. Rey, J. C. Jumas, J. Olivier-Fourcade et E. Philippot


metal-organic compounds



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Acta Cryst. (1983). C39, 975-976    [doi:10.1107/S0108270183007052]

[mu]-Carbonyl-[mu]-(hydroxooxophosphido)-bis(carbonyl-[eta]-cyclopentadienyliron)(Fe-Fe), C13H11Fe2O5P

B. Deppisch and H. Schäfer



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Acta Cryst. (1983). C39, 977-980    [doi:10.1107/S0108270183007064]

Structure of bis[dichloro-[mu]-bis(3,5-dimethyl-4-pyrazolyl)methane-cobalt(II)]-ethanol (3:2), C22H32Cl4Co2N8.2/3C2H6O

C. Foces-Foces, F. H. Cano and S. García-Blanco



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Acta Cryst. (1983). C39, 981-982    [doi:10.1107/S0108270183007076]

Dibromobis[tetracarbonyl(triphenylphosphine)rhenio]tin(IV), [SnBr2{Re(C18H15P)(CO)4}2]

H. Preut and H.-J. Haupt



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Acta Cryst. (1983). C39, 983-984    [doi:10.1107/S0108270183007088]

Potassium 3-anilino-2-phenyl-3H-naphtho[1,2-d]imidazole-5-sulphonate, K[C23H16N3O3S]

M. R. Ciajolo, M. Parrilli, P. A. Temussi and A. Tuzi



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Acta Cryst. (1983). C39, 985-987    [doi:10.1107/S010827018300709X]

Structure of benzoyl(tert-butyl isocyanide)(carbonyl)bis(dimethylphenylphosphine)(phenyl)ruthenium(II), C35H41NO2P2Ru

S. A. Chawdhury, Z. Dauter, R. J. Mawby, C. D. Reynolds, D. R. Saunders and M. Stephenson



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Acta Cryst. (1983). C39, 987-990    [doi:10.1107/S0108270183007106]

Trilithium citrate pentahydrate, C6H5O73-. 3Li+.5H2O

M. Rossi, L. F. Rickles and J. P. Glusker



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Acta Cryst. (1983). C39, 990-993    [doi:10.1107/S0108270183007118]

Structure of a,b,c,j,k,l-hexaaqua-d,e,f,g,h,i-hexakis[[mu]-(4-ethyl-1,2,4-triazole-N1,N2)]trizinc(II) hexakis(trifluoromethanesulphonate), [Zn3(C4H7N3)6(H2O)6][CF3SO3]6

A. L. Spek and G. Vos



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Acta Cryst. (1983). C39, 993-994    [doi:10.1107/S010827018300712X]

2,4-Bis[1,1-dimethyl-2-(methylthio)ethyl]-3-furyl-S,S}chloropalladium(II), [Pd(C14H23OS2)Cl]

G. Ferguson, R. McCrindle and M. Parvez



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Acta Cryst. (1983). C39, 995-996    [doi:10.1107/S0108270183007131]

The structure of bromotris(triphenylphosphine)nickel(I), C54H45BrNiP3

C. Mealli, P. Dapporto, V. Sriyunyongwat and T. A. Albright



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Acta Cryst. (1983). C39, 997-999    [doi:10.1107/S0108270183007143]

Structure of [1,2-bis(dimethylphosphino)ethane]bis(0-ethyl dithiocarbonato-S,S')cobalt(III) tetraphenylborate, [Co(C3H5OS2)2(C6H16P2)] [B(C6H5)4\]

S. Ohba, M. Ito, Y. Saito and T. Ishii



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Acta Cryst. (1983). C39, 999-1001    [doi:10.1107/S0108270183007155]

Structure of bis[N-(2-pyrrolylmethylene)-tert-butylamine]zinc(II), Zn(C9H13N2)2

J. A. Kanters, A. L. Spek, R. Postma, G. C. van Stein and G. van Koten



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Acta Cryst. (1983). C39, 1001-1005    [doi:10.1107/S0108270183007167]

Structure du complexe dimérique formé par un polyéther macrocyclique tetrafonctionnel avec l'ion potassium, 2C24H44N4O10.3KBr.7H2O: un modèle de canal transmembranaire

A.-C. Dock, D. Moras, J.-P. Behr et J.-M. Lehn



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Acta Cryst. (1983). C39, 1005-1007    [doi:10.1107/S0108270183007179]

Structure of catena-dichloro-[mu]-(1,4-dioxane-O,O')-(1,4-dioxane)zinc(II),[Zn(C4H8O2)2Cl2]

A. Boardman, R. W. H. Small and I. J. Worrall



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Acta Cryst. (1983). C39, 1007-1009    [doi:10.1107/S0108270183007180]

Structure of tris(tetraphenylphosphonium) tris[chlorocopper(I)]oxotrithiomolybdate(VI) dichlorocuprate(I), [Ph4P]3[MoOS3(CuCl)3][CuCl2]

W. Clegg, C. D. Garner, J. R. Nicholson and P. R. Raithby



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Acta Cryst. (1983). C39, 1010-1012    [doi:10.1107/S0108270183007192]

10-Chlorophenothiarsenin, C12H8AsClS

W. T. Pennington, A. W. Cordes, J. C. Graham and Y. W. Jung



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Acta Cryst. (1983). C39, 1012-1015    [doi:10.1107/S0108270183007209]

Carbonato[tris(2-aminoethyl)amine]cobalt(III) chloride trihydrate, [Co(C6H18N4)(CO3)]Cl.3H2O

E. O. Schlemper, P. K. Sen Gupta and T. P. Dasgupta



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Acta Cryst. (1983). C39, 1015-1017    [doi:10.1107/S0108270183007210]

Structure of a complex of trans-dichlorobis(triphenylphosphine)palladium(II) with p-dichlorobenzene, [PdCl2{P(C6H5)3}2]. 1/2(p-C6H4Cl2)

Y. Kitano, Y. Kinoshita, R. Nakamura and T. Ashida



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Acta Cryst. (1983). C39, 1018-1020    [doi:10.1107/S0108270183007222]

Structure of bis[bis(2-hydroxyethyl)dithiocarbamato]diiodotellurium(IV), [Te(C5H10NO2S2)2I2]

G. V. N. Appa Rao, M. Seshasayee, G. Aravamudan and K. Radha



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Acta Cryst. (1983). C39, 1021-1023    [doi:10.1107/S0108270183007234]

Structure of bis[bis(2-hydroxyethyl)dithiocarbamato]tellurium(II), [Te(C5H10NO2S2)2]

G. C. Rout, M. Seshasayee, K. Radha and G. Aravamudan



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Acta Cryst. (1983). C39, 1024-1027    [doi:10.1107/S0108270183007246]

The X-ray single-crystal and molecular structures of [Co2(CO)6C2R2] for R = Ph (I), CO2Me (II) (292 K) and R = But (III) (200 K)

D. Gregson and J. A. K. Howard



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Acta Cryst. (1983). C39, 1027-1031    [doi:10.1107/S0108270183007258]

Hexakis(imidazole)manganese(II) dichloride tetrahydrate, [Mn(C3H4N2)6]Cl2.4H2O, and hexakis(imidazole)zinc(II) dichloride tetrahydrate, [Zn(C3H4N2)6\]Cl2.4H2O

T. P. J. Garrett, J. M. Guss and H. C. Freeman



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Acta Cryst. (1983). C39, 1031-1034    [doi:10.1107/S010827018300726X]

trans-Diaquatetrakis(imidazole)manganese(II) dichloride, [Mn(C3H4N2)4(H2O)2]Cl2

T. P. J. Garrett, J. M. Guss and H. C. Freeman



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Acta Cryst. (1983). C39, 1034-1036    [doi:10.1107/S0108270183007271]

Dibromo[[alpha]-(tert-butyl-1 aziridinyl-2)benzylidèneamine]zinc(II), [ZnBr2(C13H18N2)] (1), et dibromo[[alpha]-(tert-butyl-1 aziridinyl-2)benzylamine]zinc(II), [ZnBr2(C13H20N2)] (2)

R. Bartnik, S. Lesniak, A. Laurent, R. Faure et H. Loiseleur



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Acta Cryst. (1983). C39, 1037-1038    [doi:10.1107/S0108270183007283]

Structure of sodium acetylacetonate monohydrate, Na[C5H7O2].H2O

J. J. Sahbari and M. M. Olmstead



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Acta Cryst. (1983). C39, 1039-1041    [doi:10.1107/S0108270183007295]

Structure of the pyridine-ferric chloride (4:1) complex, Fe(C5H5N)3Cl3.C5H5N, at 190 K

A. Hoser, Z. Kaluski, M. Januszczyk, J. Pietrzak and T. Glowiak



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Acta Cryst. (1983). C39, 1041-1043    [doi:10.1107/S0108270183007301]

Structure of indenyluranium trichloride-bis(tetrahydrofuran), [U(C9H7)]Cl3.2C4H8O

J. Rebizant, M. R. Spirlet and J. Goffart


organic compounds



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Acta Cryst. (1983). C39, 1044-1048    [doi:10.1107/S0108270183007313]

Push-pull ethylenes: the structures of 3-(2-imidazolidinylidene)-2,4-pentanedione (I), C8H12N2O2, and 3-(1,3-dimethyl-2-imidazolidinylidene)-2,4-pentanedione trihydrate (II), C10H16N2O2.3H2O

D. Adhikesavalu and K. Venkatesan



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Acta Cryst. (1983). C39, 1048-1051    [doi:10.1107/S0108270183007325]

Structure of 2,2-bis(1,1,1,3,3,3-hexafluoro-2-propyloxy)-2-phenyl-4,4,5,5-tetrakis(trifluoromethyl)-1,3,2[lambda]5-dioxaphospholane, C18H7F24O4P

Mazhar-ul-Haque, J. Ahmed and W. Horne



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Acta Cryst. (1983). C39, 1051-1053    [doi:10.1107/S0108270183007337]

c-4,t-5-Bis(p-methoxyphenyl)-t-3-methyl-r-2-phenyl-1,3-oxazolidine, C24H25NO3

T. Skarzynski, A. M. Brozozowski, Z. Derewenda and G. Mloston



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Acta Cryst. (1983). C39, 1053-1055    [doi:10.1107/S0108270183007349]

1,4,7,14,22-Pentaoxa[7]orthocyclo[2]metacyclo[2]orthocyclophane, C24H24O5

G. Weber and P. G. Jones



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Acta Cryst. (1983). C39, 1055-1057    [doi:10.1107/S0108270183007350]

Structure of tefludazine, 2-{4-[3-(4-fluorophenyl)-6-(trifluoromethyl)-1-indanyl]piperazinyl}ethanol, C22H24F4N2O

B. Jensen



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Acta Cryst. (1983). C39, 1057-1059    [doi:10.1107/S0108270183007362]

trans-2-Isopropyl-N,N-dimethyl-1,3-dioxane-5-carbothioamide, C10H19NO2S

M. Shoja and M. K. Kaloustian



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Acta Cryst. (1983). C39, 1059-1062    [doi:10.1107/S0108270183007374]

Structure of a racemic compound: the dicyclohexylammonium salt of (2R,4R,2S,4S)-cis-4-methyl-2-oxido-1,3,2-dioxaphosphorinane 2-sulphide, C12H24N+.C4H8O3PS-

T. J. Bartczak



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Acta Cryst. (1983). C39, 1062-1063    [doi:10.1107/S0108270183007386]

4-Phenyl-1,6-dioxaspiro[4.5]decan-4-ol, C14H18O3

P. Bron, L. Cottier, G. Descotes, R. Faure and H. Loiseleur



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Acta Cryst. (1983). C39, 1064-1065    [doi:10.1107/S0108270183007398]

Structure of 6,6-dimethyl-6a-dimethylamino-2,3a-diphenyl-6,6a-dihydropyrrolo[3,4-d]oxazol-4(3aH)-one, C21H23N3O2

J. H. Bieri, H. Heimgartner, G. Germain and J.-P. Declercq



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Acta Cryst. (1983). C39, 1066-1070    [doi:10.1107/S0108270183007404]

Structure of sinomenine hydrochloride dihydrate, C19H24NO4+.Cl-.2H2O

S. V. Bjørnevåg, B. C. Hauback, F. Mo and H. Sørum



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Acta Cryst. (1983). C39, 1070-1072    [doi:10.1107/S0108270183007416]

Structure of [sigma](+)-5-bromo-6,9-bis(dimethylsulphido)-nido-decaborane(12), C4H23B10BrS2, determined with a twinned crystal

V. Petrícek, I. Císarová and V. Subrtová



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Acta Cryst. (1983). C39, 1073-1075    [doi:10.1107/S0108270183007428]

Haplociliatic acid, C20H32O4

W. H. Watson, V. Zabel and M. L. Bittner



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Acta Cryst. (1983). C39, 1075-1076    [doi:10.1107/S010827018300743X]

Structure of 3-(o-carboxyphenyl)-1-phenyltriazene 1-oxide, C13H11N3O3

S. B. Sarkar, Md. Khalil, S. C. Saha and S. K. Talapatra



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Acta Cryst. (1983). C39, 1077-1078    [doi:10.1107/S0108270183007441]

Structure of N,N-bis(p-nitrophenylsulfonyl)phenethylamine, C20H17N3O8S2

V. A. Curtis and S. F. Pavkovic



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Acta Cryst. (1983). C39, 1079-1082    [doi:10.1107/S0108270183007453]

Structure of 4-methyl-5-(2-pyrazinyl)-3H-1,2-dithiole-3-thione (oltipraz), C8H6N2S3: a new antischistosomal drug

C. H. Wei



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Acta Cryst. (1983). C39, 1082-1084    [doi:10.1107/S0108270183007465]

Structure of dihydroxyacetic acid (glyoxylic acid monohydrate), C2H4O4

T. Lis



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Acta Cryst. (1983). C39, 1084-1087    [doi:10.1107/S0108270183007477]

Détermination structurale du monomère bis(butoxycarbonylméthylcarbamate) de hexadiyne-2,4 diyle-1,6, C20H28N2O8

P. Spinat, A. Whuler et C. Brouty



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Acta Cryst. (1983). C39, 1087-1089    [doi:10.1107/S0108270183007489]

Structure du chlorhydrate de {[(o-méthoxyphényl)-4 pipérazinyl-1]-2 éthyl}-2 diméthyl-4,4 2H,4H-isoquinolinedione-1,3-éthanol (AR-C239), C24H30N3O3+.Cl-.C2H6O

A. Carpy, M. Goursolle et J.-M. Léger



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Acta Cryst. (1983). C39, 1089-1092    [doi:10.1107/S0108270183007490]

Benzotriazole 1-oxide and 1-hydroxybenzotriazole, C6H5N3O: structures of both tautomeric forms

R. Bosch, G. Jung and W. Winter



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Acta Cryst. (1983). C39, 1092-1094    [doi:10.1107/S0108270183007507]

2-Benzoylcyclohexanecarboxylic acid, C14H16O3

J. H. Choney, E. M. Holt, N. Pourahmady and E. J. Eisenbraun



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Acta Cryst. (1983). C39, 1094-1096    [doi:10.1107/S0108270183007519]

Structure of 5,6,7,8-tetrahydro-4H-3,1-benzothiazine-2(1H)-spirocyclohexane-4-thione, C13H19NS2

A. Castieiras-Campos, A. Ruiz-Amil, S. Martínez-Carrera and S. García-Blanco



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Acta Cryst. (1983). C39, 1097-1101    [doi:10.1107/S0108270183007520]

An X-ray crystallographic study of 1,2,5- and 1,3,5-triazapentadienium salts, C6H14N3+.ClO4-, C6H14N3+.ClO4-, C6H14N3+.C6H2N3O7-

R. O. Gould, H. McNab and M. D. Walkinshaw



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Acta Cryst. (1983). C39, 1101-1103    [doi:10.1107/S0108270183007532]

Structure d'agents mutagènes. II. Le méthoxy-8 nitro-2 naphto[2,1-b]furanne, C13H9NO4

J.-P. Bideau, G. Bravic, M. Cotrait et C. Courseille



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Acta Cryst. (1983). C39, 1103-1105    [doi:10.1107/S0108270183007544]

3',5'-Di-O-acetyl-2'-deoxy-5-iodouridine, C13H15IN2O7

C. C. Wilson, J. N. Low and D. W. Young



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Acta Cryst. (1983). C39, 1106-1108    [doi:10.1107/S0108270183007556]

Structures of 2,9-di-tert-butyl-1,1,4,6,8,8,11,12-octamethyl-6,12-diphenyl-2,3,9,10-tetraaza-1,6,8,12-tetrasiladispiro[4.1.4.1]dodeca-3,10-diene, C32H52N4Si4, (1), and 1,6-bis[bis(trimethylsily)amino]-3,5,8,10-tetramethyl-4,5,9,10-tetraaza-1,6-disilatricyclo[5.3.0.02,6]deca-3,8-diene, C20H50N6Si6, (2)

W. Clegg



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Acta Cryst. (1983). C39, 1108-1111    [doi:10.1107/S0108270183007568]

Structure of crogyroidine dihydrate, C20H34Br2N2.2H2O

R. S. Sawhney, P. K. Sen Gupta, M. B. Hossain and D. van der Helm



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Acta Cryst. (1983). C39, 1111-1113    [doi:10.1107/S010827018300757X]

Structure of 2-furoic acid, C5H4O3: a redetermination

C. J. Gilmore, P. R. Mallinson and J. C. Speakman



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Acta Cryst. (1983). C39, 1113-1114    [doi:10.1107/S0108270183007581]

A redetermination of the structure of 1,1,2,2-tetracarbomethoxyethane, C10H14O8, at 145 K

F. R. Fronczek, V. K. Gupta and G. R. Newkome



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Acta Cryst. (1983). C39, 1115-1117    [doi:10.1107/S0108270183007593]

Taurin from Artemisia cretacea Fiori, C15H20O3

M. Calleri, G. Chiari and D. Viterbo



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Acta Cryst. (1983). C39, 1118-1120    [doi:10.1107/S010827018300760X]

13,13-Dimethyl-1,10-diphenyl-13-silatricyclo[8.2.1.02,9]trideca-2(9),11-diene, C26H30Si (I), and 1,4-dihydro-9,9-dimethyl-1,4-diphenyl-1,4-silanonaphthalene, C24H22Si (II)

H. Preut, B. Mayer and W. P. Neumann



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Acta Cryst. (1983). C39, 1121-1123    [doi:10.1107/S0108270183007611]

Structural studies of the system trans-azobenzene/trans-stilbene. I. A reinvestigation of the disorder in the crystal structure of trans-azobenzene, C12H10N2

J. A. Bouwstra, A. Schouten and J. Kroon



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Acta Cryst. (1983). C39, 1123-1127    [doi:10.1107/S0108270183007623]

Disordered structure of 2,3-dichloro-6,7-dimethylanthracene, C16H12Cl2, for sublimation-grown (I) and solution-grown (II) crystals

T. R. Welberry, R. D. G. Jones and M. Puza



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Acta Cryst. (1983). C39, 1127-1129    [doi:10.1107/S0108270183007635]

Méthyl-4 oxo-7 phényl-5 tétrahydro-2,3,4,7 oxazépine-1,4 carbonitrile-6, C13H12N2O2 (1), et méthyl-4 oxo-7 phényl-5 tétrahydro-2,3,4,7 oxazépine-1,4 carboxylate-6 d'éthyle, C15H17NO4 (2)

M. Drême, P. Le Perchec, R. Faure et H. Loiseleur



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Acta Cryst. (1983). C39, 1130-1132    [doi:10.1107/S0108270183007647]

Structure and absolute configuration of N-tert-butyl-1-methyl-3,3-diphenylpropylamine (terodiline) hydrochloride, C20H28N+.Cl-

D. Carlström and I. Hacksell



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Acta Cryst. (1983). C39, 1132-1133    [doi:10.1107/S0108270183007659]

N,N'-Dinitrosopentamethylenetetramine, C5H10N6O2

C. J. Brown and J. L. Craft



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Acta Cryst. (1983). C39, 1134-1136    [doi:10.1107/S0108270183007660]

(E)-4-Chloro-2,6-dimethylbenzaldehyde O-methyloxime, C10H12ClNO, at 93K

B. Jerslev, J. Lerche and I. K. Larsen



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Acta Cryst. (1983). C39, 1136-1138    [doi:10.1107/S0108270183007672]

Structure du dithiosalicylide, C14H8O2S2

J.-M. Medard, N. Rodier, P. Reynaud, J. D. Brion and NguyenTri Xuong



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Acta Cryst. (1983). C39, 1139-1141    [doi:10.1107/S0108270183007684]

Structure of helioscopinolide A, C20H28O3, a novel diterpene

S. Ohba, M. Ito, Y. Saito, Y. Shizuri, S. Kosemura and S. Yamamura


short communications



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Acta Cryst. (1983). C39, 1141-1142    [doi:10.1107/S0108270183007696]

Ring asymmetry parameters from out-of-plane atomic displacements

M. Nardelli


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