Acta Crystallographica Section C

Crystal Structure Communications

Volume 39, Part 9 (September 1983)



research papers


inorganic compounds



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Acta Cryst. (1983). C39, 1143-1146    [doi:10.1107/S0108270183007702]

New structure determination of murdochite, Cu6PbO8

E. Dubler, A. Vedani and H. R. Oswald



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Acta Cryst. (1983). C39, 1146-1150    [doi:10.1107/S0108270183007714]

Room-temperature structure of carbon monoxide at 2.7 and 3.6 GPa

D. T. Cromer, D. Schiferl, R. LeSar and R. L. Mills



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Acta Cryst. (1983). C39, 1151-1153    [doi:10.1107/S0108270183007726]

Structure of N2 at 2.94 GPa and 300 K

D. Schiferl, D. T. Cromer, R. R. Ryan, A. C. Larson, R. LeSar and R. L. Mills



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Acta Cryst. (1983). C39, 1153-1156    [doi:10.1107/S0108270183007738]

Synthèse et structure d'un niobate de césium non stoechiométrique, Cs3Nb5,96O16,4

M.-C. Saine et M. Gasperin



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Acta Cryst. (1983). C39, 1156-1159    [doi:10.1107/S010827018300774X]

Tricobalt hexasodium hexakis(hexahydroxohexaborate) hexacosahydrate, Na6Co3[B6O7(OH)6]6.26H2O

H. Behm



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Acta Cryst. (1983). C39, 1160-1163    [doi:10.1107/S0108270183007751]

Structures of 20 new polytypes of cadmium iodide

B. Palosz



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Acta Cryst. (1983). C39, 1163-1165    [doi:10.1107/S0108270183007763]

Orthorhombic uranium(IV) molybdenum(VI) oxide, UMo2O8

T. L. Cremers, P. G. Eller, R. A. Penneman and C. C. Herrick



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Acta Cryst. (1983). C39, 1165-1167    [doi:10.1107/S0108270183007775]

Orthorhombic thorium(IV) molybdate, Th(MoO4)2

T. L. Cremers, P. G. Eller and R. A. Penneman



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Acta Cryst. (1983). C39, 1167-1169    [doi:10.1107/S0108270183007787]

Ammonium trifluoroberyllate(II), (NH4)[BeF3], at room temperature

A. Waskowska



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Acta Cryst. (1983). C39, 1169-1172    [doi:10.1107/S0108270183007799]

Structure of orthopyroxene-type and clinopyroxene-type magnesium germanium oxide MgGeO3

M. Ozima



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Acta Cryst. (1983). C39, 1173-1174    [doi:10.1107/S0108270183007805]

Disilver(I) decachlorodioxotetraaluminate(III), Ag2[Al4Cl10O2]

D. Jentsch, P. G. Jones, E. Schwarzmann and G. M. Sheldrick


metal-organic compounds



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Acta Cryst. (1983). C39, 1175-1177    [doi:10.1107/S0108270183007817]

The structure of Ni(cyclam)I2.H2O, [Ni(C10H24N4)I]I.H2O

L. Prasad and A. McAuley



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Acta Cryst. (1983). C39, 1177-1180    [doi:10.1107/S0108270183007829]

Etude stéréochimique du tricarbonyl[5a-9a-[eta]-(méthyl-4 tétrahydro-3a,4,5,9b 1H-benz[e]indazolecarboxylate-3a de méthyle)]chrome(III), [Cr(C14H16N2O2)(CO)3\]

R. Mercier, J. Douglade et J. Vebrel



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Acta Cryst. (1983). C39, 1180-1182    [doi:10.1107/S0108270183007830]

Structure of tricarbonylbis(methyl isocyanide)iron(0), Fe(C2H3N)2(CO)3

G. W. Harris, J. C. A. Boeyens and N. J. Coville



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Acta Cryst. (1983). C39, 1182-1185    [doi:10.1107/S0108270183007842]

Dimeric methyl(diphenylamino)zinc, C26H26N2Zn2

N. A. Bell, H. M. M. Shearer and C. B. Spencer



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Acta Cryst. (1983). C39, 1186-1188    [doi:10.1107/S0108270183007854]

Bis(2-methylimidazolium) tetrachlorodioxouranate(VI), 2C4H7N2+.UCl4O22-

A. Zalkin, D. Perry, L. Tsao and D. Zhang



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Acta Cryst. (1983). C39, 1188-1190    [doi:10.1107/S0108270183007866]

Structure of dimeric dichlorotetramethyldistannoxane, (C4H12Cl2OSn2)2

R. Graziani, U. Casellato and G. Plazzogna



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Acta Cryst. (1983). C39, 1190-1192    [doi:10.1107/S0108270183007878]

Pseudo-polymeric chain structure of dibromo(1,2-cyclohexanedione dioxime)copper(II), CuBr2(C6H10N2O2)

M. Mégnamisi-Bélombé and H. Endres



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Acta Cryst. (1983). C39, 1192-1194    [doi:10.1107/S010827018300788X]

An unusual chloro bridge in the polymeric chain structure of dichloro(oxamide dioxime)copper(II) phase II, Cu(C2H6N4O2)Cl2

H. Endres



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Acta Cryst. (1983). C39, 1194-1196    [doi:10.1107/S0108270183007891]

Structure of (tert-butyl isocyanide)carbonyl(chloro)bis[dimethyl(phenyl)phosphine]phenylruthenium(II), [Ru(C6H5)(C5H9N)(C8H11P)2(CO)Cl]

Z. Dauter, R. J. Mawby, C. D. Reynolds and D. R. Saunders



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Acta Cryst. (1983). C39, 1197-1200    [doi:10.1107/S0108270183007908]

Reactions of H2Os3(CO)9NMe3 with thiobenzophenone: structures of 1,1,2,2,3,3,3,3-octacarbonyl-1,2;2,3-di-[mu]-hydrido-1,2-[mu]-(mercapto)diphenylethanalato(2-)-[mu]-S:C'-1-thiobenzophenone-triangulo-triosmium, C35H22O9Os3S2, and 1,1,2,2,2,3,3,3,3-nonacarbonyl-1,2-[mu]-diphenylmethylthiolato-1,2-[mu]-hydrido-1-thiobenzophenone-triangulo-triosmium, C35H22O9Os3S2

H. D. Holden, B. F. G. Johnson, J. Lewis, P. R. Raithby and G. Uden



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Acta Cryst. (1983). C39, 1200-1203    [doi:10.1107/S010827018300791X]

Structure of 1,1,1,2,2,2,3,3,3,3-decacarbonyl-1,2-[mu]-diphenylmethylthiolato-1,2-[mu]-hydrido-triangulo-triosmium, C23H12O10Os3S

H. D. Holden, B. F. G. Johnson, J. Lewis, P. R. Raithby and G. Uden



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Acta Cryst. (1983). C39, 1203-1205    [doi:10.1107/S0108270183007921]

Structure of S,S'-trimethylenebis(1,1,1,2,2,2,3,3,3,3-decacarbonyl-1,2-[mu]-hydrido-1,2-[mu]-sulphido-triangulo-triosmium), C23H8O20Os6S2

H. D. Holden, B. F. G. Johnson, J. Lewis, P. R. Raithby and G. Uden



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Acta Cryst. (1983). C39, 1205-1207    [doi:10.1107/S0108270183007933]

The structure of (1,4-dioxane)thallium(I) tetrabromothallate(III), Tl(C4H8O2)+.TlBr4-

S. E. Jeffs, R. W. H. Small and I. J. Worrall



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Acta Cryst. (1983). C39, 1207-1209    [doi:10.1107/S0108270183007945]

catena-Di-[mu]-thiocyanato-N,S-bis(1H-1,2,4-triazole-N4)cadmium, [Cd(C2H3N3)2(NCS)2]; a third structure type of composition M(NCS)2(1,2,4-triazole)2

J. G. Haasnoot, G. C. M. de Keyzer and G. C. Verschoor



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Acta Cryst. (1983). C39, 1210-1211    [doi:10.1107/S0108270183007957]

Structure of ([eta]-cyclotriphosphenyl)[1,1,1-tris(diphenylphosphinomethyl)ethane]nickel(II) triiodide 0.5-acetone solvate, [Ni(C41H39P3)(P3)]I3.0.5C3H6O

M. Di Vaira, M. Peruzzini and P. Stoppioni



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Acta Cryst. (1983). C39, 1212-1214    [doi:10.1107/S0108270183007969]

The structure of the three-dimensional polymer poly[[mu]-hexakis(2-methylimidazolato-N,N')-triiron(II)], [Fe3(C4H5N2)6]n

A. L. Spek, A. J. M. Duisenberg and M. C. Feiters



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Acta Cryst. (1983). C39, 1214-1216    [doi:10.1107/S0108270183007970]

Structure of [1,3-dimethyl-2,4,5,6(1H,3H)-pyrimidinetetrone 5-oximato][1,3-dimethyl-2,4,5,6(1H,3H)-pyrimidinetetrone 5-oxime]silver(I), [Ag(C6H6N3O4)(C6H7N3O4)\]

C. Ruiz-Valero, A. Monge, E. Gutiérrez-Puebla and E. Gutiérrez-Ríos



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Acta Cryst. (1983). C39, 1216-1217    [doi:10.1107/S0108270183007982]

Redetermination of the structure of (isothiocyanato)(2,2',2''-triaminotriethylamine)nickel(II), [Ni(C6H18N4)(NCS)2 ]

B. D. Santarsiero and V. Schomaker



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Acta Cryst. (1983). C39, 1218-1221    [doi:10.1107/S0108270183007994]

Structure of a new modification of bromobis(N,N-diethyldithiocarbamato)iron(III), Fe[S2CN(C2H5)2]2Br

S. Decurtins, C. B. Shoemaker and H. H. Wickman



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Acta Cryst. (1983). C39, 1221-1225    [doi:10.1107/S0108270183008008]

Structure of bis(1,10-phenanthroline)bis(2,4,6-trinitrophenolato)barium(II) acetone (1:1), [Ba(C12H8N2)2(C6H2N3O7)2].C3H6O

R. Postma, J. A. Kanters, A. J. M. Duisenberg, K. Venkatasubramanian and N. S. Poonia



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Acta Cryst. (1983). C39, 1225-1226    [doi:10.1107/S010827018300801X]

Structure of carbonyl-mer-trichloro-trans-bis(triphenylphosphine)iridium(III), C37H30Cl3IrOP2

F. Demartin and N. Masciocchi


organic compounds



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Acta Cryst. (1983). C39, 1227-1230    [doi:10.1107/S0108270183008021]

Grantaline, C18H25NO6, a pyrrolizidine alkaloid

M. F. Mackay and C. C. J. Culvenor



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Acta Cryst. (1983). C39, 1230-1233    [doi:10.1107/S0108270183008033]

Dehydrosenecionine, C18H23NO5: active metabolite of the pyrrolizidine alkaloid senecionine

M. F. Mackay, M. Sadek, C. C. J. Culvenor and L. W. Smith



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Acta Cryst. (1983). C39, 1233-1235    [doi:10.1107/S0108270183008045]

Structure of perylene-chloranil molecular complex (1:1), C20H12.C6Cl4O2

K. Kozawa and T. Uchida



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Acta Cryst. (1983). C39, 1236-1237    [doi:10.1107/S0108270183008057]

Structure of N-methylsulphamic acid, CH5NO3S

A. J. Morris, C. H. L. Kennard, J. R. Hall, G. Smith and A. H. White



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Acta Cryst. (1983). C39, 1238-1239    [doi:10.1107/S0108270183008069]

Structure du thréo-(hydroxy-1 éthyl)-2 dihydro-2,3 benzo[b]thiophènedioxyde-1,1, C10H12O3S

J. Tréhoux, F. Abraham et P. Grandclaudon



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Acta Cryst. (1983). C39, 1240-1241    [doi:10.1107/S0108270183008070]

1-Amino(imino)methyl-2-hydroxypyrrolidine-2-carboxylic acid monohydrate, C6H11N3O3.H2O. A cyclic form of the [alpha]-keto acid derived from arginine

W. H. Watson, J. Galloy, W. Steglich and C. Klein



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Acta Cryst. (1983). C39, 1242-1245    [doi:10.1107/S0108270183008082]

Structure and crystal packing of the organic salt 2-(dimethylamino)-5-methyl-1,3-thiazolium 1,1,2,3,3-pentacyanopropenide, C6H11N2S+.C8N5-

V. Bertolasi and G. Gilli



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Acta Cryst. (1983). C39, 1245-1248    [doi:10.1107/S0108270183008094]

Structure of methyl 10-ethylidicyclohepta[cd,gh]pentalene-5-carboxylate, C20H16O2

C. Kabuto, K. Fujimori, M. Yasunami, K. Takase, N. Morita and T. Asao



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Acta Cryst. (1983). C39, 1248-1253    [doi:10.1107/S0108270183008100]

Structures of two N-bridgehead C-nucleosides: 5,7-dimethyl-3-[beta]-D-ribofuranosyl[1,2,4]triazolo[4,3-a]pyrimidine, C12H16N4O4 (I), and 5,7-dimethyl-2-[beta]-D-ribofuranosyl[1,2,4]triazolo[1,5-a]pyrimidine-methanol, C12H16N4O4.CH4O (II)

B. Kojic-Prodic, Z. Ruzic-Toros and J. Kobe



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Acta Cryst. (1983). C39, 1253-1255    [doi:10.1107/S0108270183008112]

(E)-3-Hexenedinitrile, C6H6N2

W. B. Gleason and D. Britton



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Acta Cryst. (1983). C39, 1255-1257    [doi:10.1107/S0108270183008124]

Structure of N-cyano-N'-methyl-N''-(2-{[(5-methyl-1H-imidazol-4-yl)methyl]thio}ethyl)guanidine (cimetidine) monohydrochloride monohydrate, C10H17N6S+.Cl-.H2O

M. Shibata, M. Kagawa, K. Morisaka, T. Ishida and M. Inoue



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Acta Cryst. (1983). C39, 1257-1259    [doi:10.1107/S0108270183008136]

1,2,-O-Isopropylidene-[alpha]-D-glucofuranurono-6,3-lactone, C9H12O6

B. Sheldrick, W. Mackie and D. Akrigg



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Acta Cryst. (1983). C39, 1259-1261    [doi:10.1107/S0108270183008148]

5-Hydroxy-1,2-O-isopropylidene-[alpha]-D-xylo-hexofuranurono-6,3-lactone, C9H12O7

B. Sheldrick, W. Mackie and D. Akrigg



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Acta Cryst. (1983). C39, 1261-1263    [doi:10.1107/S010827018300815X]

Structure of 9-annulene derivatives. 1. 5,13-Diphenyl-8H-cyclonona[b]naphthalene, C29H22

Mazhar-ul-Haque, J. Ahmed and W. Horne



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Acta Cryst. (1983). C39, 1263-1267    [doi:10.1107/S0108270183008161]

Structure of 2-(2-hydroxy-1,1-dimethylethyl)-5,5-dimethyl-1,3-dioxan-4-ol, C10H20O4, a dimer of 3-hydroxy-2,2-dimethylpropanal. Example of an anhydrous acetal hydrolysis

D. S. Sake Gowda, N. Federlein and R. Rudman



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Acta Cryst. (1983). C39, 1267-1271    [doi:10.1107/S0108270183008173]

Polymorphism of crystalline poly(hydroxymethyl) compounds. VIII. Structures of the tris(hydroxymethyl)aminomethane hydrogenhalides, (HOH2C)3CNH3+.X- (X=F,Cl,Br,I)

R. Rudman, R. Lippman, D. S. Sake Gowda and D. Eilerman



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Acta Cryst. (1983). C39, 1271-1273    [doi:10.1107/S0108270183008185]

DL-Glutamic acid monohydrate, C5H9NO4.H2O

Z. Ciunik and T. Glowiak



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Acta Cryst. (1983). C39, 1273-1275    [doi:10.1107/S0108270183008197]

Quinone oligomerization. IV. Structure of tetraphenyleno[1,16-bcd:4,5-b'c'd':8,9-b''c''d'':12,13-b'''c'''d''']tetrafuran, C24H8O4

B. Karlsson, A.-M. Pilotti and A.-C. Söderholm



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Acta Cryst. (1983). C39, 1275-1277    [doi:10.1107/S0108270183008203]

Quinone oligomerization. V. Structure of benzo[1,2-b:6,5-b']bis[1]benzofuran, C18H10O2

B. Karlsson, A.-M. Pilotti and A.-C. Söderholm



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Acta Cryst. (1983). C39, 1278-1280    [doi:10.1107/S0108270183008215]

Structure of 7-chloro-4-ethyl-2,3,3a,4-tetrahydro-1H-pyrrolo[2,1-c][1,2,4]benzothiadiazine 5,5-dioxide, C12H15ClN2O2S

R. Oberti, M. T. Bernabei, F. Forni, R. Cameroni and E. Galli



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Acta Cryst. (1983). C39, 1280-1282    [doi:10.1107/S0108270183008227]

3',3'',3'''-Phosphinetriyltripropionitrile, C9H12N3P, at 100 K

S. Larsen, P. Vinzents and O. Dahl



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Acta Cryst. (1983). C39, 1282-1284    [doi:10.1107/S0108270183008239]

Structure of syn-9-acetyl-1,6-imino-8,13-methano[14]annulene, C17H15NO

R. Destro, E. Ortoleva and M. Simonetta



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Acta Cryst. (1983). C39, 1285-1287    [doi:10.1107/S0108270183008240]

N-[(Ethyl-1 pyrrolidinyl-2)méthyl] hydroxy-2 sulfamoyl-5 benzamide (un métabolite du sulpiride), C14H21N3O4S

C. Houttemane, J. C. Boivin, D. J. Thomas, P. Berthelot et M. Debaert



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Acta Cryst. (1983). C39, 1287-1291    [doi:10.1107/S0108270183008252]

Structure of bilirubin IX[alpha] (isopropylammonium salt) chloroform solvate, C33H34N4O62-.2C3H10N+.2CHCl3

A. Mugnoli, P. Manitto and D. Monti



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Acta Cryst. (1983). C39, 1291-1294    [doi:10.1107/S0108270183008264]

A rhodinol dye derivative. 2-Chloro-6-(dimethylamino)-9-phenyl-3H-xanthen-3-one methylene chloride solvate, C21H16ClNO2.CH2Cl2

J. A. Potenza, B. H. Toby, G. R. Bird and R. A. Lalancette



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Acta Cryst. (1983). C39, 1294-1297    [doi:10.1107/S0108270183008276]

Structures of 1,3-dicyclohexyl-1-(1H-indol-3-ylacetyl)urea, C23H31N3O2 (I), and 3-cyclohexyl-1-[2-(1H-indol-3-yl)ethyl]urea, C17H23N3O (II)

T. Ishida, M. Yamashita, H. Takai and M. Inoue



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Acta Cryst. (1983). C39, 1297-1300    [doi:10.1107/S0108270183008288]

The structure of acetone diethyl sulfone, C7H16O4S2, at 293 K and at 138 K

M. B. Hossain, D. van der Helm and A. K. Roy



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Acta Cryst. (1983). C39, 1301-1303    [doi:10.1107/S010827018300829X]

Structure of 1,5,6-trimethylbicyclo[2.2.1]hepta-2,5-diene-2,3-dicarbonitrile, C12H12N2

H. Maeda, H. Terauchi, K. Nakatsu, Z.-I. Yoshida, Y. Asako, S. Miki and Y. Yamada



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Acta Cryst. (1983). C39, 1303-1305    [doi:10.1107/S0108270183008306]

Structure of the melampolide sesquiterpene lactone alloschkuhriolide, C15H18O4

U. Rychlewska



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Acta Cryst. (1983). C39, 1306-1309    [doi:10.1107/S0108270183008318]

L'azido-2 désoxy-2 [beta]-D-galactopyrannoside tert-butylique, C10H19N3O5

Y. Oddon, B. Ferrari, E. Guy, A. A. Pavia, J. P. Reboul et G. Pèpe



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Acta Cryst. (1983). C39, 1309-1310    [doi:10.1107/S010827018300832X]

Tétrafluoro-2,3,5,6 benzènediamine-1,4, C6H4F4N2

M. M. Granger, L. Toupet et G. P. Charbonneau



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Acta Cryst. (1983). C39, 1311-1312    [doi:10.1107/S0108270183008331]

Structure et configuration absolue de l'iodométhylate de sébiférine-(9S), C21H26NO4+.I-

A. Chiaroni, C. Riche, F. Roblot, R. Hocquemiller et A. Cavé



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Acta Cryst. (1983). C39, 1313-1315    [doi:10.1107/S0108270183008343]

6-Benzyl-6,10-dimethyl-11-oxatricyclo[5.3.1.05,10]undecan-1-ol, C19H26O2

J. A. Kanters, R. Postma, A. J. M. Duisenberg and K. Venkatasubramanian


short communications



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Acta Cryst. (1983). C39, 1316    [doi:10.1107/S0108270183008355]

Single-crystal refinement of the structure of LaOCl

L. H. Brixner and E. P. Moore


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