Acta Crystallographica Section C

Crystal Structure Communications

Volume 39, Part 9 (September 1983)

• research papers
  • inorganic compounds
  • metal-organic compounds
  • organic compounds
• short communications

research papers

inorganic compounds

Acta Cryst. (1983). C39, 1143-1146    [doi:10.1107/S0108270183007702]

New structure determination of murdochite, Cu₆PbO₈

E. Dubler, A. Vedani and H. R. Oswald

Acta Cryst. (1983). C39, 1146-1150    [doi:10.1107/S0108270183007714]

Room-temperature structure of carbon monoxide at 2.7 and 3.6 GPa

D. T. Cromer, D. Schiferl, R. LeSar and R. L. Mills

Acta Cryst. (1983). C39, 1151-1153    [doi:10.1107/S0108270183007726]

Structure of N₂ at 2.94 GPa and 300 K

D. Schiferl, D. T. Cromer, R. R. Ryan, A. C. Larson, R. LeSar and R. L. Mills

Acta Cryst. (1983). C39, 1153-1156    [doi:10.1107/S0108270183007738]

Synthèse et structure d'un niobate de césium non stoechiométrique, Cs₃Nb_5,96O_16,4

M.-C. Saine et M. Gasperin

Acta Cryst. (1983). C39, 1156-1159    [doi:10.1107/S010827018300774X]

Tricobalt hexasodium hexakis(hexahydroxohexaborate) hexacosahydrate, Na₆Co₃[B₆O₇(OH)₆]₆.26H₂O

H. Behm

Acta Cryst. (1983). C39, 1160-1163    [doi:10.1107/S0108270183007751]

Structures of 20 new polytypes of cadmium iodide

B. Palosz

Acta Cryst. (1983). C39, 1163-1165    [doi:10.1107/S0108270183007763]

Orthorhombic uranium(IV) molybdenum(VI) oxide, UMo₂O₈

T. L. Cremers, P. G. Eller, R. A. Penneman and C. C. Herrick

Acta Cryst. (1983). C39, 1165-1167    [doi:10.1107/S0108270183007775]

Orthorhombic thorium(IV) molybdate, Th(MoO₄)₂

T. L. Cremers, P. G. Eller and R. A. Penneman

Acta Cryst. (1983). C39, 1167-1169    [doi:10.1107/S0108270183007787]

Ammonium trifluoroberyllate(II), (NH₄)[BeF₃], at room temperature

A. Waskowska

Acta Cryst. (1983). C39, 1169-1172    [doi:10.1107/S0108270183007799]

Structure of orthopyroxene-type and clinopyroxene-type magnesium germanium oxide MgGeO₃

M. Ozima

Acta Cryst. (1983). C39, 1173-1174    [doi:10.1107/S0108270183007805]

Disilver(I) decachlorodioxotetraaluminate(III), Ag₂[Al₄Cl₁₀O₂]

D. Jentsch, P. G. Jones, E. Schwarzmann and G. M. Sheldrick

metal-organic compounds

Acta Cryst. (1983). C39, 1175-1177    [doi:10.1107/S0108270183007817]

The structure of Ni(cyclam)I₂.H₂O, [Ni(C₁₀H₂₄N₄)I]I.H₂O

L. Prasad and A. McAuley

Acta Cryst. (1983). C39, 1177-1180    [doi:10.1107/S0108270183007829]

Etude stéréochimique du tricarbonyl[5a-9a--(méthyl-4 tétrahydro-3a,4,5,9b 1H-benz[e]indazolecarboxylate-3a de méthyle)]chrome(III), [Cr(C₁₄H₁₆N₂O₂)(CO)₃\]

R. Mercier, J. Douglade et J. Vebrel

Acta Cryst. (1983). C39, 1180-1182    [doi:10.1107/S0108270183007830]

Structure of tricarbonylbis(methyl isocyanide)iron(0), Fe(C₂H₃N)₂(CO)₃

G. W. Harris, J. C. A. Boeyens and N. J. Coville

Acta Cryst. (1983). C39, 1182-1185    [doi:10.1107/S0108270183007842]

Dimeric methyl(diphenylamino)zinc, C₂₆H₂₆N₂Zn₂

N. A. Bell, H. M. M. Shearer and C. B. Spencer

Acta Cryst. (1983). C39, 1186-1188    [doi:10.1107/S0108270183007854]

Bis(2-methylimidazolium) tetrachlorodioxouranate(VI), 2C₄H₇N₂⁺.UCl₄O₂^2-

A. Zalkin, D. Perry, L. Tsao and D. Zhang

Acta Cryst. (1983). C39, 1188-1190    [doi:10.1107/S0108270183007866]

Structure of dimeric dichlorotetramethyldistannoxane, (C₄H₁₂Cl₂OSn₂)₂

R. Graziani, U. Casellato and G. Plazzogna

Acta Cryst. (1983). C39, 1190-1192    [doi:10.1107/S0108270183007878]

Pseudo-polymeric chain structure of dibromo(1,2-cyclohexanedione dioxime)copper(II), CuBr₂(C₆H₁₀N₂O₂)

M. Mégnamisi-Bélombé and H. Endres

Acta Cryst. (1983). C39, 1192-1194    [doi:10.1107/S010827018300788X]

An unusual chloro bridge in the polymeric chain structure of dichloro(oxamide dioxime)copper(II) phase II, Cu(C₂H₆N₄O₂)Cl₂

H. Endres

Acta Cryst. (1983). C39, 1194-1196    [doi:10.1107/S0108270183007891]

Structure of (tert-butyl isocyanide)carbonyl(chloro)bis[dimethyl(phenyl)phosphine]phenylruthenium(II), [Ru(C₆H₅)(C₅H₉N)(C₈H₁₁P)₂(CO)Cl]

Z. Dauter, R. J. Mawby, C. D. Reynolds and D. R. Saunders

Acta Cryst. (1983). C39, 1197-1200    [doi:10.1107/S0108270183007908]

Reactions of H₂Os₃(CO)₉NMe₃ with thiobenzophenone: structures of 1,1,2,2,3,3,3,3-octacarbonyl-1,2;2,3-di--hydrido-1,2--(mercapto)diphenylethanalato(2-)--S:C'-1-thiobenzophenone-triangulo-triosmium, C₃₅H₂₂O₉Os₃S₂, and 1,1,2,2,2,3,3,3,3-nonacarbonyl-1,2--diphenylmethylthiolato-1,2--hydrido-1-thiobenzophenone-triangulo-triosmium, C₃₅H₂₂O₉Os₃S₂

H. D. Holden, B. F. G. Johnson, J. Lewis, P. R. Raithby and G. Uden

Acta Cryst. (1983). C39, 1200-1203    [doi:10.1107/S010827018300791X]

Structure of 1,1,1,2,2,2,3,3,3,3-decacarbonyl-1,2--diphenylmethylthiolato-1,2--hydrido-triangulo-triosmium, C₂₃H₁₂O₁₀Os₃S

H. D. Holden, B. F. G. Johnson, J. Lewis, P. R. Raithby and G. Uden

Acta Cryst. (1983). C39, 1203-1205    [doi:10.1107/S0108270183007921]

Structure of S,S'-trimethylenebis(1,1,1,2,2,2,3,3,3,3-decacarbonyl-1,2--hydrido-1,2--sulphido-triangulo-triosmium), C₂₃H₈O₂₀Os₆S₂

H. D. Holden, B. F. G. Johnson, J. Lewis, P. R. Raithby and G. Uden

Acta Cryst. (1983). C39, 1205-1207    [doi:10.1107/S0108270183007933]

The structure of (1,4-dioxane)thallium(I) tetrabromothallate(III), Tl(C₄H₈O₂)⁺.TlBr₄^-

S. E. Jeffs, R. W. H. Small and I. J. Worrall

Acta Cryst. (1983). C39, 1207-1209    [doi:10.1107/S0108270183007945]

catena-Di--thiocyanato-N,S-bis(1H-1,2,4-triazole-N⁴)cadmium, [Cd(C₂H₃N₃)₂(NCS)₂]; a third structure type of composition M(NCS)₂(1,2,4-triazole)₂

J. G. Haasnoot, G. C. M. de Keyzer and G. C. Verschoor

Acta Cryst. (1983). C39, 1210-1211    [doi:10.1107/S0108270183007957]

Structure of (-cyclotriphosphenyl)[1,1,1-tris(diphenylphosphinomethyl)ethane]nickel(II) triiodide 0.5-acetone solvate, [Ni(C₄₁H₃₉P₃)(P₃)]I₃.0.5C₃H₆O

M. Di Vaira, M. Peruzzini and P. Stoppioni

Acta Cryst. (1983). C39, 1212-1214    [doi:10.1107/S0108270183007969]

The structure of the three-dimensional polymer poly[-hexakis(2-methylimidazolato-N,N')-triiron(II)], [Fe₃(C₄H₅N₂)₆]_n

A. L. Spek, A. J. M. Duisenberg and M. C. Feiters

Acta Cryst. (1983). C39, 1214-1216    [doi:10.1107/S0108270183007970]

Structure of [1,3-dimethyl-2,4,5,6(1H,3H)-pyrimidinetetrone 5-oximato][1,3-dimethyl-2,4,5,6(1H,3H)-pyrimidinetetrone 5-oxime]silver(I), [Ag(C₆H₆N₃O₄)(C₆H₇N₃O₄)\]

C. Ruiz-Valero, A. Monge, E. Gutiérrez-Puebla and E. Gutiérrez-Ríos

Acta Cryst. (1983). C39, 1216-1217    [doi:10.1107/S0108270183007982]

Redetermination of the structure of (isothiocyanato)(2,2',2''-triaminotriethylamine)nickel(II), [Ni(C₆H₁₈N₄)(NCS)₂ ]

B. D. Santarsiero and V. Schomaker

Acta Cryst. (1983). C39, 1218-1221    [doi:10.1107/S0108270183007994]

Structure of a new modification of bromobis(N,N-diethyldithiocarbamato)iron(III), Fe[S₂CN(C₂H₅)₂]₂Br

S. Decurtins, C. B. Shoemaker and H. H. Wickman

Acta Cryst. (1983). C39, 1221-1225    [doi:10.1107/S0108270183008008]

Structure of bis(1,10-phenanthroline)bis(2,4,6-trinitrophenolato)barium(II) acetone (1:1), [Ba(C₁₂H₈N₂)₂(C₆H₂N₃O₇)₂].C₃H₆O

R. Postma, J. A. Kanters, A. J. M. Duisenberg, K. Venkatasubramanian and N. S. Poonia

Acta Cryst. (1983). C39, 1225-1226    [doi:10.1107/S010827018300801X]

Structure of carbonyl-mer-trichloro-trans-bis(triphenylphosphine)iridium(III), C₃₇H₃₀Cl₃IrOP₂

F. Demartin and N. Masciocchi

organic compounds

Acta Cryst. (1983). C39, 1227-1230    [doi:10.1107/S0108270183008021]

Grantaline, C₁₈H₂₅NO₆, a pyrrolizidine alkaloid

M. F. Mackay and C. C. J. Culvenor

Acta Cryst. (1983). C39, 1230-1233    [doi:10.1107/S0108270183008033]

Dehydrosenecionine, C₁₈H₂₃NO₅: active metabolite of the pyrrolizidine alkaloid senecionine

M. F. Mackay, M. Sadek, C. C. J. Culvenor and L. W. Smith

Acta Cryst. (1983). C39, 1233-1235    [doi:10.1107/S0108270183008045]

Structure of perylene-chloranil molecular complex (1:1), C₂₀H₁₂.C₆Cl₄O₂

K. Kozawa and T. Uchida

Acta Cryst. (1983). C39, 1236-1237    [doi:10.1107/S0108270183008057]

Structure of N-methylsulphamic acid, CH₅NO₃S

A. J. Morris, C. H. L. Kennard, J. R. Hall, G. Smith and A. H. White

Acta Cryst. (1983). C39, 1238-1239    [doi:10.1107/S0108270183008069]

Structure du thréo-(hydroxy-1 éthyl)-2 dihydro-2,3 benzo[b]thiophènedioxyde-1,1, C₁₀H₁₂O₃S

J. Tréhoux, F. Abraham et P. Grandclaudon

Acta Cryst. (1983). C39, 1240-1241    [doi:10.1107/S0108270183008070]

1-Amino(imino)methyl-2-hydroxypyrrolidine-2-carboxylic acid monohydrate, C₆H₁₁N₃O₃.H₂O. A cyclic form of the -keto acid derived from arginine

W. H. Watson, J. Galloy, W. Steglich and C. Klein

Acta Cryst. (1983). C39, 1242-1245    [doi:10.1107/S0108270183008082]

Structure and crystal packing of the organic salt 2-(dimethylamino)-5-methyl-1,3-thiazolium 1,1,2,3,3-pentacyanopropenide, C₆H₁₁N₂S⁺.C₈N₅^-

V. Bertolasi and G. Gilli

Acta Cryst. (1983). C39, 1245-1248    [doi:10.1107/S0108270183008094]

Structure of methyl 10-ethylidicyclohepta[cd,gh]pentalene-5-carboxylate, C₂₀H₁₆O₂

C. Kabuto, K. Fujimori, M. Yasunami, K. Takase, N. Morita and T. Asao

Acta Cryst. (1983). C39, 1248-1253    [doi:10.1107/S0108270183008100]

Structures of two N-bridgehead C-nucleosides: 5,7-dimethyl-3--D-ribofuranosyl[1,2,4]triazolo[4,3-a]pyrimidine, C₁₂H₁₆N₄O₄ (I), and 5,7-dimethyl-2--D-ribofuranosyl[1,2,4]triazolo[1,5-a]pyrimidine-methanol, C₁₂H₁₆N₄O₄.CH₄O (II)

B. Kojic-Prodic, Z. Ruzic-Toros and J. Kobe

Acta Cryst. (1983). C39, 1253-1255    [doi:10.1107/S0108270183008112]

(E)-3-Hexenedinitrile, C₆H₆N₂

W. B. Gleason and D. Britton

Acta Cryst. (1983). C39, 1255-1257    [doi:10.1107/S0108270183008124]

Structure of N-cyano-N'-methyl-N''-(2-{[(5-methyl-1H-imidazol-4-yl)methyl]thio}ethyl)guanidine (cimetidine) monohydrochloride monohydrate, C₁₀H₁₇N₆S⁺.Cl^-.H₂O

M. Shibata, M. Kagawa, K. Morisaka, T. Ishida and M. Inoue

Acta Cryst. (1983). C39, 1257-1259    [doi:10.1107/S0108270183008136]

1,2,-O-Isopropylidene--D-glucofuranurono-6,3-lactone, C₉H₁₂O₆

B. Sheldrick, W. Mackie and D. Akrigg

Acta Cryst. (1983). C39, 1259-1261    [doi:10.1107/S0108270183008148]

5-Hydroxy-1,2-O-isopropylidene--D-xylo-hexofuranurono-6,3-lactone, C₉H₁₂O₇

B. Sheldrick, W. Mackie and D. Akrigg

Acta Cryst. (1983). C39, 1261-1263    [doi:10.1107/S010827018300815X]

Structure of 9-annulene derivatives. 1. 5,13-Diphenyl-8H-cyclonona[b]naphthalene, C₂₉H₂₂

Mazhar-ul-Haque, J. Ahmed and W. Horne

Acta Cryst. (1983). C39, 1263-1267    [doi:10.1107/S0108270183008161]

Structure of 2-(2-hydroxy-1,1-dimethylethyl)-5,5-dimethyl-1,3-dioxan-4-ol, C₁₀H₂₀O₄, a dimer of 3-hydroxy-2,2-dimethylpropanal. Example of an anhydrous acetal hydrolysis

D. S. Sake Gowda, N. Federlein and R. Rudman

Acta Cryst. (1983). C39, 1267-1271    [doi:10.1107/S0108270183008173]

Polymorphism of crystalline poly(hydroxymethyl) compounds. VIII. Structures of the tris(hydroxymethyl)aminomethane hydrogenhalides, (HOH₂C)₃CNH₃⁺.X^- (X=F,Cl,Br,I)

R. Rudman, R. Lippman, D. S. Sake Gowda and D. Eilerman

Acta Cryst. (1983). C39, 1271-1273    [doi:10.1107/S0108270183008185]

DL-Glutamic acid monohydrate, C₅H₉NO₄.H₂O

Z. Ciunik and T. Glowiak

Acta Cryst. (1983). C39, 1273-1275    [doi:10.1107/S0108270183008197]

Quinone oligomerization. IV. Structure of tetraphenyleno[1,16-bcd:4,5-b'c'd':8,9-b''c''d'':12,13-b'''c'''d''']tetrafuran, C₂₄H₈O₄

B. Karlsson, A.-M. Pilotti and A.-C. Söderholm

Acta Cryst. (1983). C39, 1275-1277    [doi:10.1107/S0108270183008203]

Quinone oligomerization. V. Structure of benzo[1,2-b:6,5-b']bis[1]benzofuran, C₁₈H₁₀O₂

B. Karlsson, A.-M. Pilotti and A.-C. Söderholm

Acta Cryst. (1983). C39, 1278-1280    [doi:10.1107/S0108270183008215]

Structure of 7-chloro-4-ethyl-2,3,3a,4-tetrahydro-1H-pyrrolo[2,1-c][1,2,4]benzothiadiazine 5,5-dioxide, C₁₂H₁₅ClN₂O₂S

R. Oberti, M. T. Bernabei, F. Forni, R. Cameroni and E. Galli

Acta Cryst. (1983). C39, 1280-1282    [doi:10.1107/S0108270183008227]

3',3'',3'''-Phosphinetriyltripropionitrile, C₉H₁₂N₃P, at 100 K

S. Larsen, P. Vinzents and O. Dahl

Acta Cryst. (1983). C39, 1282-1284    [doi:10.1107/S0108270183008239]

Structure of syn-9-acetyl-1,6-imino-8,13-methano[14]annulene, C₁₇H₁₅NO

R. Destro, E. Ortoleva and M. Simonetta

Acta Cryst. (1983). C39, 1285-1287    [doi:10.1107/S0108270183008240]

N-[(Ethyl-1 pyrrolidinyl-2)méthyl] hydroxy-2 sulfamoyl-5 benzamide (un métabolite du sulpiride), C₁₄H₂₁N₃O₄S

C. Houttemane, J. C. Boivin, D. J. Thomas, P. Berthelot et M. Debaert

Acta Cryst. (1983). C39, 1287-1291    [doi:10.1107/S0108270183008252]

Structure of bilirubin IX (isopropylammonium salt) chloroform solvate, C₃₃H₃₄N₄O₆^2-.2C₃H₁₀N⁺.2CHCl₃

A. Mugnoli, P. Manitto and D. Monti

Acta Cryst. (1983). C39, 1291-1294    [doi:10.1107/S0108270183008264]

A rhodinol dye derivative. 2-Chloro-6-(dimethylamino)-9-phenyl-3H-xanthen-3-one methylene chloride solvate, C₂₁H₁₆ClNO₂.CH₂Cl₂

J. A. Potenza, B. H. Toby, G. R. Bird and R. A. Lalancette

Acta Cryst. (1983). C39, 1294-1297    [doi:10.1107/S0108270183008276]

Structures of 1,3-dicyclohexyl-1-(1H-indol-3-ylacetyl)urea, C₂₃H₃₁N₃O₂ (I), and 3-cyclohexyl-1-[2-(1H-indol-3-yl)ethyl]urea, C₁₇H₂₃N₃O (II)

T. Ishida, M. Yamashita, H. Takai and M. Inoue

Acta Cryst. (1983). C39, 1297-1300    [doi:10.1107/S0108270183008288]

The structure of acetone diethyl sulfone, C₇H₁₆O₄S₂, at 293 K and at 138 K

M. B. Hossain, D. van der Helm and A. K. Roy

Acta Cryst. (1983). C39, 1301-1303    [doi:10.1107/S010827018300829X]

Structure of 1,5,6-trimethylbicyclo[2.2.1]hepta-2,5-diene-2,3-dicarbonitrile, C₁₂H₁₂N₂

H. Maeda, H. Terauchi, K. Nakatsu, Z.-I. Yoshida, Y. Asako, S. Miki and Y. Yamada

Acta Cryst. (1983). C39, 1303-1305    [doi:10.1107/S0108270183008306]

Structure of the melampolide sesquiterpene lactone alloschkuhriolide, C₁₅H₁₈O₄

U. Rychlewska

Acta Cryst. (1983). C39, 1306-1309    [doi:10.1107/S0108270183008318]

L'azido-2 désoxy-2 -D-galactopyrannoside tert-butylique, C₁₀H₁₉N₃O₅

Y. Oddon, B. Ferrari, E. Guy, A. A. Pavia, J. P. Reboul et G. Pèpe

Acta Cryst. (1983). C39, 1309-1310    [doi:10.1107/S010827018300832X]

Tétrafluoro-2,3,5,6 benzènediamine-1,4, C₆H₄F₄N₂

M. M. Granger, L. Toupet et G. P. Charbonneau

Acta Cryst. (1983). C39, 1311-1312    [doi:10.1107/S0108270183008331]

Structure et configuration absolue de l'iodométhylate de sébiférine-(9S), C₂₁H₂₆NO₄⁺.I^-

A. Chiaroni, C. Riche, F. Roblot, R. Hocquemiller et A. Cavé

Acta Cryst. (1983). C39, 1313-1315    [doi:10.1107/S0108270183008343]

6-Benzyl-6,10-dimethyl-11-oxatricyclo[5.3.1.0^5,10]undecan-1-ol, C₁₉H₂₆O₂

J. A. Kanters, R. Postma, A. J. M. Duisenberg and K. Venkatasubramanian

short communications

Acta Cryst. (1983). C39, 1316    [doi:10.1107/S0108270183008355]

Single-crystal refinement of the structure of LaOCl

L. H. Brixner and E. P. Moore

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