Acta Crystallographica Section C

Crystal Structure Communications

Volume 40, Part 4 (April 1984)



research papers


inorganic compounds



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Acta Cryst. (1984). C40, 573-576    [doi:10.1107/S0108270184004935]

Two new members of a series of monoclinic sodium phosphate tungsten bronzes NaxP4O8(WO3)2m: NaxP4W8O32 (m = 4) and NaxP4W12O44 (m = 6)

A. Benmoussa, D. Groult, Ph. Labbé and B. Raveau



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Acta Cryst. (1984). C40, 576-579    [doi:10.1107/S0108270184004947]

The structure of the [kappa] phase, Mn5Ge2

T. Ohba, K. Ueyama, Y. Kitano and Y. Komura



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Acta Cryst. (1984). C40, 580-581    [doi:10.1107/S0108270184004959]

A redetermination of the structure of strontium chloride hexahydrate, SrCl2.6H2O

R. B. English and L. R. Nassimbeni



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Acta Cryst. (1984). C40, 581-584    [doi:10.1107/S0108270184004960]

Structure determination of diantimony tritin hexasulphide, Sn3Sb2S6, by high-resolution transmission electron microscopy

P. P. K. Smith



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Acta Cryst. (1984). C40, 584-586    [doi:10.1107/S0108270184004972]

Neutron diffraction refinement of magnesium sulfite hexahydrate, MgSO3.6H2O

L. Andersen and O. Lindqvist



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Acta Cryst. (1984). C40, 586-589    [doi:10.1107/S0108270184004984]

The structures of magnesium tellurate(IV) hexahydrate, MgTeO3.6H2O, and magnesium selenate(IV) hexahydrate, MgSeO3.6H2O

L. Andersen, O. Lindqvist and J. Moret


metal-organic compounds



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Acta Cryst. (1984). C40, 590-592    [doi:10.1107/S0108270184004996]

Structure of iodo(methylene)tetrakis(trimethylphosphine)tungsten trifluoromethanesulfonate, [WI(CH2){P(CH3)3}4][CF3SO3]

A. J. Schultz, J. M. Williams, R. R. Schrock and S. J. Holmes



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Acta Cryst. (1984). C40, 592-597    [doi:10.1107/S010827018400500X]

The structures of 1,4,7,14,23-pentaoxa[7]orthobenzeno[2](2,6)pyridino[2]orthobenzenophane ('dibenzopyridino-18-crown-6') in its hydrated ethanol inclusion compound (1), C23H23NO5.CH3CH2OH.0.12H2O, and its sodium isothiocyanate complex (2), C23H23NO5.NaNCS

G. Weber



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Acta Cryst. (1984). C40, 598-600    [doi:10.1107/S0108270184005011]

Electronic structural effects in the structure of trichloro([eta]5-ethyltetramethylcyclopentadienyl)titanium(IV), Ti(C11H17)Cl3

N. W. Alcock, G. E. Toogood and M. G. H. Wallbridge



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Acta Cryst. (1984). C40, 600-602    [doi:10.1107/S0108270184005023]

Octacarbonyl-bis([mu]-{iodo[tetracarbonyl(triphenylphosphine)rhenio]stannio(IV)})dirhenium, [Re2(CO)8{Sn(I)Re(CO)4[P(C6H5)3]}2]

H. Preut, H.-J. Haupt and U. Flörke



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Acta Cryst. (1984). C40, 602-604    [doi:10.1107/S0108270184005035]

Dimeric tert-butoxymagnesium bromide-diethyl ether adduct, [Mg2Br2(C4H9O)2(C4H10O)2]: the addition product of a Grignard reagent with acetone

N. A. Bell, P. T. Moseley and H. M. M. Shearer



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Acta Cryst. (1984). C40, 605-607    [doi:10.1107/S0108270184005047]

Dimeric tert-butoxyberyllium bromide-diethyl ether adduct, [Be2Br2(C4H9O)2(C4H10O)2], and a comparison with the magnesium analogue

N. A. Bell, H. M. M. Shearer and J. Twiss



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Acta Cryst. (1984). C40, 608-610    [doi:10.1107/S0108270184005059]

Terminal beryllium-hydrogen bonding in dimeric (2-dimethylamino-N-methylethylamido)hydridoberyllium, [Be2(C5H13N2)2H2]

N. A. Bell, G. E. Coates, M. L. Schneider and H. M. M. Shearer



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Acta Cryst. (1984). C40, 610-613    [doi:10.1107/S0108270184005060]

[pi]-Bonding around three-coordinate beryllium in tetra-[mu]-tert-butoxodichlorotriberyllium, [Be3Cl2(C4H9O)4]

N. A. Bell, H. M. M. Shearer and J. Twiss



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Acta Cryst. (1984). C40, 613-616    [doi:10.1107/S0108270184005072]

Tetrameric methylzinc acetoximate, [Zn4(CH3)4(C3H6NO)4]

N. A. Bell, H. M. M. Shearer and C. B. Spencer



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Acta Cryst. (1984). C40, 616-618    [doi:10.1107/S0108270184005084]

Aquadichloro-[mu]-[3,6-di(2-pyridyl)pyridazine-N,N',N'',N''']-[mu]-hydroxo-nitrato-O-dicopper(II) dichloro-[mu]-[3,6-di(2-pyridyl)pyridazine-N,N',N'',N''']-[mu]-hydroxo-[mu]-nitrato-O,O'-dicopper(II) sesquihydrate, {[Cu2Cl2(OH)(NO3)(C14H10N4)(H2O)][Cu2Cl2(OH)(NO3)(C14H10N4)]}.1.5H2O

G. De Munno and G. Denti



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Acta Cryst. (1984). C40, 619-620    [doi:10.1107/S0108270184005096]

Structure of (dithiopivalato)(trithioperoxypivalato)platinum(II), [Pt(C5H9S2)(C5H9S3)]

E. Agostinelli, C. Bellitto, G. Dessy, V. Fares and A. Flamini



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Acta Cryst. (1984). C40, 620-622    [doi:10.1107/S0108270184005102]

trans-(Acetylacetonato)dichloro(1,5-cyclooctadiene)iridium(III), [IrCl2(C5H7O2)(C8H12)]

P. A. Tucker



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Acta Cryst. (1984). C40, 623-625    [doi:10.1107/S0108270184005114]

Nickel-germanium bonding in ([eta]5-cyclopentadienyl)(trichlorogermyl)(triphenylphosphine)nickel(II) hemibenzene solvate, C23H20Cl3GeNiP.1/2C6H6

N. A. Bell, F. Glockling, A. McGregor, M. L. Schneider and H. M. M. Shearer



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Acta Cryst. (1984). C40, 625-628    [doi:10.1107/S0108270184005126]

Carbonyldihydrido(trimethylgermyl)bis(triphenylphosphine)iridium(III) hemibenzene solvate, C40H41GeIrOP2.1/2C6H6

N. A. Bell, F. Glockling, M. L. Schneider, H. M. M. Shearer and M. D. Wilbey



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Acta Cryst. (1984). C40, 628-630    [doi:10.1107/S0108270184005138]

Bis(morpholine)aluminium trichloride, [Al(C4H9NO)2]Cl3

G. Müller and C. Krüger



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Acta Cryst. (1984). C40, 631-635    [doi:10.1107/S010827018400514X]

The structure of helices of rubidium deoxycholate-water (3/10), 3(Rb+.C24H39O4-).10H2O

A. R. Campanelli, S. Candeloro De Sanctis, E. Giglio and S. Petriconi



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Acta Cryst. (1984). C40, 635-638    [doi:10.1107/S0108270184005151]

Crystal structures of ethylenediaminetetraacetato metal complexes. V. Structures containing the [Fe(C10H12N2O8)(H2O)]- anion

X. Solans, M. Font Altaba and J. Garcia-Oricain



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Acta Cryst. (1984). C40, 639-641    [doi:10.1107/S0108270184005163]

Structure of dichloro(3-methylsulfinylpropylamine)platinum(II), [PtCl2(C4H11NOS)]

G. R. Champion, L. G. Marzilli, J. P. Hutchinson, K. Gebreyes and J. Zubieta



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Acta Cryst. (1984). C40, 641-644    [doi:10.1107/S0108270184005175]

Structure of the blue copper(II) complex {[7R(S),14R(S)]-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane}nitratocopper(II) perchlorate, [Cu(NO3)(C16H36N4)](ClO4)

T.-J. Lee, H. Y. J. Lee, C.-S. Lee and C.-S. Chung


organic compounds



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Acta Cryst. (1984). C40, 645-647    [doi:10.1107/S0108270184005187]

Conformational aspects of meso-tartaric acid. VI. Structure of (-)-[alpha]-methylbenzylammonium hydrogen meso-tartrate, C8H12N+.C4H5O6-

J. Kroon, A. J. M. Duisenberg and A. F. Peerdeman



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Acta Cryst. (1984). C40, 647-650    [doi:10.1107/S0108270184005199]

Structure of DL-selenomethionine, C5H11NO2Se

M. Rajeswaran and R. Parthasarathy



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Acta Cryst. (1984). C40, 650-653    [doi:10.1107/S0108270184005205]

Structure of 2,4-diamino-5-(3,4,5-trimethoxybenzyl)pyrimidinium benzoate (trimethoprim monobenzoate), C14H19N4O3+.C7H5O2-

G. Giuseppetti, C. Tadini, G. P. Bettinetti, F. Giordano and A. La Manna



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Acta Cryst. (1984). C40, 653-655    [doi:10.1107/S0108270184005217]

1,2,5-Telluradiazole, C2H2N2Te

V. Bertini, P. Dapporto, F. Lucchesini, A. Sega and A. De Munno



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Acta Cryst. (1984). C40, 655-657    [doi:10.1107/S0108270184005229]

Structure of 4-amino-N-(4,6-dimethyl-2-pyrimidinyl)benzenesulphonamide (sulfadimidine), C12H14N4O2S

R. K. Tiwari, M. Haridas and T. P. Singh



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Acta Cryst. (1984). C40, 658-660    [doi:10.1107/S0108270184005230]

Structure of 4-amino-N-(4,5-dimethyl-2-oxazolyl)benzenesulphonamide (sulfamoxole), C11H13N3O3S

M. Haridas, R. K. Tiwari and T. P. Singh



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Acta Cryst. (1984). C40, 660-663    [doi:10.1107/S0108270184005242]

Radioprotectant bis(2-guanidinoethyl) disulfide dihydrobromide, C6H18N6S22+.2Br-

T. Ishida, M. Inoue, K. Kitamura, A. Wakahara, K.-i. Tomita and M. Shinoda



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Acta Cryst. (1984). C40, 663-666    [doi:10.1107/S0108270184005254]

The monoclinic structure of tetracyanoethylene (TCNE), C6N4, at 5,150 and 295 K; powder diffraction analysis

S. L. Chaplot, A. Mierzejewski and G. S. Pawley



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Acta Cryst. (1984). C40, 666-671    [doi:10.1107/S0108270184005266]

Inclusion behavior of 2-hydroxy-3,5-dinitro-N'-(5-nitrofurfurylidene)benzohydrazide, C12H7N5O9. Crystal structures with acetonitrile and acetic acid

I. Goldberg and Z. Stein



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Acta Cryst. (1984). C40, 671-674    [doi:10.1107/S0108270184005278]

Structure of 2,2'-bis(4-chlorophenyl)-5,5'-dimethyl-[3,3'-bi-1,3-thiazolidine]-4,4'-dione, C20H18Cl2N2O2S2

G. Bruno, G. Bombieri, A. Del Pra, T. Previtera, M. G. Vigorita and M. Basile



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Acta Cryst. (1984). C40, 674-676    [doi:10.1107/S010827018400528X]

Structure of 1,3,5,7-tetranitroadamantane, C10H12N4O8

C. George and R. Gilardi



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Acta Cryst. (1984). C40, 676-679    [doi:10.1107/S0108270184005291]

Structure of a novel and reproducible polymorph (Z) of the histamine H2-receptor antagonist cimetidine, C10H16N6S

L. Párkányi, A. Kálmán, B. Hegedüs, K. Harsányi and J. Kreidl



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Acta Cryst. (1984). C40, 679-683    [doi:10.1107/S0108270184005308]

Stereochemical studies of oligomers. IX. Structures of 1,4-butanediyl bis[o(m- and p-)chlorobenzoates] (BDDO, BDDM and BDDP), C18H16Cl2O4

G. Bocelli and M. F. Grenier-Loustalot



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Acta Cryst. (1984). C40, 683-685    [doi:10.1107/S010827018400531X]

The structure of the five-membered cyclic sultone 9,10-dihydro-10a-methyl-3a,9-methano-3H-benzo[5,6]cyclohept[1,2-d][1,2]oxathiol-4(3aH)-one dioxide, C14H14O4S

D. S. Brown, H. Heaney and K. G. Mason



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Acta Cryst. (1984). C40, 685-687    [doi:10.1107/S0108270184005321]

4-Hydroxy-4-phenylpentanamide, C11H15NO2, a moderately active anticonvulsant

J. Zukerman-Schpector, E. E. Castellano, G. Oliva and G. Carvajal



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Acta Cryst. (1984). C40, 687-690    [doi:10.1107/S0108270184005333]

The structures of 3-allyl-9-benzoyl-2-methyl-9-phenyl-4,9-dihydropyrazolo[5,1-b]quinazoline, C27H23N3O, and 6,7-dimethyl-1,3,3-triphenyl-1H-imidazo[1,2-b]pyrazol-2(3H)-one, C25H21N3O

A. L. Rheingold, W. C. Fultz, E. E. Schweizer and K. J. Lee



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Acta Cryst. (1984). C40, 691-693    [doi:10.1107/S0108270184005345]

Structures of (1R*,2R*,3aS*,5S*,6S*,7aS*)- and (±)-(1R*,2S*,3aS*,5R*,6S*,7aS*)-perhydro-1,2,5,6-indenetetrol, (I) and (II), C9H16O4

Y. Matoba, Y. Ishii, M. Ogawa, H. Nakai and M. Shiro



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Acta Cryst. (1984). C40, 693-696    [doi:10.1107/S0108270184005357]

Détermination structurale à 213 K du monomère bis(phénylcarbamate) de hexadiyne-2,4 diyle-1,6, C20H16N2O4

A. Whuler, P. Spinat et C. Brouty



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Acta Cryst. (1984). C40, 696-700    [doi:10.1107/S0108270184005369]

Low-temperature (173 K) structure of the 'strapped' porphyrin: 2,12-diethyl-3,7,13,17-tetramethyl-8,18-nonamethylene-21H,23H-porphyrin methanol solvate, C37H46N4.2CH4O

F. W. B. Einstein and T. Jones



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Acta Cryst. (1984). C40, 700-703    [doi:10.1107/S0108270184005370]

Structure of salbomycin, C54H88O18.2H2O

E. F. Paulus, L. Vertesy and G. M. Sheldrick



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Acta Cryst. (1984). C40, 703-706    [doi:10.1107/S0108270184005382]

Structure of a Favorskii substitution product, 3[beta]-acetoxy-17[beta]-hydroxy-18-nor-5[alpha],17[alpha]-pregnan-20-one, C22H34O4

C. P. Huber and F. R. Ahmed



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Acta Cryst. (1984). C40, 706-708    [doi:10.1107/S0108270184005394]

Structure of 2-(2-hydroxy-3-{[2-(1H-indol-3-yl)-1,1-dimethylethyl]amino}propoxy)benzonitrile: MJ-13,105-1 (bucindolol), C22H25N3O2

J.-M. Léger, M. Goursolle and A. Carpy



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Acta Cryst. (1984). C40, 709-712    [doi:10.1107/S0108270184005400]

1-(2-Fluoro-2-phenylethyl)piperidine hydrochloride, C13H18FN.HCl: enantiomer and racemic solid-solution structures

B. Chion, J. Lajzérowicz, C. Charlon, D. Le Bars and Cuong Luu Duc


short communications



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Acta Cryst. (1984). C40, 712    [doi:10.1107/S0108270184005412]

Structure of 8,5'-anhydro-8-hydroxy-9-[beta]-D-ribofuranosyladenine (8,5'-O-cyclo-A) monohydrate: corrigendum

R. E. Marsh



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Acta Cryst. (1984). C40, 712-713    [doi:10.1107/S0108270184005424]

Structure of 8,5'-anhydro-8-hydroxy-9-[beta]-D-ribofuranosyladenine (8,5'-O-cyclo-A) monohydrate, C10H11N5O4.H2O: errata

S. Sugio, H. Mizuno, K. Kitamura, K. Hamada, M. Ikehara and K.-i. Tomita


addenda and errata



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Acta Cryst. (1984). C40, 714    [doi:10.1107/S0108270184005436]

The structure of transoid-(1RS,3SR,6RS,9RS)-7-hydroxyimino-9-methyl-1-(2-methylpropyl)tricyclo[4.2.1.03,9]nonan-8-one, C14H21NO2: erratum

G. E. Freeman, D. C. Fisher and S.-H. Kong



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Acta Cryst. (1984). C40, 714    [doi:10.1107/S0108270184005448]

Structure of DL-normetanephrine hydrochloride [[alpha]-(aminomethyl)vanillyl alcohol hydrochloride], C9H14NO3+.Cl-: erratum

R. R. Pattanayek, J. K. Dattagupta, S. C. Bhattacharyya and N. N. Saha


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