Acta Crystallographica Section C

Crystal Structure Communications

Volume 40, Part 4 (April 1984)

• research papers
  • inorganic compounds
  • metal-organic compounds
  • organic compounds
• short communications
• addenda and errata

research papers

inorganic compounds

Acta Cryst. (1984). C40, 573-576    [doi:10.1107/S0108270184004935]

Two new members of a series of monoclinic sodium phosphate tungsten bronzes Na_xP₄O₈(WO₃)_2m: Na_xP₄W₈O₃₂ (m = 4) and Na_xP₄W₁₂O₄₄ (m = 6)

A. Benmoussa, D. Groult, Ph. Labbé and B. Raveau

Acta Cryst. (1984). C40, 576-579    [doi:10.1107/S0108270184004947]

The structure of the phase, Mn₅Ge₂

T. Ohba, K. Ueyama, Y. Kitano and Y. Komura

Acta Cryst. (1984). C40, 580-581    [doi:10.1107/S0108270184004959]

A redetermination of the structure of strontium chloride hexahydrate, SrCl₂.6H₂O

R. B. English and L. R. Nassimbeni

Acta Cryst. (1984). C40, 581-584    [doi:10.1107/S0108270184004960]

Structure determination of diantimony tritin hexasulphide, Sn₃Sb₂S₆, by high-resolution transmission electron microscopy

P. P. K. Smith

Acta Cryst. (1984). C40, 584-586    [doi:10.1107/S0108270184004972]

Neutron diffraction refinement of magnesium sulfite hexahydrate, MgSO₃.6H₂O

L. Andersen and O. Lindqvist

Acta Cryst. (1984). C40, 586-589    [doi:10.1107/S0108270184004984]

The structures of magnesium tellurate(IV) hexahydrate, MgTeO₃.6H₂O, and magnesium selenate(IV) hexahydrate, MgSeO₃.6H₂O

L. Andersen, O. Lindqvist and J. Moret

metal-organic compounds

Acta Cryst. (1984). C40, 590-592    [doi:10.1107/S0108270184004996]

Structure of iodo(methylene)tetrakis(trimethylphosphine)tungsten trifluoromethanesulfonate, [WI(CH₂){P(CH₃)₃}₄][CF₃SO₃]

A. J. Schultz, J. M. Williams, R. R. Schrock and S. J. Holmes

Acta Cryst. (1984). C40, 592-597    [doi:10.1107/S010827018400500X]

The structures of 1,4,7,14,23-pentaoxa[7]orthobenzeno[2](2,6)pyridino[2]orthobenzenophane ('dibenzopyridino-18-crown-6') in its hydrated ethanol inclusion compound (1), C₂₃H₂₃NO₅.CH₃CH₂OH.0.12H₂O, and its sodium isothiocyanate complex (2), C₂₃H₂₃NO₅.NaNCS

G. Weber

Acta Cryst. (1984). C40, 598-600    [doi:10.1107/S0108270184005011]

Electronic structural effects in the structure of trichloro(⁵-ethyltetramethylcyclopentadienyl)titanium(IV), Ti(C₁₁H₁₇)Cl₃

N. W. Alcock, G. E. Toogood and M. G. H. Wallbridge

Acta Cryst. (1984). C40, 600-602    [doi:10.1107/S0108270184005023]

Octacarbonyl-bis(-{iodo[tetracarbonyl(triphenylphosphine)rhenio]stannio(IV)})dirhenium, [Re₂(CO)₈{Sn(I)Re(CO)₄[P(C₆H₅)₃]}₂]

H. Preut, H.-J. Haupt and U. Flörke

Acta Cryst. (1984). C40, 602-604    [doi:10.1107/S0108270184005035]

Dimeric tert-butoxymagnesium bromide-diethyl ether adduct, [Mg₂Br₂(C₄H₉O)₂(C₄H₁₀O)₂]: the addition product of a Grignard reagent with acetone

N. A. Bell, P. T. Moseley and H. M. M. Shearer

Acta Cryst. (1984). C40, 605-607    [doi:10.1107/S0108270184005047]

Dimeric tert-butoxyberyllium bromide-diethyl ether adduct, [Be₂Br₂(C₄H₉O)₂(C₄H₁₀O)₂], and a comparison with the magnesium analogue

N. A. Bell, H. M. M. Shearer and J. Twiss

Acta Cryst. (1984). C40, 608-610    [doi:10.1107/S0108270184005059]

Terminal beryllium-hydrogen bonding in dimeric (2-dimethylamino-N-methylethylamido)hydridoberyllium, [Be₂(C₅H₁₃N₂)₂H₂]

N. A. Bell, G. E. Coates, M. L. Schneider and H. M. M. Shearer

Acta Cryst. (1984). C40, 610-613    [doi:10.1107/S0108270184005060]

-Bonding around three-coordinate beryllium in tetra--tert-butoxodichlorotriberyllium, [Be₃Cl₂(C₄H₉O)₄]

N. A. Bell, H. M. M. Shearer and J. Twiss

Acta Cryst. (1984). C40, 613-616    [doi:10.1107/S0108270184005072]

Tetrameric methylzinc acetoximate, [Zn₄(CH₃)₄(C₃H₆NO)₄]

N. A. Bell, H. M. M. Shearer and C. B. Spencer

Acta Cryst. (1984). C40, 616-618    [doi:10.1107/S0108270184005084]

Aquadichloro--[3,6-di(2-pyridyl)pyridazine-N,N',N'',N''']--hydroxo-nitrato-O-dicopper(II) dichloro--[3,6-di(2-pyridyl)pyridazine-N,N',N'',N''']--hydroxo--nitrato-O,O'-dicopper(II) sesquihydrate, {[Cu₂Cl₂(OH)(NO₃)(C₁₄H₁₀N₄)(H₂O)][Cu₂Cl₂(OH)(NO₃)(C₁₄H₁₀N₄)]}.1.5H₂O

G. De Munno and G. Denti

Acta Cryst. (1984). C40, 619-620    [doi:10.1107/S0108270184005096]

Structure of (dithiopivalato)(trithioperoxypivalato)platinum(II), [Pt(C₅H₉S₂)(C₅H₉S₃)]

E. Agostinelli, C. Bellitto, G. Dessy, V. Fares and A. Flamini

Acta Cryst. (1984). C40, 620-622    [doi:10.1107/S0108270184005102]

trans-(Acetylacetonato)dichloro(1,5-cyclooctadiene)iridium(III), [IrCl₂(C₅H₇O₂)(C₈H₁₂)]

P. A. Tucker

Acta Cryst. (1984). C40, 623-625    [doi:10.1107/S0108270184005114]

Nickel-germanium bonding in (⁵-cyclopentadienyl)(trichlorogermyl)(triphenylphosphine)nickel(II) hemibenzene solvate, C₂₃H₂₀Cl₃GeNiP.1/2C₆H₆

N. A. Bell, F. Glockling, A. McGregor, M. L. Schneider and H. M. M. Shearer

Acta Cryst. (1984). C40, 625-628    [doi:10.1107/S0108270184005126]

Carbonyldihydrido(trimethylgermyl)bis(triphenylphosphine)iridium(III) hemibenzene solvate, C₄₀H₄₁GeIrOP₂.1/2C₆H₆

N. A. Bell, F. Glockling, M. L. Schneider, H. M. M. Shearer and M. D. Wilbey

Acta Cryst. (1984). C40, 628-630    [doi:10.1107/S0108270184005138]

Bis(morpholine)aluminium trichloride, [Al(C₄H₉NO)₂]Cl₃

G. Müller and C. Krüger

Acta Cryst. (1984). C40, 631-635    [doi:10.1107/S010827018400514X]

The structure of helices of rubidium deoxycholate-water (3/10), 3(Rb⁺.C₂₄H₃₉O₄^-).10H₂O

A. R. Campanelli, S. Candeloro De Sanctis, E. Giglio and S. Petriconi

Acta Cryst. (1984). C40, 635-638    [doi:10.1107/S0108270184005151]

Crystal structures of ethylenediaminetetraacetato metal complexes. V. Structures containing the [Fe(C₁₀H₁₂N₂O₈)(H₂O)]^- anion

X. Solans, M. Font Altaba and J. Garcia-Oricain

Acta Cryst. (1984). C40, 639-641    [doi:10.1107/S0108270184005163]

Structure of dichloro(3-methylsulfinylpropylamine)platinum(II), [PtCl₂(C₄H₁₁NOS)]

G. R. Champion, L. G. Marzilli, J. P. Hutchinson, K. Gebreyes and J. Zubieta

Acta Cryst. (1984). C40, 641-644    [doi:10.1107/S0108270184005175]

Structure of the blue copper(II) complex {[7R(S),14R(S)]-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane}nitratocopper(II) perchlorate, [Cu(NO₃)(C₁₆H₃₆N₄)](ClO₄)

T.-J. Lee, H. Y. J. Lee, C.-S. Lee and C.-S. Chung

organic compounds

Acta Cryst. (1984). C40, 645-647    [doi:10.1107/S0108270184005187]

Conformational aspects of meso-tartaric acid. VI. Structure of (-)--methylbenzylammonium hydrogen meso-tartrate, C₈H₁₂N⁺.C₄H₅O₆^-

J. Kroon, A. J. M. Duisenberg and A. F. Peerdeman

Acta Cryst. (1984). C40, 647-650    [doi:10.1107/S0108270184005199]

Structure of DL-selenomethionine, C₅H₁₁NO₂Se

M. Rajeswaran and R. Parthasarathy

Acta Cryst. (1984). C40, 650-653    [doi:10.1107/S0108270184005205]

Structure of 2,4-diamino-5-(3,4,5-trimethoxybenzyl)pyrimidinium benzoate (trimethoprim monobenzoate), C₁₄H₁₉N₄O₃⁺.C₇H₅O₂^-

G. Giuseppetti, C. Tadini, G. P. Bettinetti, F. Giordano and A. La Manna

Acta Cryst. (1984). C40, 653-655    [doi:10.1107/S0108270184005217]

1,2,5-Telluradiazole, C₂H₂N₂Te

V. Bertini, P. Dapporto, F. Lucchesini, A. Sega and A. De Munno

Acta Cryst. (1984). C40, 655-657    [doi:10.1107/S0108270184005229]

Structure of 4-amino-N-(4,6-dimethyl-2-pyrimidinyl)benzenesulphonamide (sulfadimidine), C₁₂H₁₄N₄O₂S

R. K. Tiwari, M. Haridas and T. P. Singh

Acta Cryst. (1984). C40, 658-660    [doi:10.1107/S0108270184005230]

Structure of 4-amino-N-(4,5-dimethyl-2-oxazolyl)benzenesulphonamide (sulfamoxole), C₁₁H₁₃N₃O₃S

M. Haridas, R. K. Tiwari and T. P. Singh

Acta Cryst. (1984). C40, 660-663    [doi:10.1107/S0108270184005242]

Radioprotectant bis(2-guanidinoethyl) disulfide dihydrobromide, C₆H₁₈N₆S₂²⁺.2Br^-

T. Ishida, M. Inoue, K. Kitamura, A. Wakahara, K.-i. Tomita and M. Shinoda

Acta Cryst. (1984). C40, 663-666    [doi:10.1107/S0108270184005254]

The monoclinic structure of tetracyanoethylene (TCNE), C₆N₄, at 5,150 and 295 K; powder diffraction analysis

S. L. Chaplot, A. Mierzejewski and G. S. Pawley

Acta Cryst. (1984). C40, 666-671    [doi:10.1107/S0108270184005266]

Inclusion behavior of 2-hydroxy-3,5-dinitro-N'-(5-nitrofurfurylidene)benzohydrazide, C₁₂H₇N₅O₉. Crystal structures with acetonitrile and acetic acid

I. Goldberg and Z. Stein

Acta Cryst. (1984). C40, 671-674    [doi:10.1107/S0108270184005278]

Structure of 2,2'-bis(4-chlorophenyl)-5,5'-dimethyl-[3,3'-bi-1,3-thiazolidine]-4,4'-dione, C₂₀H₁₈Cl₂N₂O₂S₂

G. Bruno, G. Bombieri, A. Del Pra, T. Previtera, M. G. Vigorita and M. Basile

Acta Cryst. (1984). C40, 674-676    [doi:10.1107/S010827018400528X]

Structure of 1,3,5,7-tetranitroadamantane, C₁₀H₁₂N₄O₈

C. George and R. Gilardi

Acta Cryst. (1984). C40, 676-679    [doi:10.1107/S0108270184005291]

Structure of a novel and reproducible polymorph (Z) of the histamine H₂-receptor antagonist cimetidine, C₁₀H₁₆N₆S

L. Párkányi, A. Kálmán, B. Hegedüs, K. Harsányi and J. Kreidl

Acta Cryst. (1984). C40, 679-683    [doi:10.1107/S0108270184005308]

Stereochemical studies of oligomers. IX. Structures of 1,4-butanediyl bis[o(m- and p-)chlorobenzoates] (BDDO, BDDM and BDDP), C₁₈H₁₆Cl₂O₄

G. Bocelli and M. F. Grenier-Loustalot

Acta Cryst. (1984). C40, 683-685    [doi:10.1107/S010827018400531X]

The structure of the five-membered cyclic sultone 9,10-dihydro-10a-methyl-3a,9-methano-3H-benzo[5,6]cyclohept[1,2-d][1,2]oxathiol-4(3aH)-one dioxide, C₁₄H₁₄O₄S

D. S. Brown, H. Heaney and K. G. Mason

Acta Cryst. (1984). C40, 685-687    [doi:10.1107/S0108270184005321]

4-Hydroxy-4-phenylpentanamide, C₁₁H₁₅NO₂, a moderately active anticonvulsant

J. Zukerman-Schpector, E. E. Castellano, G. Oliva and G. Carvajal

Acta Cryst. (1984). C40, 687-690    [doi:10.1107/S0108270184005333]

The structures of 3-allyl-9-benzoyl-2-methyl-9-phenyl-4,9-dihydropyrazolo[5,1-b]quinazoline, C₂₇H₂₃N₃O, and 6,7-dimethyl-1,3,3-triphenyl-1H-imidazo[1,2-b]pyrazol-2(3H)-one, C₂₅H₂₁N₃O

A. L. Rheingold, W. C. Fultz, E. E. Schweizer and K. J. Lee

Acta Cryst. (1984). C40, 691-693    [doi:10.1107/S0108270184005345]

Structures of (1R*,2R*,3aS*,5S*,6S*,7aS*)- and (±)-(1R*,2S*,3aS*,5R*,6S*,7aS*)-perhydro-1,2,5,6-indenetetrol, (I) and (II), C₉H₁₆O₄

Y. Matoba, Y. Ishii, M. Ogawa, H. Nakai and M. Shiro

Acta Cryst. (1984). C40, 693-696    [doi:10.1107/S0108270184005357]

Détermination structurale à 213 K du monomère bis(phénylcarbamate) de hexadiyne-2,4 diyle-1,6, C₂₀H₁₆N₂O₄

A. Whuler, P. Spinat et C. Brouty

Acta Cryst. (1984). C40, 696-700    [doi:10.1107/S0108270184005369]

Low-temperature (173 K) structure of the 'strapped' porphyrin: 2,12-diethyl-3,7,13,17-tetramethyl-8,18-nonamethylene-21H,23H-porphyrin methanol solvate, C₃₇H₄₆N₄.2CH₄O

F. W. B. Einstein and T. Jones

Acta Cryst. (1984). C40, 700-703    [doi:10.1107/S0108270184005370]

Structure of salbomycin, C₅₄H₈₈O₁₈.2H₂O

E. F. Paulus, L. Vertesy and G. M. Sheldrick

Acta Cryst. (1984). C40, 703-706    [doi:10.1107/S0108270184005382]

Structure of a Favorskii substitution product, 3-acetoxy-17-hydroxy-18-nor-5,17-pregnan-20-one, C₂₂H₃₄O₄

C. P. Huber and F. R. Ahmed

Acta Cryst. (1984). C40, 706-708    [doi:10.1107/S0108270184005394]

Structure of 2-(2-hydroxy-3-{[2-(1H-indol-3-yl)-1,1-dimethylethyl]amino}propoxy)benzonitrile: MJ-13,105-1 (bucindolol), C₂₂H₂₅N₃O₂

J.-M. Léger, M. Goursolle and A. Carpy

Acta Cryst. (1984). C40, 709-712    [doi:10.1107/S0108270184005400]

1-(2-Fluoro-2-phenylethyl)piperidine hydrochloride, C₁₃H₁₈FN.HCl: enantiomer and racemic solid-solution structures

B. Chion, J. Lajzérowicz, C. Charlon, D. Le Bars and Cuong Luu Duc

short communications

Acta Cryst. (1984). C40, 712    [doi:10.1107/S0108270184005412]

Structure of 8,5'-anhydro-8-hydroxy-9--D-ribofuranosyladenine (8,5'-O-cyclo-A) monohydrate: corrigendum

R. E. Marsh

Acta Cryst. (1984). C40, 712-713    [doi:10.1107/S0108270184005424]

Structure of 8,5'-anhydro-8-hydroxy-9--D-ribofuranosyladenine (8,5'-O-cyclo-A) monohydrate, C₁₀H₁₁N₅O₄.H₂O: errata

S. Sugio, H. Mizuno, K. Kitamura, K. Hamada, M. Ikehara and K.-i. Tomita

addenda and errata

Acta Cryst. (1984). C40, 714    [doi:10.1107/S0108270184005436]

The structure of transoid-(1RS,3SR,6RS,9RS)-7-hydroxyimino-9-methyl-1-(2-methylpropyl)tricyclo[4.2.1.0³,⁹]nonan-8-one, C₁₄H₂₁NO₂: erratum

G. E. Freeman, D. C. Fisher and S.-H. Kong

Acta Cryst. (1984). C40, 714    [doi:10.1107/S0108270184005448]

Structure of DL-normetanephrine hydrochloride [-(aminomethyl)vanillyl alcohol hydrochloride], C₉H₁₄NO₃⁺.Cl^-: erratum

R. R. Pattanayek, J. K. Dattagupta, S. C. Bhattacharyya and N. N. Saha

Copyright © International Union of Crystallography
IUCr Webmaster