Acta Crystallographica Section C

Crystal Structure Communications

Volume 40, Part 5 (May 1984)



research papers


inorganic compounds



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Acta Cryst. (1984). C40, 715-718    [doi:10.1107/S010827018400545X]

Structure of dierbium decavanadate 25-hydrate, Er2V10O28.25H2O

B. E. Rivero, G. Rigotti, G. Punte and A. Navaza



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Acta Cryst. (1984). C40, 718-720    [doi:10.1107/S0108270184005461]

Structure of monoclinic rubidium dideuteriumphosphate, RbD2PO4, in the intermediate phase

T. Hagiwara, K. Itoh, E. Nakamura, M. Komukae and Y. Makita



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Acta Cryst. (1984). C40, 720-722    [doi:10.1107/S0108270184005473]

Structure of ammonium dihydrogenphosphite, NH4H2PO3

Z. Melichar, B. Kratochvíl, J. Podlahová, V. Petrícek, K. Malý and I. Císarová



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Acta Cryst. (1984). C40, 722-725    [doi:10.1107/S0108270184005485]

Structure of a second form of 1,2;2,3-di-[mu]-hydrido-[mu]3-tetracarbonylferrio-cyclo-tris(tricarbonylruthenium)(3Ru-Ru), H2FeRu3(CO)13

L.-Y. Hsu, A. A. Bhattacharyya and S. G. Shore



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Acta Cryst. (1984). C40, 725-728    [doi:10.1107/S0108270184005497]

Structures of mercury dichloride-dipotassium dichromate (1/1), HgCl2.K2Cr2O7, and mercury dichloride-diammonium dichromate (1/1), HgCl2.(NH4)2Cr2O7

M. T. Averbuch-Pouchot, N. El-Horr and J. C. Guitel



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Acta Cryst. (1984). C40, 728-730    [doi:10.1107/S0108270184005503]

Structure du triphosphate de cuivre(II) et de trisodium dodécahydraté, CuNa3P3O10.12H2O

O. Jouini, M. Dabbabi, M. T. Averbuch-Pouchot, A. Durif et J. C. Guitel



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Acta Cryst. (1984). C40, 730-733    [doi:10.1107/S0108270184005515]

Two-layer structure of tricalcium germanate, Ca3-x[GeO4](O1-2x,F2x) with X[proportional to]0.275

F. Nishi and Y. Takéuchi



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Acta Cryst. (1984). C40, 733-736    [doi:10.1107/S0108270184005527]

Location and anisotropic refinement of deuterium atoms in deuterium sodium silicate-deuterium oxide (1/8) Na2D2SiO4.8D2O by neutron diffraction; hydrogen bonding at 173 K

R. L. Schmid, J. Felsche and G. J. McIntyre


metal-organic compounds



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Acta Cryst. (1984). C40, 736-738    [doi:10.1107/S0108270184005539]

Structure of calcium thymidine 5'-phosphate dihydrate, Ca2+.C10H13N2O8P2-.2H2O

T. Sato



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Acta Cryst. (1984). C40, 738-740    [doi:10.1107/S0108270184005540]

Structure of calcium 2'-deoxyadenosine 5'-phosphate pentahydrate, Ca2+.C10H12N5O6P2-.5H2O

T. Sato



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Acta Cryst. (1984). C40, 740-742    [doi:10.1107/S0108270184005552]

Dipotassium salt of 3-hydroxy-4-mercapto-2-thioxo-3-cyclobuten-1-one dihydrate (potassium 1,3-dithiosquarate dihydrate), K2[C4O2S2].2H2O, at 140 K

R. Mattes and G. Johann



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Acta Cryst. (1984). C40, 742-746    [doi:10.1107/S0108270184005564]

Structures of azidobis(dimethylglyoximato)(triphenylphosphine)cobalt(III), C26H29CoN7O4P, and [4,5-bis(methoxycarbonyl)-1,2,3-triazolato]bis(dimethylglyoximato)(triphenylphosphine)cobalt(III), C32H35CoN7O8P

J. H. Nelson, N. E. Takach, N. Bresciani-Pahor, L. Randaccio and E. Zangrando



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Acta Cryst. (1984). C40, 746-748    [doi:10.1107/S0108270184005576]

Structure of trans-bis(dimethylphenylphosphine)bis(pyrazole)platinum, [Pt(C3H4N2)2{P(CH3)2(C6H5)}2]

J. D. Oliver, D. F. Mullica, D. A. Grossie, W. O. Milligan and H. O. Perkins



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Acta Cryst. (1984). C40, 749-751    [doi:10.1107/S0108270184005588]

trans-Chloro(dimethylamine-N)bis[dimethylglyoximato-(1-)-N,N']cobalt(III), [CoCl(C4H7N2O2)2{NH(CH3)2}]

A. T. H. Lenstra, H. J. Geise and S. K. Tyrlik



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Acta Cryst. (1984). C40, 751-753    [doi:10.1107/S010827018400559X]

Structure of (5,10,15,20-tetraphenyl-21H,23H-porphinato)platinum(II), C44H28N4Pt

A. C. Hazell



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Acta Cryst. (1984). C40, 754-756    [doi:10.1107/S0108270184005606]

Structure of bis(tetraphenylphosphonium) (dichlorodithioferrato-S,S')disulphidooxomolybdate(2-) methyl cyanide solvate, [P(C6H5)4]2.[FeCl2{MoO(S2)}(S2)].C2H3N

W. Clegg, C. D. Garner and P. A. Fletcher



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Acta Cryst. (1984). C40, 756-759    [doi:10.1107/S0108270184005618]

Copper(I)-olefin complexes. Structure of 1-chloro-2-(1-2-[eta]-cyclohexene)-[mu]-[hydrotri(1-pyrazolyl)borato-N:N',N'']-dicopper(I), C15H20BClCu2N6

J. S. Thompson and J. F. Whitney



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Acta Cryst. (1984). C40, 759-761    [doi:10.1107/S010827018400562X]

The structure of [mu]3-thio-[mu]3-tris(disulfido)-chlorato-cyclo-tris[(diethyl dioxodithiophosphato-S,S')molybdenum](3Mo-Mo), C12H30ClMo3O6P3S13

M.-Y. Shang, J.-L. Huang and J.-X. (C.-S. ) Lu



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Acta Cryst. (1984). C40, 761-762    [doi:10.1107/S0108270184005631]

The structure of bis(tetraethylammonium) bis([mu]-acetato-O,O')-tri-[mu]-chloro-pentachloro-[mu]3-oxo-cyclo-trimolybdate(3Mo-Mo), 2C8H20N+.C4H6Cl8Mo3O52-

M.-Y. Shang, J.-L. Huang and J.-X. (C.-S. ) Lu



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Acta Cryst. (1984). C40, 763-765    [doi:10.1107/S0108270184005643]

Structure of diaquabis(4-methyl-N-8-quinolylbenzenesulphonamide-N,N')cobalt(II)-acetone (1/1), [Co(C16H13N2O2S)2(H2O)2].C3H6O

J. M. Castresana, M. P. Elizalde, J. M. Arrieta, G. Germain and J.-P. Declercq



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Acta Cryst. (1984). C40, 765-767    [doi:10.1107/S0108270184005655]

Bis(succinimido-N,N')argentate(I) de sodium pentahydraté, Na[Ag(C4H4NO2)2].5H2O

W. Khayata, D. Baylocq, F. Pellerin et N. Rodier



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Acta Cryst. (1984). C40, 768-769    [doi:10.1107/S0108270184005667]

Structure of tetrakis(N-methylimidazole-N')copper(I) perchlorate, [Cu(C4H6N2)4][ClO4]

W. Clegg, S. R. Acott and C. D. Garner



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Acta Cryst. (1984). C40, 770-772    [doi:10.1107/S0108270184005679]

The ribbon structure of catena-{[mu]4-(dihydrogen mellitato)-bis[bis(oxamide oxime-N,N')nickel(II)]} tetrahydrate, [Ni2(C12H2O12)(C2H6N4O2)2\].4H2O

H. Endres and A. Knieszner



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Acta Cryst. (1984). C40, 772-775    [doi:10.1107/S0108270184005680]

Structure of bis(9-methylhypoxanthine)silver(I) nitrate dihydrate, [Ag(C6H6N4O)2](NO3).2H2O

K. Aoki and W. Saenger



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Acta Cryst. (1984). C40, 775-778    [doi:10.1107/S0108270184005692]

Structure of (1-methyluracilato)silver(I), [Ag(C5H5N2O2)]

K. Aoki and W. Saenger



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Acta Cryst. (1984). C40, 778-781    [doi:10.1107/S0108270184005709]

Structure of the copper(II) dichloride complex of 1,4,10,13-tetraoxa-7,16-diazacyclooctadecane-7,16-diacetatocopper(II) methanol solvate, [Cu(C16H28N2O8)].CuCl2.CH3OH

P. Gluzinski, J. W. Krajewski, Z. Urbanczyk-Lipkowska, G. D. Andreetti and G. Bocelli



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Acta Cryst. (1984). C40, 781-786    [doi:10.1107/S0108270184005710]

The structures of the lanthanide ethyl sulfate enneahydrates, M(C2H5SO4)3.9H2O [M = La-Lu (except Pm)], at 171 K

R. E. Gerkin and W. J. Reppart



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Acta Cryst. (1984). C40, 786-788    [doi:10.1107/S0108270184005722]

Structure of tricarbonylbis(triphenylphosphine)ruthenium(0)-tetrahydrofuran (2/1), [Ru(CO)3{P(C6H5)3}2].1/2C4H8O

F. Dahan, S. Sabo and B. Chaudret



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Acta Cryst. (1984). C40, 789-790    [doi:10.1107/S0108270184005734]

Tetramethylammonium diiodoargentate(I), [N(CH3)4][AgI2]

K. Peters, H. G. von Schnering, W. Ott and H.-M. Seidenspinner



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Acta Cryst. (1984). C40, 790-793    [doi:10.1107/S0108270184005746]

The structure of 1,2;3,4-bis{[mu]-[bis(diphenylphosphino)methane]-P,P'}-1,2;2,4;4,1-tri-[mu]-carbonyl-1,2,3,3,4-pentacarbonyl-tetrahedro-tetrairidium(0), C58H44Ir4O8P4

M. M. Harding, B. S. Nicholls and A. K. Smith



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Acta Cryst. (1984). C40, 793-795    [doi:10.1107/S0108270184005758]

trans-Dichloro(dimethyl sulfoxide)(isopropylamine)platinum(II), C5H15Cl2NOPtS

R. Melanson and F. D. Rochon



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Acta Cryst. (1984). C40, 795-797    [doi:10.1107/S010827018400576X]

Trinitrato-(O,O')(triethylene glycol)europium(III), Eu(NO3)3(C6H14O4)

E. Forsellini, U. Casellato, G. Tomat, R. Graziani and P. Di Bernardo



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Acta Cryst. (1984). C40, 797-801    [doi:10.1107/S0108270184005771]

Structures du tris(nitroso-1 éthanal oximato-N,O')ferrate(II) de tétraphénylphosphonium, [P(C6H5)4][Fe(C2H3N2O2)3], et du tris(nitroso-1 éthanal oximato-N,O')ferrate(II) de tétraphénylarsonium, [As(C6H5)4][Fe(C2H3N2O2)3]: deux exemples de dédoublement spontané des isomères optiques lors de la cristallisation

P. Gouzerh, Y. Jeannin, E. Miler-Srenger et F. Valentini



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Acta Cryst. (1984). C40, 801-804    [doi:10.1107/S0108270184005783]

Structure of disodium 1,4-piperazinedicarbodithioate hexahydrate, 2Na+.C6H8N2S42-.6H2O

J.-P. Legros, D. Troy and J. Galy



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Acta Cryst. (1984). C40, 804-805    [doi:10.1107/S0108270184005795]

Digold(III) strontium octaacetate dihydrate, Au2Sr(C2H3O2)8.2H2O

P. G. Jones



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Acta Cryst. (1984). C40, 806-811    [doi:10.1107/S0108270184005801]

The structure of two yellow tris(2,2'-bipyridine)iridium(III) complexes: bis(2,2'-bipyridine-N,N')(NH+-2,2'-bipyridinium-3-yl-N')iridium(III) trisperchlorate-water(1/1), [Ir(C10H8N2)3](ClO4)3.H2O, and tris(2,2'-bipyridine-N,N')iridium(III) trisperchlorate-water(1/2.33), [Ir(C10H8N2)3](ClO4)3.2.33H2O

A. C. Hazell and R. G. Hazell



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Acta Cryst. (1984). C40, 811-812    [doi:10.1107/S0108270184005813]

Structure of hexaaquairon(II) bis{tris[1,3-dimethyl-2,4,5,6(1H,3H)-pyrimidinetrone 5-oximato]ferrate(II)} dodecahydrate, [Fe(H2O)6]2+.2[Fe(C6H6N3O4)3]-.12H2O

C. Ruiz-Valero, A. Monge, E. Gutiérrez-Puebla and E. Gutiérrez-Rios


organic compounds



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Acta Cryst. (1984). C40, 813-816    [doi:10.1107/S0108270184005825]

Structure of 3,3'-(trimethylenediimino)bis(3-methyl-2-butanone oxime), C13H28N4O2

M. S. Hussain, Mazhar-ul-Haque and J. Ahmed



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Acta Cryst. (1984). C40, 816-818    [doi:10.1107/S0108270184005837]

Structures of the cis and trans isomers of 2,4,6-tri-tert-butyl-2,4,6-trifluorocyclotrisilazane, C12H30F3N3Si3

W. Clegg, G. M. Sheldrick and D. Stalke



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Acta Cryst. (1984). C40, 819-820    [doi:10.1107/S0108270184005849]

Structure of the 1:1 adduct of di-tert-butylfluorosilanol and pyridine N-oxide, C8H19FOSi.C5H5NO

W. Clegg, G. M. Sheldrick, U. Klingebiel, D. Bentmann, G. Henkel and B. Krebs



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Acta Cryst. (1984). C40, 820-824    [doi:10.1107/S0108270184005850]

Structure of sucrose octaacetate, C28H38O19, at 173 K

J. D. Oliver and L. C. Strickland



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Acta Cryst. (1984). C40, 825-828    [doi:10.1107/S0108270184005862]

(R,R)-Labetalol hydrochloride: determination of the absolute configuration of the high-melting polymorph, C19H25N2O3+.Cl-

P. Murray-Rust, J. Murray-Rust, D. Hartley, P. Hallett and J. Clifton



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Acta Cryst. (1984). C40, 828-830    [doi:10.1107/S0108270184005874]

Pyridin-bortrifluorid (1/1), C5H5N.BF3

K. Töpel, K. Hensen and J. W. Bats



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Acta Cryst. (1984). C40, 830-832    [doi:10.1107/S0108270184005886]

3-Chlorobiphenyl-4-carbonitrile, C13H8ClN

H. H. Sutherland and A. Rawas



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Acta Cryst. (1984). C40, 832-834    [doi:10.1107/S0108270184005898]

Garuganin-I, an antibiotic, C22H24O5

V. Pattabhi, S. Krishnaswami and E. J. Gabe



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Acta Cryst. (1984). C40, 834-836    [doi:10.1107/S0108270184005904]

Structure of 4-(p-chlorobenzoyl)pyridine, C12H8ClNO

A. Syed, L. I. Foss and E. D. Stevens



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Acta Cryst. (1984). C40, 836-839    [doi:10.1107/S0108270184005916]

[beta]-Modifikation von Naphtho[2,3-c][1,2,5]thiadiazol-4,9-dion, C10H4N2O2S

A. Gieren, T. Hübner und V. Lamm



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Acta Cryst. (1984). C40, 839-842    [doi:10.1107/S0108270184005928]

Structural studies of colchicine derivatives. III. Structure of 7-deacetamidocolchiceine, C19H20O5

J. Rius, E. Molins, C. Miravitlles and A. Bladé-Font



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Acta Cryst. (1984). C40, 842-844    [doi:10.1107/S010827018400593X]

9-Methylthioxanthenium-10-bis(methoxycarbonyl)methylide 10-oxide, C19H18O5S

I. Vickovic, W. H. Watson and A. L. Ternay Jnr



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Acta Cryst. (1984). C40, 844-846    [doi:10.1107/S0108270184005941]

N1-Phenylsulphanilamide, C12H12N2O2S

C. J. Brown, D. S. Cook and L. Sengier



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Acta Cryst. (1984). C40, 846-848    [doi:10.1107/S0108270184005953]

Structure of 1-diphenylmethyl-3-hydroxyazetidinium chloride, C16H18NO+.Cl-

K. R. Acharya, S. S. Tavale, T. N. Guru Row and K. Venkatesan



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Acta Cryst. (1984). C40, 848-850    [doi:10.1107/S0108270184005965]

Structure of 8-chloro-1-[(dimethylamino)methyl]-6-phenyl-4H-imidazo[1,2-a][1,4]benzodiazepine, C20H19ClN4

H. J. Butcher and T. A. Hamor



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Acta Cryst. (1984). C40, 850-853    [doi:10.1107/S0108270184005977]

Stereochemical aspects of narcotic action. II. 9-(m-Hydroxyphenyl)-9[alpha]-methoxy-3-methyl-3-azoniabicyclo[3.3.1]nonane p-toluenesulfonate monohydrate, C16H24NO2+.C7H7O3S-.H2O

G. Hite, P. Salva, J. B. Anderson, M. Rapposch, M. Mangion and M. Froimowitz



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Acta Cryst. (1984). C40, 853-855    [doi:10.1107/S0108270184005989]

Methyl 8-oxotricyclo[5.4.0.02,6]undecane-1-carboxylate, C13H18O3

G. Ferguson



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Acta Cryst. (1984). C40, 856-858    [doi:10.1107/S0108270184005990]

Covalently linked purine-pyrimidine analogs. Structure of 7-(4,6-dioxo-5-pyrimidinyl)theophylline dihydrate, C11H10N6O4.2H2O

E. Gavuzzo, F. Mazza, A. Tamburrini, G. Casini and A. Carotti



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Acta Cryst. (1984). C40, 859-861    [doi:10.1107/S0108270184006004]

(E)-1-(2-Bromo-4,5-dimethoxyphenyl)-2-(2-hydroxy-3,4-dimethoxyphenyl)ethylene, C18H19BrO5

J. M. Arrieta, E. Domínguez, E. Lete, M. J. Villa and G. Germain



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Acta Cryst. (1984). C40, 861-863    [doi:10.1107/S0108270184006016]

1,2,2a,4a,5,6,7,8-Octahydro-5,8-methanocyclobut[c]indene-1,1,2,2-tetracarbonitrile, C16H12N4

R. P. Kashyap, W. H. Watson, C. Wu and P. D. Bartlett



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Acta Cryst. (1984). C40, 863-866    [doi:10.1107/S0108270184006028]

rel-(1R,4S,5S,8R)-1,2,3,4,5,6,7,8-Octahydro-1,4:5,8-dimethanonaphthalene-2,2,3,3-tetracarbonitrile, C16H12N4

W. H. Watson, R. P. Kashyap, P. D. Bartlett and C. Wu



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Acta Cryst. (1984). C40, 866-869    [doi:10.1107/S010827018400603X]

rel-(1R,4S,4aR,7R)- (1) and rel-(1R,4S,4aS,7S)- (2) isomers of 1,2,3,4,4a,5,6,7-octahydro-1,4:4a,7-dimethanonaphthalene-5,5,6,6-tetracarbonitrile, C16H12N4

W. H. Watson, R. P. Kashyap, C. Wu and P. D. Bartlett



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Acta Cryst. (1984). C40, 869-871    [doi:10.1107/S0108270184006041]

Structure of 1,2-dipiperidinoethane mono-N-oxide monoperchlorate monohydrate, (C12H25N2O)+.ClO4-.H2O

M. Jaskólski and Z. Kosturkiewicz



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Acta Cryst. (1984). C40, 871-873    [doi:10.1107/S0108270184006053]

Structure of 1,3-di-tert-butyl-2,2,4,4-tetraisopropylcyclodisilazane, C20H46N2Si2

W. Clegg, M. Haase, G. M. Sheldrick and N. Vater



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Acta Cryst. (1984). C40, 873-875    [doi:10.1107/S0108270184006065]

Structure of 2-(1,2-dihydro-1-methyl-2-pyridylidene)-3-(4-ethoxyphenyl)-3-oxopropanenitrile, C17H16N2O2

K. R. Acharya, S. S. Tavale and T. N. Guru Row



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Acta Cryst. (1984). C40, 875-877    [doi:10.1107/S0108270184006077]

Structure of 2-chloro-5-methyl-6-phenyl-3-(p-tolyl)perhydro-1,3,2[lambda]5-oxazaphosphorine 2-oxide, C17H19ClNO2P

K. R. Acharya, S. S. Tavale and T. N. Guru Row



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Acta Cryst. (1984). C40, 877-879    [doi:10.1107/S0108270184006089]

Structure of bis(trifluoroacetato)(phenyl)iodine(III), C10H5F6IO4

G. A. Stergioudis, S. C. Kokkou, A. P. Bozopoulos and P. J. Rentzeperis



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Acta Cryst. (1984). C40, 880-882    [doi:10.1107/S0108270184006090]

Structure of 2'-deoxyadenosine, C10H13N5O3

T. Sato



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Acta Cryst. (1984). C40, 882-884    [doi:10.1107/S0108270184006107]

Structure of (3aS)-7-chloro-4-(2-dimethylaminoethyl)-8-methyl-2,3,3a,4-tetrahydro-1H-pyrrolo[2,1-c][1,2,4]benzothiadiazine 5,5-dioxide, C15H22ClN3O2S

R. Oberti, M. T. Bernabei, F. Forni, R. Cameroni and E. Galli



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Acta Cryst. (1984). C40, 885-887    [doi:10.1107/S0108270184006119]

Structure of 2',3'-O-cyclohexylidene-4'-C-(2-methyl-2-propenyl)uridine, C19H26N2O6

W. J. Cook, S. E. Ealick and J. A. III. Secrist



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Acta Cryst. (1984). C40, 887-889    [doi:10.1107/S0108270184006120]

Structureof methyl 3,3-dimethyl-7-phenylsulfinyl-1,5-dioxaspiro[5.5]undecane-9-carboxylate, C19H26O5S

M. Soriano-García, R. A. Toscano, G. García, M. I. Larraza and I. H. Sánchez



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Acta Cryst. (1984). C40, 889-891    [doi:10.1107/S0108270184006132]

Structure of 2-(4,6-dimethyl-2-pyridyliminomethyl)phenol, C14H14N2O

C. Escobar and M. T. Garland



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Acta Cryst. (1984). C40, 891-894    [doi:10.1107/S0108270184006144]

Low-temperature (163 K) structure of 1,8-naphthyridine, C8H6N2

P. Dapporto, C. A. Ghilardi, C. Mealli, A. Orlandini and S. Pacinotti



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Acta Cryst. (1984). C40, 895-897    [doi:10.1107/S0108270184006156]

Structure of the dimethylsilylamine pentamer, (C2H9NSi)5. A redetermination

A. J. Blake, E. A. V. Ebsworth and A. J. Welch



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Acta Cryst. (1984). C40, 898-901    [doi:10.1107/S0108270184006168]

Structure of 1'-(p-bromophenyl)-3'-ethyl-1',3',4',5'-tetrahydro-1,2-dideoxy-D-glycero-D-gulo-heptofuranoso[1,2-d]imidazole-2'-thione, C16H21BrN2O5S

M. D. Estrada, A. Conde and R. Márquez


short communications



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Acta Cryst. (1984). C40, 901    [doi:10.1107/S010827018400617X]

Structure of 2-amino-3,5-dibromo-N-cyclohexyl-N-methylbenzenemethanamine-salicylic acid (1:1): corrigendum

R. E. Marsh



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Acta Cryst. (1984). C40, 902    [doi:10.1107/S0108270184006181]

Structure of 2-amino-3,5-dibromo-N-cyclohexyl-N-methylbenzenemethanamine-salicylic acid (1:1) (ABCMBMA-SALA), C14H20Br2N2.C7H6O3: errata

N. Shimizu, S. Nishigaki, Y. Nakai and K. Osaki



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Acta Cryst. (1984). C40, 903-904    [doi:10.1107/S0108270184006193]

Structure of diaqua-bis[[mu]-(N-salicylidene-L-phenylalaninato)-O,N,[mu]-O']-dicopper(II), C32H30Cu2N2O8: a reappraisal

J. E. Davies


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