Acta Crystallographica Section C

Crystal Structure Communications

Volume 40, Part 7 (July 1984)



research papers


inorganic compounds



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Acta Cryst. (1984). C40, 1111-1113    [doi:10.1107/S0108270184006995]

Structure of ammonium calcium phosphate heptahydrate, Ca(NH4)PO4.7H2O

S. Takagi, M. Mathew and W. E. Brown



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Acta Cryst. (1984). C40, 1114-1116    [doi:10.1107/S0108270184007009]

Structure determination on a twinned crystal of cesium pentaborate tetrahydrate, Cs[B5O6(OH)4].2H2O

H. Behm



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Acta Cryst. (1984). C40, 1117-1119    [doi:10.1107/S0108270184007010]

Structures of 21 new polytypes of cadmium iodide

B. Palosz and S. Gierlotka



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Acta Cryst. (1984). C40, 1120-1121    [doi:10.1107/S0108270184007022]

Lanthanum(III) chlorite trihydrate, La(ClO2)3.3H2O: a redetermination

C. Castellani Bisi



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Acta Cryst. (1984). C40, 1121-1124    [doi:10.1107/S0108270184007034]

The deuterium-atom positions in deuterated molybdic acid, MoO3.2D2O, by powder neutron diffraction

S. Crouch-Baker and P. G. Dickens



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Acta Cryst. (1984). C40, 1124-1127    [doi:10.1107/S0108270184007046]

The structure of barium aluminate, Ba0.75Al11O17.25

F. P. F. van Berkel, H. W. Zandbergen, G. C. Verschoor and D. J. W. IJdo



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Acta Cryst. (1984). C40, 1127-1131    [doi:10.1107/S0108270184007058]

Hexagonal Y13Pd40Sn31, a new structure type containing intergrown CaCu5- and MnCu2Al-type derived structure segments

K. Cenzual and E. Parthé


metal-organic compounds



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Acta Cryst. (1984). C40, 1131-1135    [doi:10.1107/S010827018400706X]

Structures of copper(II) complexes with N,N'-bis([beta]-carbamoylethyl)ethylenediamine and its deprotonated form, [Cu(NO3)(C8H18N4O2)(H2O)].NO3.H2Oand [Cu(C8H16N4O2)(H2O)].H2O

T.-J. Lee, T.-H. Lu, S.-H. Liu, C.-S. Chung and T.-Y. Lee



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Acta Cryst. (1984). C40, 1135-1137    [doi:10.1107/S0108270184007071]

Structure of [2,2'-(1,4,10,13-tetraoxa-7,16-diaza-7,16-cyclooctadecylene)dipropionato]copper(II), [Cu(C18H32N2O8)]

J. W. Krajewski, P. Gluzinski, Z. Urbanczyk-Lipkowska and M. Dobler



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Acta Cryst. (1984). C40, 1137-1139    [doi:10.1107/S0108270184007083]

Di(4,4',5,5'-tetramethyl-2,2'-bi-1,3-diselenolyliden)ium perrhenate, C20H24Se8+.ReO4-, (TMTSF)2ReO4. Detailed superstructure at 120 K

G. Rindorf, H. Soling and N. Thorup



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Acta Cryst. (1984). C40, 1140-1141    [doi:10.1107/S0108270184007095]

Di-[mu]-aqua-tetrakis[[mu]-(methanol)-(methanol)sodium] octamolybdate, [Na4(CH4O)8(H2O)2][Mo8O26]

E. M. McCarron III and R. L. Harlow



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Acta Cryst. (1984). C40, 1142-1145    [doi:10.1107/S0108270184007101]

Structure of tetrakis[bis(2-hydroxyethyl)dithiocarbamato]tellurium(IV), C20H40N4O8S8Te

G. C. Rout, M. Seshasayee, G. Aravamudan and K. Radha



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Acta Cryst. (1984). C40, 1145-1147    [doi:10.1107/S0108270184007113]

Structure of trans-diaquabis(ethylenediamine)nickel(II) bis(trichloroacetate), [Ni(C2H8N2)2(H2O)2](C2Cl3O2)2

S. García-Granda and F. Gómez-Beltrán



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Acta Cryst. (1984). C40, 1147-1150    [doi:10.1107/S0108270184007125]

Structural studies of tetraaquabis(saccharinato-N)zinc(II) dihydrate, [Zn(C7H4NO3S)2(H2O)4].2H2O, and tetraaquabis(saccharinato-N)cadmium(II) dihydrate, [Cd(C7H4NO3S)2(H2O)4\].2H2O

S. Z. Haider, K. M. A. Malik, S. Das and M. B. Hursthouse



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Acta Cryst. (1984). C40, 1150-1152    [doi:10.1107/S0108270184007137]

Dimeric N-tert-butyl(chloroarsine)imine, C8H18As2Cl2N2

R. Bohra, H. W. Roesky, M. Noltemeyer and G. M. Sheldrick



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Acta Cryst. (1984). C40, 1152-1154    [doi:10.1107/S0108270184007149]

Tetraaquabis(hydrogen maleato)nickel(II), [Ni(C4H3O4)2(H2O)4]

M. P. Gupta, H. J. Geise and A. T. H. Lenstra



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Acta Cryst. (1984). C40, 1155-1156    [doi:10.1107/S0108270184007150]

Structure of trans-bis(2,3-butanedione dioximato-N,N')(imidazole-N3)methylcobalt(III), C12H21CoN6O4

V. Pattabhi, M. Nethaji, E. J. Gabe, F. L. Lee and Y. Le Page



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Acta Cryst. (1984). C40, 1157-1159    [doi:10.1107/S0108270184007162]

Lithium hydrogen adipate, Li+.C6H9O4-

X. He and B. M. Craven



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Acta Cryst. (1984). C40, 1160-1161    [doi:10.1107/S0108270184007174]

Structure of ([eta]5-cyclopentadienyl)([eta]6-tetraphenylborato)iron, [Fe(C5H5){B(C6H5)4}]

R. D. Rogers and D. C. Hrncir



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Acta Cryst. (1984). C40, 1161-1164    [doi:10.1107/S0108270184007186]

Tris(2,6-dimethyl-4H-pyran-4-one)dinitratocadmium(II), [Cd(NO3)2(C7H8O2)3]

A. Banerjee, C. J. Brown, P. C. Jain and P. Gautam



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Acta Cryst. (1984). C40, 1164-1169    [doi:10.1107/S0108270184007198]

Structures of cis-dichloro(methanol)(salicylaldehyde benzoylhydrazonato)iron(III), [FeCl2(C14H11N2O2)(CH4O)], and chloro(salicylaldehyde benzoylhydrazonato)copper(II) monohydrate,[CuCl(C14H11N2O2)].H2O

A. A. Aruffo, T. B. Murphy, D. K. Johnson, N. J. Rose and V. Schomaker



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Acta Cryst. (1984). C40, 1169-1172    [doi:10.1107/S0108270184007204]

Structure of tetrakis(2,6-dimethylphenyl isocyanide)rhodium(I) tetraphenylborate ethanol solvate, [Rh(C9H9N)4][B(C6H5)4].C2H6O

T. V. Ashworth, D. C. Liles, H. E. Oosthuizen and E. Singleton



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Acta Cryst. (1984). C40, 1172-1175    [doi:10.1107/S0108270184007216]

Structures of bis(1,5-dithiacyclooctan-3-ol-O,S,S')nickel(II) diperchlorate dimethanol, [Ni(C6H12OS2)2](ClO4)2.2CH4O, and bis(1,5-dithiacyclooctan-3-ol-O,S,S')iron(II) diperchlorate, [Fe(C6H12OS2)2](ClO4)2

M. M. Olmstead, W. K. Musker and R. M. Kessler



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Acta Cryst. (1984). C40, 1175-1177    [doi:10.1107/S0108270184007228]

Structure of catena-tetraaqua-di-[mu]3-(N-salicylidene-DL-glutamato)-tricopper(II) heptahydrate [Cu3(C12H10NO5)2(H2O)4].7H2O

K. Korhonen, R. Hämäläinen and U. Turpeinen



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Acta Cryst. (1984). C40, 1178-1181    [doi:10.1107/S010827018400723X]

Structural studies on metal complexes of chiral cyclen. V. Chloro[(2RS,5RS,8RS,11SR)-1,4,7,10-tetrabenzyl-2,5,8,11-tetraethyl-1,4,7,10-tetraazacyclododecane]copper(II) dichlorocuprate(I) ethanol solvate, [CuCl(C44H60N4)][CuCl2].3C2H6O

S. Tsuboyama, K. Kobayashi, T. Sakurai and K. Tsuboyama



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Acta Cryst. (1984). C40, 1181-1183    [doi:10.1107/S0108270184007241]

Structure du tricarbonyl(hydroxyméthyl-2 phényl-2 propanol)chrome(III), [Cr(CO)3(C10H14O2)]

F. Abraham, G. Nowogrocki, J. Brocard, J. Lebibi et C. Brémard



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Acta Cryst. (1984). C40, 1183-1186    [doi:10.1107/S0108270184007253]

The barium 3,5-dinitrobenzoate benzo-15-crown-5 complex, Ba2+.2C7H3N2O6-.C14H20O5

D. L. Ward, A. I. Popov and N. S. Poonia



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Acta Cryst. (1984). C40, 1186-1188    [doi:10.1107/S0108270184007265]

The structure of tetrakis(acetonitrile)tetrachlorouranium(IV), [UCl4(C2H3N)4]

F. A. Cotton, D. O. Marler and W. Schwotzer


organic compounds



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Acta Cryst. (1984). C40, 1188-1190    [doi:10.1107/S0108270184007277]

Structure of (+)-(7S,11S)-11-hydroxy-10-methylbicyclo[5.3.1]dec-1(10)-en-7-ylmethyl (+)-10-camphorsulfonate, C23H36O5S

L. Lebioda, J. A. Marshall and K. E. Flynn



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Acta Cryst. (1984). C40, 1191-1193    [doi:10.1107/S0108270184007289]

Structure of the thermodynamic benzenethiol 1,4 adduct of the cembranolide crassin alcohol, C26H36O4S

L. Lebioda, J. A. Marshall and M. J. Coghlan



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Acta Cryst. (1984). C40, 1193-1196    [doi:10.1107/S0108270184007290]

Structure of 3-hydroxyimino-2-butanone thiosemicarbazone, a tridentate N-S ligand, C5H10N4OS

A. K. Nandi, S. Chaudhuri, S. K. Mazumdar and S. Ghosh



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Acta Cryst. (1984). C40, 1197-1198    [doi:10.1107/S0108270184007307]

Structure of 1-[ethyl(phenyl)phosphinyl]-1-phenylethanol, C16H19O2P

Z. Galdecki, P. Grochulski, B. Luciak, Z. Wawrzak and W. L. Duax



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Acta Cryst. (1984). C40, 1199-1200    [doi:10.1107/S0108270184007319]

Acetone O-[2-(1-hydroxy-3-phenyl-2-triazeno)-2-propyl]oxime, C12H18N4O2

K. R. Acharya, A. M. Shaikh and Nizamuddin



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Acta Cryst. (1984). C40, 1201-1204    [doi:10.1107/S0108270184007320]

Conformation and structure of [alpha]-tert-butyl N-(N-tert-butoxycarbonyl-O5-benzyl-[alpha]-L-glutamyl)-O5-benzyl-L-glutamate, C33H44N2O9

D. S. Eggleston and D. J. Hodgson



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Acta Cryst. (1984). C40, 1204-1205    [doi:10.1107/S0108270184007332]

Triméthyl-1,3,6 diphényl-4,5 oxa-9 diaza-2,7 tricyclo[3.3.1.02,4]nonanone-8, C21H22N2O2

R. Faure, H. Loiseleur, G. Alvernhe et A. Laurent



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Acta Cryst. (1984). C40, 1206-1207    [doi:10.1107/S0108270184007344]

O-Isopropylidène-1,2 O-méthyl-3 O-[tétra-O-acétyl-2,3,4,6 désoxy-1 D-glucopyrannosylidène-1-(1S)]-5,6 [alpha]-D-glucofurannose, C24H34O15

J.-P. Praly, G. Descotes, R. Faure et H. Loiseleur



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Acta Cryst. (1984). C40, 1208-1210    [doi:10.1107/S0108270184007356]

cis-Hexaméthyl-1,3,4b,6,8,9b dihydro-4b,9b benzofuro[3,2-b]benzofuranne, C20H22O2

R. Mercier, M. Ramah, B. Laude, R. Faure et H. Loiseleur



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Acta Cryst. (1984). C40, 1210-1211    [doi:10.1107/S0108270184007368]

Fluorene, C13H10

V. K. Belsky, V. E. Zavodnik and V. M. Vozzhennikov



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Acta Cryst. (1984). C40, 1211-1214    [doi:10.1107/S010827018400737X]

A polarized, twisted, ethylene: structure of 3,3-bis(methylthio)-2-nitro-2-propene-1-nitrile, C5H6N2O2S2

N. U. Kamath and K. Venkatesan



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Acta Cryst. (1984). C40, 1214-1217    [doi:10.1107/S0108270184007381]

Structure of 3,5,3'-triiodothyronamine bis(salicylato)borate (1:1) salt, T3AM.BSA, C14H13I3NO2+.C14H8BO6-

V. Cody



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Acta Cryst. (1984). C40, 1217-1219    [doi:10.1107/S0108270184007393]

N-{(1R*,5S*,7R*)-6-Oxobicyclo[3.2.0]hept-2-en-7-yl}phthalimide, C15H11NO3

B. Sheldrick, D. Akrigg, M. I. Page and D. Agathocleous



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Acta Cryst. (1984). C40, 1219-1220    [doi:10.1107/S010827018400740X]

Configuration absolue du p-bromobenzoyl-1 perhydroindolecarboxylate-2 d'éthyle-(2S,3aS,7aS) hydraté, C18H22BrNO3.H2O

F. Robert, Y. Jeannin, M. Vincent et M. Laubie



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Acta Cryst. (1984). C40, 1221-1223    [doi:10.1107/S0108270184007411]

Structure du p-toluènesulfonate de dithia-1,4 spiro[4.5]décyle-8, C15H20O3S3

A. Dubourg, P. Iratçabal, M. F. Grenier-Loustalot, R. Roques, J.-P. Declercq et G. Germain



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Acta Cryst. (1984). C40, 1224-1226    [doi:10.1107/S0108270184007423]

Structure and absolute configuration of (R)-N-chloroacetyl-(+)-3,3,3-trifluoro-2-aminoisobutyric acid, C6H7ClF3NO3

J. W. Keller and C. S. Day



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Acta Cryst. (1984). C40, 1226-1228    [doi:10.1107/S0108270184007435]

Structure of 3-(p-ethoxyphenyl)sydnone (1), C10H10N2O3, and 3-(p-tolyl)sydnone (2), C9H8N2O2

Y. Wang, P. L. Lee and M.-H. Yeh



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Acta Cryst. (1984). C40, 1229-1231    [doi:10.1107/S0108270184007447]

Structure of 4,4a-dihydro-9-methyl-4a-[2,2,2-trifluoro-1-(2-hydroxy-9-methylcarbazol-3-yl)ethyl]carbazol-2(3H)-one nitromethane solvate, C28H23F3N2O2.CH3NO2

K. Prout and J. M. Marín



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Acta Cryst. (1984). C40, 1231-1233    [doi:10.1107/S0108270184007459]

Covalently linked purine-pyrimidine analogs. The structure of 7-(5-hydroxy-3-oxo-2,3-dihydro-4-pyrazolyl)theophylline monohydrate, C10H10N6O4.H2O

E. Gavuzzo, F. Mazza, A. Carotti and G. Casini



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Acta Cryst. (1984). C40, 1234-1236    [doi:10.1107/S0108270184007460]

Structure of 9-aminobicyclo[3.3.1]nonane-9-carboxylic acid dihydrate, C10H17NO2.2H2O

P. Narasimhan and K. K. Chacko



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Acta Cryst. (1984). C40, 1236-1239    [doi:10.1107/S0108270184007472]

Structures of a hydrocarbon C58H40 and its photo-oxidation products. II. 4',5'-Dihydro-1',2,2',3,4,4,4'-heptaphenylspiro[cyclopent-2-ene-5,5'-naphtho[2,1-b]furan]-1-one, C58H40O2

C. T. Grainger



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Acta Cryst. (1984). C40, 1239-1242    [doi:10.1107/S0108270184007484]

Thiocarbonohydrazide dihydrochloride hemihydrate, CH8N4S2+.2Cl-.0.5H2O

M. Lanfranchi, A. M. Manotti Lanfredi, M. A. Pellinghelli and A. Tiripicchio



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Acta Cryst. (1984). C40, 1242-1245    [doi:10.1107/S0108270184007496]

Structure of 5-azatricyclo[4.3.1.03,8]decan-4-one hemihydrate, C9H13NO.1/2H2O

P. Kálal, K. Bláha and V. Langer



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Acta Cryst. (1984). C40, 1245-1248    [doi:10.1107/S0108270184007502]

Structure of (Z)-N-acetyl-[alpha],[beta]-didehydrophenylalanyl-L-alanine hydrate, C14H16N2O4.1/3H2O

V. Busetti, D. Ajò and M. Casarin



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Acta Cryst. (1984). C40, 1248-1250    [doi:10.1107/S0108270184007514]

Structure of L-tyrosyl-L-valine monohydrate, C14H20N2O4.H2O

B. Ramakrishnan, T. P. Seshadri and M. A. Viswamitra



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Acta Cryst. (1984). C40, 1250-1252    [doi:10.1107/S0108270184007526]

Conformation and structure of L-valyl-L-glutamic acid, C10H18N2O5

D. S. Eggleston



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Acta Cryst. (1984). C40, 1253-1255    [doi:10.1107/S0108270184007538]

trans-Decalin-1,4-dione, C10H14O2

S. Ariel and J. Trotter



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Acta Cryst. (1984). C40, 1255-1260    [doi:10.1107/S010827018400754X]

The disordered structures of 1,4-dibromo-2,5-diethyl-3,6-dimethylbenzene (BEMB1) and 1,3-dibromo-2,5-diethyl-4,6-dimethylbenzene (BEMB2), C12H16Br2

R. A. Wood, T. R. Welberry and M. Puza



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Acta Cryst. (1984). C40, 1260-1262    [doi:10.1107/S0108270184007551]

Structure of difluoro(methylamino)phosphine, CH4F2NP, at 97 K

A. J. Blake, E. A. V. Ebsworth and A. J. Welch



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Acta Cryst. (1984). C40, 1263-1264    [doi:10.1107/S0108270184007563]

2-Methyl-5,5-diphenyl-1,3,2[lambda]5-dioxaphosphorinane 2-sulfide, C16H17O2PS

P. Van Nuffel, C. Van Alsenoy, A. T. H. Lenstra, H. J. Geise and G. R. Van den Berg



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Acta Cryst. (1984). C40, 1265-1267    [doi:10.1107/S0108270184007575]

Structure of 3-(2,6-dichlorobenzylidenehydrazino)-1,2,4-triazol-4-amine: nebidrazine (FLA-136), C9H8Cl2N6

A. Carpy, M. Saux and M. Montagut



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Acta Cryst. (1984). C40, 1267-1269    [doi:10.1107/S0108270184007587]

Structure of 2-[(1-ethyl-2-imidazolyl)methyl]-2,3-dihydro-1,4-benzodioxin hydrochloride monohydrate: RS-21361, C14H16N2O2.HCl.H2O

A. Carpy, M. Montagut and J.-M. Léger



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Acta Cryst. (1984). C40, 1269-1271    [doi:10.1107/S0108270184007599]

Structure du (méthyl-1 nitro-4 imidazolyl-5)thio-3 1H-triazole-1,2,4, C6H6N6O2S

L. Dupont, O. Dideberg et J. Cl. Jamoulle



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Acta Cryst. (1984). C40, 1271-1273    [doi:10.1107/S0108270184007605]

The structure of 2,2'-diphenyl-1,1'-(1,3-phenylene)diethanedione, C22H14O4

A. Syed, E. D. Stevens and C. L. Klein



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Acta Cryst. (1984). C40, 1273-1276    [doi:10.1107/S0108270184007617]

The structure of 2,2'-diphenyl-1,1'-(1,4-phenylene)diethanedione, C22H14O4

A. Syed and E. D. Stevens



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Acta Cryst. (1984). C40, 1276-1278    [doi:10.1107/S0108270184007629]

Structure of 3-acetyl-5-([alpha]-methylbenzylidene)-2,4-oxolanedione, C14H12O4

Mazhar-ul-Haque, P. Pollet, J. Ahmed and W. Horne



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Acta Cryst. (1984). C40, 1278-1281    [doi:10.1107/S0108270184007630]

Structures comparées de deux pyrroles: le diphényl-3,5 pyrroledicarboxylate-1,2 de diéthyle, C22H21NO4 (1) et le (chloro-2 phényl)-3 phényl-5 pyrroledicarboxylate-1,2 de diéthyle,C22H20ClNO4 (2)

A. Laarif, F. Théobald, M. Birouk et J.-F. Robert



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Acta Cryst. (1984). C40, 1281-1283    [doi:10.1107/S0108270184007642]

1-Isopropyl-10-methylphenothiazine, C16H17NS

S. S. C. Chu, S. V. L. Narayana and R. D. Rosenstein



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Acta Cryst. (1984). C40, 1284-1286    [doi:10.1107/S0108270184007654]

Structure of 4-deoxy-4-fluoro-[beta]-D-fructopyranose, C6H11FO5

J. Podlahová and J. Loub



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Acta Cryst. (1984). C40, 1286-1288    [doi:10.1107/S0108270184007666]

(R,S)-2,3-Dihydroxy-2,3-dimethylbutanedioic acid monohydrate (meso-dimethyltartaric acid), C6H10O6.H2O

E. N. Duesler, M. Mondragon and R. E. Tapscott



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Acta Cryst. (1984). C40, 1289-1290    [doi:10.1107/S0108270184007678]

Struktur von Cuneancarbonsäureamid (Pentacyclo[4.3.0.02,4.03,8.05,7]nonan-4-carbonsäureamid), C10H11NO

R. Fröhlich



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Acta Cryst. (1984). C40, 1291-1294    [doi:10.1107/S010827018400768X]

Bis{1a,8b-dihydro(1,1-2H2)-2H-benzo[a]cyclopropa[c]cyclohepten-2-one}hydrogen(I) hexachloroantimonate, [H(C12H8D2O)2][SbCl6]

R. F. Childs, R. Faggiani, C. J. L. Lock and A. Varadarajan



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Acta Cryst. (1984). C40, 1294-1295    [doi:10.1107/S0108270184007691]

1-(p-Chlorophenyl)biguanide hydrochloride, C8H11ClN5+.Cl-

C. J. Brown and L. Sengier



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Acta Cryst. (1984). C40, 1296-1298    [doi:10.1107/S0108270184007708]

The molecular structures of chiral and meso pentacyclic bis(amino)alcohols related to amitriptyline: (I) 5,7-bis(3-dimethylaminopropyl)-12,13,15,16-tetrahydrotribenzo[1,2-d:1',2'-a':1'',2''-d']dicycloheptene-5,7-diol, C34H44N2O2, and (II) 5,13-bis(3-dimethylaminopropyl)-7,8,15,16-tetrahydrotribenzo[1,2-d:1',2'-a:4',5'-a':1'',2''-d']dicycloheptene-5,13-diol, C34H44N2O2

C. Horsburgh, P. F. Lindley, F. Stride, Y. Asscher and I. Agranat


short communications



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Acta Cryst. (1984). C40, 1299    [doi:10.1107/S010827018400771X]

Erratum to Kinetics of dehydration of single crystals of copper formate tetrahydrate by Fichte and Flanagan

R. F. Baggio



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Acta Cryst. (1984). C40, 1299-1300    [doi:10.1107/S0108270184007721]

On the aplanarity of the CO3 group in buetschliite, dipotassium calcium dicarbonate, K2Ca(CO3)2: a further refinement of the atomic arrangement

H. Effenberger and H. Langhof


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