Acta Crystallographica Section C

Crystal Structure Communications

Volume 40, Part 8 (August 1984)



research papers


inorganic compounds



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Acta Cryst. (1984). C40, 1301-1303    [doi:10.1107/S0108270184007733]

The room-temperature structures of mercury niobium fluoride, Hg3-[delta]NbF6, and mercury tantalum fluoride, Hg3-[delta]TaF6

Z. Tun, D. Brown and P. K. Ummat



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Acta Cryst. (1984). C40, 1303-1306    [doi:10.1107/S0108270184007745]

Na7Nb15W13O80 - A new type of tunnel structure studied by X-ray diffraction and HREM techniques

B.-O. Marinder and M. Sundberg



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Acta Cryst. (1984). C40, 1306-1309    [doi:10.1107/S0108270184007757]

Structure de la phase cubique de l'hexacyanoferrate(III) de zinc: Zn3[Fe(CN)6]2.nH2O

P. Gravereau and E. Garnier



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Acta Cryst. (1984). C40, 1309-1311    [doi:10.1107/S0108270184007769]

Structure of langite, Cu4[(OH)6|SO4].2H2O

M. Gentsch and K. Weber



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Acta Cryst. (1984). C40, 1311-1312    [doi:10.1107/S0108270184007770]

Dirhodium triyttrium disilicide, Y3Rh2Si2

J. M. Moreau, D. Paccard and L. Paccard


metal-organic compounds



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Acta Cryst. (1984). C40, 1313-1315    [doi:10.1107/S0108270184007782]

(2,3,9,10-Tetramethyl-1,4,8,11-tetraazacyclotetradeca-1,3,8,10-tetraene)(thiocyanato-N)copper(II) hexafluorophosphate, [Cu(NCS)(C14H24N4)](PF6)

A. E. Elia, E. C. Lingafelter and V. Schomaker



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Acta Cryst. (1984). C40, 1315-1318    [doi:10.1107/S0108270184007794]

Structure of tetraphenylarsonium bis([mu]6-carbido-2,3;4,5-di-[mu]-carbonyl-1,1,1,2,2,3,3,4,4,5,5,6,6,6-tetradecarbonyl-octahedro-hexaruthenio-Ru3,Ru4)thallate(1-)(4Tl-Ru), [As(C6H5)4][{Ru6C(CO)16}2Tl]

G. B. Ansell, M. A. Modrick and J. S. Bradley



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Acta Cryst. (1984). C40, 1318-1320    [doi:10.1107/S0108270184007800]

Structure of bis[[mu]-([beta]-alanine)-O,O']-disilver(I) dinitrate, [Ag2(C3H7NO2)2](NO3)2

M. E. Kamwaya, E. Papavinasam, S. G. Teoh and R. K. Rajaram



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Acta Cryst. (1984). C40, 1320-1322    [doi:10.1107/S0108270184007812]

Acetato(triphenylphosphine)gold(I), [Au(C2H3O2)(C18H15P)]

P. G. Jones



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Acta Cryst. (1984). C40, 1322-1324    [doi:10.1107/S0108270184007824]

Structure of bis(L-histidinato-O,N,N')chromium(III) nitrate, [Cr(C6H8N3O2)2]NO3

W. T. Pennington, A. W. Cordes, D. Kyle and E. W. Wilson Jnr



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Acta Cryst. (1984). C40, 1324-1327    [doi:10.1107/S0108270184007836]

Structure of (benzenethiolato)(2,3,7,8,12,13,17,18-octaethylporphinato)iron(III), [Fe(C36H44N4)(C6H5S)]

K. M. Miller and C. E. Strouse



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Acta Cryst. (1984). C40, 1327-1328    [doi:10.1107/S0108270184007848]

Structure of mer-trichlorotris(pyridine)rhodium(III), [RhCl3(C5H5N)3]

K. R. Acharya, S. S. Tavale and T. N. Guru Row



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Acta Cryst. (1984). C40, 1329-1331    [doi:10.1107/S010827018400785X]

Structure of the 4:1 complexes formed by pyridine and the Group III halides InCl3 and TlCl3: mer-trichlorotris(pyridine)indium(III)-pyridine (1/1), [InCl3(C5H5N)3].C5H5N, and mer-trichlorotris(pyridine)thallium(III)-pyridine (1/1), [TlCl3(C5H5N)3].C5H5N

S. E. Jeffs, R. W. H. Small and I. J. Worrall



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Acta Cryst. (1984). C40, 1331-1334    [doi:10.1107/S0108270184007861]

Structure of semiconducting 3,4;3',4'-bis(ethylenedithio)-2,2',5,5'-tetrathiafulvalene-hexafluoroarsenate (2:1), (BEDT-TTF)2AsF6, (C10H8S8)2AsF6

P. C. W. Leung, M. A. Beno, G. S. Blackman, B. R. Coughlin, C. A. Miderski, W. Joss, G. W. Crabtree and J. M. Williams



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Acta Cryst. (1984). C40, 1334-1337    [doi:10.1107/S0108270184007873]

Structure of 3,4;3',4'-bis(ethylenedithio)-2,2',5,5'-tetrathiafulvalene-tetrabromoindate (2:1), (BEDT-TTF)2InBr4, (C10H8S8)2InBr4

M. A. Beno, D. D. Cox, J. M. Williams and J. F. Kwak



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Acta Cryst. (1984). C40, 1338-1340    [doi:10.1107/S0108270184007885]

Structure of the disodium salt of glucose 1-phosphate hydrate, 2Na+.C6H11O9P2-.3.5H2O

N. Narendra, T. P. Seshadri and M. A. Viswamitra



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Acta Cryst. (1984). C40, 1340-1342    [doi:10.1107/S0108270184007897]

Structure de l'aqua(aza-4 azonia-1 bicyclo[2.2.2]octane)trinitratocobalt(II), [Co(C6H13N2)(NO3)3(H2O)]

B. Viossat, S. Bénazeth, P. Khodadad and N. Rodier



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Acta Cryst. (1984). C40, 1343-1346    [doi:10.1107/S0108270184007903]

Structure studies of technetium complexes. VII. Structure of tetraphenylarsonium hexachlorotechnetate(IV), [As(C6H5)4]2[TcCl6]

J. Baldas, J. Bonnyman, D. L. Samuels and G. A. Williams



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Acta Cryst. (1984). C40, 1346-1349    [doi:10.1107/S0108270184007915]

Structure of tris(cyclohexylammonium) chloride tetrachlorocobaltate(II), (C6H14N)3Cl(CoCl4)

U. Geiser, R. D. Willett and R. M. Gaura



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Acta Cryst. (1984). C40, 1349-1352    [doi:10.1107/S0108270184007927]

Structure of dichlorobis(p-methoxyphenyl)tellurium(IV), [TeCl2(C7H7O)2]

R. K. Chadha and J. E. Drake



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Acta Cryst. (1984). C40, 1352-1355    [doi:10.1107/S0108270184007939]

[2,2-Di(2-pyridyl)-1,3-dioxolane-N,N']dichloropalladium(II), [PdCl2(C13H12N2O2)]

G. R. Newkome, V. K. Gupta, K. J. Theriot, J. C. Ewing, S. P. Wicelinski, W. R. Huie, F. R. Fronczek and S. F. Watkins



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Acta Cryst. (1984). C40, 1355-1357    [doi:10.1107/S0108270184007940]

Structure de (diméthyl-5,5' tétraphényl-1,2,8,9 tétraaza-3,4,6,7 nonatétraène-1,3,6,8 diolato-1,9-O,O',N,N')nickel(II), Ni(C31H26N4O2)

F. Abraham, J. M. Capon, G. Nowogrocki, S. Sueur et C. Brémard



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Acta Cryst. (1984). C40, 1357-1359    [doi:10.1107/S0108270184007952]

Tribromo(triethylphosphine)gold(III), [AuBr3{P(C2H5)3}]

D. S. Eggleston, D. F. Chodosh, D. T. Hill and G. R. Girard



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Acta Cryst. (1984). C40, 1359-1362    [doi:10.1107/S0108270184007964]

Structure of tris(1,10-phenanthroline)cobalt(II) diperchlorate monohydrate, [Co(C12H8N2)3](ClO4)2.H2O

D. Boys, C. Escobar and O. Wittke



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Acta Cryst. (1984). C40, 1362-1364    [doi:10.1107/S0108270184007976]

[mu]-Oxo-bis{[hydrotris(3,5-dimethyl-1-pyrazolyl)borato]dioxomolybdenum(VI)}, Mo2(C15H22BN6)2O5

K. M. Barnhart and J. H. Enemark



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Acta Cryst. (1984). C40, 1364-1367    [doi:10.1107/S0108270184007988]

The structure of the monobasic lead salt of 2,4,6-trinitro-1,3-benzenediol ([beta] polymorph), Pb2(OH)22+.C6HN3O82-

M. A. Pierce-Butler



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Acta Cryst. (1984). C40, 1367-1369    [doi:10.1107/S010827018400799X]

Structure of 2-hydroxyethanethiolatolead(II) nitrate, Pb(SCH2CH2OH)(NO3), a sheet polymer

W. Clegg, I. L. Abrahams and C. D. Garner


organic compounds



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Acta Cryst. (1984). C40, 1369-1371    [doi:10.1107/S0108270184008003]

Structure of N-(3-cyanophenyl)acetohydroxamic acid hydrate C9H8N2O2.1/3H2O

R. Mocharla, D. R. Powell and D. van der Helm



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Acta Cryst. (1984). C40, 1372-1373    [doi:10.1107/S0108270184008015]

3,4-Dichloro-6-selenatricyclo[5.4.0.02,5]undeca-1(7),8,10-trien-2-yl acetate, C12H10Cl2O2Se

F. Baert, V. Warin and P. Grandclaudon



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Acta Cryst. (1984). C40, 1374-1376    [doi:10.1107/S0108270184008027]

Structure de l'oxo-3 phénylamino-5 hexène-4 anilide, C18H18N2O2

P. Briard, A. Dubourg, R. Roques, S. Castillo, V. Hérault et J.-P. Declercq



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Acta Cryst. (1984). C40, 1376-1378    [doi:10.1107/S0108270184008039]

2-{8-Hydroxybicyclo[5.1.0]oct-1(7)-en-8-yl}-1-cycloheptene-1-carboxylic acid [gamma]-lactone, C16H20O2 (I), and 2-{(1[alpha],7[alpha],8[alpha])-8-hydroxybicyclo[5.1.0]oct-8-yl}-1-cycloheptene-1-carboxylic acid [gamma]-lactone, C16H22O2 (II)

C. M. Weeks, W. L. Duax, R. A. Finnegan, D. J. Delecki and B. Kojic-Prodic



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Acta Cryst. (1984). C40, 1378-1381    [doi:10.1107/S0108270184008040]

The low-temperature X-ray study of thianthrene 5,5,10,10-tetraoxide, C12H8O4S2

V. M. Lynch, S. B. Larson, S. H. Simonsen and S. N. Thomas



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Acta Cryst. (1984). C40, 1381-1386    [doi:10.1107/S0108270184008052]

Crystal form II of cycloamanide A, cyclo(-L-prolyl-L-valyl-L-phenylalanyl-L-phenylalanyl-L-alanyl-glycyl)-water-ethanol (1/1/3), C33H42N6O6.H2O.3C2H6O, containing an unusual [beta]-bend

I. L. Karle and C. C. Chiang



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Acta Cryst. (1984). C40, 1387-1390    [doi:10.1107/S0108270184008064]

Redetermination of the structure of the 3:1 complex of 4,4'-dinitrobiphenyl with 4-hydroxybiphenyl, 3C12H8N2O4.C12H10O: crystal packing, molecular geometry and thermal motion

C. P. Brock and K. L. Haller



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Acta Cryst. (1984). C40, 1391-1394    [doi:10.1107/S0108270184008076]

Stereochemical studies of oligomers. X. The structure of 1,6-hexanediyl bis[o-(m- and p-)chlorobenzoates] (HDDO, HDDM and HDDP), C20H20Cl2O4

G. Bocelli and M. F. Grenier-Loustalot



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Acta Cryst. (1984). C40, 1394-1397    [doi:10.1107/S0108270184008088]

Stereochemical studies of oligomers. XI. The structure of 1,2-propanediyl bis(p-chlorobenzoate) (PDP), C17H14Cl2O4, and 2,3-butanediyl bis(p-chlorobenzoate) (BDP), C18H16Cl2O4

G. Bocelli and M. F. Grenier-Loustalot



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Acta Cryst. (1984). C40, 1397-1399    [doi:10.1107/S010827018400809X]

Stereochemical studies of oligomers. XII. The structure of 1,10-decanediyl bis(o-chlorobenzoate), C24H28Cl2O4

G. Bocelli and M. F. Grenier-Loustalot



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Acta Cryst. (1984). C40, 1400-1402    [doi:10.1107/S0108270184008106]

Stereochemical studies of oligomers. XIII. The structures of 2,5-hexanediyl bis(p-chlorobenzoate) and 2,5-hexanediyl bis(m-chlorobenzoate) (HDP and HDM), C20H20Cl2O4

G. Bocelli and M. F. Grenier-Loustalot



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Acta Cryst. (1984). C40, 1402-1404    [doi:10.1107/S0108270184008118]

The structure of 1,7-heptanediamine dihydrobromide at 173 K, C7H18N2.2HBr

J. Brisson and F. Brisse



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Acta Cryst. (1984). C40, 1405-1407    [doi:10.1107/S010827018400812X]

The structure of 1,8-octanediamine dihydrobromide, C8H20N2.2HBr

J. Brisson and F. Brisse



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Acta Cryst. (1984). C40, 1407-1409    [doi:10.1107/S0108270184008131]

Structure of 1,1,1',1',3,3,3',3'-octamethyl-2,2'-biindanylidene, C26H32

T. Pilati and M. Simonetta



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Acta Cryst. (1984). C40, 1409-1412    [doi:10.1107/S0108270184008143]

The structure of 1-methylisoguanine dihydrate, C6H7N5O.2H2O

R. Y. Wong and R. J. Nachman



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Acta Cryst. (1984). C40, 1412-1416    [doi:10.1107/S0108270184008155]

Structure and conformation of L-tyrosyl-L-tyrosine dihydrate, C18H20N2O5.2H2O

M. Cotrait, J.-P. Bideau, G. Beurskens, W. P. Bosman and P. T. Beurskens



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Acta Cryst. (1984). C40, 1416-1418    [doi:10.1107/S0108270184008167]

rel-(1S,3aR,4R,7S,7aR)-5,6,7,7a-Tetrahydro-4,7-methano-1H-indene-1,3a(4H)-diol, C10H14O2

D. A. Grossie, W. H. Watson, C. Wu and P. D. Bartlett



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Acta Cryst. (1984). C40, 1418-1420    [doi:10.1107/S0108270184008179]

rel-(1S,2S,3S,3aR,4R,7S,7aR)-1,2,3,4,5,6,7,7a-Octahydro-1,3a-etheno-4,7-methano-3aH-indene-2,3-dicarboxylic anhydride, C14H14O3

W. H. Watson, J. Galloy, C. Wu and P. D. Bartlett



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Acta Cryst. (1984). C40, 1420-1422    [doi:10.1107/S0108270184008180]

Tri-[b,e,h]-(4,5-dimethoxybenzo)cyclonona-2,5,8-trien-1-one, C27H28O7

M. N. Ponnuswamy and J. Trotter



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Acta Cryst. (1984). C40, 1423-1425    [doi:10.1107/S0108270184008192]

Structure and absolute configuration of (-)-3-(1-cyclopropylmethyl-3-isobutyl-3-pyrrolidinyl)phenol hydrobromide, C18H28NO+.Br-

F. R. Ahmed



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Acta Cryst. (1984). C40, 1425-1427    [doi:10.1107/S0108270184008209]

Structure of (4[beta]H,6[beta]H,11[alpha]H)-3[beta],10[beta]-epoxy-8[beta]-isobutyryloxy-1-oxogermacr-2-en-6,12-olide (tetrahydrozexbrevin), C19H26O6, a sesquiterpenoid lactone

M. Soriano-García and R. A. Toscano



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Acta Cryst. (1984). C40, 1428-1429    [doi:10.1107/S0108270184008210]

Structure of 6-[cinnamoyl(2-morpholinoethyl)amino]-1,3-dimethyluracil, C21H26N4O4

V. Warin, M. Lobry, J. L. Bernier and J. P. Henichart



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Acta Cryst. (1984). C40, 1430-1432    [doi:10.1107/S0108270184008222]

Betaxolol hydrochloride: 1-{4-[2-(cyclopropylmethoxy)ethyl]phenoxy}-3-isopropylamino-2-propanol hydrochloride, C18H30NO3+.Cl-

C. Pascard, E. Tran Huu Dau, P. Manoury and B. Mompon



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Acta Cryst. (1984). C40, 1432-1434    [doi:10.1107/S0108270184008234]

Structure du chlorhydrate de l'[hydroxy-1-(R,S) isopropylamino-2 éthyl]-6 dihydro-2,3 benzoxazole-1,3 one-2, C12H16N2O3.HCl

G. Mairesse, J. C. Boivin, D. J. Thomas, J. P. Bonte, D. Lesieur et C. Lespagnol



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Acta Cryst. (1984). C40, 1434-1436    [doi:10.1107/S0108270184008246]

Structure of 9,10-bis(p-nitrobenzeneazo)-cis-decalin (PNPAD), C22H24N6O4

C. A. Kavounis and P. J. Rentzeperis



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Acta Cryst. (1984). C40, 1436-1438    [doi:10.1107/S0108270184008258]

(±)-Norphenylephrine hydrochloride (m-octopamine hydrochloride), C8H12NO2+.Cl-

G. Ferguson, M. Parvez, B. L. Ruhl, J. F. Malone and J. M. Midgley



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Acta Cryst. (1984). C40, 1439-1440    [doi:10.1107/S010827018400826X]

Structure of 1,4,7,10,13,16-hexaazapentacyclo[11.5.1.14,10.07,20.016,19]icosane, C14H26N6

M. M. Olmstead, P. P. Power and M. Viggiano



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Acta Cryst. (1984). C40, 1441-1443    [doi:10.1107/S0108270184008271]

Structure of 2-[(methylsulfonyl)acetyl]pyridine, C8H9NO3S: an immunosuppressive agent

T. Srikrishnan



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Acta Cryst. (1984). C40, 1443-1445    [doi:10.1107/S0108270184008283]

cis-1,5-Diphenyl-3-(diphenylmethylene)-4-morpholinocarbonyl-2-pyrrolidinone, C34H30N2O3

A. E. Baydar, G. V. Boyd, F. Stride and P. F. Lindley



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Acta Cryst. (1984). C40, 1445-1449    [doi:10.1107/S0108270184008295]

Grantianine, C18H23NO7: a pyrrolizidine alkaloid

H. Stoeckli-Evans and D. J. Robins



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Acta Cryst. (1984). C40, 1449-1452    [doi:10.1107/S0108270184008301]

Structure of jacobine methanol solvate, C18H25NO6.CH4O

D. C. Rohrer, J. Karchesy and M. Deinzer



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Acta Cryst. (1984). C40, 1452-1454    [doi:10.1107/S0108270184008313]

Structure of 2,11,20,29-tetrathia[3.3.3.3]parabenzenophane, C32H32S4

T.-L. Chan and T. C. W. Mak



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Acta Cryst. (1984). C40, 1455-1458    [doi:10.1107/S0108270184008325]

Steroid intermediates: (1) 3,4-dinor-2,5-seco-9[alpha]-estrane-1,15,17-trione, C16H22O3; (2) D-homo-4-norestr-3(5)-ene-2,17-dione, C18H24O2; and (3) 1,2,3,4-tetranorestr-9-ene-5,17-dione, C14H18O2

E. O. Schlemper, B. Nassim and P. Crabbé



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Acta Cryst. (1984). C40, 1458-1460    [doi:10.1107/S0108270184008337]

Structure of 3,3'-dichlorodibenzoyl peroxide, C14H8Cl2O4

A. Syed, P. Umrigar, E. D. Stevens, G. W. Griffin and R. J. Majeste



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Acta Cryst. (1984). C40, 1460-1462    [doi:10.1107/S0108270184008349]

Structure and stereochemistry of 2-methylthio-7-(p-bromophenyl)-8-phenoxy-4,5-benzo-3-aza-2-nonem, C24H19BrN2O2S

M. Soriano-García, R. A. Toscano, E. Cortés and R. Martínez



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Acta Cryst. (1984). C40, 1463-1465    [doi:10.1107/S0108270184008350]

The low-temperature structure of cis-cisoid-cis-perhydroanthracene, C14H24

H. van Koningsveld, J. M. A. Baas and B. van de Graaf



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Acta Cryst. (1984). C40, 1465-1466    [doi:10.1107/S0108270184008362]

Dimeric tert-butylaminoboron difluoride, [(CH3)3CNHBF2]2

P. G. Jones



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Acta Cryst. (1984). C40, 1467-1469    [doi:10.1107/S0108270184008374]

Structure of 3-(1-cytosinyl)propionamide, C7H10N4O2

S. Fujita, A. Takenaka and Y. Sasada



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Acta Cryst. (1984). C40, 1469-1471    [doi:10.1107/S0108270184008386]

Drimenol, (1S,2R,6S)-1,3,7,7-tetramethylbicyclo[4.4.0]dec-3-ene-2-methanol, C15H26O

C. Escobar and O. Wittke



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Acta Cryst. (1984). C40, 1472-1473    [doi:10.1107/S0108270184008398]

Structure du méthyl-2 oxo-5 (p-toluènesulfonamido)-4 (p-toluènesulfonyl)-1 dihydro-2,5 pyrrolecarboxylate-2 d'éthyle, C22H24N2O7S2

L. Dupont, O. Dideberg et J. Cl. Jamoulle



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Acta Cryst. (1984). C40, 1474-1475    [doi:10.1107/S0108270184008404]

Structure of 1,1'-di(4-pyridyl)-2,2',6,6'-bi(4-piperidone) dihydrochloride dihydrate, C20H22N4O22+.2Cl-.2H2O

C. J. Cheer, J. P. Cosgrove and B. M. Vittimberga



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Acta Cryst. (1984). C40, 1476-1477    [doi:10.1107/S0108270184008416]

Structure of ethyl 3-methylene-2a-phenyl-2a,3-dihydro[1,2]diazeto[3,2-c][1,4]benzothiazine-2-carboxylate, C19H16N2O2S

T. Pilati and M. Simonetta



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Acta Cryst. (1984). C40, 1478-1480    [doi:10.1107/S0108270184008428]

Structure du diiodure de diazonia-6,9 dispiro[5.2.5.2]hexadécane, C14H28N22+.2I-

J. Estienne, M. Pierrot, A. Baldy, J. Rosenberg et G. Robert



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Acta Cryst. (1984). C40, 1481-1482    [doi:10.1107/S010827018400843X]

Cyclopentene-1,2,3-trione, C5H2O3

H. Irngartinger, M. Nixdorf, W. Dobler and R. Gleiter



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Acta Cryst. (1984). C40, 1483-1486    [doi:10.1107/S0108270184008441]

The structure of 6,7,9-trimethyl-4-azaphenoxathiin, C14H13NOS

V. M. Lynch, S. H. Simonsen, G. E. Martin, S. Puig-Torres and K. Smith



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Acta Cryst. (1984). C40, 1486-1490    [doi:10.1107/S0108270184008453]

Structures of morphine methyl iodide monohydrate, (C18H22NO3)+.I-.H2O, and di(morphine) dihydrogensulfate pentahydrate, 2(C17H20NO3)+.SO42-.5H2O

C. Wongweichintana, E. M. Holt and N. Purdie


addenda and errata



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Acta Cryst. (1984). C40, 1490    [doi:10.1107/S0108270184008465]

Structure of 6-chloro-4-phenyl-1,2,3-benzoxathiazine 2,2-dioxide, C13H8ClNO3S: erratum

S. Mehdi and B. R. Rao



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Acta Cryst. (1984). C40, 1490    [doi:10.1107/S0108270184008477]

Structure of methyl 8-isopropyl-3,3a,8,8a-tetrahydroindeno[2,1-c]pyrazole-8a-carboxylate, C15H18N2O2: erratum

L. Toupet and J. C. Messager


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