Acta Crystallographica Section C

Crystal Structure Communications

Volume 41, Part 3 (March 1985)



research papers


inorganic compounds



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Acta Cryst. (1985). C41, 301-303    [doi:10.1107/S0108270185003705]

The treatment of data collected with a single-crystal diffractometer

T. A. Hamor, H. Steinfink and B. T. M. Willis



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Acta Cryst. (1985). C41, 304-306    [doi:10.1107/S0108270185003717]

Tripotassium cis-dichloro(hydrogenbissulfito)palladate(II), K3[Pd{(SO3)2H}Cl2]

G. Liehr, D. K. Breitinger and M. Raidel



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Acta Cryst. (1985). C41, 306-307    [doi:10.1107/S0108270185003729]

Structure of Pb0.15Nb3S4

E. Amberger, K. Polborn and P. Grimm



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Acta Cryst. (1985). C41, 308-310    [doi:10.1107/S0108270185003730]

Structure of tetrapotassium dodeca-[mu]-bromo-hexabromo-octahedro-hexaniobate(4-), K4[(Nb6Br12)Br6]

F. Ueno and A. Simon



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Acta Cryst. (1985). C41, 310-313    [doi:10.1107/S0108270185003742]

Pr15Ni7Si10 with an atom ordering on the trigonal-prism-centre sites in agreement with the waist-contact restriction rule

E. Hovestreydt and E. Parthé



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Acta Cryst. (1985). C41, 313-319    [doi:10.1107/S0108270185003754]

Cubic Sc57Rh13 and orthorhombic Hf54Os17, two geometrically related crystal structures with rhodium- and osmium-centred icosahedra

K. Cenzual, B. Chabot and E. Parthé


metal-organic compounds



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Acta Cryst. (1985). C41, 319-322    [doi:10.1107/S0108270185003766]

Structure of potassium [meso-2,3-butanediaminetetraacetato(4-)]cobalt(III) 2.5 hydrate, K[Co(C12H16N2O8)].2.5H2O

M. E. Kalina, V. Kettmann and F. Pavelcík



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Acta Cryst. (1985). C41, 322-324    [doi:10.1107/S0108270185003778]

Structure of bis(O,O'-diisopropyl phosphorodithioato)nickel(II), Ni[S2P(OiC3H7)2]2

B. F. Hoskins and E. R. T. Tiekink



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Acta Cryst. (1985). C41, 324-327    [doi:10.1107/S010827018500378X]

Pentakis(imidazole)copper(II) monophenyl phosphate tetrahydrate, [Cu(C3H4N2)5][P(C6H5O)O3].4H2O

T. Glowiak and I. Wnek



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Acta Cryst. (1985). C41, 327-329    [doi:10.1107/S0108270185003791]

Disordered structure of dibenzouranocene, [U(C12H10)2]

A. Zalkin, D. H. Templeton, R. Kluttz and A. Streitwieser Jnr



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Acta Cryst. (1985). C41, 329-332    [doi:10.1107/S0108270185003808]

Tetraphenylphosphonium-octachlorodiarsenat, (PPh4)2[As2Cl8]

A. T. Mohammed and U. Müller



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Acta Cryst. (1985). C41, 332-334    [doi:10.1107/S010827018500381X]

Structure of dichloro[N-(2-pyridylmethylene)histamine-N,N',N'']copper(II) hemihydrate, [CuCl2(C11H12N4)].0.5H2O

F. Nepveu and L. Walz



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Acta Cryst. (1985). C41, 334-336    [doi:10.1107/S0108270185003821]

Structure of ([eta]5-indenyl)uranium tribromide-bis(tetrahydrofuran), [U(C9H7)]Br3.2C4H8O

J. Rebizant, M. R. Spirlet and J. Goffart



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Acta Cryst. (1985). C41, 336-338    [doi:10.1107/S0108270185003833]

Structure of 1,1,2,2,3,3-hexacarbonyl-1,2;2,3;3,1-tris([mu]-diphenylphosphido)-triangulo-tricobalt(I)(3Co-Co) acetonitrile solvate, [Co3{P(C6H5)2}3(CO)6].C2H3N

M. K. Markiewicz, M. E. Fraser, R. K. Ungar, S. Fortier and M. C. Baird



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Acta Cryst. (1985). C41, 338-341    [doi:10.1107/S0108270185003845]

Synthèse et structure d'un complexe trinucléaire du cobalt(II) à multiples coordinats chélatant et ponteur: [mu]3-chloro-tris(diméthoxy-1,2 éthane)-[mu]3-sulfato-tris([mu]-trifluoroacétato-O,O')-tricobalt(II), [Co3Cl(C2F3O2)3(SO4)(C4H10O2)3]

J. Estienne



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Acta Cryst. (1985). C41, 341-347    [doi:10.1107/S0108270185003857]

Ferrichrome conformations: ferrirubin, two crystal forms: C41H64FeN9O17.10.5H2O (I) and C41H64FeN9O17.CH3CN.H2O (II)

C. L. Barnes, M. B. Hossain, M. A. F. Jalal, D. L. Eng-Wilmot, S. L. Grayson, B. A. Benson, S. K. Agarwal, R. Mocherla and D. van der Helm



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Acta Cryst. (1985). C41, 347-350    [doi:10.1107/S0108270185003869]

Structure of diaquaoxodiperoxomolybdenum(VI)-1,4,7,10,13,16-hexaoxacyclooctadecane (18-crown-6) monohydrate, [MoO(O2)2(H2O)2].C12H24O6.H2O

C. B. Shoemaker, D. P. Shoemaker, L. V. McAfee and C. W. DeKock



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Acta Cryst. (1985). C41, 350-352    [doi:10.1107/S0108270185003870]

trans-Bis(tert-butylamine)dichloroplatinum(II), C8H22Cl2N2Pt

R. Melanson and F. D. Rochon



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Acta Cryst. (1985). C41, 352-355    [doi:10.1107/S0108270185003882]

1,1,1,2,2,2,3,3,3-Nonacarbonyl-[mu]3-cyclopropylmethylidyne-triangulo-tricobalt, ([mu]3-c-C3H5C)Co3(CO)9

P. F. Seidler, S. T. McKenna, M. A. Kulzick and T. M. Gilbert



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Acta Cryst. (1985). C41, 355-358    [doi:10.1107/S0108270185003894]

Structure of monoclinic sodium (ethylenediaminetetraacetato)holmate(III) octahydrate, Na[Ho(C10H12N2O8)].8H2O: disorder induced by radiation

L. K. Templeton, D. H. Templeton and A. Zalkin



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Acta Cryst. (1985). C41, 358-360    [doi:10.1107/S0108270185003900]

Structure of [mu]-oxo-bis[(2-hydroxyethanesulfonato)triphenylantimony(V)], [Sb2O(C2H5O4S)2(C6H5)6]

H. Preut, R. Rüther and F. Huber



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Acta Cryst. (1985). C41, 360-363    [doi:10.1107/S0108270185003912]

Structure of acetato(acetylacetonato)diaquacalcium, [Ca(CH3COO)(C5H7O2)(H2O)2]

J. J. Sahbari and M. M. Olmstead



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Acta Cryst. (1985). C41, 363-365    [doi:10.1107/S0108270185003924]

Structure of di-[mu]-(+)-tartrato-bis[aquazinc(II)] trihydrate, [Zn2(C4H4O6)2(H2O)2].3H2O and anomalous scattering by zinc

L. K. Templeton, D. H. Templeton, D. Zhang and A. Zalkin



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Acta Cryst. (1985). C41, 365-369    [doi:10.1107/S0108270185003936]

Crystallographic analysis of two rhodium(III) hydride complexes, bis{1,1'-bis[tert-butyl(phenyl)phosphino]ferrocene-P,P'}-tri-[mu]-hydrido-dihydridodirhodium(III) chlorate methanol solvate, [Rh2H5{Fe[P(C4H9)(C5H4)(C6H5)]2}2]ClO4.CH3OH (1), and bis[1,1'-bis(di-tert-butylphosphino)ferrocene-P,P']-tri-[mu]-hydrido-dihydridodirhodium(III) chlorate, [Rh2H5{Fe[P(C4H9)2(C5H4)]2}2]ClO4 (2)

F. W. B. Einstein and T. Jones



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Acta Cryst. (1985). C41, 369-371    [doi:10.1107/S0108270185003948]

Structure of tetraphenylphosphonium triiodomercurate(II), [P(C6H5)4][HgI3]

B. Zacharie, J. D. Wuest, M. J. Olivier and A. L. Beauchamp



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Acta Cryst. (1985). C41, 372-374    [doi:10.1107/S010827018500395X]

The structure of bis(1,2-dihydro-4-phenyl-4H-[1,4]oxazino[4,3-[alpha]]benzimidazole)dinitratonickel(II) acetonitrile solvate, [Ni(C16H14N2O)2(NO3)2].CH3CN

P. Carr, B. Piggott and H. J. Tinton



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Acta Cryst. (1985). C41, 374-377    [doi:10.1107/S0108270185003961]

The structure of bis[(R,S)-N,N'-bis(5-methyl-2-thienylmethylene)-1,2-cyclohexanediamine]copper(I) trifluoromethanesulfonate, C36H44CuN4S4+.CF3SO3-

A. L. Spek, A. J. M. Duisenberg, G. C. van Stein and G. van Koten


organic compounds



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Acta Cryst. (1985). C41, 377-379    [doi:10.1107/S0108270185003973]

Guanidinium tetraborate(2-) dihydrate, (CH6N3)2[B4O5(OH)4].2H2O

T. J. R. Weakley



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Acta Cryst. (1985). C41, 379-383    [doi:10.1107/S0108270185003985]

Structure of decentapicrin A: (-)-(4aS)-6-[3'-O-(3-hydroxybenzoyl)-[beta]-D-glucopyranosyloxy]-5-vinyl-4,4a[alpha],5[beta],6[alpha]-tetrahydro-1H,3H-pyrano[3,4-c]pyran-1-one, C23H26O11

B. Kojic-Prodic, A. L. Spek, W. G. van der Sluis and R. P. Labadie



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Acta Cryst. (1985). C41, 383-386    [doi:10.1107/S0108270185003997]

The structures of (dimethylaminopropyl)phenothiazine drugs and their metabolites. II. Chlorpromazine sulphoxide, C17H19ClN2OS, at 120 K

E. Hough, M. Hjorth and S. G. Dahl



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Acta Cryst. (1985). C41, 386-389    [doi:10.1107/S0108270185004000]

The structures of (dimethylaminopropyl)phenothiazine drugs and their metabolites. III. Monode-N-methylchlorpromazine sulphoxide, C16H17ClN2OS, at 120 K

E. Hough, E. Wold and S. G. Dahl



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Acta Cryst. (1985). C41, 389-392    [doi:10.1107/S0108270185004012]

Structure of 4:1 sulfuric acid-N,N'-(p-phenylene)dibenzamide complex, C20H16N2O2.4H2SO4

J. C. Calabrese and K. H. Gardner



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Acta Cryst. (1985). C41, 392-394    [doi:10.1107/S0108270185004024]

Isobaimonidine, C27H45NO3: a new alkaloid from Fritillaria imperialis L.

V. Kettmann, F. Pavelcík, I. Masterová and J. Tomko



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Acta Cryst. (1985). C41, 395-397    [doi:10.1107/S0108270185004036]

Hygrophylline, C18H27NO6: a pyrrolizidine alkaloid

M. F. Mackay, P. Mitrprachachon and C. C. J. Culvenor



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Acta Cryst. (1985). C41, 397-400    [doi:10.1107/S0108270185004048]

Structure of the [beta] form of 2,4,6-triphenyl-1,3,5-trithiane, C21H18S3

K. Sekido and S. Hirokawa



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Acta Cryst. (1985). C41, 400-404    [doi:10.1107/S010827018500405X]

Structure of N-[1'(9-adenyl)-[beta]-D-ribofuranuronosyl]-L-phenylalanine water ethanol (1/0.5/0.25), C19H20N6O6.0.5H2O.0.25C2H6O

F. Takusagawa, H. M. Berman, M. Dabrow and R. K. Robins



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Acta Cryst. (1985). C41, 404-406    [doi:10.1107/S0108270185004061]

6,6,8-Trinitropentacyclo[5.3.0.02,5.03,9.04,8]decane, C10H9N3O6

H. L. Ammon, D. Zhang, C. S. Choi, O. Sandus, A. P. Marchand and S. C. Suri



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Acta Cryst. (1985). C41, 406-409    [doi:10.1107/S0108270185004073]

Structure of 7,12-diphenyl-4a,12-dihydroindeno[7a,1-b]naphthalene, C29H22

Mazhar-ul-Haque, J. Ahmed and W. Horne



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Acta Cryst. (1985). C41, 409-411    [doi:10.1107/S0108270185004085]

Structure of 2-[hydroxy(methoxycarbonyl)methyl]-2-methoxycarbonyl-4,6-dimethyl-1-phenyl-1,2-dihydropyrimidinium picrate, C17H21N2O5+.C6H2N3O7-

E. Gutiérrez-Puebla, A. Monge, C. Ruiz-Valero and A. Rodríguez-Roldán



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Acta Cryst. (1985). C41, 411-413    [doi:10.1107/S0108270185004097]

Structure of diethyl 1,4-dihydro-2,4,6-trimethyl-3,5-pyridinedicarboxylate, C14H21NO4

S. Fortier, M. E. Fraser, N. J. Moore, Y. S. Park, R. A. Whitney and G. S. Marks



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Acta Cryst. (1985). C41, 413-415    [doi:10.1107/S0108270185004103]

Structure of 2-(o-ammoniobenzyl)-3-(3-indolyl)-1H-quinolinium bis(ethanesulfonate), C24H21N32+.2C2H5SO3-

V. Cody



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Acta Cryst. (1985). C41, 415-417    [doi:10.1107/S0108270185004115]

Structures of 3,8-dihydroxy-3-methyl-3,4-dihydroisocoumarin (I), C10H10O4, and 2-acetonyl-6-methoxybenzoic acid (II), C11H12O4

K.-I. Kawai, H. Ito, H. Nagase, R. Yamaguchi and S. Nakajima



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Acta Cryst. (1985). C41, 417-419    [doi:10.1107/S0108270185004127]

Structure and conformation of two diastereomers of (±)-1-(2,3-dichlorophenyl)-3,5,6,7-tetrahydro-3-hydroxy-3,6,6-trimethyl-1H-indole-2,4-dione, C17H17Cl2NO3

K. Go, G. Kartha and N. Viswanathan



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Acta Cryst. (1985). C41, 420-426    [doi:10.1107/S0108270185004139]

Structural studies of the system trans-stilbene/trans-azobenzene. III. The structures of three mixed crystals of trans-azobenzene/trans-stilbene; determinations by X-ray and neutron diffraction

J. A. Bouwstra, A. Schouten, J. Kroon and R. B. Helmholdt



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Acta Cryst. (1985). C41, 426-427    [doi:10.1107/S0108270185004140]

cis-6,11,17,18-Tetrahydro-5,12-dioxatribenzo[a,e,i]cyclododecene-17,18-diol, C22H20O4

F. R. Fronczek, S. J. Jungk and R. D. Gandour



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Acta Cryst. (1985). C41, 428-431    [doi:10.1107/S0108270185004152]

Structure of the aromatic glutarimide antibiotic actiphenol, 4-[2-(2-hydroxy-3,5-dimethylphenyl)-2-oxoethyl]-2,6-piperidinedione, C15H17NO4

K. D. Onan, H. S. P. Rao and R. J. Parry



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Acta Cryst. (1985). C41, 431-433    [doi:10.1107/S0108270185004164]

2,3:5,6-Di-O-isopropylidene-[alpha]-D-mannofuranose, C12H20O6

B. Sheldrick, W. Mackie and D. Akrigg



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Acta Cryst. (1985). C41, 433-436    [doi:10.1107/S0108270185004176]

Structure of a diterpene from the Austroeupatorium inulaefolia (HBK) K et R: 2,18-diacetoxy-15,16-epoxy-3-hydroxy-12-oxo-19-norlabdane-8(17),13(16),14-triene monohydrate, C23H30O7.H2O

A. Mosquera, A. V. Rivera, E. Rodulfo de Gil and A. Bahsas



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Acta Cryst. (1985). C41, 436-439    [doi:10.1107/S0108270185004188]

(E,E)-8-Acetoxygermacra-1(10),4-dien-6,12-olide, C17H22O4

I. Vickovic, W. H. Watson, M. Silva, M. E. Garvez and M. Hoeneisen



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Acta Cryst. (1985). C41, 439-441    [doi:10.1107/S010827018500419X]

9[alpha]-Bromo-16[alpha]-methylprednisolone (I), C22H29BrO5, and 9[alpha]-bromoprednisolone (II), C21H27BrO5

J. Iball, J. N. Low, R. J. Nash and B. P. Thompson



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Acta Cryst. (1985). C41, 441-443    [doi:10.1107/S0108270185004206]

Anthranilic acid, C7H7NO2, by neutron diffraction

C. J. Brown and M. Ehrenberg



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Acta Cryst. (1985). C41, 443-446    [doi:10.1107/S0108270185004218]

Refinement of 4-methyl-5-sulfosalicylic acid tetrahydrate, C8H8O6S.4H2O

T. Gustafsson



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Acta Cryst. (1985). C41, 446-450    [doi:10.1107/S010827018500422X]

Structures of five [alpha]-cyclohexylacetophenones, XC6H4COCH2C6H11

S. Ariel and J. Trotter



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Acta Cryst. (1985). C41, 450-453    [doi:10.1107/S0108270185004231]

Effect of metal ions in organic synthesis. XXVI. Structure of methyl 1-(3-chlorobenzoylamino)-4-diethylaminocarbonyl-2,5-dimethyl-1H-pyrrole-3-carboxylate, C20H24ClN3O4

G. Giuseppetti, C. Tadini, O. Attanasi, M. Grossi and F. Serra-Zanetti



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Acta Cryst. (1985). C41, 453-456    [doi:10.1107/S0108270185004243]

Structure of 2-amino-3-phosphonopropionic acid, C3H8NO5P

W. Sawka-Dobrowolska, T. Glowiak, Z. Siatecki and M. Soroka



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Acta Cryst. (1985). C41, 456-458    [doi:10.1107/S0108270185004255]

Methyl 3-phenyl-4a,7,8,8a-tetrahydropyrido[4,3-e][1,4,2]dioxazine-7-carboxylate, C14H14N2O4

R. G. Ball, E. E. Knaus and S. K. Dubey



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Acta Cryst. (1985). C41, 458-460    [doi:10.1107/S0108270185004267]

15,30-Dihydroxy-12,27-dimethyl-5,20-dioxa-2,8,17,23-tetrathia[9.9]metacyclophane ([beta] form), C26H36O4S4, and 15-hydroxy-12-methyl-5-oxa-2,8-dithia[9]metacyclophane, C13H18O2S2

M. Cannas, G. Marongiu and G. Navarra



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Acta Cryst. (1985). C41, 461-463    [doi:10.1107/S0108270185004279]

Structure of 2-(p-bromophenoxy)-N-ethyl-2-phenyl-N-(p-tolyl)ethanesulfonamide, C23H24BrNO3S

K. Sekido, Y. Yokomori, S. Hirokawa, K. Okuma and H. Ohta



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Acta Cryst. (1985). C41, 463-465    [doi:10.1107/S0108270185004280]

Structure of 2-[5'-aminocyclohexanespiro-4'-(4'H-imidazol)-2'-yl]-1-methylpyridinium iodide, C14H19N4+.I-

P. Rubio, F. Florencio and S. García-Blanco



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Acta Cryst. (1985). C41, 465-468    [doi:10.1107/S0108270185004292]

Structure of a 1/1 complex of 3',5'-di-O-acetyl-5-bromo-2'-deoxyuridine and 3',5'-di-O-acetyl-5-iodo-2'-deoxyuridine, C13H15Br0.5I0.5N2O7

C. C. Wilson and P. Tollin



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Acta Cryst. (1985). C41, 468-470    [doi:10.1107/S0108270185004309]

Absolute configuration of (-)-cis-2-ethylcyclohexanamine hydrochloride 0.39-ethanol solvate, C8H18N+.Cl-.0.39C2H6O

G. Knupp, A. W. Frahm, A. Kirfel, T. Fröhlich and G. Will



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Acta Cryst. (1985). C41, 470-472    [doi:10.1107/S0108270185004310]

[alpha]-Fluoro-trans-cinnamoyl peroxide, C18H12F2O4

D. Bethell, D. J. Chadwick, M. M. Harding, G. Q. Maling and M. D. Wiley



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Acta Cryst. (1985). C41, 472-474    [doi:10.1107/S0108270185004322]

Structure of 4-oxopyrido[1,2-a]pyrimidin-1-ium-2-olate, C8H6N2O2

N. Thorup and O. Simonsen



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Acta Cryst. (1985). C41, 474-476    [doi:10.1107/S0108270185004334]

3-Ethoxy-5,6,7,8-tetrahydro-1-hydroxyisoquinoline-4-carbonitrile, C12H14N2O2

S. Salisi, J. L. Briansó, X. Solans and M. Font-Altaba



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Acta Cryst. (1985). C41, 476-479    [doi:10.1107/S0108270185004346]

sym-Triphenylcyclopropenylium hexabromotellurate(IV), (C21H15)2[TeBr6]

B. A. Borgias, R. C. Scarrow, M. D. Seidler and W. P. Weiner



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Acta Cryst. (1985). C41, 479-483    [doi:10.1107/S0108270185004358]

Structure of the [beta] phase of 4-aminopyridinium hemiperchlorate, [H(C5H6N2)2]ClO4

P. Teulon, R. G. Delaplane, I. Olovsson and J. Rozière



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Acta Cryst. (1985). C41, 483-485    [doi:10.1107/S010827018500436X]

Azinobis(ethylidyne-p-phenylene) dipropionate, C22H24N2O4

M. R. Ciajolo, A. Sirigu and A. Tuzi



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Acta Cryst. (1985). C41, 485-487    [doi:10.1107/S0108270185004371]

Stereochemical studies of oligomers. XV. Structure of 2-methyl-1,4-butanediyl dibenzoate, C19H20O4

G. Bocelli, F. Ugozzoli and M. F. Grenier-Loustalot



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Acta Cryst. (1985). C41, 487-490    [doi:10.1107/S0108270185004383]

Structure and absolute configuration of euphoscopin A p-bromobenzoate, C38H43BrO9, and euphornin acetal p-bromobenzoate, C37H45BrO7

S. Ohba, M. Ito, Y. Saito, Y. Shizuri, S. Kosemura, J. Ohtsuka and S. Yamamura


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