Acta Crystallographica Section C

Crystal Structure Communications

Volume 41, Part 5 (May 1985)



research papers


inorganic compounds



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Acta Cryst. (1985). C41, 633-636    [doi:10.1107/S0108270185004917]

Structure of pentaammineaquacobalt(III) hexacyanochromate(III), [Co(NH3)5(H2O)][Cr(CN)6], by time-of-flight neutron diffraction at 11.5 K

B. N. Figgis, P. C. W. Leung and A. J. Schultz



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Acta Cryst. (1985). C41, 636-638    [doi:10.1107/S0108270185004929]

Lanthanum thallium bis(sulphate) dihydrate, TlLa(SO4)2.2H2O

V. Kaucic, N. Bukovec and Lj. Golic



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Acta Cryst. (1985). C41, 638-641    [doi:10.1107/S0108270185004930]

Location and anisotropic refinement of hydrogen atoms in disodium dihydrogensilicate tetrahydrate, Na2H2SiO4.4H2O, by neutron diffraction; hydrogen bonding at 173 K

R. L. Schmid, J. Felsche and G. J. McIntyre



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Acta Cryst. (1985). C41, 642-645    [doi:10.1107/S0108270185004942]

Hexapotassium (cyclo-octahydroxotetracosaoxohexadecarborato)dioxouranate(VI) dodecahydrate, K6[UO2{B16O24(OH)8}].12H2O

H. Behm



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Acta Cryst. (1985). C41, 645-647    [doi:10.1107/S0108270185004954]

Structure du tétrathiophosphate(V) de zinc et d'argent, ZnAgPS4

P. Toffoli, J. C. Rouland, P. Khodadad et N. Rodier



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Acta Cryst. (1985). C41, 647-649    [doi:10.1107/S0108270185004966]

Pentapotassium trivanadate, K5V3O10

K. Kato and E. Takayama-Muromachi



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Acta Cryst. (1985). C41, 649-651    [doi:10.1107/S0108270185004978]

Structure de l'oxysulfure de lanthane et d'étain (LaO)4Sn2S6

S. Bénazeth, M. Guittard et P. Laruelle



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Acta Cryst. (1985). C41, 652-654    [doi:10.1107/S010827018500498X]

Structure of calcium selenite(IV) monohydrate, CaSeO3.H2O

J. Valkonen, T. Losoi and A. Pajunen



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Acta Cryst. (1985). C41, 654-657    [doi:10.1107/S0108270185004991]

Structure de la roubaultite, Cu2(UO2)3(CO3)2O2(OH)2.4H2O

D. Ginderow and F. Cesbron



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Acta Cryst. (1985). C41, 657-660    [doi:10.1107/S0108270185005005]

Room-temperature structure of ammonium tetrafluoroferrate(III), NH4[FeF4]

M. Leblanc, G. Ferey, R. De Pape and J. Teillet



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Acta Cryst. (1985). C41, 660-663    [doi:10.1107/S0108270185005017]

Verfeinerung der Kristallstruktur des ammoniumtriiodids, NH4I3

K.-F. Tebbe, B. Freckmann, M. Hörner, W. Hiller und J. Strähle



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Acta Cryst. (1985). C41, 663-665    [doi:10.1107/S0108270185005029]

Structure of iron diniobium hexaoxide, FeNb2O6: an example of metal-disordered trirutile structure

A. Aruga, E. Tokizaki, I. Nakai and Y. Sugitani



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Acta Cryst. (1985). C41, 665-667    [doi:10.1107/S0108270185005030]

Structure of a new form of rubidium dihydrogenphosphate, RbH2PO4

M. T. Averbuch-Pouchot and A. Durif



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Acta Cryst. (1985). C41, 667-668    [doi:10.1107/S0108270185005042]

Structure du tétrasulfure de dierbium(III) et d'europium(II), EuEr2S4

P. Lemoine, D. Carré et M. Guittard


metal-organic compounds



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Acta Cryst. (1985). C41, 669-671    [doi:10.1107/S0108270185005054]

Structure of tri(2H)aqua(N-methyliminodiacetato)nickel(II) (2H)monohydrate, [Ni(C5H7NO4)(D2O)3].D2O

M. R. Wagner and D. B. Beach



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Acta Cryst. (1985). C41, 671-673    [doi:10.1107/S0108270185005066]

Redetermination of the structure of [mu]-oxo-bis[(5,10,15,20-tetraphenylporphyrinato)iron(III)] at 122K, [Fe2O(C44H28N4)2]

P. N. Swepston and J. A. Ibers



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Acta Cryst. (1985). C41, 673-678    [doi:10.1107/S0108270185005078]

The structures and solid-state and solution 113Cd NMR of diaquabis(p-chlorobenzoato)cadmium(II), [Cd(C7H4ClO2)2(H2O)2] (A), diaquabis(p-nitrobenzoato)cadmium(II), [Cd(C7H4NO4)2(H2O)2] (B), and aquabis(p-chlorobenzoato)bis(pyridine)cadmium(II), [Cd(C7H4ClO2)2(C5H5N)2(H2O)] (C)

P. F. Rodesiler, E. A. H. Griffith, N. G. Charles and E. L. Amma



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Acta Cryst. (1985). C41, 678-681    [doi:10.1107/S010827018500508X]

Dihydrogen (±)-trans-1,2-cyclohexanediaminetetraacetic acid tetrachloropalladate(II) and tetrachloroplatinate(II) pentahydrates, [C14H24N2O8][PdCl4].5H2O and [C14H24N2O8][PtCl4].5H2O

E. N. Duesler, R. E. Tapscott, M. Garcia-Basallote and F. Gonzalez-Vílchez



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Acta Cryst. (1985). C41, 681-683    [doi:10.1107/S0108270185005091]

Structure of trans-diaquabis(oxalato)vanadate(III) complexes: A[V(C2O4)2(H2O)2].xH2O, A = Cs (x = 4) and A = CH3NH3 (x = 4.5)

I. E. Grey, I. C. Madsen, K. Sirat and P. W. Smith



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Acta Cryst. (1985). C41, 684-686    [doi:10.1107/S0108270185005108]

Structure of cis-bis(acetonitrile)bis(2,2'-bipyridine)ruthenium(II) hexafluorophosphate, [Ru(C2H3N)2(C10H8N2)2](PF6)2

M. J. Heeg, R. Kroener and E. Deutsch



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Acta Cryst. (1985). C41, 686-688    [doi:10.1107/S010827018500511X]

Solid-state structure of ferrocenecarboxylic acid, [Fe(C5H4CO2H)(C5H5)]

F. A. Cotton and A. H. Reid Jnr



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Acta Cryst. (1985). C41, 688-690    [doi:10.1107/S0108270185005121]

Structure of the 2/1 complex dibenzotetrathiafulvalenium hexabromodicuprate(II), 2C14H8S4+.Cu2Br62-

M. Honda, C. Katayama, J. Tanaka and M. Tanaka



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Acta Cryst. (1985). C41, 690-693    [doi:10.1107/S0108270185005133]

Structures of [alpha]- and [beta]-copper(II) pipecolinate dihydrate, diaquabis(2-piperidinecarboxylato)copper(II), [Cu(C6H10NO2)2(H2O)2]

H. M. Haendler



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Acta Cryst. (1985). C41, 693-695    [doi:10.1107/S0108270185005145]

Calcium D-glucarate tetrahydrate Ca2+.C6H8O82-.4H2O: a redetermination

C. Burden, W. Mackie and B. Sheldrick



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Acta Cryst. (1985). C41, 695-697    [doi:10.1107/S0108270185005157]

Structure of trans-dichlorobis[3,4,5,6-tetrafluoro-o-phenylenebis(dimethylphosphine)]iron(III) tetrafluoroborate, [FeCl2(C10H12F4P2)2]BF4

S. J. Higgins, H. C. Jewiss, W. Levason and M. Webster



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Acta Cryst. (1985). C41, 698-699    [doi:10.1107/S0108270185005169]

Structure of dichlorotris(triphenylphosphine)osmium(II), [OsCl2{P(C6H5)3}3]

A. R. Chakravarty, F. A. Cotton and D. A. Tocher



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Acta Cryst. (1985). C41, 700-702    [doi:10.1107/S0108270185005170]

Structure of tetrachlorobis(dimethyl sulphoxide)tin(IV), [SnCl4(C2H6OS)2]

J. M. Kisenyi, G. R. Willey and M. G. B. Drew



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Acta Cryst. (1985). C41, 702-703    [doi:10.1107/S0108270185005182]

Structure du chlorure de trans-diamminechloro(diméthylsulfoxyde)platine(II), [PtCl(NH3)2(C2H6OS)]Cl

J.-M. Delafontaine, P. Khodadad, P. Toffoli et N. Rodier



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Acta Cryst. (1985). C41, 704-706    [doi:10.1107/S0108270185005194]

Structure of trans-carbonylchlorobis(methyldiphenylphosphine)rhodium(I), [RhCl(CO){PCH3(C6H5)2}2]

F. Dahan and R. Choukroun



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Acta Cryst. (1985). C41, 706-709    [doi:10.1107/S0108270185005200]

Structure de (diméthyl-5,5 diphényl-1,9 tétraaza-3,4,6,7 nonatétraène-1,3,6,8 diolato-1,9-O,O',N,N')nickel(II), [Ni(C19H18N4O2)]

F. Abraham, J. M. Capon, G. Nowogrocki, S. Sueur et C. Brémard



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Acta Cryst. (1985). C41, 709-712    [doi:10.1107/S0108270185005212]

Structure of 1,3-(1,1'-ruthenocenediyl)-1-propanone, [Ru(C13H12O)], and 1,3-[1,1'-(3,4-trimethyleneruthenocenediyl)]propane, [Ru(C16H18)]

S. Ohba, Y. Saito, T. Ishii, S. Kamiyama and A. Kasahara



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Acta Cryst. (1985). C41, 712-715    [doi:10.1107/S0108270185005224]

Structure d'un complexe du nickel(II) avec l'aminoacétohydroxamate monosodique, Na[Ni(C2H4N2O2)(C2H5N2O2)].3H2O

M. Julien-Pouzol, S. Jaulmes, P. Laruelle, S. Carvalho et E. D. Paniago



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Acta Cryst. (1985). C41, 716-718    [doi:10.1107/S0108270185005236]

[(2-3)Pentaboran(9)yl](triphenylphosphine)gold(I), [Au(B5H8)(C18H15P)]

N. W. Alcock, L. Parkhill and M. G. H. Wallbridge



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Acta Cryst. (1985). C41, 718-720    [doi:10.1107/S0108270185005248]

Bis[N1-(2-pyrimidinyl)sulphanilamido]zinc-ammonia (1/2), [Zn(C10H9N4O2S)2].2NH3

C. J. Brown, D. S. Cook and L. Sengier


organic compounds



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Acta Cryst. (1985). C41, 720-722    [doi:10.1107/S010827018500525X]

The structure of 3,5-di-O-benzoyl-1,2-dideoxy-1-phenyl-[beta]-D-ribofuranose, C25H22O5

J. Gunning, S. Neidle, T. A. Millican, M. A. W. Eaton, G. A. Mock and J. Mann



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Acta Cryst. (1985). C41, 722-725    [doi:10.1107/S0108270185005261]

Supinine, C15H25NO4, and heleurine, C16H27NO4, pyrrolizidine alkaloids

M. F. Mackay, P. Mitrprachachon, P. J. Oliver and C. C. J. Culvenor



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Acta Cryst. (1985). C41, 726-728    [doi:10.1107/S0108270185005273]

Crystal structure and molecular conformation of 2-deamino-L-cystine, C6H11NO4S2, a mixed disulfide

M. Rajeswaran and R. Parthasarathy



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Acta Cryst. (1985). C41, 728-731    [doi:10.1107/S0108270185005285]

The structure of phyllanthose hexaacetate, C24H34O15

L. R. Nassimbeni, M. L. Niven, G. M. Cragg and G. R. Pettit



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Acta Cryst. (1985). C41, 732-734    [doi:10.1107/S0108270185005297]

Structure of 1,2,5-trihydroxy-2,5-dimethylphospholane 1-oxide, C6H13O4P

Z. Galdecki, T. J. Bartczak, W. M. Wolf, H. Krawczyk and P. Majewski



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Acta Cryst. (1985). C41, 734-736    [doi:10.1107/S0108270185005303]

Structure of 1-methylhydrazinium trifluoroacetate, CH7N2+.C2F3O2-

V. E. Shklover and Yu. T. Struchkov



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Acta Cryst. (1985). C41, 736-739    [doi:10.1107/S0108270185005315]

Détermination structurale à 205 K du monomère bis[(o-méthoxyphényl)carbamate] de hexadiyne-2,4 diyle-1,6, C22H20N2O6

A. Whuler, M.-C. Sichère, P. Spinat et C. Brouty



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Acta Cryst. (1985). C41, 739-741    [doi:10.1107/S0108270185005327]

9[alpha],10[alpha]-Epoxy-5-methyl-19-nor-5[beta]-cholest-1-ene-3,6-dione, C27H40O3

J. M. Coxon, P. D. Quaid and P. J. Steel



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Acta Cryst. (1985). C41, 741-743    [doi:10.1107/S0108270185005339]

Structure of 1,4-dinitrosopiperazine, C4H8N4O2

K. Sekido, K. Okamoto and S. Hirokawa



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Acta Cryst. (1985). C41, 743-746    [doi:10.1107/S0108270185005340]

Structure of 2-[(hydroxyimino)(phenylthio)methyl]-1-methylpyridinium chloride, C13H13N2OS+.Cl-

B. J. Oleksyn and K. M. Stadnicka



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Acta Cryst. (1985). C41, 746-749    [doi:10.1107/S0108270185005352]

Absolute structure of (+)-8[alpha]-acetoxy-12-(4-bromobenzoyloxy)-13,14,15,16-tetranorlabdane, C25H35BrO4 (I), and structure of (-)-8[alpha],12-dihydroxy-13,14,15,16-tetranor-9-epilabdane, C16H30O2 (II)

G. Bernardinelli and W. Giersch



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Acta Cryst. (1985). C41, 749-752    [doi:10.1107/S0108270185005364]

Structure of the hydrogen oxalate of formamide oxime, CH5N2O+.C2HO4-, at 105 K

I. K. Larsen



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Acta Cryst. (1985). C41, 752-755    [doi:10.1107/S0108270185005376]

Structure of N1-(2,6-dimethyl-4-pyrimidinyl)sulphanilamide (sulfisomidine), C12H14N4O2S

T. P. Singh, R. K. Tiwari and M. Singh



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Acta Cryst. (1985). C41, 755-758    [doi:10.1107/S0108270185005388]

Structure of (7S)-N-acetyldemecolcine, C23H27NO6

J. V. Silverton, P. N. Sharma and A. Brossi



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Acta Cryst. (1985). C41, 758-760    [doi:10.1107/S010827018500539X]

Structure of 4-amino-2-thioxo-6-pyrimidinone monohydrate, C4H5N3OS.H2O

E. S. Raper, R. E. Oughtred and I. W. Nowell



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Acta Cryst. (1985). C41, 760-763    [doi:10.1107/S0108270185005406]

Structure of modification I of cortisone acetate, 21-acetoxy-17[alpha]-hydroxy-4-pregnene-3,11,20-trione, C23H30O6

J. A. Kanters, A. de Koster, V. J. van Geerestein and L. A. van Dijck



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Acta Cryst. (1985). C41, 763-766    [doi:10.1107/S0108270185005418]

11[beta]-Hydroxy-16[alpha],17[alpha],21-trimethyl-5[alpha]-pregna-1,4-diene-3,20-dione (I), C24H34O3, and 11[beta],17[alpha]-dihydroxy-21-methyl-5[alpha]-pregn-4-en-3,20-dione 17-butyrate (II), C26H38O5

J. C. Barnes, J. D. Paton, R. T. Logan and J. Redpath



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Acta Cryst. (1985). C41, 767-769    [doi:10.1107/S010827018500542X]

The structure of 1,3-dihydro-4-[(2S)-2,5-dihydro-2-furyl]-3-methyl-1-p-tolyl-2H-imidazole-2-thione, C15H16N2OS

E. Moreno, A. López-Castro and R. Márquez



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Acta Cryst. (1985). C41, 769-771    [doi:10.1107/S0108270185005431]

Structure of (E)-3-(2-methoxyphenyl)-1-phenyl-3-(1H-1,2,4-triazol-1-yl)-2-propen-1-one, C18H15N3O2

S. K. Branch and I. W. Nowell



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Acta Cryst. (1985). C41, 771-773    [doi:10.1107/S0108270185005443]

(1R,2R,3R,6S,10R)-1-Fluoro-3-(2-hydroxy-2-propyl)-6,10-dimethylbicyclo[4.4.0]decan-2-ol, C15H27FO2

R. G. Pritchard, R. Ramage and I. A. Southwell



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Acta Cryst. (1985). C41, 773-775    [doi:10.1107/S0108270185005455]

Structure of [2.2.2.2]paracyclophane, C32H32

A. Renault and C. Cohen-Addad



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Acta Cryst. (1985). C41, 775-778    [doi:10.1107/S0108270185005467]

Structures du N1-(méthoxy-6 méthyl-2 pyrimidinyl-4)sulfanilamide (sulfamétomidine), C12H14N4O3S, et d'un de ses solvates, C12H14N4O3S.H2O

J. Rambaud, L. Maury, B. Pauvert, G. Berge, M. Audran, Y. Lasserre et J.-P. Declercq



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Acta Cryst. (1985). C41, 778-780    [doi:10.1107/S0108270185005479]

Structure of pentathia[9]heterohelicene, C28H12S5

H. Nakagawa, H. Nagashima, K. Yamada and H. Kawazura



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Acta Cryst. (1985). C41, 781-783    [doi:10.1107/S0108270185005480]

[alpha]-(Hydroxy-3 oxo-5 phényl-4 2H-furylidène-2)-phénylacétate de méthyle, acide vulpinique, C19H14O5

C. Brassy, B. Bachet, L. Molho et D. Molho



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Acta Cryst. (1985). C41, 783-785    [doi:10.1107/S0108270185005492]

Structure of acetanilide (C8H9NO) at 113 K

H. J. Wasserman, R. R. Ryan and S. P. Layne



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Acta Cryst. (1985). C41, 785-788    [doi:10.1107/S0108270185005509]

Synthesis and structure of (E)-3-fluoro-4-pyridinecarbaldehyde oxime, C6H5FN2O, and conversion to its quaternary methyl iodide derivative

J. M. Sorof, H. L. Carrell, J. P. Glusker, J. McLick and E. Kun



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Acta Cryst. (1985). C41, 788-791    [doi:10.1107/S0108270185005510]

Structure of 6,6,10,10-tetranitropentacyclo[5.3.0.02,5.03,9.04,8]decane, C10H8N4O8

C. George, R. Gilardi, J. L. Flippen-Anderson, C. S. Choi, A. P. Marchand and D. S. Reddy



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Acta Cryst. (1985). C41, 791-793    [doi:10.1107/S0108270185005522]

Acétoxy-4 tert-butyl-2 cyclohexène-3 carboxylate-1 de méthyle-cis, C14H22O4

R. Viani, J. Lapasset et J.-P. Aycard



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Acta Cryst. (1985). C41, 793-795    [doi:10.1107/S0108270185005534]

Hexahydro-4b,6,7,8,9,9a 5H-benzo[3,4]cyclobuta[1,2]cyclohepténol-1-cis, C13H16O

A. Courtois, V. Pesme-Pichon, M. C. Carré et P. Caubère



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Acta Cryst. (1985). C41, 796-798    [doi:10.1107/S0108270185005546]

Structure of 7,8,17,18-tetrahydro-10,20-diphenyl-5,9,15,19-tetraazadibenzo[ai]cyclohexadecene-6,16(5H,15H)-dione, C32H28N4O2

A. A. Dvorkin, T. I. Malinowsky, Yu. A. Simonov, S. A. Andronati, A. V. Kuzmina and A. S. Yavorsky



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Acta Cryst. (1985). C41, 798-802    [doi:10.1107/S0108270185005558]

Structure of gentiopicrin hemihydrate: (-)-(5R,6S)-5-ethenyl-6-([beta]-D-glucopyranosyloxy)-5,6-dihydro-1H,3H-pyrano[3,4-c]pyran-1-one hemihydrate, C16H20O9.1/2H2O

B. Kojic-Prodic, A. L. Spek, W. G. van der Sluis and R. P. Labadie



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Acta Cryst. (1985). C41, 802-804    [doi:10.1107/S010827018500556X]

Structure of 3-acetyl-4-hydroxy-6-phenyl-2-pyrone, C13H10O4

V. G. Thailambal and V. Pattabhi


short communications



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Acta Cryst. (1985). C41, 804-805    [doi:10.1107/S0108270185005571]

Nouvelle description du tétrafluorure de neptunium hydraté, Np3F12.H2O

A. Cousson et M. Gasperin



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Acta Cryst. (1985). C41, 806    [doi:10.1107/S0108270185005583]

Structure of 25-ethoxycarbonyl-2,3,7,8,12,13,17,18-octaethyl-21,22-methano-21H,22H-porphyrin hydrobromide, C40H51N4O2+.Br-. The first example of a cis-N,N-bridged porphyrin. Erratum

T. J. Bartczak



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Acta Cryst. (1985). C41, 806    [doi:10.1107/S0108270185005595]

trans-Azido(dimethylglyoximato-N,N')(dimethylglyoxime-N,N')(pyridine)cobalt(III): addition

S. V. Evans, M. N. Ponnuswamy and J. Trotter


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