Acta Crystallographica Section C

Crystal Structure Communications

Volume 41, Part 5 (May 1985)

• research papers
  • inorganic compounds
  • metal-organic compounds
  • organic compounds
• short communications

research papers

inorganic compounds

Acta Cryst. (1985). C41, 633-636    [doi:10.1107/S0108270185004917]

Structure of pentaammineaquacobalt(III) hexacyanochromate(III), [Co(NH₃)₅(H₂O)][Cr(CN)₆], by time-of-flight neutron diffraction at 11.5 K

B. N. Figgis, P. C. W. Leung and A. J. Schultz

Acta Cryst. (1985). C41, 636-638    [doi:10.1107/S0108270185004929]

Lanthanum thallium bis(sulphate) dihydrate, TlLa(SO₄)₂.2H₂O

V. Kaucic, N. Bukovec and Lj. Golic

Acta Cryst. (1985). C41, 638-641    [doi:10.1107/S0108270185004930]

Location and anisotropic refinement of hydrogen atoms in disodium dihydrogensilicate tetrahydrate, Na₂H₂SiO₄.4H₂O, by neutron diffraction; hydrogen bonding at 173 K

R. L. Schmid, J. Felsche and G. J. McIntyre

Acta Cryst. (1985). C41, 642-645    [doi:10.1107/S0108270185004942]

Hexapotassium (cyclo-octahydroxotetracosaoxohexadecarborato)dioxouranate(VI) dodecahydrate, K₆[UO₂{B₁₆O₂₄(OH)₈}].12H₂O

H. Behm

Acta Cryst. (1985). C41, 645-647    [doi:10.1107/S0108270185004954]

Structure du tétrathiophosphate(V) de zinc et d'argent, ZnAgPS₄

P. Toffoli, J. C. Rouland, P. Khodadad et N. Rodier

Acta Cryst. (1985). C41, 647-649    [doi:10.1107/S0108270185004966]

Pentapotassium trivanadate, K₅V₃O₁₀

K. Kato and E. Takayama-Muromachi

Acta Cryst. (1985). C41, 649-651    [doi:10.1107/S0108270185004978]

Structure de l'oxysulfure de lanthane et d'étain (LaO)₄Sn₂S₆

S. Bénazeth, M. Guittard et P. Laruelle

Acta Cryst. (1985). C41, 652-654    [doi:10.1107/S010827018500498X]

Structure of calcium selenite(IV) monohydrate, CaSeO₃.H₂O

J. Valkonen, T. Losoi and A. Pajunen

Acta Cryst. (1985). C41, 654-657    [doi:10.1107/S0108270185004991]

Structure de la roubaultite, Cu₂(UO₂)₃(CO₃)₂O₂(OH)₂.4H₂O

D. Ginderow and F. Cesbron

Acta Cryst. (1985). C41, 657-660    [doi:10.1107/S0108270185005005]

Room-temperature structure of ammonium tetrafluoroferrate(III), NH₄[FeF₄]

M. Leblanc, G. Ferey, R. De Pape and J. Teillet

Acta Cryst. (1985). C41, 660-663    [doi:10.1107/S0108270185005017]

Verfeinerung der Kristallstruktur des ammoniumtriiodids, NH₄I₃

K.-F. Tebbe, B. Freckmann, M. Hörner, W. Hiller und J. Strähle

Acta Cryst. (1985). C41, 663-665    [doi:10.1107/S0108270185005029]

Structure of iron diniobium hexaoxide, FeNb₂O₆: an example of metal-disordered trirutile structure

A. Aruga, E. Tokizaki, I. Nakai and Y. Sugitani

Acta Cryst. (1985). C41, 665-667    [doi:10.1107/S0108270185005030]

Structure of a new form of rubidium dihydrogenphosphate, RbH₂PO₄

M. T. Averbuch-Pouchot and A. Durif

Acta Cryst. (1985). C41, 667-668    [doi:10.1107/S0108270185005042]

Structure du tétrasulfure de dierbium(III) et d'europium(II), EuEr₂S₄

P. Lemoine, D. Carré et M. Guittard

metal-organic compounds

Acta Cryst. (1985). C41, 669-671    [doi:10.1107/S0108270185005054]

Structure of tri(²H)aqua(N-methyliminodiacetato)nickel(II) (²H)monohydrate, [Ni(C₅H₇NO₄)(D₂O)₃].D₂O

M. R. Wagner and D. B. Beach

Acta Cryst. (1985). C41, 671-673    [doi:10.1107/S0108270185005066]

Redetermination of the structure of -oxo-bis[(5,10,15,20-tetraphenylporphyrinato)iron(III)] at 122K, [Fe₂O(C₄₄H₂₈N₄)₂]

P. N. Swepston and J. A. Ibers

Acta Cryst. (1985). C41, 673-678    [doi:10.1107/S0108270185005078]

The structures and solid-state and solution ¹¹³Cd NMR of diaquabis(p-chlorobenzoato)cadmium(II), [Cd(C₇H₄ClO₂)₂(H₂O)₂] (A), diaquabis(p-nitrobenzoato)cadmium(II), [Cd(C₇H₄NO₄)₂(H₂O)₂] (B), and aquabis(p-chlorobenzoato)bis(pyridine)cadmium(II), [Cd(C₇H₄ClO₂)₂(C₅H₅N)₂(H₂O)] (C)

P. F. Rodesiler, E. A. H. Griffith, N. G. Charles and E. L. Amma

Acta Cryst. (1985). C41, 678-681    [doi:10.1107/S010827018500508X]

Dihydrogen (±)-trans-1,2-cyclohexanediaminetetraacetic acid tetrachloropalladate(II) and tetrachloroplatinate(II) pentahydrates, [C₁₄H₂₄N₂O₈][PdCl₄].5H₂O and [C₁₄H₂₄N₂O₈][PtCl₄].5H₂O

E. N. Duesler, R. E. Tapscott, M. Garcia-Basallote and F. Gonzalez-Vílchez

Acta Cryst. (1985). C41, 681-683    [doi:10.1107/S0108270185005091]

Structure of trans-diaquabis(oxalato)vanadate(III) complexes: A[V(C₂O₄)₂(H₂O)₂].xH₂O, A = Cs (x = 4) and A = CH₃NH₃ (x = 4.5)

I. E. Grey, I. C. Madsen, K. Sirat and P. W. Smith

Acta Cryst. (1985). C41, 684-686    [doi:10.1107/S0108270185005108]

Structure of cis-bis(acetonitrile)bis(2,2'-bipyridine)ruthenium(II) hexafluorophosphate, [Ru(C₂H₃N)₂(C₁₀H₈N₂)₂](PF₆)₂

M. J. Heeg, R. Kroener and E. Deutsch

Acta Cryst. (1985). C41, 686-688    [doi:10.1107/S010827018500511X]

Solid-state structure of ferrocenecarboxylic acid, [Fe(C₅H₄CO₂H)(C₅H₅)]

F. A. Cotton and A. H. Reid Jnr

Acta Cryst. (1985). C41, 688-690    [doi:10.1107/S0108270185005121]

Structure of the 2/1 complex dibenzotetrathiafulvalenium hexabromodicuprate(II), 2C₁₄H₈S₄⁺.Cu₂Br₆^2-

M. Honda, C. Katayama, J. Tanaka and M. Tanaka

Acta Cryst. (1985). C41, 690-693    [doi:10.1107/S0108270185005133]

Structures of - and -copper(II) pipecolinate dihydrate, diaquabis(2-piperidinecarboxylato)copper(II), [Cu(C₆H₁₀NO₂)₂(H₂O)₂]

H. M. Haendler

Acta Cryst. (1985). C41, 693-695    [doi:10.1107/S0108270185005145]

Calcium D-glucarate tetrahydrate Ca²⁺.C₆H₈O₈^2-.4H₂O: a redetermination

C. Burden, W. Mackie and B. Sheldrick

Acta Cryst. (1985). C41, 695-697    [doi:10.1107/S0108270185005157]

Structure of trans-dichlorobis[3,4,5,6-tetrafluoro-o-phenylenebis(dimethylphosphine)]iron(III) tetrafluoroborate, [FeCl₂(C₁₀H₁₂F₄P₂)₂]BF₄

S. J. Higgins, H. C. Jewiss, W. Levason and M. Webster

Acta Cryst. (1985). C41, 698-699    [doi:10.1107/S0108270185005169]

Structure of dichlorotris(triphenylphosphine)osmium(II), [OsCl₂{P(C₆H₅)₃}₃]

A. R. Chakravarty, F. A. Cotton and D. A. Tocher

Acta Cryst. (1985). C41, 700-702    [doi:10.1107/S0108270185005170]

Structure of tetrachlorobis(dimethyl sulphoxide)tin(IV), [SnCl₄(C₂H₆OS)₂]

J. M. Kisenyi, G. R. Willey and M. G. B. Drew

Acta Cryst. (1985). C41, 702-703    [doi:10.1107/S0108270185005182]

Structure du chlorure de trans-diamminechloro(diméthylsulfoxyde)platine(II), [PtCl(NH₃)₂(C₂H₆OS)]Cl

J.-M. Delafontaine, P. Khodadad, P. Toffoli et N. Rodier

Acta Cryst. (1985). C41, 704-706    [doi:10.1107/S0108270185005194]

Structure of trans-carbonylchlorobis(methyldiphenylphosphine)rhodium(I), [RhCl(CO){PCH₃(C₆H₅)₂}₂]

F. Dahan and R. Choukroun

Acta Cryst. (1985). C41, 706-709    [doi:10.1107/S0108270185005200]

Structure de (diméthyl-5,5 diphényl-1,9 tétraaza-3,4,6,7 nonatétraène-1,3,6,8 diolato-1,9-O,O',N,N')nickel(II), [Ni(C₁₉H₁₈N₄O₂)]

F. Abraham, J. M. Capon, G. Nowogrocki, S. Sueur et C. Brémard

Acta Cryst. (1985). C41, 709-712    [doi:10.1107/S0108270185005212]

Structure of 1,3-(1,1'-ruthenocenediyl)-1-propanone, [Ru(C₁₃H₁₂O)], and 1,3-[1,1'-(3,4-trimethyleneruthenocenediyl)]propane, [Ru(C₁₆H₁₈)]

S. Ohba, Y. Saito, T. Ishii, S. Kamiyama and A. Kasahara

Acta Cryst. (1985). C41, 712-715    [doi:10.1107/S0108270185005224]

Structure d'un complexe du nickel(II) avec l'aminoacétohydroxamate monosodique, Na[Ni(C₂H₄N₂O₂)(C₂H₅N₂O₂)].3H₂O

M. Julien-Pouzol, S. Jaulmes, P. Laruelle, S. Carvalho et E. D. Paniago

Acta Cryst. (1985). C41, 716-718    [doi:10.1107/S0108270185005236]

[(2-3)Pentaboran(9)yl](triphenylphosphine)gold(I), [Au(B₅H₈)(C₁₈H₁₅P)]

N. W. Alcock, L. Parkhill and M. G. H. Wallbridge

Acta Cryst. (1985). C41, 718-720    [doi:10.1107/S0108270185005248]

Bis[N¹-(2-pyrimidinyl)sulphanilamido]zinc-ammonia (1/2), [Zn(C₁₀H₉N₄O₂S)₂].2NH₃

C. J. Brown, D. S. Cook and L. Sengier

organic compounds

Acta Cryst. (1985). C41, 720-722    [doi:10.1107/S010827018500525X]

The structure of 3,5-di-O-benzoyl-1,2-dideoxy-1-phenyl--D-ribofuranose, C₂₅H₂₂O₅

J. Gunning, S. Neidle, T. A. Millican, M. A. W. Eaton, G. A. Mock and J. Mann

Acta Cryst. (1985). C41, 722-725    [doi:10.1107/S0108270185005261]

Supinine, C₁₅H₂₅NO₄, and heleurine, C₁₆H₂₇NO₄, pyrrolizidine alkaloids

M. F. Mackay, P. Mitrprachachon, P. J. Oliver and C. C. J. Culvenor

Acta Cryst. (1985). C41, 726-728    [doi:10.1107/S0108270185005273]

Crystal structure and molecular conformation of 2-deamino-L-cystine, C₆H₁₁NO₄S₂, a mixed disulfide

M. Rajeswaran and R. Parthasarathy

Acta Cryst. (1985). C41, 728-731    [doi:10.1107/S0108270185005285]

The structure of phyllanthose hexaacetate, C₂₄H₃₄O₁₅

L. R. Nassimbeni, M. L. Niven, G. M. Cragg and G. R. Pettit

Acta Cryst. (1985). C41, 732-734    [doi:10.1107/S0108270185005297]

Structure of 1,2,5-trihydroxy-2,5-dimethylphospholane 1-oxide, C₆H₁₃O₄P

Z. Galdecki, T. J. Bartczak, W. M. Wolf, H. Krawczyk and P. Majewski

Acta Cryst. (1985). C41, 734-736    [doi:10.1107/S0108270185005303]

Structure of 1-methylhydrazinium trifluoroacetate, CH₇N₂⁺.C₂F₃O₂^-

V. E. Shklover and Yu. T. Struchkov

Acta Cryst. (1985). C41, 736-739    [doi:10.1107/S0108270185005315]

Détermination structurale à 205 K du monomère bis[(o-méthoxyphényl)carbamate] de hexadiyne-2,4 diyle-1,6, C₂₂H₂₀N₂O₆

A. Whuler, M.-C. Sichère, P. Spinat et C. Brouty

Acta Cryst. (1985). C41, 739-741    [doi:10.1107/S0108270185005327]

9,10-Epoxy-5-methyl-19-nor-5-cholest-1-ene-3,6-dione, C₂₇H₄₀O₃

J. M. Coxon, P. D. Quaid and P. J. Steel

Acta Cryst. (1985). C41, 741-743    [doi:10.1107/S0108270185005339]

Structure of 1,4-dinitrosopiperazine, C₄H₈N₄O₂

K. Sekido, K. Okamoto and S. Hirokawa

Acta Cryst. (1985). C41, 743-746    [doi:10.1107/S0108270185005340]

Structure of 2-[(hydroxyimino)(phenylthio)methyl]-1-methylpyridinium chloride, C₁₃H₁₃N₂OS⁺.Cl^-

B. J. Oleksyn and K. M. Stadnicka

Acta Cryst. (1985). C41, 746-749    [doi:10.1107/S0108270185005352]

Absolute structure of (+)-8-acetoxy-12-(4-bromobenzoyloxy)-13,14,15,16-tetranorlabdane, C₂₅H₃₅BrO₄ (I), and structure of (-)-8,12-dihydroxy-13,14,15,16-tetranor-9-epilabdane, C₁₆H₃₀O₂ (II)

G. Bernardinelli and W. Giersch

Acta Cryst. (1985). C41, 749-752    [doi:10.1107/S0108270185005364]

Structure of the hydrogen oxalate of formamide oxime, CH₅N₂O⁺.C₂HO₄^-, at 105 K

I. K. Larsen

Acta Cryst. (1985). C41, 752-755    [doi:10.1107/S0108270185005376]

Structure of N¹-(2,6-dimethyl-4-pyrimidinyl)sulphanilamide (sulfisomidine), C₁₂H₁₄N₄O₂S

T. P. Singh, R. K. Tiwari and M. Singh

Acta Cryst. (1985). C41, 755-758    [doi:10.1107/S0108270185005388]

Structure of (7S)-N-acetyldemecolcine, C₂₃H₂₇NO₆

J. V. Silverton, P. N. Sharma and A. Brossi

Acta Cryst. (1985). C41, 758-760    [doi:10.1107/S010827018500539X]

Structure of 4-amino-2-thioxo-6-pyrimidinone monohydrate, C₄H₅N₃OS.H₂O

E. S. Raper, R. E. Oughtred and I. W. Nowell

Acta Cryst. (1985). C41, 760-763    [doi:10.1107/S0108270185005406]

Structure of modification I of cortisone acetate, 21-acetoxy-17-hydroxy-4-pregnene-3,11,20-trione, C₂₃H₃₀O₆

J. A. Kanters, A. de Koster, V. J. van Geerestein and L. A. van Dijck

Acta Cryst. (1985). C41, 763-766    [doi:10.1107/S0108270185005418]

11-Hydroxy-16,17,21-trimethyl-5-pregna-1,4-diene-3,20-dione (I), C₂₄H₃₄O₃, and 11,17-dihydroxy-21-methyl-5-pregn-4-en-3,20-dione 17-butyrate (II), C₂₆H₃₈O₅

J. C. Barnes, J. D. Paton, R. T. Logan and J. Redpath

Acta Cryst. (1985). C41, 767-769    [doi:10.1107/S010827018500542X]

The structure of 1,3-dihydro-4-[(2S)-2,5-dihydro-2-furyl]-3-methyl-1-p-tolyl-2H-imidazole-2-thione, C₁₅H₁₆N₂OS

E. Moreno, A. López-Castro and R. Márquez

Acta Cryst. (1985). C41, 769-771    [doi:10.1107/S0108270185005431]

Structure of (E)-3-(2-methoxyphenyl)-1-phenyl-3-(1H-1,2,4-triazol-1-yl)-2-propen-1-one, C₁₈H₁₅N₃O₂

S. K. Branch and I. W. Nowell

Acta Cryst. (1985). C41, 771-773    [doi:10.1107/S0108270185005443]

(1R,2R,3R,6S,10R)-1-Fluoro-3-(2-hydroxy-2-propyl)-6,10-dimethylbicyclo[4.4.0]decan-2-ol, C₁₅H₂₇FO₂

R. G. Pritchard, R. Ramage and I. A. Southwell

Acta Cryst. (1985). C41, 773-775    [doi:10.1107/S0108270185005455]

Structure of [2.2.2.2]paracyclophane, C₃₂H₃₂

A. Renault and C. Cohen-Addad

Acta Cryst. (1985). C41, 775-778    [doi:10.1107/S0108270185005467]

Structures du N¹-(méthoxy-6 méthyl-2 pyrimidinyl-4)sulfanilamide (sulfamétomidine), C₁₂H₁₄N₄O₃S, et d'un de ses solvates, C₁₂H₁₄N₄O₃S.H₂O

J. Rambaud, L. Maury, B. Pauvert, G. Berge, M. Audran, Y. Lasserre et J.-P. Declercq

Acta Cryst. (1985). C41, 778-780    [doi:10.1107/S0108270185005479]

Structure of pentathia[9]heterohelicene, C₂₈H₁₂S₅

H. Nakagawa, H. Nagashima, K. Yamada and H. Kawazura

Acta Cryst. (1985). C41, 781-783    [doi:10.1107/S0108270185005480]

-(Hydroxy-3 oxo-5 phényl-4 2H-furylidène-2)-phénylacétate de méthyle, acide vulpinique, C₁₉H₁₄O₅

C. Brassy, B. Bachet, L. Molho et D. Molho

Acta Cryst. (1985). C41, 783-785    [doi:10.1107/S0108270185005492]

Structure of acetanilide (C₈H₉NO) at 113 K

H. J. Wasserman, R. R. Ryan and S. P. Layne

Acta Cryst. (1985). C41, 785-788    [doi:10.1107/S0108270185005509]

Synthesis and structure of (E)-3-fluoro-4-pyridinecarbaldehyde oxime, C₆H₅FN₂O, and conversion to its quaternary methyl iodide derivative

J. M. Sorof, H. L. Carrell, J. P. Glusker, J. McLick and E. Kun

Acta Cryst. (1985). C41, 788-791    [doi:10.1107/S0108270185005510]

Structure of 6,6,10,10-tetranitropentacyclo[5.3.0.0^2,5.0^3,9.0^4,8]decane, C₁₀H₈N₄O₈

C. George, R. Gilardi, J. L. Flippen-Anderson, C. S. Choi, A. P. Marchand and D. S. Reddy

Acta Cryst. (1985). C41, 791-793    [doi:10.1107/S0108270185005522]

Acétoxy-4 tert-butyl-2 cyclohexène-3 carboxylate-1 de méthyle-cis, C₁₄H₂₂O₄

R. Viani, J. Lapasset et J.-P. Aycard

Acta Cryst. (1985). C41, 793-795    [doi:10.1107/S0108270185005534]

Hexahydro-4b,6,7,8,9,9a 5H-benzo[3,4]cyclobuta[1,2]cyclohepténol-1-cis, C₁₃H₁₆O

A. Courtois, V. Pesme-Pichon, M. C. Carré et P. Caubère

Acta Cryst. (1985). C41, 796-798    [doi:10.1107/S0108270185005546]

Structure of 7,8,17,18-tetrahydro-10,20-diphenyl-5,9,15,19-tetraazadibenzo[ai]cyclohexadecene-6,16(5H,15H)-dione, C₃₂H₂₈N₄O₂

A. A. Dvorkin, T. I. Malinowsky, Yu. A. Simonov, S. A. Andronati, A. V. Kuzmina and A. S. Yavorsky

Acta Cryst. (1985). C41, 798-802    [doi:10.1107/S0108270185005558]

Structure of gentiopicrin hemihydrate: (-)-(5R,6S)-5-ethenyl-6-(-D-glucopyranosyloxy)-5,6-dihydro-1H,3H-pyrano[3,4-c]pyran-1-one hemihydrate, C₁₆H₂₀O₉.1/2H₂O

B. Kojic-Prodic, A. L. Spek, W. G. van der Sluis and R. P. Labadie

Acta Cryst. (1985). C41, 802-804    [doi:10.1107/S010827018500556X]

Structure of 3-acetyl-4-hydroxy-6-phenyl-2-pyrone, C₁₃H₁₀O₄

V. G. Thailambal and V. Pattabhi

short communications

Acta Cryst. (1985). C41, 804-805    [doi:10.1107/S0108270185005571]

Nouvelle description du tétrafluorure de neptunium hydraté, Np₃F₁₂.H₂O

A. Cousson et M. Gasperin

Acta Cryst. (1985). C41, 806    [doi:10.1107/S0108270185005583]

Structure of 25-ethoxycarbonyl-2,3,7,8,12,13,17,18-octaethyl-21,22-methano-21H,22H-porphyrin hydrobromide, C₄₀H₅₁N₄O₂⁺.Br^-. The first example of a cis-N,N-bridged porphyrin. Erratum

T. J. Bartczak

Acta Cryst. (1985). C41, 806    [doi:10.1107/S0108270185005595]

trans-Azido(dimethylglyoximato-N,N')(dimethylglyoxime-N,N')(pyridine)cobalt(III): addition

S. V. Evans, M. N. Ponnuswamy and J. Trotter

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