Acta Crystallographica Section C

Crystal Structure Communications

Volume 41, Part 6 (June 1985)

• research papers
  • inorganic compounds
  • metal-organic compounds
  • organic compounds
• short format
  • metal-organic compounds
• short communications

research papers

inorganic compounds

Acta Cryst. (1985). C41, 807-811    [doi:10.1107/S0108270185005601]

Polytypism of crystals of tin disulphide; structures of 21 polytypes of SnS₂

B. Palosz, W. Palosz and S. Gierlotka

Acta Cryst. (1985). C41, 811-814    [doi:10.1107/S0108270185005613]

Structure de l'orthophosphate acide de thallium à valence mixte, Tl₃{Tl/ri0,5/rt(H₃O)/ri0,5/rt}H₁₄(PO₄)₈.4H₂O

M. Chiadmi, J. Vicat, D. Tran Qui and A. Boudjada

Acta Cryst. (1985). C41, 814-816    [doi:10.1107/S0108270185005625]

Structure of dodecacalcium potassium fluoride dioxide tetrasilicate bis(sulphate), KF.2[Ca₆(SO₄)(SiO₄)₂O]: a fluorine-containig phase encountered in cement clinker production process

J. Fayos, F. P. Glasser, R. A. Howie, E. Lachowski and M. Perez-Mendez

Acta Cryst. (1985). C41, 817-820    [doi:10.1107/S0108270185005637]

Diytterbium decavanadate 24-hydrate, Yb₂V₁₀O₂₈.24H₂O

B. E. Rivero, G. Punte, G. Rigotti and A. Navaza

Acta Cryst. (1985). C41, 820-823    [doi:10.1107/S0108270185005649]

Zr₃Ir with tetragonal -V₃S structure

K. Cenzual and E. Parthé

Acta Cryst. (1985). C41, 824-827    [doi:10.1107/S0108270185005650]

Structures of the perhalogenated cyclopentasilanes Si₅Br₁₀ and Si₅I₁₀ at normal and low temperatures

Ch. Kratky, H. Hengge, H. Stüger and A. L. Rheingold

Acta Cryst. (1985). C41, 827-832    [doi:10.1107/S0108270185005662]

The structure of lazurite, ideally Na₆Ca₂(Al₆Si₆O₂₄)S₂, a member of the sodalite group

I. Hassan, R. C. Peterson and H. D. Grundy

metal-organic compounds

Acta Cryst. (1985). C41, 833-835    [doi:10.1107/S0108270185005674]

Structure of (-cyclopentadienyl){(3R*,3aR*)-5-5a-9a-9b--3-methoxy-5-trimethylsilyl-2,3,3a,4,6,7,8,9-octahydro-1H-benz[e]indene}cobalt, [Co(C₅H₅)(C₁₇H₂₈OSi)]

J. M. Boncella, F. Okino, C. Orvig, R. P. Planalp and G. L. Rosenthal

Acta Cryst. (1985). C41, 835-838    [doi:10.1107/S0108270185005686]

Structure of trans-dichloro[dimethyl(phenyl)phosphine](trans-2,3-dimethylpyrrolidine)platinum(II), [PtCl₂(C₆H₁₃N)(C₈H₁₁P)]

F. Bachechi and L. Zambonelli

Acta Cryst. (1985). C41, 838-840    [doi:10.1107/S0108270185005698]

(Hexafluoroacetylacetonato-O,O')(1-hydroxy-2,2,6,6-tetramethylpiperidinato-O,N)palladium(II), [Pd(C₅HF₆O₂)(C₉H₁₈NO)], a metal complex containing a reduced nitroxyl radical

L. C. Porter and R. J. Doedens

Acta Cryst. (1985). C41, 841-844    [doi:10.1107/S0108270185005704]

Structure of two isomers of bromo[(2-bromo-3,4,5,6-tetrafluorophenyl)diphenylphosphine-Br,P]chloro(2-diphenylphosphinoyl-3,4,5,6-tetrafluorophenyl-O)rhodium(III), C₃₆H₂₀Br₂ClF₈OP₂Rh and C₃₆H₂₀Br₂ClF₈OP₂Rh.C₂H₆O

X. Solans, M. Font-Altaba, M. Aguiló, C. Miravitlles, J. C. Besteiro and P. Lahuerta

Acta Cryst. (1985). C41, 844-846    [doi:10.1107/S0108270185005716]

Structure of {diaqua[N,N'-bis(-carbamoylethyl)-2-hydroxytrimethylenediamine]}nickel(II) dichloride, [Ni(C₉H₂₀N₄O₃)(H₂O)₂]Cl₂

T.-Y. Lee, C.-Y. Hong, T.-J. Lee, S.-H. Liu and C.-S. Chung

Acta Cryst. (1985). C41, 846-850    [doi:10.1107/S0108270185005728]

Studies of tetramethylammonium tetrabromometallates. II. Structure of tetramethylammonium tetrabromozincate, [N(CH₃)₄]₂[ZnBr₄], in its low-temperature phase

P. Trouélan, J. Lefebvre and P. Derollez

Acta Cryst. (1985). C41, 850-855    [doi:10.1107/S010827018500573X]

Structures of two 6,6-diaryfulvene complexes of rhodium: (1,5-cyclooctadiene)(6,6-diphenylfulvene)rhodium(I) perchlorate, [Rh(C₈H₁₂)(C₁₈H₁₄)]ClO₄, (I), and [6,6-bis(4-chlorophenyl)fulvene]bis(triphenyl phosphite)rhodium(I) perchlorate, [Rh(C₁₈H₁₂Cl₂)(C₁₈H₁₅O₃P)₂]ClO₄, (II)

Z. Dauter, L. K. Hansen, R. J. Mawby, E. J. Probitts and C. D. Reynolds

Acta Cryst. (1985). C41, 855-858    [doi:10.1107/S0108270185005741]

Structure of (di-2-pyridylamine)salicylaldehydatocopper(II) perchlorate, [Cu(C₇H₅O₂)(C₁₀H₉N₃)]ClO₄

M. T. Garland, J. Y. Le Marouille and E. Spodine

Acta Cryst. (1985). C41, 858-860    [doi:10.1107/S0108270185005753]

Structure of bis[2-(salicylideneamino)ethanolato]copper(II), [Cu(C₉H₁₀NO₂)₂]

F. Nepveu and H. Paulus

Acta Cryst. (1985). C41, 860-862    [doi:10.1107/S0108270185005765]

Structure of trichloro(7,8--morphinium)platinum(II) hemihydrate acetone solvate, [PtCl₃(C₁₇H₂₀NO₃)].C₃H₆O.0.5H₂O

J.-P. Macquet and A. L. Beauchamp

Acta Cryst. (1985). C41, 862-865    [doi:10.1107/S0108270185005777]

Structure of tetraphenylphosphonium bis(benzenethiolato)aurate(I), [P(C₆H₅)₄][Au(C₆H₅S)₂]

P. A. Bates and J. M. Waters

Acta Cryst. (1985). C41, 865-869    [doi:10.1107/S0108270185005789]

The structure of cis-dichloro(25-ethoxycarbonyl-2,3,7,8,12,13,17,18-octaethyl-23,24-methano-23H,24H-porphyrin-N²¹,N²²,H)palladium(II)chloroform solvate, [PdCl₂(C₄₀H₅₀N₄O₂)\].CHCl₃

T. J. Bartczak

Acta Cryst. (1985). C41, 869-871    [doi:10.1107/S0108270185005790]

Structure of (N,N-dimethylbenzylaminato-N,C)iodo(4-methoxyphenyl)(4-methylphenyl)lead(IV), [PbI(C₇H₇)(C₉H₁₂N)(C₇H₇O)]

H. O. van der Kooi, W. H. den Brinker and A. J. de Kok

Acta Cryst. (1985). C41, 871-873    [doi:10.1107/S0108270185005807]

Structure of -oxo-bis{[N-(2-mercaptoethyl)-N',N'-dimethylethylenediamino]dioxomolybdenum(VI)}, [Mo₂O₅{(CH₃)₂NCH₂CH₂NHCH₂CH₂S}₂\]

K. Gebreyes, S. N. Shaikh and J. Zubieta

Acta Cryst. (1985). C41, 873-876    [doi:10.1107/S0108270185005819]

Synthesis and structure of cis-tetrakis(acetamidine)carbonatocobalt(III) chloride dihydrate, [Co(CO₃)(C₂H₆N₂)₄]Cl.2H₂O at 117 K

R. Norrestam

Acta Cryst. (1985). C41, 876-878    [doi:10.1107/S0108270185005820]

Structure of a bromo-bridged one-dimensional Pd^II-Pd^IV mixed-valence complex, catena--bromo-bis(ethylenediamine)palladium(II,IV) diperchlorate, [Pd(C₂H₈N₂)₂][PdBr₂(C₂H₈N₂)₂\](ClO₄)₄

M. Yamashita, K. Toriumi and T. Ito

Acta Cryst. (1985). C41, 878-881    [doi:10.1107/S0108270185005832]

Structure of di--chloro-tetrachlorobis(tetrahydrofuran)-[-(dimethyl sulfide)]-diniobium(Nb-Nb), [Nb₂Cl₆(C₄H₈O)₂(C₂H₆S)], and di--chloro-tetrachlorobis(tetrahydrofuran)-[-(dimethyl sulfide)]-ditantalum(Ta-Ta), [Ta₂Cl₆(C₄H₈O)₂(C₂H₆S)]

F. A. Cotton, S. A. Duraj and W. J. Roth

Acta Cryst. (1985). C41, 881-883    [doi:10.1107/S0108270185005844]

Structure of tetrakis[dimethyl(phenyl)phosphine]mercury(II) decachloro--oxo-ditantalate(V), [Hg{P(CH₃)₂(C₆H₅)}₄][Ta₂Cl₁₀O]

F. A. Cotton, S. A. Duraj and W. J. Roth

Acta Cryst. (1985). C41, 884-886    [doi:10.1107/S0108270185005856]

Structure du dinitratodioxobis(triamide hexaméthylphosphorique)uranium(VI), [UO₂(NO₃)₂(C₆H₁₈N₃OP)₂]

P. Charpin, M. Lance, E. Soulie et D. Vigner

Acta Cryst. (1985). C41, 886-888    [doi:10.1107/S0108270185005868]

The structure of tricarbonyl{C,13,14,C--(2RS,5SR,8SR,13RS,14SR)-8-methyl-13,14-dimethylene-9-oxatetracyclo[6.2.2.2^2,5.0^1,6]tetradeca-3,6-diene-11,11,12,12-tetracarbonitrile}iron(0), [Fe(C₂₀H₁₄N₄O)(CO)₃]

F. Pilloud, R. Roulet and G. Chapuis

Acta Cryst. (1985). C41, 888-890    [doi:10.1107/S010827018500587X]

The structure of tetramethylammonium ₃-oxo-cyclo-tri--bromo-tri--formato-(O,O')-tris(chloromolybdate)(3 Mo-Mo), [N(CH₃)₄][{MoBrCl(CHO₂)}₃O\]

D. Wu, J.-L. Huang and J.-Q. Huang

Acta Cryst. (1985). C41, 890-892    [doi:10.1107/S0108270185005881]

Copper(I)-olefin complexes. Structure of (1-2--cyclohexene)(di-2-pyridylamine)copper(I) perchlorate, [Cu(C₆H₁₀)(C₁₀H₉N₃)]ClO₄

J. S. Thompson, J. C. Calabrese and J. F. Whitney

Acta Cryst. (1985). C41, 893-895    [doi:10.1107/S0108270185005893]

Structure of {2,6-bis[(dimethylamino)methyl]phenyl}dichloroiron(III), [Fe(C₁₂H₁₉N₂)Cl₂]

A. de Koster, J. A. Kanters, A. L. Spek, A. A. H. van der Zeijden, G. van Koten and K. Vrieze

Acta Cryst. (1985). C41, 895-896    [doi:10.1107/S010827018500590X]

Dicarbonylchloro(⁵-cyclopentadienyl)eisen(II), [Fe(⁵-C₅H₅)(CO)₂Cl]

K.-J. Jens and E. Weiss

Acta Cryst. (1985). C41, 897-899    [doi:10.1107/S0108270185005911]

Structure of an asymmetric bridged binuclear copper(II) complex

J. Lorösch, H. Paulus and W. Haase

Acta Cryst. (1985). C41, 899-902    [doi:10.1107/S0108270185005923]

Structure of trans-amminebis(ethylenediamine)fluorochromium(III) perchlorate, [CrF(NH₃)(C₂H₈N₂)₂](ClO₄)₂

K. A. Beveridge, G. W. Bushnell and A. D. Kirk

Acta Cryst. (1985). C41, 902-905    [doi:10.1107/S0108270185005935]

Structure of bis(pyridine)(5,10,15,20-tetraphenylporphyrinato)iron(II)-pyridine solvate, [Fe(C₄₄H₂₈N₄)(C₅H₅N)₂].2C₅H₅N

N. Li, V. Petrícek, P. Coppens and J. Landrum

Acta Cryst. (1985). C41, 905-906    [doi:10.1107/S0108270185005947]

Benzoato(triphenylphosphine)gold(I) benzene solvate, [Au(C₇H₅O₂){P(C₆H₅)₃}].C₆H₆

P. G. Jones

organic compounds

Acta Cryst. (1985). C41, 907-909    [doi:10.1107/S0108270185005959]

Structural analysis of picene, C₂₂H₁₄

A. De, R. Ghosh, S. Roychowdhury and P. Roychowdhury

Acta Cryst. (1985). C41, 909-912    [doi:10.1107/S0108270185005960]

Structures of tifluadom [5-(2-fluorophenyl)-1-methyl-2-(3-thenoylaminomethyl)-2,3-dihydro-1H-1,4-benzodiazepine] hydrochloride, C₂₂H₂₁FN₃OS⁺.Cl^-, and of (+)-tifluadom p-toluenesulphonate, C₂₂H₂₁FN₃OS⁺.C₇H₇O₃S^-, and the absolute configuration of the latter

T. J. Petcher, A. Widmer, U. Maetzel and H. Zeugner

Acta Cryst. (1985). C41, 912-915    [doi:10.1107/S0108270185005972]

1,1-Dimethyl-3,3,4,4-tetraphenylgermacyclopentane, C₃₀H₃₀Ge

H. Preut, J. Köcher and W. P. Neumann

Acta Cryst. (1985). C41, 915-917    [doi:10.1107/S0108270185005984]

Methyl 3,3,7,7-tetramethyl-2-oxocycloheptanesulphinate, C₁₂H₂₂O₃S

M. N. Ponnuswamy and J. Trotter

Acta Cryst. (1985). C41, 917-919    [doi:10.1107/S0108270185005996]

N-Acetyl-DL-methionine, C₇H₁₃NO₃S

M. N. Ponnuswamy and J. Trotter

Acta Cryst. (1985). C41, 919-921    [doi:10.1107/S010827018500600X]

Structure of 4,10-dibenzyl-4,10-diazabicyclo[5.5.0]dodec-1(7)-ene dihydrochloride, C₂₄H₃₂N₂²⁺.2Cl^-

S. Kashino, M. Kimura, S. Morosawa and M. Haisa

Acta Cryst. (1985). C41, 921-924    [doi:10.1107/S0108270185006011]

3,5-Diamino-2,4,6-trinitrobenzoic acid, C₇H₅N₅O₈

H. L. Ammon and S. M. Prasad

Acta Cryst. (1985). C41, 924-926    [doi:10.1107/S0108270185006023]

Structure of 3-benzylidenephthalide, C₁₅H₁₀O₂

Y. Wang, M. C. Cheng, L. C. Lin, V. C. Koh and M. Yang

Acta Cryst. (1985). C41, 926-927    [doi:10.1107/S0108270185006035]

4-Acetyl-3'-chlorobiphenyl, C₁₄H₁₁ClO

H. H. Sutherland, A. Rawas and M. J. Mottram

Acta Cryst. (1985). C41, 928-929    [doi:10.1107/S0108270185006047]

Structure of 3,4'-dimethyl-3',4-bis(methylthio)-2,2',5,5'-tetrathiafulvalene, C₁₀H₁₂S₆

L. Ouahab and P. Batail

Acta Cryst. (1985). C41, 929-931    [doi:10.1107/S0108270185006059]

2-Methyl-1-benzothiophene, C₉H₈S

H. H. Sutherland and A. Rawas

Acta Cryst. (1985). C41, 931-933    [doi:10.1107/S0108270185006060]

Structure from a twinned crystal of the triclinic form of the 1:1 complex between N,N-dimethylaniline and hexafluorobenzene [C₈H₁₁N.C₆F₆] at 120 K

T. Dahl

Acta Cryst. (1985). C41, 933-935    [doi:10.1107/S0108270185006072]

Méthyl-4 (propyn-2 yloxy)-7 chroménone-2 (giparmène), C₁₃H₁₀O₃

P. Toffoli, P. Khodadad, N. Rodier, R. Céolin et J. Astoin

Acta Cryst. (1985). C41, 935-937    [doi:10.1107/S0108270185006084]

Structure of 1-dimethylamino-2,2,3,4,4-pentamethyl-1⁵-phosphetane 1-sulphide, C₁₀H₂₂NPS, at 105 K

M. Gajhede, O. Dahl and J. Nielsen

Acta Cryst. (1985). C41, 938-940    [doi:10.1107/S0108270185006096]

N,N'-Bis(1-methylethyl)-6-methylthio-1,3,5-triazine-2,4-diamine, prometryn, C₁₀H₁₉N₅S

H. P. Avey, C. H. L. Kennard and G. Smith

Acta Cryst. (1985). C41, 941-942    [doi:10.1107/S0108270185006102]

Diethylsilanediol, C₄H₁₂O₂Si, a redetermination

P. E. Tomlins, J. E. Lydon, D. Akrigg and B. Sheldrick

Acta Cryst. (1985). C41, 942-944    [doi:10.1107/S0108270185006114]

Structure of a carbocyclic analogue of penicillin

B. Sheldrick, D. Akrigg, M. I. Page and D. Agathocleous

Acta Cryst. (1985). C41, 944-946    [doi:10.1107/S0108270185006126]

Structure of a ten-membered macrocyclic diester of (+)-retronecine, C₁₂H₁₅NO₄: a pyrrolizidine alkaloid analogue

M. Burton, A. A. Freer and D. J. Robins

Acta Cryst. (1985). C41, 946-950    [doi:10.1107/S0108270185006138]

Structure of Boc-Pro-Met-Gly-OBzl, C₂₄H₃₅N₃O₆S

T. Yamane, Y. Shiraishi and T. Ashida

Acta Cryst. (1985). C41, 950-953    [doi:10.1107/S010827018500614X]

Structures of 1,4-bis(3,5-dichloro-2-pyridyloxy)benzene (1), C₁₆H₈Cl₄N₂O₂, 1,4-bis(5-chloro-2 pyridyloxy)benzene (2), C₁₆H₁₀Cl₂N₂O₂ and 1,4-bis(3-chloro-2-pyridyloxy)benzene (3), C₁₆H₁₀Cl₂N₂O₂

W. B. Drendel and M. Sundaralingam

Acta Cryst. (1985). C41, 954-956    [doi:10.1107/S0108270185006151]

2:1 molecular complex of 2-(-hydroxyimino-2,6-dimethylbenzyl)-5-p-tolyl-2H-tetrazole with triethylammonium 5-p-tolyltetrazolide, 2C₁₇H₁₇N₅O.C₆H₁₆N⁺.C₈H₇N₄^-

M. Cannas, G. Gelli, G. Marongiu and G. Navarra

Acta Cryst. (1985). C41, 956-959    [doi:10.1107/S0108270185006163]

The structure of (±)-malic acid, (±)-C₄H₆O₅

P. van der Sluis and J. Kroon

Acta Cryst. (1985). C41, 959-961    [doi:10.1107/S0108270185006175]

3,4,5-Triiodotoluene, C₇H₅I₃

Y.-X. Liu, C. B. Knobler, K. N. Trueblood and R. Helgeson

Acta Cryst. (1985). C41, 961-963    [doi:10.1107/S0108270185006187]

Structure of dinaphtho[1,2-b:2',1'-d]furan, C₂₀H₁₂O

R. E. Gerkin and W. J. Reppart

Acta Cryst. (1985). C41, 963-965    [doi:10.1107/S0108270185006199]

Structure of the 1/1 complex between octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX), C₄H₈N₈O₈, and N-methyl-2-pyrrolidinone (NMP), C₅H₉NO

T. M. Haller, A. L. Rheingold and T. B. Brill

Acta Cryst. (1985). C41, 965-967    [doi:10.1107/S0108270185006205]

Structure of N-(5-nitro-2-thiazolyl)acetamide (aminitrozole), C₅H₅N₃O₃S

O. M. Peeters, N. M. Blaton and C. J. De Ranter

Acta Cryst. (1985). C41, 967-971    [doi:10.1107/S0108270185006217]

Structural investigation of the triaryl derivatives of the Group V elements. IX. Structure of triphenylamine, C₁₈H₁₅N

A. N. Sobolev, V. K. Belsky, I. P. Romm, N. Yu. Chernikova and E. N. Guryanova

Acta Cryst. (1985). C41, 971-973    [doi:10.1107/S0108270185006229]

Structure of (trans-2-hydroxycyclohexyl)dimethylphosphine oxide, C₈H₁₇O₂P

R. D. Rosenstein, S. S. C. Chu and J. D. Buynak

Acta Cryst. (1985). C41, 973-975    [doi:10.1107/S0108270185006230]

Structure of 1-azacarbazole, C₁₁H₈N₂

K. Suwinska

Acta Cryst. (1985). C41, 975-977    [doi:10.1107/S0108270185006242]

Structure of 2,2,3,4,4-pentamethyl-1-(1-naphthyl)-⁵-phosphetane 1-oxide, C₁₈H₂₃OP

Mazhar-ul-Haque, J. Ahmed and W. Horne

Acta Cryst. (1985). C41, 977-980    [doi:10.1107/S0108270185006254]

10-Hydroxy-10-methyl-10,11-dihydroquinine, C₂₁H₂₈N₂O₃, a new derivative of quinine

A. Suszko-Purzycka, T. Lipinska, E. Piotrowska and B. J. Oleksyn

Acta Cryst. (1985). C41, 981-983    [doi:10.1107/S0108270185006266]

Structure of N,N-dimethyl-2-nitrovinylamine, C₄H₈N₂O₂

M. J. Diánez, A. López-Castro and R. Márquez

Acta Cryst. (1985). C41, 983-985    [doi:10.1107/S0108270185006278]

19-(p-Bromophenyl)-12-methoxypodocarpa-8,11,13-trien-19-one, C₂₄H₂₇BrO₂

M. C. Couldwell, R. A. J. Smith and J. Simpson

Acta Cryst. (1985). C41, 985-987    [doi:10.1107/S010827018500628X]

2-Chloro-9-oxothioxanthenium-10-bis(methoxycarbonyl)methylide, C₁₈H₁₃ClO₅S

S. S. C. Chu, V. Napoleone, P. de Meester and T. L. Chu

Acta Cryst. (1985). C41, 988-990    [doi:10.1107/S0108270185006291]

Crystal structure of sorbinil, C₁₁H₉FN₂O₃

C. R. Kissinger, E. T. Adman, J. I. Clark and R. E. Stenkamp

Acta Cryst. (1985). C41, 990-994    [doi:10.1107/S0108270185006308]

Structures of strychnine (I), C₂₁H₂₂N₂O₂, and a solvate of brucine (II), C₂₃H₂₆N₂O₄.C₂H₆O.2H₂O

S. S. B. Glover, R. O. Gould and M. D. Walkinshaw

short format

metal-organic compounds

Acta Cryst. (1985). C41, 995-996    [doi:10.1107/S010827018500631X]

An organomolybdenum complex

A. J. Graham, D. Akrigg and B. Sheldrick

short communications

Acta Cryst. (1985). C41, 996    [doi:10.1107/S0108270185006321]

Structure d'un polyphosphate mixte de lithium et de potassium, LiK(PO₃)₂: errata

N. El-Horr, M. Bagieu et I. Tordjman

Copyright © International Union of Crystallography
IUCr Webmaster