Acta Crystallographica Section C

Crystal Structure Communications

Volume 41, Part 6 (June 1985)



research papers


inorganic compounds



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Acta Cryst. (1985). C41, 807-811    [doi:10.1107/S0108270185005601]

Polytypism of crystals of tin disulphide; structures of 21 polytypes of SnS2

B. Palosz, W. Palosz and S. Gierlotka



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Acta Cryst. (1985). C41, 811-814    [doi:10.1107/S0108270185005613]

Structure de l'orthophosphate acide de thallium à valence mixte, Tl3{Tl/ri0,5/rt(H3O)/ri0,5/rt}H14(PO4)8.4H2O

M. Chiadmi, J. Vicat, D. Tran Qui and A. Boudjada



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Acta Cryst. (1985). C41, 814-816    [doi:10.1107/S0108270185005625]

Structure of dodecacalcium potassium fluoride dioxide tetrasilicate bis(sulphate), KF.2[Ca6(SO4)(SiO4)2O]: a fluorine-containig phase encountered in cement clinker production process

J. Fayos, F. P. Glasser, R. A. Howie, E. Lachowski and M. Perez-Mendez



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Acta Cryst. (1985). C41, 817-820    [doi:10.1107/S0108270185005637]

Diytterbium decavanadate 24-hydrate, Yb2V10O28.24H2O

B. E. Rivero, G. Punte, G. Rigotti and A. Navaza



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Acta Cryst. (1985). C41, 820-823    [doi:10.1107/S0108270185005649]

Zr3Ir with tetragonal [alpha]-V3S structure

K. Cenzual and E. Parthé



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Acta Cryst. (1985). C41, 824-827    [doi:10.1107/S0108270185005650]

Structures of the perhalogenated cyclopentasilanes Si5Br10 and Si5I10 at normal and low temperatures

Ch. Kratky, H. Hengge, H. Stüger and A. L. Rheingold



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Acta Cryst. (1985). C41, 827-832    [doi:10.1107/S0108270185005662]

The structure of lazurite, ideally Na6Ca2(Al6Si6O24)S2, a member of the sodalite group

I. Hassan, R. C. Peterson and H. D. Grundy


metal-organic compounds



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Acta Cryst. (1985). C41, 833-835    [doi:10.1107/S0108270185005674]

Structure of ([eta]-cyclopentadienyl){(3R*,3aR*)-5-5a-9a-9b-[eta]-3-methoxy-5-trimethylsilyl-2,3,3a,4,6,7,8,9-octahydro-1H-benz[e]indene}cobalt, [Co(C5H5)(C17H28OSi)]

J. M. Boncella, F. Okino, C. Orvig, R. P. Planalp and G. L. Rosenthal



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Acta Cryst. (1985). C41, 835-838    [doi:10.1107/S0108270185005686]

Structure of trans-dichloro[dimethyl(phenyl)phosphine](trans-2,3-dimethylpyrrolidine)platinum(II), [PtCl2(C6H13N)(C8H11P)]

F. Bachechi and L. Zambonelli



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Acta Cryst. (1985). C41, 838-840    [doi:10.1107/S0108270185005698]

(Hexafluoroacetylacetonato-O,O')(1-hydroxy-2,2,6,6-tetramethylpiperidinato-O,N)palladium(II), [Pd(C5HF6O2)(C9H18NO)], a metal complex containing a reduced nitroxyl radical

L. C. Porter and R. J. Doedens



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Acta Cryst. (1985). C41, 841-844    [doi:10.1107/S0108270185005704]

Structure of two isomers of bromo[(2-bromo-3,4,5,6-tetrafluorophenyl)diphenylphosphine-Br,P]chloro(2-diphenylphosphinoyl-3,4,5,6-tetrafluorophenyl-O)rhodium(III), C36H20Br2ClF8OP2Rh and C36H20Br2ClF8OP2Rh.C2H6O

X. Solans, M. Font-Altaba, M. Aguiló, C. Miravitlles, J. C. Besteiro and P. Lahuerta



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Acta Cryst. (1985). C41, 844-846    [doi:10.1107/S0108270185005716]

Structure of {diaqua[N,N'-bis([beta]-carbamoylethyl)-2-hydroxytrimethylenediamine]}nickel(II) dichloride, [Ni(C9H20N4O3)(H2O)2]Cl2

T.-Y. Lee, C.-Y. Hong, T.-J. Lee, S.-H. Liu and C.-S. Chung



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Acta Cryst. (1985). C41, 846-850    [doi:10.1107/S0108270185005728]

Studies of tetramethylammonium tetrabromometallates. II. Structure of tetramethylammonium tetrabromozincate, [N(CH3)4]2[ZnBr4], in its low-temperature phase

P. Trouélan, J. Lefebvre and P. Derollez



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Acta Cryst. (1985). C41, 850-855    [doi:10.1107/S010827018500573X]

Structures of two 6,6-diaryfulvene complexes of rhodium: (1,5-cyclooctadiene)(6,6-diphenylfulvene)rhodium(I) perchlorate, [Rh(C8H12)(C18H14)]ClO4, (I), and [6,6-bis(4-chlorophenyl)fulvene]bis(triphenyl phosphite)rhodium(I) perchlorate, [Rh(C18H12Cl2)(C18H15O3P)2]ClO4, (II)

Z. Dauter, L. K. Hansen, R. J. Mawby, E. J. Probitts and C. D. Reynolds



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Acta Cryst. (1985). C41, 855-858    [doi:10.1107/S0108270185005741]

Structure of (di-2-pyridylamine)salicylaldehydatocopper(II) perchlorate, [Cu(C7H5O2)(C10H9N3)]ClO4

M. T. Garland, J. Y. Le Marouille and E. Spodine



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Acta Cryst. (1985). C41, 858-860    [doi:10.1107/S0108270185005753]

Structure of bis[2-(salicylideneamino)ethanolato]copper(II), [Cu(C9H10NO2)2]

F. Nepveu and H. Paulus



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Acta Cryst. (1985). C41, 860-862    [doi:10.1107/S0108270185005765]

Structure of trichloro(7,8-[eta]-morphinium)platinum(II) hemihydrate acetone solvate, [PtCl3(C17H20NO3)].C3H6O.0.5H2O

J.-P. Macquet and A. L. Beauchamp



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Acta Cryst. (1985). C41, 862-865    [doi:10.1107/S0108270185005777]

Structure of tetraphenylphosphonium bis(benzenethiolato)aurate(I), [P(C6H5)4][Au(C6H5S)2]

P. A. Bates and J. M. Waters



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Acta Cryst. (1985). C41, 865-869    [doi:10.1107/S0108270185005789]

The structure of cis-dichloro(25-ethoxycarbonyl-2,3,7,8,12,13,17,18-octaethyl-23,24-methano-23H,24H-porphyrin-N21,N22,H)palladium(II)chloroform solvate, [PdCl2(C40H50N4O2)\].CHCl3

T. J. Bartczak



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Acta Cryst. (1985). C41, 869-871    [doi:10.1107/S0108270185005790]

Structure of (N,N-dimethylbenzylaminato-N,C)iodo(4-methoxyphenyl)(4-methylphenyl)lead(IV), [PbI(C7H7)(C9H12N)(C7H7O)]

H. O. van der Kooi, W. H. den Brinker and A. J. de Kok



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Acta Cryst. (1985). C41, 871-873    [doi:10.1107/S0108270185005807]

Structure of [mu]-oxo-bis{[N-(2-mercaptoethyl)-N',N'-dimethylethylenediamino]dioxomolybdenum(VI)}, [Mo2O5{(CH3)2NCH2CH2NHCH2CH2S}2\]

K. Gebreyes, S. N. Shaikh and J. Zubieta



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Acta Cryst. (1985). C41, 873-876    [doi:10.1107/S0108270185005819]

Synthesis and structure of cis-tetrakis(acetamidine)carbonatocobalt(III) chloride dihydrate, [Co(CO3)(C2H6N2)4]Cl.2H2O at 117 K

R. Norrestam



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Acta Cryst. (1985). C41, 876-878    [doi:10.1107/S0108270185005820]

Structure of a bromo-bridged one-dimensional PdII-PdIV mixed-valence complex, catena-[mu]-bromo-bis(ethylenediamine)palladium(II,IV) diperchlorate, [Pd(C2H8N2)2][PdBr2(C2H8N2)2\](ClO4)4

M. Yamashita, K. Toriumi and T. Ito



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Acta Cryst. (1985). C41, 878-881    [doi:10.1107/S0108270185005832]

Structure of di-[mu]-chloro-tetrachlorobis(tetrahydrofuran)-[[mu]-(dimethyl sulfide)]-diniobium(Nb-Nb), [Nb2Cl6(C4H8O)2(C2H6S)], and di-[mu]-chloro-tetrachlorobis(tetrahydrofuran)-[[mu]-(dimethyl sulfide)]-ditantalum(Ta-Ta), [Ta2Cl6(C4H8O)2(C2H6S)]

F. A. Cotton, S. A. Duraj and W. J. Roth



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Acta Cryst. (1985). C41, 881-883    [doi:10.1107/S0108270185005844]

Structure of tetrakis[dimethyl(phenyl)phosphine]mercury(II) decachloro-[mu]-oxo-ditantalate(V), [Hg{P(CH3)2(C6H5)}4][Ta2Cl10O]

F. A. Cotton, S. A. Duraj and W. J. Roth



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Acta Cryst. (1985). C41, 884-886    [doi:10.1107/S0108270185005856]

Structure du dinitratodioxobis(triamide hexaméthylphosphorique)uranium(VI), [UO2(NO3)2(C6H18N3OP)2]

P. Charpin, M. Lance, E. Soulie et D. Vigner



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Acta Cryst. (1985). C41, 886-888    [doi:10.1107/S0108270185005868]

The structure of tricarbonyl{C,13,14,C-[eta]-(2RS,5SR,8SR,13RS,14SR)-8-methyl-13,14-dimethylene-9-oxatetracyclo[6.2.2.22,5.01,6]tetradeca-3,6-diene-11,11,12,12-tetracarbonitrile}iron(0), [Fe(C20H14N4O)(CO)3]

F. Pilloud, R. Roulet and G. Chapuis



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Acta Cryst. (1985). C41, 888-890    [doi:10.1107/S010827018500587X]

The structure of tetramethylammonium [mu]3-oxo-cyclo-tri-[mu]-bromo-tri-[mu]-formato-(O,O')-tris(chloromolybdate)(3 Mo-Mo), [N(CH3)4][{MoBrCl(CHO2)}3O\]

D. Wu, J.-L. Huang and J.-Q. Huang



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Acta Cryst. (1985). C41, 890-892    [doi:10.1107/S0108270185005881]

Copper(I)-olefin complexes. Structure of (1-2-[eta]-cyclohexene)(di-2-pyridylamine)copper(I) perchlorate, [Cu(C6H10)(C10H9N3)]ClO4

J. S. Thompson, J. C. Calabrese and J. F. Whitney



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Acta Cryst. (1985). C41, 893-895    [doi:10.1107/S0108270185005893]

Structure of {2,6-bis[(dimethylamino)methyl]phenyl}dichloroiron(III), [Fe(C12H19N2)Cl2]

A. de Koster, J. A. Kanters, A. L. Spek, A. A. H. van der Zeijden, G. van Koten and K. Vrieze



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Acta Cryst. (1985). C41, 895-896    [doi:10.1107/S010827018500590X]

Dicarbonylchloro([eta]5-cyclopentadienyl)eisen(II), [Fe([eta]5-C5H5)(CO)2Cl]

K.-J. Jens and E. Weiss



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Acta Cryst. (1985). C41, 897-899    [doi:10.1107/S0108270185005911]

Structure of an asymmetric bridged binuclear copper(II) complex

J. Lorösch, H. Paulus and W. Haase



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Acta Cryst. (1985). C41, 899-902    [doi:10.1107/S0108270185005923]

Structure of trans-amminebis(ethylenediamine)fluorochromium(III) perchlorate, [CrF(NH3)(C2H8N2)2](ClO4)2

K. A. Beveridge, G. W. Bushnell and A. D. Kirk



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Acta Cryst. (1985). C41, 902-905    [doi:10.1107/S0108270185005935]

Structure of bis(pyridine)(5,10,15,20-tetraphenylporphyrinato)iron(II)-pyridine solvate, [Fe(C44H28N4)(C5H5N)2].2C5H5N

N. Li, V. Petrícek, P. Coppens and J. Landrum



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Acta Cryst. (1985). C41, 905-906    [doi:10.1107/S0108270185005947]

Benzoato(triphenylphosphine)gold(I) benzene solvate, [Au(C7H5O2){P(C6H5)3}].C6H6

P. G. Jones


organic compounds



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Acta Cryst. (1985). C41, 907-909    [doi:10.1107/S0108270185005959]

Structural analysis of picene, C22H14

A. De, R. Ghosh, S. Roychowdhury and P. Roychowdhury



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Acta Cryst. (1985). C41, 909-912    [doi:10.1107/S0108270185005960]

Structures of tifluadom [5-(2-fluorophenyl)-1-methyl-2-(3-thenoylaminomethyl)-2,3-dihydro-1H-1,4-benzodiazepine] hydrochloride, C22H21FN3OS+.Cl-, and of (+)-tifluadom p-toluenesulphonate, C22H21FN3OS+.C7H7O3S-, and the absolute configuration of the latter

T. J. Petcher, A. Widmer, U. Maetzel and H. Zeugner



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Acta Cryst. (1985). C41, 912-915    [doi:10.1107/S0108270185005972]

1,1-Dimethyl-3,3,4,4-tetraphenylgermacyclopentane, C30H30Ge

H. Preut, J. Köcher and W. P. Neumann



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Acta Cryst. (1985). C41, 915-917    [doi:10.1107/S0108270185005984]

Methyl 3,3,7,7-tetramethyl-2-oxocycloheptanesulphinate, C12H22O3S

M. N. Ponnuswamy and J. Trotter



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Acta Cryst. (1985). C41, 917-919    [doi:10.1107/S0108270185005996]

N-Acetyl-DL-methionine, C7H13NO3S

M. N. Ponnuswamy and J. Trotter



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Acta Cryst. (1985). C41, 919-921    [doi:10.1107/S010827018500600X]

Structure of 4,10-dibenzyl-4,10-diazabicyclo[5.5.0]dodec-1(7)-ene dihydrochloride, C24H32N22+.2Cl-

S. Kashino, M. Kimura, S. Morosawa and M. Haisa



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Acta Cryst. (1985). C41, 921-924    [doi:10.1107/S0108270185006011]

3,5-Diamino-2,4,6-trinitrobenzoic acid, C7H5N5O8

H. L. Ammon and S. M. Prasad



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Acta Cryst. (1985). C41, 924-926    [doi:10.1107/S0108270185006023]

Structure of 3-benzylidenephthalide, C15H10O2

Y. Wang, M. C. Cheng, L. C. Lin, V. C. Koh and M. Yang



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Acta Cryst. (1985). C41, 926-927    [doi:10.1107/S0108270185006035]

4-Acetyl-3'-chlorobiphenyl, C14H11ClO

H. H. Sutherland, A. Rawas and M. J. Mottram



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Acta Cryst. (1985). C41, 928-929    [doi:10.1107/S0108270185006047]

Structure of 3,4'-dimethyl-3',4-bis(methylthio)-2,2',5,5'-tetrathiafulvalene, C10H12S6

L. Ouahab and P. Batail



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Acta Cryst. (1985). C41, 929-931    [doi:10.1107/S0108270185006059]

2-Methyl-1-benzothiophene, C9H8S

H. H. Sutherland and A. Rawas



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Acta Cryst. (1985). C41, 931-933    [doi:10.1107/S0108270185006060]

Structure from a twinned crystal of the triclinic form of the 1:1 complex between N,N-dimethylaniline and hexafluorobenzene [C8H11N.C6F6] at 120 K

T. Dahl



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Acta Cryst. (1985). C41, 933-935    [doi:10.1107/S0108270185006072]

Méthyl-4 (propyn-2 yloxy)-7 chroménone-2 (giparmène), C13H10O3

P. Toffoli, P. Khodadad, N. Rodier, R. Céolin et J. Astoin



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Acta Cryst. (1985). C41, 935-937    [doi:10.1107/S0108270185006084]

Structure of 1-dimethylamino-2,2,3,4,4-pentamethyl-1[lambda]5-phosphetane 1-sulphide, C10H22NPS, at 105 K

M. Gajhede, O. Dahl and J. Nielsen



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Acta Cryst. (1985). C41, 938-940    [doi:10.1107/S0108270185006096]

N,N'-Bis(1-methylethyl)-6-methylthio-1,3,5-triazine-2,4-diamine, prometryn, C10H19N5S

H. P. Avey, C. H. L. Kennard and G. Smith



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Acta Cryst. (1985). C41, 941-942    [doi:10.1107/S0108270185006102]

Diethylsilanediol, C4H12O2Si, a redetermination

P. E. Tomlins, J. E. Lydon, D. Akrigg and B. Sheldrick



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Acta Cryst. (1985). C41, 942-944    [doi:10.1107/S0108270185006114]

Structure of a carbocyclic analogue of penicillin

B. Sheldrick, D. Akrigg, M. I. Page and D. Agathocleous



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Acta Cryst. (1985). C41, 944-946    [doi:10.1107/S0108270185006126]

Structure of a ten-membered macrocyclic diester of (+)-retronecine, C12H15NO4: a pyrrolizidine alkaloid analogue

M. Burton, A. A. Freer and D. J. Robins



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Acta Cryst. (1985). C41, 946-950    [doi:10.1107/S0108270185006138]

Structure of Boc-Pro-Met-Gly-OBzl, C24H35N3O6S

T. Yamane, Y. Shiraishi and T. Ashida



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Acta Cryst. (1985). C41, 950-953    [doi:10.1107/S010827018500614X]

Structures of 1,4-bis(3,5-dichloro-2-pyridyloxy)benzene (1), C16H8Cl4N2O2, 1,4-bis(5-chloro-2 pyridyloxy)benzene (2), C16H10Cl2N2O2 and 1,4-bis(3-chloro-2-pyridyloxy)benzene (3), C16H10Cl2N2O2

W. B. Drendel and M. Sundaralingam



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Acta Cryst. (1985). C41, 954-956    [doi:10.1107/S0108270185006151]

2:1 molecular complex of 2-([alpha]-hydroxyimino-2,6-dimethylbenzyl)-5-p-tolyl-2H-tetrazole with triethylammonium 5-p-tolyltetrazolide, 2C17H17N5O.C6H16N+.C8H7N4-

M. Cannas, G. Gelli, G. Marongiu and G. Navarra



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Acta Cryst. (1985). C41, 956-959    [doi:10.1107/S0108270185006163]

The structure of (±)-malic acid, (±)-C4H6O5

P. van der Sluis and J. Kroon



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Acta Cryst. (1985). C41, 959-961    [doi:10.1107/S0108270185006175]

3,4,5-Triiodotoluene, C7H5I3

Y.-X. Liu, C. B. Knobler, K. N. Trueblood and R. Helgeson



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Acta Cryst. (1985). C41, 961-963    [doi:10.1107/S0108270185006187]

Structure of dinaphtho[1,2-b:2',1'-d]furan, C20H12O

R. E. Gerkin and W. J. Reppart



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Acta Cryst. (1985). C41, 963-965    [doi:10.1107/S0108270185006199]

Structure of the 1/1 complex between octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX), C4H8N8O8, and N-methyl-2-pyrrolidinone (NMP), C5H9NO

T. M. Haller, A. L. Rheingold and T. B. Brill



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Acta Cryst. (1985). C41, 965-967    [doi:10.1107/S0108270185006205]

Structure of N-(5-nitro-2-thiazolyl)acetamide (aminitrozole), C5H5N3O3S

O. M. Peeters, N. M. Blaton and C. J. De Ranter



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Acta Cryst. (1985). C41, 967-971    [doi:10.1107/S0108270185006217]

Structural investigation of the triaryl derivatives of the Group V elements. IX. Structure of triphenylamine, C18H15N

A. N. Sobolev, V. K. Belsky, I. P. Romm, N. Yu. Chernikova and E. N. Guryanova



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Acta Cryst. (1985). C41, 971-973    [doi:10.1107/S0108270185006229]

Structure of (trans-2-hydroxycyclohexyl)dimethylphosphine oxide, C8H17O2P

R. D. Rosenstein, S. S. C. Chu and J. D. Buynak



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Acta Cryst. (1985). C41, 973-975    [doi:10.1107/S0108270185006230]

Structure of 1-azacarbazole, C11H8N2

K. Suwinska



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Acta Cryst. (1985). C41, 975-977    [doi:10.1107/S0108270185006242]

Structure of 2,2,3,4,4-pentamethyl-1-(1-naphthyl)-[lambda]5-phosphetane 1-oxide, C18H23OP

Mazhar-ul-Haque, J. Ahmed and W. Horne



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Acta Cryst. (1985). C41, 977-980    [doi:10.1107/S0108270185006254]

10-Hydroxy-10-methyl-10,11-dihydroquinine, C21H28N2O3, a new derivative of quinine

A. Suszko-Purzycka, T. Lipinska, E. Piotrowska and B. J. Oleksyn



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Acta Cryst. (1985). C41, 981-983    [doi:10.1107/S0108270185006266]

Structure of N,N-dimethyl-2-nitrovinylamine, C4H8N2O2

M. J. Diánez, A. López-Castro and R. Márquez



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Acta Cryst. (1985). C41, 983-985    [doi:10.1107/S0108270185006278]

19-(p-Bromophenyl)-12-methoxypodocarpa-8,11,13-trien-19-one, C24H27BrO2

M. C. Couldwell, R. A. J. Smith and J. Simpson



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Acta Cryst. (1985). C41, 985-987    [doi:10.1107/S010827018500628X]

2-Chloro-9-oxothioxanthenium-10-bis(methoxycarbonyl)methylide, C18H13ClO5S

S. S. C. Chu, V. Napoleone, P. de Meester and T. L. Chu



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Acta Cryst. (1985). C41, 988-990    [doi:10.1107/S0108270185006291]

Crystal structure of sorbinil, C11H9FN2O3

C. R. Kissinger, E. T. Adman, J. I. Clark and R. E. Stenkamp



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Acta Cryst. (1985). C41, 990-994    [doi:10.1107/S0108270185006308]

Structures of strychnine (I), C21H22N2O2, and a solvate of brucine (II), C23H26N2O4.C2H6O.2H2O

S. S. B. Glover, R. O. Gould and M. D. Walkinshaw


short format


metal-organic compounds



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Acta Cryst. (1985). C41, 995-996    [doi:10.1107/S010827018500631X]

An organomolybdenum complex

A. J. Graham, D. Akrigg and B. Sheldrick


short communications



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Acta Cryst. (1985). C41, 996    [doi:10.1107/S0108270185006321]

Structure d'un polyphosphate mixte de lithium et de potassium, LiK(PO3)2: errata

N. El-Horr, M. Bagieu et I. Tordjman


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