Acta Crystallographica Section C

Crystal Structure Communications

Volume 42, Part 9 (September 1986)



research papers


inorganic compounds



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Acta Cryst. (1986). C42, 1101-1105    [doi:10.1107/S0108270186093253]

Zr5Ir3 with a deformation superstructure of the Mn5Si3 structure

K. Cenzual and E. Parthé



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Acta Cryst. (1986). C42, 1105-1109    [doi:10.1107/S0108270186093241]

Structure of the linear chain tetraammineplatinum(II)diiodotetraammineplatinum(IV) hydrogensulfate dihydrate

M. Tanaka, I. Tsujikawa, K. Toriumi and T. Ito



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Acta Cryst. (1986). C42, 1109-1111    [doi:10.1107/S010827018609323X]

Structure de l'oxysulfure d'uranium et d'erbium (UO)2ErS3

S. Jaulmes, M. Julien-Pouzol, M. Guittard, T. Vovan, P. Laruelle et J. Flahaut



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Acta Cryst. (1986). C42, 1111-1113    [doi:10.1107/S0108270186093228]

Structure d'un oxysulfure de gallium et de thallium

S. Jaulmes, M. Julien-Pouzol, J. Dugué, P. Laruelle et M. Guittard



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Acta Cryst. (1986). C42, 1113-1115    [doi:10.1107/S0108270186093216]

Structure of ammonium hexachloroselenate(IV)

W. Abriel



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Acta Cryst. (1986). C42, 1115-1118    [doi:10.1107/S0108270186093204]

Hexasodium hexatungstotellurate(VI) 22-hydrate

K. J. Schmidt, G. J. Schrobilgen and J. F. Sawyer



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Acta Cryst. (1986). C42, 1118-1120    [doi:10.1107/S0108270186093198]

Hydrated aluminophosphate (A1PO4.1·5H2O) with PO4, A1O4 and A1O4(H2O)2 groups and encapsulated water

J. J. Pluth and J. V. Smith


metal-organic compounds



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Acta Cryst. (1986). C42, 1121-1123    [doi:10.1107/S0108270186093186]

Structure of ([eta]5-cyclopentadienyl)(dicarbonyl)(O,O'-diisopropyl dithiophosphato)iron(II)

J. Sanz-Aparicio, S. Martínez-Carrera and S. García-Blanco



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Acta Cryst. (1986). C42, 1123-1125    [doi:10.1107/S0108270186093174]

Structure of sodium succinate hexahydrate

I. Fonseca, S. Martínez-Carrera and S. García-Blanco



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Acta Cryst. (1986). C42, 1125-1128    [doi:10.1107/S0108270186093162]

Structure of a mononuclear gold(I) complex containing a covalently bound ylide ligand

L. C. Porter, H. Knachel and J. P. Fackler Jnr



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Acta Cryst. (1986). C42, 1128-1131    [doi:10.1107/S0108270186093150]

Structure of the first example of an organometallic dinuclear gold(II) complex possessing bonds to oxygen

L. C. Porter and J. P. Fackler Jnr



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Acta Cryst. (1986). C42, 1131-1133    [doi:10.1107/S0108270186093149]

Structure of a seven-coordinated complex of nickel, diaqua[2,6-diacetylpyridine bis(2-hydroxybenzoylhydrazone)]nickel(II) nitrate sesquihydrate

C. Pelizzi, G. Pelizzi, S. Porretta and F. Vitali



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Acta Cryst. (1986). C42, 1133-1136    [doi:10.1107/S0108270186093137]

Reactions of coordinated molecules. 48. The structure of a Pt-W cluster containing a bridging [eta]1,[eta]3-p-tolylmethylene ligand

J. H. Davis Jnr, P. G. Lenhert, C. M. Lukehart and L. A. Sacksteder



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Acta Cryst. (1986). C42, 1136-1138    [doi:10.1107/S0108270186093125]

Strucktur von Di-[mu]-acetato(O,O')-bis[N-(2,3,4-trimethoxybenziliden)-2,4,6-trimethylanilinato-N,C]dipalladium(II)

W. Hiller, A. Castineiras, J. M. Vila, A. Suarez, M. T. Pereira und M. Gayoso



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Acta Cryst. (1986). C42, 1138-1140    [doi:10.1107/S0108270186093113]

Diphenyl[8-quinolinethiolato(1-)-S]antimony(III)

H. Preut, U. Praeckel and F. Huber



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Acta Cryst. (1986). C42, 1141-1144    [doi:10.1107/S0108270186093101]

(Hexaphenylcarbodiphosphorane)copper(I) chloride: A mononuclear organocopper complex

G. Müller, C. Krüger, C. Zybill and H. Schmidbaur



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Acta Cryst. (1986). C42, 1144-1148    [doi:10.1107/S0108270186093095]

Structure of the hexafluorophosphate salts of [mu]-([eta]6:[eta]6-phenoxazine)bis[[eta]5-cyclopentadienyliron(II)] (1) and ([eta]5-cyclopentadienyl)([eta]6-phenoxathiin)iron(II) (2)

V. M. Lynch, S. N. Thomas, S. H. Simonsen, A. Piórko and R. G. Sutherland



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Acta Cryst. (1986). C42, 1148-1151    [doi:10.1107/S0108270186093083]

Structure of dinitratobis(triphenylphosphine oxide)copper(II) toluene solvate (1/1)

M. B. Ferrari, G. F. Gasparri, C. Pelizzi and P. Tarasconi



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Acta Cryst. (1986). C42, 1151-1154    [doi:10.1107/S0108270186093071]

Structures of N,N'-ethylenebis(salicylideneiminato)manganese(III) chloride acetonitrile solvate

V. L. Pecoraro and W. M. Butler



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Acta Cryst. (1986). C42, 1154-1157    [doi:10.1107/S010827018609306X]

Structures of [mu]-oxo-bis[(benzensulfonato)triphenylantimony(V)] and [mu]-oxo-bis[(trifluoromethylsulfonato)triphenylantimony(V)]

H. Preut, R. Rüther and F. Huber



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Acta Cryst. (1986). C42, 1157-1159    [doi:10.1107/S0108270186093058]

Structural investigations of NiII complexes. VI. Two isomers of tetrakis(3-ethylpyridine)bis(isothiocyanato)nickel(II)

E. Durcanská, M. Jamnický, M. Koman, I. Wnek and T. Glowiak


organic compounds



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Acta Cryst. (1986). C42, 1159-1161    [doi:10.1107/S0108270186093046]

Structure of diacetato(m-tolyl)iodine(III)

S. C. Kokkou and C. J. Cheer



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Acta Cryst. (1986). C42, 1161-1164    [doi:10.1107/S0108270186093034]

3,3-Bis(methylnitraminomethyl)oxetane (I) and 3,3-bis(nitratomethyl)oxetane (II)

C. George and R. Gilardi



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Acta Cryst. (1986). C42, 1164-1166    [doi:10.1107/S0108270186093022]

Structure of 7-(2,4-dinitrophenylthio)-5-exo-nitrobicyclo[2.2.1]hept-2-exo-yl acetate

M. V. Sergeyeva, D. S. Yufit, Yu. T. Struchkov, E. N. Kurkutova, N. S. Zefirov, N. V. Zyk, A. G. Kutateladze and S. I. Kolbasenko



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Acta Cryst. (1986). C42, 1166-1169    [doi:10.1107/S0108270186093010]

1-(4-Chlorophenyl)-2-cyclopentylethanone

S. Ariel and J. Trotter



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Acta Cryst. (1986). C42, 1169-1172    [doi:10.1107/S0108270186093009]

Structures of radical anion TCNQ.- salts with 1,2-dithiole derivatives. II. 3-p-Methoxyphenyl-1,2-dithiolylium 7,7,8,8-tetracyano-p-quinodimethanide (1/1.5)

F. Mathieu



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Acta Cryst. (1986). C42, 1172-1175    [doi:10.1107/S0108270186092995]

Crystal and energy-refined structures of 2,2',4,4',5,5'-hexachlorobiphenyl

P. Singh, L. G. Pedersen and J. D. McKinney



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Acta Cryst. (1986). C42, 1176-1178    [doi:10.1107/S0108270186092983]

2,2',4,4',5,5'-Hexachlorobiphenyl (PCB 153)

H. J. Geise, A. T. H. Lenstra, C. de Borst and G. W. H. Moes



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Acta Cryst. (1986). C42, 1178-1181    [doi:10.1107/S0108270186092971]

Structure of (Z)-N-benzoyl-[alpha],[beta]-dehydroleucine

V. Busetti, D. Ajò and A. Vittadini



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Acta Cryst. (1986). C42, 1181-1183    [doi:10.1107/S010827018609296X]

Structural studies of radical reaction products. II. 2,4-Bis(4-chlorophenyl)-5,5-dimethyl-3-pyrazolidinone

F. Ganazzoli, A. Citterio and A. Albinati



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Acta Cryst. (1986). C42, 1184-1185    [doi:10.1107/S0108270186092958]

Structure of isororidin E

J. L. Flippen-Anderson and R. Gilardi



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Acta Cryst. (1986). C42, 1185-1189    [doi:10.1107/S0108270186092946]

Neurotoxins producing Parkinson's syndrome

J. L. Flippen-Anderson, R. Gilardi and C. George



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Acta Cryst. (1986). C42, 1189-1191    [doi:10.1107/S0108270186092934]

Structure of trans-N-(1-benzyl-4-methyl-3-pyrrolidinyl)-5-chloro-2-methoxy-4-methylaminobenzamide hydrochloride

T. Furuya, S. Iwanami, A. Takenaka and Y. Sasada



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Acta Cryst. (1986). C42, 1191-1194    [doi:10.1107/S0108270186092922]

Nonsteroidal antiinflammatory drugs. IV. Structure of (±)-(2SR)-2-{4-[(1RS,2RS)-2-hydroxycyclopentylmethyl]phenyl}propionic acid

T. Hata, S. Sato and C. Tamura



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Acta Cryst. (1986). C42, 1194-1196    [doi:10.1107/S0108270186092910]

Structure of 10-[4-(acetoxy)phenyl]-10-hydroxy-9(10H)-anthracenone

Z. Skrzat and A. Roszak



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Acta Cryst. (1986). C42, 1197-1199    [doi:10.1107/S0108270186092909]

Structure of guanidinium bicarbonate: a model for the bicarbonate anion binding site of the transferrins

D. A. Baldwin, L. Denner, T. J. Egan and A. J. Markwell



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Acta Cryst. (1986). C42, 1199-1201    [doi:10.1107/S0108270186092892]

Pentacyclo[19.3.1.12,6.19,13.114,18]octacosa-1(25),2,4,6(28),9,11,13(27),14,16,18(26),21,23-dodecaene ([2.0.2.0]-m-cyclophane)

R. B. Bates, S. L. Merbs, R. B. Ortega and J. J. White



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Acta Cryst. (1986). C42, 1201-1204    [doi:10.1107/S0108270186092880]

Structure of 3'-acetamido-2,2-dichloro-4',5'-dimethylacetophenone

D. Chattopadhyay, T. Banerjee, S. K. Mazumdar, G. Podder, S. Kashino and M. Haisa



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Acta Cryst. (1986). C42, 1204-1206    [doi:10.1107/S0108270186092879]

Structure of 14a,17[alpha]-epoxy-3-methoxy-14-methyl-14[alpha]-estra-1,3,5(10)-trien-17[beta]-ol

J. M. L. Dillen



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Acta Cryst. (1986). C42, 1206-1208    [doi:10.1107/S0108270186092867]

Structure of an aminopyridazine derivative

C. Van der Brempt, G. Evrard and F. Durant



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Acta Cryst. (1986). C42, 1209-1211    [doi:10.1107/S0108270186092855]

Structure of propylglyoxal bis(amidinohydrazone) sulfate dihydrate

P. O. Lumme, I. Mutikainen and H. O. Elo



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Acta Cryst. (1986). C42, 1211-1217    [doi:10.1107/S0108270186092843]

Transitions de phase structurales dans les polyphényles. IX. Affinements des structures du p-terphényle hydrogéné à 200 K (diffraction des rayons X) et du biphényle deutéré à 40 K (diffraction des neutrons)

J. L. Baudour, L. Toupet, Y. Délugeard et S. Ghémid



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Acta Cryst. (1986). C42, 1217-1220    [doi:10.1107/S0108270186092831]

The structure of jateorin

R. Goddard and F. Akhtar



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Acta Cryst. (1986). C42, 1220-1222    [doi:10.1107/S010827018609282X]

Structure of (Z)-1,2-diphenyl-2-p-tolylvinyl 2,2,2-trifluoroethyl ether

Y. Luo, R. J. Barton, B. E. Robertson, C. C. Lee and D. Wanigasekera



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Acta Cryst. (1986). C42, 1222-1225    [doi:10.1107/S0108270186092818]

Bond length and reactivity: the Beckmann rearrangement. 1. Structure of cyclopentanone O-(3,5-dinitrobenzoyl)oxime n-hexane solvate (4:1)

P. G. Jones, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1986). C42, 1225-1227    [doi:10.1107/S0108270186092806]

Bond length and reactivity: the Beckmann rearrangement. 2. Structure of a protonated lactam: 5-tert-butylhexahydro-2H-azepin-2-onium p-toluensulfonate monohydrate

M. R. Edwards, H. D. Holden, A. J. Kirby and P. R. Raithby



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Acta Cryst. (1986). C42, 1228-1230    [doi:10.1107/S010827018609279X]

Bond length and reactivity: the Beckmann rearrangement. 3. Structure of 4-phenylcyclohexanone O-(2-naphthalenesulfonyl)oxime at 233 K

P. G. Jones, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1986). C42, 1230-1232    [doi:10.1107/S0108270186092788]

Bond length and reactivity: the Beckmann rearrangement. 4. Structure of 4-phenylcyclohexanone oxime O-triphenylmethyl ether at 233 K

P. G. Jones, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1986). C42, 1233-1235    [doi:10.1107/S0108270186092776]

Structure of N-{2-[3-(dimethylamino)propylthio]phenyl}-3-phenylpropenamide monohydrochloride (cinanserin hydrochloride)

O. M. Peeters, N. M. Blaton and C. J. de Ranter



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Acta Cryst. (1986). C42, 1235-1237    [doi:10.1107/S0108270186092764]

Structural chirality of an [alpha]-aminophosphonic acid derivative

M. Dyrbusch and E. Egert



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Acta Cryst. (1986). C42, 1237-1239    [doi:10.1107/S0108270186092752]

Structure of 2[alpha]-bromo-1[beta],7[beta]-epoxytrachelanthamidine: a new heterocyclic ring system

J. A. Glinski, D. G. Van Derveer and L. H. Zalkow



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Acta Cryst. (1986). C42, 1239-1242    [doi:10.1107/S0108270186092740]

Structure of 5,5,6-trimethyl-1,4-diphenyl-2,3,7-trioxa[2.2.1]bicycloheptane

A. Syed, G. P. Kirschenheuter, V. Jain, G. W. Griffin and E. D. Stevens



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Acta Cryst. (1986). C42, 1242-1246    [doi:10.1107/S0108270186092739]

Structure of 2,4,4,8,8-pentakis(dimethylamino)-9-methyl-6-methylamino-2,6-imino-2[lambda]5,4[lambda]5,6[lambda]5,8[lambda]5-cyclotetra(phosphazene) monohydrate

T. S. Cameron, R. E. Cordes and B. R. Vincent



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Acta Cryst. (1986). C42, 1246-1248    [doi:10.1107/S0108270186092727]

Structure of 3-hydroxy-6-(4'-methyl)phenylazopyridine

T. S. R. Krishna and G. R. Desiraju



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Acta Cryst. (1986). C42, 1248-1251    [doi:10.1107/S0108270186092715]

Absolute conformation of 3-(N-methyl-N-benzyl)carbamoyl-1,2,4-trimethylpyridinium iodide (I) and absolute configuration of 3-[N-methyl-N-(R)-[alpha]-methylbenzyl]carbamoyl-1,2,4-trimethylpyridinium iodide (II)

J. A. Kanters, F. H. van der Steen, L. A. M. Bastiaansen and J. A. C. de Graaf



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Acta Cryst. (1986). C42, 1252-1254    [doi:10.1107/S0108270186092703]

2,4-Diaminopteridine monohydrate

C. H. Schwalbe and G. J. B. Williams



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Acta Cryst. (1986). C42, 1254-1257    [doi:10.1107/S0108270186092697]

Structure of 2,4-diamino-6,7-dimethylpteridine hydrochloride monohydrate

C. H. Schwalbe and G. J. B. Williams



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Acta Cryst. (1986). C42, 1257-1260    [doi:10.1107/S0108270186092685]

2,4-Diaminoquinazoline monohydrate: a redetermination

C. H. Schwalbe and G. J. B. Williams



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Acta Cryst. (1986). C42, 1260-1262    [doi:10.1107/S0108270186092673]

3-[(Z)-p-Chlorophenylthio-(E)-trimethylsilylmethylidene]-1,4-dimethyl-4-trimethylsilylazetidin-2-one: an [alpha]-alkylidene-[beta]-lactam

P. de Meester, J. D. Buynak and S. S. C. Chu


short format


inorganic compounds



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Acta Cryst. (1986). C42, 1263-1264    [doi:10.1107/S0108270186092661]

Cyclopentaazathienium-tetrachloroaurat

W. Willing, S. Ruangsuttinarupap, U. Müller and K. Dehnicke


organic compounds



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Acta Cryst. (1986). C42, 1264-1266    [doi:10.1107/S010827018609265X]

Structure of an unexpected indole photolysis product

K. Harms, G. M. Sheldrick, K. Brüggemann and L.-F. Tietze



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Acta Cryst. (1986). C42, 1266-1267    [doi:10.1107/S0108270186092648]

2,3-Dimethoxy-1,4-butanedinitrile (I) and 2,3-bis(piperidino)-1,4-butanedinitrile (II)

A. Parfonry, B. Tinant, J.-P. Declercq and M. Van Meerssche



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Acta Cryst. (1986). C42, 1268-1269    [doi:10.1107/S0108270186092636]

An enantiospecific hetero Diels-Alder product

K. Harms, G. M. Sheldrick, K.-H. Glüsenkamp and L.-F. Tietze



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Acta Cryst. (1986). C42, 1269-1271    [doi:10.1107/S0108270186092624]

Structure of a photolysis product

K. Harms, G. M. Sheldrick, K.-H. Glüsenkamp and L.-F. Tietze



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Acta Cryst. (1986). C42, 1271-1272    [doi:10.1107/S0108270186092612]

Structure of tetraphenylphosphonium chloride

J. F. Richardson, J. M. Ball and P. M. Boorman



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Acta Cryst. (1986). C42, 1273-1274    [doi:10.1107/S0108270186092600]

The structure of 3,5,5-trimethyl-3-pyrazoline N,N'-dioxide

P. Jørgensen, R. Koksbang and P. Lindhardt


short communications



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Acta Cryst. (1986). C42, 1274    [doi:10.1107/S0108270186092594]

X-ray structure analysis of 1,4-dioxane, phase I at 279 K and phase II at 153 K: erratum

J. Buschmann, E. Müller and P. Luger


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