Acta Crystallographica Section C

Crystal Structure Communications

Volume 42, Part 10 (October 1986)



research papers


inorganic compounds



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Acta Cryst. (1986). C42, 1275-1277    [doi:10.1107/S0108270186092582]

Refinement of the structure of trilead(II) uranate(VI) from neutron powder diffraction data

M. Sterns, J. B. Parise and C. J. Howard



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Acta Cryst. (1986). C42, 1277-1280    [doi:10.1107/S0108270186092570]

The structure of atacamite and its relationship to spinel

J. B. Parise and B. G. Hyde



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Acta Cryst. (1986). C42, 1281-1283    [doi:10.1107/S0108270186092569]

Structure of manganese(II) sodium dihydrogenphosphite monohydrate

R. Chmelíková, J. Loub and V. Petrícek



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Acta Cryst. (1986). C42, 1283-1284    [doi:10.1107/S0108270186092557]

cis-Diamminedicyanopalladium(II)

M. Penavic, L. Soptrajanova, G. Jovanovski and B. Soptrajanov



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Acta Cryst. (1986). C42, 1285-1287    [doi:10.1107/S0108270186092545]

Structures of zinc selenite and copper selenite

F. C. Hawthorne, T. S. Ercit and L. A. Groat


metal-organic compounds



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Acta Cryst. (1986). C42, 1287-1289    [doi:10.1107/S0108270186092533]

Bis[2,2'-biphenyldiyl(dimethylarsine)]diiodonickel(II)

M. G. Fitzpatrick and L. R. Hanton



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Acta Cryst. (1986). C42, 1289-1291    [doi:10.1107/S0108270186092521]

Structure of dibromoiodobis(triphenylphosphine oxide)thallium(III)

A. Castineiras, W. Hiller, M. R. Bermejo and M. Gayoso



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Acta Cryst. (1986). C42, 1291-1294    [doi:10.1107/S010827018609251X]

Structure of an antitumor platinum(II) compound cis-[PtCl2(cyclobutylamine)(NH3)]

F. D. Rochon and R. Melanson



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Acta Cryst. (1986). C42, 1294-1296    [doi:10.1107/S0108270186092508]

Structure of the palladium(II) sulfimide complex trans-dichloro(S,S-dimethyl-N-2-pyridylsulfimide)(triethylphosphine)palladium(II)

K. W. Muir and L. Manojlovic-Muir



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Acta Cryst. (1986). C42, 1296-1298    [doi:10.1107/S0108270186092491]

The structure of cis,trans,cis-diaquabis(5-methyl[1,2,4]triazolo[1,5-a]pyrimidine-N3)bis (thiocyanato-N)iron(II)

M. Biagini Cingi, A. M. Manotti Lanfredi, A. Tiripicchio, J. P. Cornelissen, J. G. Haasnoot and J. Reedijk



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Acta Cryst. (1986). C42, 1299-1302    [doi:10.1107/S010827018609248X]

Structure of a dinuclear ruthenium(II) complex containing bridging carboxylato ligands and a bridging aqua ligand: [mu]-aqua-bis([mu]-trichloroacetato-O,O')-bis{([eta]4-bicyclo[2.2.1]hepta-2,5-diene)(trichloroacetato)ruthenium(II)

M. O. Albers, D. C. Liles, E. Singleton and J. E. Stead



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Acta Cryst. (1986). C42, 1302-1305    [doi:10.1107/S0108270186092478]

An acetone complex of platinum

A. G. Thayer and N. C. Payne



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Acta Cryst. (1986). C42, 1305-1310    [doi:10.1107/S0108270186092466]

The structure of ferrioxamine D1-ethanol-water (1/2/1)

M. B. Hossain, M. A. F. Jalal and D. van der Helm



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Acta Cryst. (1986). C42, 1310-1313    [doi:10.1107/S0108270186092454]

Structure of hydronium-1,4,7,10,13,16-hexaoxacyclooctadecane (18-crown 6)-hexamolybdate(VI) (2/2/1)

C. B. Shoemaker, L. V. McAfee, D. P. Shoemaker and C. W. DeKock



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Acta Cryst. (1986). C42, 1313-1316    [doi:10.1107/S0108270186092442]

Structures of the NiII complexes of the imine ligands derived from 2,2-diethoxyethylamine with salicylaldehyde and 1,2- and 2,3-hydroxynaphthaldehydes

J. M. Fernández-G., M. J. Rosales, R. A. Toscano and R. G. Tapia T.



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Acta Cryst. (1986). C42, 1316-1319    [doi:10.1107/S0108270186092430]

Structure of [N,N'-bis(3-aminopropyl)-1,2-ethanediamine]perchloroatocopper(II) perchlorate hemihydrate

T.-Y. Lee, T.-J. Lee, C.-Y. Hong, M.-Y. Hsieh, D.-T. Wu and C.-S. Chung



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Acta Cryst. (1986). C42, 1319-1322    [doi:10.1107/S0108270186092429]

The chain polymeric structure of lead(II) crotonate

W. Clegg, I. R. Little and B. P. Straughan



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Acta Cryst. (1986). C42, 1322-1324    [doi:10.1107/S0108270186092417]

Structure of bis(1-thia-4,7-diazacyclononane)cobalt(III) perchlorate

T. W. Hambley and L. R. Gahan



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Acta Cryst. (1986). C42, 1324-1327    [doi:10.1107/S0108270186092405]

[(+)-(R)-2,2'-Bis(diphenylphosphino)-6,6'-dimethylbiphenyl](8,9,10-trinorborna-2,5-diene)rhodium(I) tetrafluoroborate

G. Svensson, J. Albertsson, T. Frejd and T. Klingstedt



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Acta Cryst. (1986). C42, 1327-1328    [doi:10.1107/S0108270186092399]

On the structure of Zn(C4H8N2O6)

R. E. Marsh



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Acta Cryst. (1986). C42, 1329-1331    [doi:10.1107/S0108270186092387]

Dimeric lithium o-phenylenedioxydiacetate trihydrate

G. Smith, E. J. O'Reilly and C. H. L. Kennard



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Acta Cryst. (1986). C42, 1331-1333    [doi:10.1107/S0108270186092375]

Structure of methyltriphenylphosphonium tetrachloroferrate(III)

T. Glowiak, E. Durcanská, I. Ondrejkovicová and G. Ondrejovic



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Acta Cryst. (1986). C42, 1333-1336    [doi:10.1107/S0108270186092363]

Structure of bis(4-hydroxy-L-prolinato-N,O)palladium(II) trihydrate

R. P. Patel, T. N. Ranganathan and V. M. Padmanabhan


organic compounds



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Acta Cryst. (1986). C42, 1336-1340    [doi:10.1107/S0108270186092351]

Three crystalline forms of 9-(2-hydroxyethyl)adenine resulting from the different stacking of hydrogen-bonded layers

A. Takenaka, M. Shibata and Y. Sasada



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Acta Cryst. (1986). C42, 1340-1343    [doi:10.1107/S010827018609234X]

Structure of a 9-(2-carboxyethyl)guanine 1,6-hexanediamine (2:1) complex

S. Oouchi, A. Takenaka and Y. Sasada



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Acta Cryst. (1986). C42, 1343-1345    [doi:10.1107/S0108270186092338]

Structure of cyclo(-L-phenylalanyl-L-phenylalanyl-)

M. Gdaniec and B. Liberek



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Acta Cryst. (1986). C42, 1345-1347    [doi:10.1107/S0108270186092326]

Structure of N-[(3RS,5SR)-1-benzyl-5-methyl-3-pyrrolidinyl]-5-chloro-2-methoxy-4-methylaminobenzamide hydrochloride

T. Furuya, S. Fujita, S. Iwanami, A. Takenaka and Y. Sasada



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Acta Cryst. (1986). C42, 1348-1350    [doi:10.1107/S0108270186092314]

Rosmarinine: a pyrrolizidine alkaloid

A. A. Freer, H. A. Kelly and D. J. Robins



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Acta Cryst. (1986). C42, 1350-1352    [doi:10.1107/S0108270186092302]

Structure of econazole

A. A. Freer, A. Pearson and E. G. Salole



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Acta Cryst. (1986). C42, 1352-1354    [doi:10.1107/S0108270186092296]

Structure of 5[beta],24-cyclofriedelan-3-one, a novel hexacyclic triterpenoid in space group P1

J. D. Connolly, A. A. Freer, V. Anjaneyulu, K. Ravi and G. Sambasivarao



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Acta Cryst. (1986). C42, 1355-1358    [doi:10.1107/S0108270186092284]

Bond length and reactivity: 1-aryl ethers and esters. 1. Three 3,5-dinitrobenzoate esters of 1-arylethanols: 1-(4-methoxyphenyl)ethyl, 1-phenylethyl and 1-(3-fluorophenyl)ethyl 3,5-dinitrobenzoates

P. G. Jones, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1986). C42, 1359-1360    [doi:10.1107/S0108270186092272]

Bond length and reactivity: 1-arylethyl ethers and esters. 2. Structure of 1-(4-nitrophenyl)ethyl chloroacetate

P. G. Jones, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1986). C42, 1361-1364    [doi:10.1107/S0108270186092260]

Bond length and reactivity: 1-arylethyl ethers and esters. 3. Structures of three trityl ethers of 1-arylethanols: 1-phenylethyl, 1-(4-chlorophenyl)ethyl and 1-(4-nitrophenyl)ethyl triphenylmethyl ethers

P. G. Jones, G. M. Sheldrick, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1986). C42, 1365-1367    [doi:10.1107/S0108270186092259]

Bond length and reactivity: 1-arylethyl ethers and esters. 4. Structures of two p-nitrophenyl ethers of 1-arylethanols. 1-Phenylethyl and 1-(4-methoxy)phenylethyl 4-nitrophenyl ethers

P. G. Jones, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1986). C42, 1368-1369    [doi:10.1107/S0108270186092247]

Bond length and reactivity: 1-arylethyl ethers and esters. 5. Structure of 1-(4-nitrophenyl)ethyl diphenyl phosphate

P. G. Jones, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1986). C42, 1370-1372    [doi:10.1107/S0108270186092235]

Bond length and reactivity: 1-arylethyl ethers and esters. 6. Structure of 1-(4-nitrophenyl)ethyl 2-naphthalenesulfonate

P. G. Jones, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1986). C42, 1372-1374    [doi:10.1107/S0108270186092223]

Bond length and reactivity. Structure of a Grob fragmentation substrate, 4a[alpha],5[beta],8a[beta]-1-methyldecahydroquinolin-5-yl 3,5-dinitrobenzoate

P. G. Jones, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1986). C42, 1375-1378    [doi:10.1107/S0108270186092211]

Outstanding steric hindrance: structure of bis(2,4,6-tri-tert-butylphenylphosphinoyl)methane

G. Müller, G. Reber, H. H. Karsch and H.-U. Reisacher



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Acta Cryst. (1986). C42, 1378-1380    [doi:10.1107/S010827018609220X]

4,4-Dinitropentanoic acid

S. M. Prasad, H. L. Ammon and D. M. Barnhart



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Acta Cryst. (1986). C42, 1380-1383    [doi:10.1107/S0108270186092193]

Hexadecyltrimethylammonium bromide

A. R. Campanelli and L. Scaramuzza



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Acta Cryst. (1986). C42, 1383-1385    [doi:10.1107/S0108270186092181]

Structure of harman, 1-methyl-9H-pyrido[3,4-b]indole

K. El-Sayed, D. M. Barnhart, H. L. Ammon and G. M. Wassel



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Acta Cryst. (1986). C42, 1385-1390    [doi:10.1107/S010827018609217X]

Structures and quantum-mechanical calculations of two polarized nitroethylenes: C9H9ClN2O2S (I) and C6H13N3O2 (II)

F. Ganazzoli, S. V. Meille and P. Gronchi



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Acta Cryst. (1986). C42, 1390-1392    [doi:10.1107/S0108270186092168]

Structure of dibenzo[def,i]naphtho[1,8,7-vwx]pyranthrene

S. Fujisawa, I. Oonishi, J. Aoki and Y. Ohashi



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Acta Cryst. (1986). C42, 1392-1395    [doi:10.1107/S0108270186092156]

8-Methylbenz[a]anthracene

N. P. C. Walker, C. E. Briant, D. W. Jones and J. D. Shaw



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Acta Cryst. (1986). C42, 1395-1397    [doi:10.1107/S0108270186092144]

The structure of a tricyclic peroxide

J. T. Fourkas and W. P. Schaefer



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Acta Cryst. (1986). C42, 1397-1399    [doi:10.1107/S0108270186092132]

Benzoylimino-2 triméthyl-1,4,6 dihydro-1,2 pyridine

N. Rodier, M.-P. Gillo, S. Piessard et G. Le Baut



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Acta Cryst. (1986). C42, 1399-1402    [doi:10.1107/S0108270186092120]

The electrochemical synthesis and structure determination of 3,3',5,5'-tetra-tert-butyl-1,1'-biphenylidene-4,4'-quinone

M. A. Khan, A. Osman and D. G. Tuck



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Acta Cryst. (1986). C42, 1402-1404    [doi:10.1107/S0108270186092119]

Novel protein kinase C inhibitor K-252a

N. Hirayama, T. Iida and K. Shirahata



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Acta Cryst. (1986). C42, 1404-1408    [doi:10.1107/S0108270186092107]

Structure of 6-fluoro-10,10'-diphenyl-9-phenanthrone (1), 7-chloro-10,10'-diphenyl-9-phenanthrone (2) and 3-methoxy-10,10'-diphenyl-9-phenanthrone (3)

C. Krüger and M. J. Romão



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Acta Cryst. (1986). C42, 1408-1411    [doi:10.1107/S0108270186092090]

Hydrogen-bonding patterns in 8-hydroxyquinoline derivatives: (I) structure of 5-chloro-8-hydroxyquinoline and (II) refinement of the structure of 8-hydroxyquinoline

T. Banerjee and N. N. Saha



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Acta Cryst. (1986). C42, 1411-1413    [doi:10.1107/S0108270186092089]

2-Bromo-4'-phenylacetophenone

G. A. Sim



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Acta Cryst. (1986). C42, 1413-1415    [doi:10.1107/S0108270186092077]

X-ray structure of 8[alpha]-acetoxy-1,3,4,10-tetrahydro-1[alpha],10[alpha]-epoxyachillin

M. D. Estrada, A. Conde, R. Márquez and R. J. Garay



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Acta Cryst. (1986). C42, 1416-1420    [doi:10.1107/S0108270186092065]

Structures of three stereoisomers of (4S)-3-(2-chloro-3-hydroxy-4-methylpentanoyl)-4-(1-methylethyl)oxazolidine

D. S. Eggleston, A. Abdel-Magid, L. N. Pridgen and I. Lantos



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Acta Cryst. (1986). C42, 1420-1423    [doi:10.1107/S0108270186092053]

Structure of tetramethylthiuram disulfide (1) and refinement of tetraethylthiuram disulfide (2)

Y. Wang, J.-H. Liao and C.-H. Ueng



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Acta Cryst. (1986). C42, 1423-1425    [doi:10.1107/S0108270186092041]

5,6-Benzochroman-4-one

K. Ravikumar, S. S. Rajan, M. N. Ponnuswamy and J. Trotter



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Acta Cryst. (1986). C42, 1425-1428    [doi:10.1107/S010827018609203X]

Ethyl 3-phenyl-4H-pyrazolo[3,2-c][1,4]benzothiazine-2-carboxylate (I) and 4-[chloro(ethoxycarbonyl)methyleneamino]-2-methylene-2,3-dihydro-4H-1,4-benzothiazine 1,1'-dioxide (II)

T. Pilati and M. Simonetta



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Acta Cryst. (1986). C42, 1428-1430    [doi:10.1107/S0108270186092028]

Structure of 1-methyl-2,3,4,5-tetranitropyrrole, a possible high-density explosive

D. T. Cromer, M. D. Coburn, R. R. Ryan and H. J. Wasserman



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Acta Cryst. (1986). C42, 1430-1433    [doi:10.1107/S0108270186092016]

Structure and conformation of cyclo(-L-phenylalanyl-L-prolyl-D-alanyl-), form II of a synthetic cyclic hexapeptide

K. K. Bhandary, G. Kartha and K. D. Kopple



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Acta Cryst. (1986). C42, 1433-1435    [doi:10.1107/S0108270186092004]

Structure of bis(p-nitrophenyl) diselenide at 187 K

G. D. Morris and F. W. B. Einstein



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Acta Cryst. (1986). C42, 1435-1437    [doi:10.1107/S0108270186091990]

Structure of 3-benzyl-2-methylindole

D. K. Chakraborty and S. K. Talapatra



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Acta Cryst. (1986). C42, 1437-1440    [doi:10.1107/S0108270186091989]

Structure and stable conformations of a new analgesic: 4-[5-ethyl-4-(4-methoxyphenyl)-4H-1,2,4-triazol-3-yl]-N,N-dimethylbenzamine

M. Cotrait



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Acta Cryst. (1986). C42, 1440-1442    [doi:10.1107/S0108270186091977]

A hemiacetal derivative of a cis-clerodane diterpene

I. Tavanaiepour and W. H. Watson



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Acta Cryst. (1986). C42, 1442-1444    [doi:10.1107/S0108270186091965]

Structure of methyl(1,5,6-trihydroxy-1,2,3,4-tetrahydro-2-naphthyl)ammonium bromide

T. W. Hambley and J. R. Rodgers



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Acta Cryst. (1986). C42, 1445-1447    [doi:10.1107/S0108270186091953]

Structure of (3-chlorophenoxy)acetic acid

G. Smith, C. H. L. Kennard and F. van Meurs



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Acta Cryst. (1986). C42, 1447-1448    [doi:10.1107/S0108270186091941]

Structure of 3-methylxanthine

J. N. Low, P. Tollin, E. Brand and C. C. Wilson


short format


metal-organic compounds



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Acta Cryst. (1986). C42, 1449-1450    [doi:10.1107/S010827018609193X]

Structure of (tetrahydroselenophene)mercury(II) chloride

C. Stålhandske and F. Zintl



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Acta Cryst. (1986). C42, 1450-1452    [doi:10.1107/S0108270186091928]

Tetraaquatrinitratoeuropium(III) monohydrate

B. Ribár, A. Kapor, Gy. Argay and A. Kálmán


organic compounds



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Acta Cryst. (1986). C42, 1452-1454    [doi:10.1107/S0108270186091916]

Structures of (+)-8,10- and (+)-9,10-dibromocamphor

S. J. Rettig and J. Trotter



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Acta Cryst. (1986). C42, 1454-1455    [doi:10.1107/S0108270186091904]

Structure of 9-bromo-3-endo-methylcamphor

S. J. Rettig and J. Trotter



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Acta Cryst. (1986). C42, 1456-1457    [doi:10.1107/S0108270186091898]

Structure of dimethylmalonic acid, a redetermination

H. Sheng-zhi and T. C. W. Mak



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Acta Cryst. (1986). C42, 1457-1458    [doi:10.1107/S0108270186091886]

Structure of N-(4-amino-3-furazanyl)-2,2,2-trichloro-N'-methoxyacetamidine

C. George and R. Gilardi



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Acta Cryst. (1986). C42, 1458-1460    [doi:10.1107/S0108270186091874]

Structure of a 1,2-diazepine analogue of a diaza[24](1,2,4,5)cyclophane

A. W. Hanson



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Acta Cryst. (1986). C42, 1460-1461    [doi:10.1107/S0108270186091862]

Absolute crystal structure of an N-acylsultam derivative

G. Bernardinelli, W. Oppolzer and D. Dupuis



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Acta Cryst. (1986). C42, 1462-1463    [doi:10.1107/S0108270186091850]

Structure of 5-hydroxy-2-1,3,2[lambda]5-dioxaphosphacyclohexane 2-oxide

T. A. Hamor


short communications



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Acta Cryst. (1986). C42, 1463-1464    [doi:10.1107/S0108270186091849]

Structure of the isothiocyanate salt of trans-aqua(isothiocyanato)(1,4,8,12-tetraazacyclopentadecane)chromium(III): a centrosymmetric refinement

W. Clegg


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