Acta Crystallographica Section C

Crystal Structure Communications

Volume 43, Part 2 (February 1987)



research papers


inorganic compounds



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Acta Cryst. (1987). C43, 175-177    [doi:10.1107/S0108270187096549]

Structure of hexasodium dihydrogendivanadodiperiodate decahydrate

Y. Michiue, H. Ichida and Y. Sasaki



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Acta Cryst. (1987). C43, 177-179    [doi:10.1107/S0108270187096537]

Structure du tétratriacontasulfure d`octadécaindium et d`heptaétain

A. Likforman, M. Guittard et S. Jaulmes



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Acta Cryst. (1987). C43, 179-182    [doi:10.1107/S0108270187096525]

Structure of rubidium selenate at room temperature

I. Takahashi, A. Onodera and Y. Shiozaki



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Acta Cryst. (1987). C43, 182-184    [doi:10.1107/S0108270187096513]

Structure of strontium diselenite

H. Effenberger



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Acta Cryst. (1987). C43, 184-186    [doi:10.1107/S0108270187096501]

Structure of Cs6Zn5(MoO4)8

M. Mueller, B. O. Hildmann and Th. Hahn



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Acta Cryst. (1987). C43, 187-189    [doi:10.1107/S0108270187096495]

Structure of the occupationally disordered crystal of diphosphorus diarsenic trisulfide

B. H. Christian, R. J. Gillespie and J. F. Sawyer



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Acta Cryst. (1987). C43, 189-191    [doi:10.1107/S0108270187096483]

Electron-density distribution in crystals of ammonium tetrachlorozincate(II) chloride at 120 K

S. Ohba, K. Shiokawa and Y. Saito



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Acta Cryst. (1987). C43, 191-194    [doi:10.1107/S0108270187096471]

Structures of cadmium nitrite dihydrate and cadmium dipotassium tetranitrite

S. Ohba, F. Matsumoto, H. Takazawa and Y. Saito



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Acta Cryst. (1987). C43, 194-197    [doi:10.1107/S010827018709646X]

Hydrogénophosphate de zinc hydrate

A. Riou, Y. Cudennec et Y. Gerault



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Acta Cryst. (1987). C43, 197-201    [doi:10.1107/S0108270187096458]

The pseudo-orthorhombic structure of caesium dihydrogendecavanadate tetrahydrate

G. Rigotti, B. E. Rivero and E. E. Castellano



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Acta Cryst. (1987). C43, 201-202    [doi:10.1107/S0108270187096446]

Synthèse et structure cristalline de LiInP2O7

D. Tran Qui, S. Hamdoune et Y. Le Page


metal-organic compounds



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Acta Cryst. (1987). C43, 203-205    [doi:10.1107/S0108270187096434]

Structure of nonacarbonyl-tri-[mu]-hydrido-[mu]3-(p-tolylmethylidyne)-triangulo-triruthenium, ([mu]-H)3Ru3(CO)9[[mu]3-CC6H4(p-CH3)]

M. R. Churchill, T. P. Duggan, J. B. Keister and J. W. Ziller



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Acta Cryst. (1987). C43, 205-207    [doi:10.1107/S0108270187096422]

Structure of 3,4;3',4'-bis(ethylenedithio)-2,2',5,5'-tetrathiafulvalene-dichlorocuprate (BEDT-TTF)CuCl2

A. Kawamoto, J. Tanaka and M. Tanaka



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Acta Cryst. (1987). C43, 207-209    [doi:10.1107/S0108270187096410]

Structure of [mu]-perchlorato-bis[N,N'-bis([beta]-carbamoylethyl)-N,N'-dimethylethylenediaminecopper(II)] perchlorate

T.-H. Lu, H.-C. Shan, M.-S. Chao and C.-S. Chung



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Acta Cryst. (1987). C43, 209-213    [doi:10.1107/S0108270187096409]

Structures of three copper complexes with 2-dimethylaminomethyl-4-phenylphenol

Y.-L. Lee, W. J. Burke and R. B. Von Dreele



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Acta Cryst. (1987). C43, 214-216    [doi:10.1107/S0108270187096392]

Structure of (carbonyl)chloro(hydrido)tris(methyldiphenylphosphine)ruthenium(II)

M. Motevalli, M. B. Hursthouse, A. R. Barron and G. Wilkinson



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Acta Cryst. (1987). C43, 216-218    [doi:10.1107/S0108270187096380]

Structure du complexe diperchlorate de [mu]-[fumarato(2-)-O',O'',O''',O'''']-bis{[N,N-bis(diéthylaminoéthyl)-éthylamine]cuivre(II)

P. Charpin, G. Chevrier, M. Lance, D. Vigner et F. Tinti



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Acta Cryst. (1987). C43, 218-221    [doi:10.1107/S0108270187096379]

Tetraphenylphosphonium-bispentachlorowolfram-[mu]-dinitrido-sulfat(II)-dichlormethan (1/2)

W. Willing, K. Hösler, U. Müller and K. Dehnicke



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Acta Cryst. (1987). C43, 221-224    [doi:10.1107/S0108270187096367]

([eta]5-Cyclopentadienyl){[eta]4-[1,3-bis(4-methoxyphenyl)-2,4-bis(trimethylsilyl)]cyclobutadiene}cobalt(I) (1) and ([eta]5-cyclopentadienyl){[eta]4-[1,3-bis(trifluoromethylphenyl)-2,4-bis(trimethylsilyl)]cyclobutadiene}cobalt(I) (2)

T. Debaerdemaeker, D. Grafl and H. A. Brune



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Acta Cryst. (1987). C43, 224-226    [doi:10.1107/S0108270187096355]

Structure of [N(CH3)4][VOF3(H2O)]

J. Darriet, Q. Xu and A. Tressaud



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Acta Cryst. (1987). C43, 226-229    [doi:10.1107/S0108270187096343]

Intramolecular hydrogen bonding in dichlorotetrakis(pyrazole-N2)nickel(II) as studied by low-temperature neutron diffraction, X-ray diffraction and infrared spectroscopy

R. B. Helmholdt, W. Hinrichs and J. Reedijk



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Acta Cryst. (1987). C43, 229-231    [doi:10.1107/S0108270187096331]

Structure of [mu]-hydrido-bis(hydrido)bis(pentamethylcyclopentadienyl)bis(trimethylphosphino)diiridium hexafluorophosphate

C. J. Burns, N. M. Rutherford and D. J. Berg



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Acta Cryst. (1987). C43, 231-233    [doi:10.1107/S010827018709632X]

Structure du bis(N,N-di-n-butyl diméthyl-3,3 butanamide)dinitratodioxouranium(VI)

P. Charpin, M. Lance, M. Nierlich, D. Vigner et C. Musikas



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Acta Cryst. (1987). C43, 233-236    [doi:10.1107/S0108270187096318]

Amminebis(pentamethylcyclopentadienyl)(thiophenolato)ytterbium(III)

A. Zalkin, T. J. Henly and R. A. Andersen



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Acta Cryst. (1987). C43, 236-238    [doi:10.1107/S0108270187096306]

Structure of bis(2-methyl-1,2-propanediamine)nickel(II) diperchlorate

S. García-Granda, P. T. Beurskens, H. J. J. Behm and F. Gómez-Beltrán



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Acta Cryst. (1987). C43, 238-241    [doi:10.1107/S010827018709629X]

Structure du cyclobutanedicarboxylate-1,1 acide de potassium

S. Jaulmes, P. Laruelle and E. Fabrègue



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Acta Cryst. (1987). C43, 241-243    [doi:10.1107/S0108270187096288]

Structure of catena-poly[tri-[mu]-cyano-(ammine)(4-chloropyridine)cadmium-[mu]-cyano-nickel]

O. Büyükgüngör and D. Ülkü



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Acta Cryst. (1987). C43, 243-245    [doi:10.1107/S0108270187096276]

cis-Dicarbonylbis[(2-phenylazo)phenyl]ruthenium(II)

M. I. Bruce, O. bin Shawkataly, M. R. Snow and E. R. T. Tiekink


organic compounds



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Acta Cryst. (1987). C43, 245-249    [doi:10.1107/S0108270187096264]

Structures of five N,N'-bis[(dialkoxyphosphinoyl)methyl]-1,4-benzenediamines

V. Nastopoulos, G. Germain, J. Kallitsis and S. Voliotis



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Acta Cryst. (1987). C43, 249-251    [doi:10.1107/S0108270187096252]

Methyl carbamate

B. Sepehrnia, J. R. Ruble and G. A. Jeffrey



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Acta Cryst. (1987). C43, 251-254    [doi:10.1107/S0108270187096240]

Structure of 9-acetoxy-10-(4-acetoxyphenyl)anthracene at 95 K

A. Roszak and W. L. Duax



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Acta Cryst. (1987). C43, 254-256    [doi:10.1107/S0108270187096239]

Structure of 1-nitro-7H-benzo[h,i]chrysen-7-one

S. Fujisawa, I. Oonishi, J. Aoki and Y. Ohashi



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Acta Cryst. (1987). C43, 256-259    [doi:10.1107/S0108270187096227]

Structure of 5-tritylamino-1,4-dihydronaphthalene

C. W. Holzapfel, G. J. Kruger and M. S. Van Dyk



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Acta Cryst. (1987). C43, 259-260    [doi:10.1107/S0108270187096215]

Structure of 3,4-dimethylthiazole-2-thione

F. Ugozzoli and G. D. Andreetti



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Acta Cryst. (1987). C43, 260-263    [doi:10.1107/S0108270187096203]

A new polymorph of dibenzoylmethane

M. C. Etter, D. A. Jahn and Z. Urbanczyk-Lipkowska



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Acta Cryst. (1987). C43, 263-266    [doi:10.1107/S0108270187096197]

Structures of (+)-(R)-[alpha]-methylbenzylammonium (+)-(1S,6R,7S)-bicyclo[4.1.0]hept-2-ene-7-carboxylate (I) and (+)-(R)-[alpha]-methylbenzylammonium (+)-(1R,8S,9R)-bicyclo[6.1.0]non-2-ene-9-carboxylate (II)

K. Yanagi and T. Aratani



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Acta Cryst. (1987). C43, 266-269    [doi:10.1107/S0108270187096185]

Substituent effects of [pi] acceptors to prismane. Structure of methyl 2,3,5,6-tetramethyl-4-phenylprismanecarboxylate and theoretical calculations on formylprismane

H. Irngartinger, D. Kallfass, E. Litterst and R. Gleiter



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Acta Cryst. (1987). C43, 269-272    [doi:10.1107/S0108270187096173]

Structure and stereochemistry of 2-(N-methylaniline)-3-(N-methoxyaceto)-7-(p-chlorophenyl)-8-methoxy-4,5-benzo-3-aza-1-nonem

M. Soriano-García, R. A. Toscano, E. Cortés, M. C. Romero and I. Ceballos



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Acta Cryst. (1987). C43, 272-274    [doi:10.1107/S0108270187096161]

Structure and stereochemistry of 2-hydroxy-12(S)-hydroxyneoclerodane-3,13(14)-diene-15,16;19,20-diolide (semiatrin), a diterpene

M. Soriano-García, R. A. Toscano, B. Esquivel, M. Hernández and L. Rodríguez-Hahn



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Acta Cryst. (1987). C43, 274-278    [doi:10.1107/S010827018709615X]

The structures of epinine-O-sulfates

D. S. Eggleston, A. M. Tickner and W. L. Mendelson



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Acta Cryst. (1987). C43, 278-280    [doi:10.1107/S0108270187096148]

Structure of cyclohexane tetramethylene diperoxide diamine

J. T. Fourkas, W. P. Schaefer and R. E. Marsh



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Acta Cryst. (1987). C43, 280-282    [doi:10.1107/S0108270187096136]

Structure of methyl 4-hydroxy-2-methyl-2H-1,2-benzothiazine-3-carboxylate 1,1-dioxide

L. Golic and I. Leban



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Acta Cryst. (1987). C43, 282-284    [doi:10.1107/S0108270187096124]

Structure of 4-tert-butyl-1-phenoxy-1-[lambda]5-phosphorinane 1-oxide

Mazhar-ul-Haque, J. Ahmed and W. Horne



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Acta Cryst. (1987). C43, 284-287    [doi:10.1107/S0108270187096112]

Structure du morpholino o-nitrobenzènesélénénamide

C. Gicquel-Mayer, G. Perez, P. Lerouge et C. Paulmier



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Acta Cryst. (1987). C43, 287-289    [doi:10.1107/S0108270187096100]

Structure of 5-oxo-2-pyrrolidinylphosphonic acid

W. Sawka-Dobrowolska and E. Gruszecka-Kowalik



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Acta Cryst. (1987). C43, 289-291    [doi:10.1107/S0108270187096094]

Structure of 4-amino-4-phosphonobutyric acid

W. Sawka-Dobrowolska and E. Gruszecka-Kowalik



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Acta Cryst. (1987). C43, 291-293    [doi:10.1107/S0108270187096082]

Structure of 2,5,5-trimethyl-3-oxo-7-t-hydroxy-1-cycloheptanephosphonoacetic acid [gamma]-lactone diethyl ester

W. Sawka-Dobrowolska and F. Rulko



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Acta Cryst. (1987). C43, 294-296    [doi:10.1107/S0108270187096070]

Structure of 4-tert-butyl-2,6-dimethylacetophenone and comparison with its FeCl3 complex

H. van Koningsveld, J. J. Scheele and J. C. Jansen



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Acta Cryst. (1987). C43, 296-300    [doi:10.1107/S0108270187096069]

Hydrated proton complexes in methyl 3-sulfoorsellinate tetrahydrate

A. W. Hanson



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Acta Cryst. (1987). C43, 300-303    [doi:10.1107/S0108270187096057]

Bond length and reactivity: the Beckmann rearrangement. 5. Structure of 4-phenylcyclohexanone oxime O-4-nitrobenzoate ester at 290 K

M. R. Edwards, A. J. Kirby, P. R. Raithby and P. G. Jones



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Acta Cryst. (1987). C43, 303-306    [doi:10.1107/S0108270187096045]

Structure of (8S)-8-hydroxymethyl-6,9-diazaspiro[4.5]decane-7,10-dione, a spirocyclic dipeptide

J. Symerský, K. Bláha and V. Langer



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Acta Cryst. (1987). C43, 306-309    [doi:10.1107/S0108270187096033]

4,17-Diacetyl-3[alpha],8,12[alpha],18[beta]-tetramethyl-4,5,7,14,16,17-hexaazapentacyclo[10.6.2.02,11.03,8.013,18]icosa-5,7,9,13,15,19-hexaene (Ia) 0·5-methanol solvate and trimethyl 2[alpha],8[beta]-dimethyl-3,4,6-triazatricyclo[6.2.2.02,7]dodeca-4,6,9,11-tetraene-3,9,10-tricarboxylate (IIb)

G. Filippini and T. Pilati



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Acta Cryst. (1987). C43, 309-311    [doi:10.1107/S0108270187096021]

Structure of 2-phenyladamantan-2-ol

F. A. J. Singelenberg and B. P. van Eijck



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Acta Cryst. (1987). C43, 311-313    [doi:10.1107/S010827018709601X]

Structure of 4-hydroxymonophenylbutazone

V. Dhanaraj and M. Vijayan



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Acta Cryst. (1987). C43, 313-316    [doi:10.1107/S0108270187096008]

Structure of thiamin dinitrate

D. S. C. Yang, J. Pletcher, J. P. Rose, C. S. Yoo, W. Furey, B.-C. Wang and M. Sax



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Acta Cryst. (1987). C43, 316-319    [doi:10.1107/S0108270187095994]

Structure and absolute configuration of a phenylpiperidine analgesic 3-(m-methoxyphenyl)-3-methylpiperidinium hydrogen tartrate

L. Y. Y. Ma and N. Camerman



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Acta Cryst. (1987). C43, 319-322    [doi:10.1107/S0108270187095982]

Structure of 11[beta]-[4-(dimethylamino)phenyl]-17[beta]-hydroxy-17[alpha]-(2-propenyl)-estra-4,9-dien-3-one

V. J. van Geerestein, J. A. Kanters and J. Kroon



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Acta Cryst. (1987). C43, 322-324    [doi:10.1107/S0108270187095970]

Hexamethylenetetramine monohydrochloride

M. Chou, L. Lessinger and M. Chiang



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Acta Cryst. (1987). C43, 324-326    [doi:10.1107/S0108270187095969]

Structure of 7a-hydroxy-4-phenyl-1,2,4,4a,5,6,7,7a-octahydrocyclopenta[d][1,3]thiazine-2-thione

Gy. Argay, A. Kálmán, P. Perjési and D. Szabó



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Acta Cryst. (1987). C43, 326-329    [doi:10.1107/S0108270187095957]

Structure of 1,2-dihydro-1,2,2-tris[(2-hydroxyphenyl)methyl]-3H-indol-3-one (uvarindole D)

M. A. Meek, C. H. Schwalbe, P. G. Waterman and I. Mohammad



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Acta Cryst. (1987). C43, 330-333    [doi:10.1107/S0108270187095945]

Structure of 6-methylisocytosine

P. R. Lowe, C. H. Schwalbe and G. J. B. Williams



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Acta Cryst. (1987). C43, 333-335    [doi:10.1107/S0108270187095933]

Structure of (1S,6S,8S,9S,1'S)-8-(1'-hydroxyethyl)-9-hydroxymethyl-1,5,5-trimethylbicyclo[4.3.0]nonane

J. L. Briansó, J. F. Piniella, G. Germain and X. Solans



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Acta Cryst. (1987). C43, 335-339    [doi:10.1107/S0108270187095921]

Structure of 1-acetyl-2,4,5,7-tetrahydroxy-9,10-anthracenedione

L. Ulický, V. Kettmann, J. Soldánová and V. Betiba



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Acta Cryst. (1987). C43, 340-342    [doi:10.1107/S010827018709591X]

Structure of 1-benzyl-2,2,3,3-tetramethyl-1-phenylphosphetanium bromide, a cyclobutane derivative

J. A. Campbell, R. Larsen, C. Campana and S. E. Cremer



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Acta Cryst. (1987). C43, 342-344    [doi:10.1107/S0108270187095908]

4-Benzylidene-2,3,4,5-tetrahydro-1-benzoxepin-5-one

A. Katrusiak, M. Ratajczak-Sitarz, Z. Kaluski, V. D. Orlov, U. A. Borovoi and E. I. Mihedkina



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Acta Cryst. (1987). C43, 344-347    [doi:10.1107/S0108270187095891]

Structures of N-trityl-L-aspartate dibenzyl ester and N-trityl-L-leucine benzyl ester

P. Cordopatis, S. Voliotis, V. Nastopoulos, G. Germain and P. Main



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Acta Cryst. (1987). C43, 347-349    [doi:10.1107/S010827018709588X]

Structure of 1,3,4-thiadiazole-2,5-diamine

H. Senda and J. Maruha



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Acta Cryst. (1987). C43, 349-351    [doi:10.1107/S0108270187095878]

Structure of cyclo(-L-methionyl-L-prolyl-)

V. M. Padmanabhan and V. S. Jakkal


short format


metal-organic compounds



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Acta Cryst. (1987). C43, 352-353    [doi:10.1107/S0108270187095866]

Structure of bis(tetra-n-butylammonium) 1,2,3;1,2,4;1,3,4;2,3,4-tetra-[mu]3-sulfido-tetrakis[(benzenethiolato)iron]

G. Lin, H. Zhang, S.-z. Hu and T. C. W. Mak



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Acta Cryst. (1987). C43, 354-355    [doi:10.1107/S0108270187095854]

Structure of tris(1-3-[eta]-indenyl)uranium bromide

M. R. Spirlet, J. Rebizant and J. Goffart



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Acta Cryst. (1987). C43, 355-357    [doi:10.1107/S0108270187095842]

Bis(triphenylphosphoranediyl)ammonium tetrachloronitridomolybdate(IV)

P. G. Jones, T. Schroeder and G. M. Sheldrick



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Acta Cryst. (1987). C43, 357-358    [doi:10.1107/S0108270187095830]

Bis(triphenylphosphoranediyl)ammonium tetrachloroferrate(III)

P. G. Jones, T. Schroeder and G. M. Sheldrick


organic compounds



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Acta Cryst. (1987). C43, 358-360    [doi:10.1107/S0108270187095829]

Helenalin, a pseudoguaianolide from Helenium amarum

F. R. Fronczek, A. G. Ober and N. H. Fischer



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Acta Cryst. (1987). C43, 360-361    [doi:10.1107/S0108270187095817]

Structure of a local anaesthetic: dyclonine hydrochloride

B. K. Sinha, V. Pattabhi, M. Nethaji and E. J. Gabe



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Acta Cryst. (1987). C43, 362-363    [doi:10.1107/S0108270187095805]

Structure of a substituted isoxazoline

C. George and R. Gilardi



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Acta Cryst. (1987). C43, 363-364    [doi:10.1107/S0108270187095799]

Structure of an azapyrimidine derivative

R. Gilardi and C. George



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Acta Cryst. (1987). C43, 364-366    [doi:10.1107/S0108270187095787]

Bis(m-nitrobenzyl) ether

P. G. Jones



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Acta Cryst. (1987). C43, 366-367    [doi:10.1107/S0108270187095775]

1-(4-Nitrophenyl)ethyl p-toluenesulfonate

P. G. Jones, K. Meyer-Bäse and G. M. Sheldrick



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Acta Cryst. (1987). C43, 367-368    [doi:10.1107/S0108270187095763]

Bis(cyclohexylammonium) hydrogenphosphate

P. G. Jones



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Acta Cryst. (1987). C43, 369-370    [doi:10.1107/S0108270187095751]

Bis(triphenylphosphoranediyl)ammonium 2,5,7-tricyanoimidazo[3,4-b][1,2,4]triazol-1-ide, a salt of the C7N7- anion

P. G. Jones, W. Pinkert and G. M. Sheldrick



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Acta Cryst. (1987). C43, 370-372    [doi:10.1107/S010827018709574X]

[alpha]-[2',5'-Bis(methoxymethyl)phenyl]-3,4,5-trimethoxyphenylacetonitrile

P. de Meester, S. P. Khanapure, S. S. C. Chu and E. R. Biehl



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Acta Cryst. (1987). C43, 372-374    [doi:10.1107/S0108270187095738]

Structure of the tri-O-isopropylidene derivative of D-glucosone hydrate

C. W. Holzapfel, G. J. Kruger, M. S. Van Dyk and L. den Drijver



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Acta Cryst. (1987). C43, 374-375    [doi:10.1107/S0108270187095726]

Diphenyl(2,2-diphenylvinyloxy)acetaldehyde

H. Preut, R. Stapel and W. P. Neumann



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Acta Cryst. (1987). C43, 375-376    [doi:10.1107/S0108270187095714]

Structure of S-benzyl-L-cysteine methyl ester hydrochloride

V. Nastopoulos, G. Germain, P. Cordopatis and S. Voliotis



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Acta Cryst. (1987). C43, 377-378    [doi:10.1107/S0108270187095702]

Structure of 2,5,7,9-tetrathiabicyclo[4.3.0]non-1(6)-en-8-one (TTBEO)

C. Tucker, J. Welch and R. Bereman



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Acta Cryst. (1987). C43, 378-380    [doi:10.1107/S0108270187095696]

Structure of 7-phenylthio-1,4-dioxaspiro[4.5]decan-8-one

V. M. Lynch, B. E. Wiechman and J. C. Gilbert


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