Acta Crystallographica Section C

Crystal Structure Communications

Volume 43, Part 6 (June 1987)



research papers


inorganic compounds



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Acta Cryst. (1987). C43, 1015-1019    [doi:10.1107/S010827018709317X]

Location and anisotropic refinement of deuterium atoms in disodium dideuteriumsilicate heptahydrate (D2O) by neutron diffraction; hydrogen bonding at 296 K and thermal properties

J. Felsche, B. Ketterer, R. L. Schmid and D. Gregson



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Acta Cryst. (1987). C43, 1019-1022    [doi:10.1107/S0108270187093168]

Redetermination of the structures of CuTaS3 and Nb2Se9

S. A. Sunshine and J. A. Ibers



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Acta Cryst. (1987). C43, 1022-1025    [doi:10.1107/S0108270187093156]

Absolute structure of LiH2AsO4

E. Fanchon, J. Vicat, D. Tran Qui and A. Boudjada



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Acta Cryst. (1987). C43, 1025-1027    [doi:10.1107/S0108270187093144]

Die Struktur des Monoklinen Tetranatriumdivanadathydrats

K. Kato and E. Takayama-Muromachi



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Acta Cryst. (1987). C43, 1027-1030    [doi:10.1107/S0108270187093132]

Die Struktur des Tetrakaliumdivanadatdihydrats

K. Kato and E. Takayama-Muromachi



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Acta Cryst. (1987). C43, 1030-1032    [doi:10.1107/S0108270187093120]

Die Struktur des Trinatriumvanadattrihydrats

K. Kato and E. Takayama-Muromachi



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Acta Cryst. (1987). C43, 1033-1036    [doi:10.1107/S0108270187093119]

The monoclinic perovskites Sr2CaUO6 and Ba2SrUO6. A Rietveld refinement of neutron powder diffraction data

W. A. Groen and D. J. W. IJdo


metal-organic compounds



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Acta Cryst. (1987). C43, 1036-1038    [doi:10.1107/S0108270187093107]

Structure of the binuclear rhodium(II) complex dichloro-di-[mu]-formato-bis(1,10-phenanthroline)dirhodium(II)

T. Glowiak, H. Pasternak and F. Pruchnik



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Acta Cryst. (1987). C43, 1038-1042    [doi:10.1107/S0108270187093090]

The structure of Ni(cyclam)(ClO4)2

L. Prasad, S. C. Nyburg and A. McAuley



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Acta Cryst. (1987). C43, 1042-1045    [doi:10.1107/S0108270187093089]

Coordination chemistry of alkali and alkaline earth cations: the structure of bis(3,5-dinitrobenzoato)(tetraethyleneglycol)strontium(II) monohydrate

J. A. Kanters, S. Harder and N. S. Poonia



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Acta Cryst. (1987). C43, 1045-1048    [doi:10.1107/S0108270187093077]

Bis[[mu]-{[(R)-1,1-bis(2-butoxy-5-tert-butylphenyl)-3-phenyl-2-salicylideneamino-1-propanolato]-O}copper(II)]: a phenolic-oxygen-bridged binuclear copper(II) complex with a chiral Schiff base

K. Yanagi and M. Minobe



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Acta Cryst. (1987). C43, 1048-1050    [doi:10.1107/S0108270187093065]

Chlorure hexachloroplatinate(IV) de bis(pentanediammonium-1,5) (chlorure hexachloroplatinate de cadavérine)

J.-M. Delafontaine, P. Toffoli, P. Khodadad, N. Rodier et R. Julien



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Acta Cryst. (1987). C43, 1050-1053    [doi:10.1107/S0108270187093053]

Structure of bis(2-amino-5-methylpyridinium) tetrachlorocuprate(II) and bis(2-amino-5-methylpyridinium) tetrabromocuprate(II)

H. Place and R. D. Willett



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Acta Cryst. (1987). C43, 1053-1055    [doi:10.1107/S0108270187093041]

Structure of cis-dichlorobis(dimethylphenylphosphine)platinum(II)

W. M. Attia, G. Balducci and M. Calligaris



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Acta Cryst. (1987). C43, 1056-1058    [doi:10.1107/S010827018709303X]

Structure of thorium nitrate-1,4,7,10,13,16-hexaoxacyclooctadecane-water (1/1/3), [Th(OH2)3(NO3)4].18-crown-6 at 123 K

R. D. Rogers, L. K. Kurihara and M. M. Benning



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Acta Cryst. (1987). C43, 1058-1061    [doi:10.1107/S0108270187093028]

Structure of catena-aqua(2,2'-bipyridine)(2-imidazolidinethione-S)-[mu]-[sulfato(2-)-O:O']-cadmium(II) monohydrate and its solid-state 113Cd NMR spectrum

P. F. Rodesiler, N. G. Charles, E. A. H. Griffith and E. L. Amma



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Acta Cryst. (1987). C43, 1061-1064    [doi:10.1107/S0108270187093016]

Structure of (2,4-dinitrophenolato)(triethanolamine)lithium monohydrate

V. M. Padmanabhan, V. S. Jakkal and N. S. Poonia



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Acta Cryst. (1987). C43, 1064-1067    [doi:10.1107/S0108270187093004]

Structure of (2,2'-bipyridyl)(4-hydroxy-L-prolinato)palladium(II) chloride dihydrate

V. M. Padmanabhan and R. P. Patel



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Acta Cryst. (1987). C43, 1067-1069    [doi:10.1107/S0108270187092990]

1-(2,2'-Bipyridyl)-2-methyl-3-(trimethylsilyl)-2,3-dicarba-1-stanna-closo-heptaborane(6)

U. Siriwardane, N. S. Hosmane and S. S. C. Chu



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Acta Cryst. (1987). C43, 1070-1073    [doi:10.1107/S0108270187092989]

Structure of the solid solution [N(CH3)4]2ZnCl1.8Br2.2 in the high- and in a new low-temperature phase

E. Colla, V. Gramlich and W. Petter



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Acta Cryst. (1987). C43, 1073-1075    [doi:10.1107/S0108270187092977]

Structure of the charge-transfer salt bis(methylenedithio)tetrathiafulvalene hexafluoroantimonate(V)

P. J. Nigrey, E. Duesler, H. H. Wang and J. M. Williams



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Acta Cryst. (1987). C43, 1076-1080    [doi:10.1107/S0108270187092965]

Oligoether complexes of alkaline-earth metal ions. I. Structures of 2,5,8,11,14-pentaoxapentadecane (`tetraglyme`) complexed with calcium, strontium and barium thiocyanates

Y. Y. Wei, B. Tinant, J.-P. Declercq, M. Van Meerssche and J. Dale



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Acta Cryst. (1987). C43, 1080-1083    [doi:10.1107/S0108270187092953]

Oligoether complexes of alkaline-earth metal ions. II. Structures of 2,5,8,11-tetraoxadodecane (`triglyme`) complexed with calcium and strontium thiocyanates

Y. Y. Wei, B. Tinant, J.-P. Declercq, M. Van Meerssche and J. Dale



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Acta Cryst. (1987). C43, 1083-1087    [doi:10.1107/S0108270187092941]

Structures of tetrakis(benzylamine)diisothiocyanatonickel(II) and tris(benzylamine)diisothiocyananto(1-phenyl-1-ethylamine)nickel(II)

L. R. Nassimbeni, M. L. Niven and K. J. Zemke



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Acta Cryst. (1987). C43, 1087-1089    [doi:10.1107/S010827018709293X]

Potassium naphthionate

C. J. Brown and H. R. Yadav



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Acta Cryst. (1987). C43, 1089-1091    [doi:10.1107/S0108270187092928]

Bis(methyltriphenylphosphonium) di-[mu]-bromo-dibromodicuprate(I)

S. Andersson and S. Jagner


organic compounds



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Acta Cryst. (1987). C43, 1092-1094    [doi:10.1107/S0108270187092916]

Benzyltrimethylammonium p-nitrophenolate trihydrate

G. L. Butt, M. F. Mackay and R. D. Topsom



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Acta Cryst. (1987). C43, 1094-1097    [doi:10.1107/S0108270187092904]

Structure of 1,2,3,3a-tetrahydro-3a,7-diphenyl-5-(p-tolyl)pyrazolo[1,5-a]pyridine-3-carbonitrile

N. O. Pante, H. Beltrami, X. Ysern and M. V. Capparelli



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Acta Cryst. (1987). C43, 1097-1100    [doi:10.1107/S0108270187092898]

Triamterene

C. H. Schwalbe and G. J. B. Williams



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Acta Cryst. (1987). C43, 1100-1103    [doi:10.1107/S0108270187092886]

Structure of (6,7)-benzo-2,3,4[alpha],4a[beta],8a[beta]-pentamethyl-4a[beta],5,8,8a[beta]-tetrahydro-1-naphthoquin-4[beta]-ol

S. Ariel and J. Trotter



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Acta Cryst. (1987). C43, 1103-1105    [doi:10.1107/S0108270187092874]

Structure of (6,7)-benzo-2,3,4a[beta],8a[beta]-tetramethyl-4a,5,8,8a-tetrahydro-1-naphthoquin-4[beta]-yl acetate

S. Ariel and J. Trotter



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Acta Cryst. (1987). C43, 1106-1108    [doi:10.1107/S0108270187092862]

L-Aspartyl([beta]-benzyl ester)glycylglycine methyl ester trifluoroacetic acid [L-Asp([beta]-Bzl)-Gly-Gly-OMe.Tfa]

S. Capasso, F. Sica and A. Zagari



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Acta Cryst. (1987). C43, 1108-1112    [doi:10.1107/S0108270187092850]

Structures of new salts: S-methylthiouronium-TCNQ (I) and Se-methylselenouronium-TCNQ (II)

G. G. Abashev, R. M. Vlasova, N. F. Kartenko, A. M. Kuzmin, I. V. Rozhdestvenskaya, V. N. Semkin, O. A. Usov and V. S. Russkikh



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Acta Cryst. (1987). C43, 1112-1114    [doi:10.1107/S0108270187092849]

Structure of (1S*,5S*,SR*)-1-(3-p-toluenesulfinyl-2-propenyl)-2-methylene-7,7-dimethylbicyclo[3.3.0]octan-3-one

D. H. Hua, I. Badejo, P. J. McCann and F. Takusagawa



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Acta Cryst. (1987). C43, 1114-1116    [doi:10.1107/S0108270187092837]

The structure of 1,5-bis(salicylidene)carbonohydrazide monohydrate

J. Dan, S. Seth and S. Chakraborty



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Acta Cryst. (1987). C43, 1117-1119    [doi:10.1107/S0108270187092825]

Structure of the nematogenic compound 2-cyano-N-[4-(4-n-pentyloxybenzoyloxy)benzylidene]aniline

U. Baumeister, H. Hartung and M. Gdaniec



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Acta Cryst. (1987). C43, 1119-1122    [doi:10.1107/S0108270187092813]

Structures of (-)-cytisine and (-)-N-methylcytisine: tricyclic quinolizidine alkaloids

A. A. Freer, D. J. Robins and G. N. Sheldrake



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Acta Cryst. (1987). C43, 1122-1125    [doi:10.1107/S0108270187092801]

Structures of 4-acetyl-3-(p-tolyl)sydnone (1) and 4-acetyl-3-phenylsydnone oxime (2)

C.-H. Ueng, Y. Wang and M.-Y. Yeh



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Acta Cryst. (1987). C43, 1125-1127    [doi:10.1107/S0108270187092795]

(±)-(5[alpha],8[alpha],9[alpha])-2-Chloro-5,8,9,10-tetrahydro-5,9-methanobenzocycloocten-8-amine hydrochloride sesquihydrate

J. C. Barnes, W. Golnazarians, D. R. Rae and J. Redpath



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Acta Cryst. (1987). C43, 1128-1131    [doi:10.1107/S0108270187092783]

Structure of [alpha]-benzylidene-(±)-piperitone, an exception to topochemical behaviour

D. Kanagapushpam, V. Ramamurthy and K. Venkatesan



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Acta Cryst. (1987). C43, 1131-1134    [doi:10.1107/S0108270187092771]

Structure of 5-(p-aminobenzenesulfonamido)-1-phenylpyrazole (sulfaphenazole)

H. C. Patel and T. P. Singh



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Acta Cryst. (1987). C43, 1134-1138    [doi:10.1107/S010827018709276X]

Structure and molecular-packing analysis of a heptofuranosoimidazolidine-2-thione

M. D. Estrada, A. Conde and R. Márquez



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Acta Cryst. (1987). C43, 1138-1142    [doi:10.1107/S0108270187092758]

Structure of 5-([beta]-D-glucopyranosyl)barbituric acid trihydrate

M. Millan, C. F. Conde, A. Conde and R. Márquez



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Acta Cryst. (1987). C43, 1142-1145    [doi:10.1107/S0108270187092746]

1,1',3,3'-Tetrakis(dimethylamino)-4H,4'H-4,4'-biisoquinolyldiium diperchlorate (II) and 1,1',3,3'-tetrakis(dimethylamino)-4,4'-biisoquinolyl (III)

P. F. Lindley, A. R. Walton, G. V. Boyd, G. A. Nicolaou and O. Hammerich



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Acta Cryst. (1987). C43, 1145-1147    [doi:10.1107/S0108270187092734]

Structure of a novel oxygenated dimer: dilongicyclyl-12-ether

V. G. Puranik, S. S. Tavale, T. N. Guru Row, R. T. Reddy and U. R. Nayak



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Acta Cryst. (1987). C43, 1147-1151    [doi:10.1107/S0108270187092722]

Structure of dichloro(p-methoxyphenyl)(8-oxo-7-oxabicyclo[4.3.0]non-5-yl)tellurium(IV)-chloroform (1/0·27)

S. Husebye, E. A. Meyers, R. A. Zingaro, J. V. Comasseto and N. Petragnani



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Acta Cryst. (1987). C43, 1151-1153    [doi:10.1107/S0108270187092710]

Structure of 10-(2,6-dichlorophenyl)-8-oxa-9-aza[5.3.3]propell-9-en-2-one (DCPOP)

C. A. Kavounis, P. J. Rentzeperis, E. Malamidou-Xenikaki and E. Coutouli-Argyropoulou



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Acta Cryst. (1987). C43, 1153-1155    [doi:10.1107/S0108270187092709]

Structure of (5RS,6RS)-1,5-diacetyl-6-benzoxymethyl-2-hydroxy-4-methyl-1,3-cyclohexadiene

E. Moreno, S. Perez, A. López-Castro and R. Márquez



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Acta Cryst. (1987). C43, 1156-1158    [doi:10.1107/S0108270187092692]

Structure of 3,10-dithiabicyclo[10.2.2]hexadeca-12,14(1),15-triene

T. Sakai, Z. Taira and S. Ueji



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Acta Cryst. (1987). C43, 1158-1160    [doi:10.1107/S0108270187092680]

Structure of a galacto-benzofuranone oxime

M. J. Diánez, R. Vega, A. López-Castro and R. Márquez



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Acta Cryst. (1987). C43, 1161-1163    [doi:10.1107/S0108270187092679]

Structure and stereochemistry of 11-(o-chlorophenyl)-3,3-dimethyl-2,3,4,5,10,11-hexahydro-1H-dibenzo[b,e][1,4]diazepin-1-one hemiethanol solvate

M. Soriano-García, E. Cortés, R. A. Toscano, M. delR. Arellano and R. Martínez



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Acta Cryst. (1987). C43, 1163-1166    [doi:10.1107/S0108270187092667]

Structure of (3[beta],25R)-spirost-5-ene-3,17-diol hemihydrate (pennogenin)

M. Soriano-García, I. López y Celis, R. A. Toscano, J. M. Barba Chávez, P. Enríquez, A. Hernández R. and A. Rodríguez



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Acta Cryst. (1987). C43, 1166-1168    [doi:10.1107/S0108270187092655]

Structure of 1,5-bis[(4-ethylphenyl)amino]-9,10-anthracenedione

J. K. Foitzik, H. Paulus and U. Quotschalla



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Acta Cryst. (1987). C43, 1168-1171    [doi:10.1107/S0108270187092643]

Tétrabenzo[c,h,l,q]-(tétrathia-1,2,10,11 tétraaza-5,7,14,16 cyclooctadécane)

L. Balde, N. Rodier, J. Mayrargue, M. Miocque, D. Besanty et G. E. Moussa



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Acta Cryst. (1987). C43, 1171-1173    [doi:10.1107/S0108270187092631]

Structure of 4,4'-dimethyl-2,2'-bithiazole

A. Bolognesi, M. Catellani, S. Destri and W. Porzio



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Acta Cryst. (1987). C43, 1173-1174    [doi:10.1107/S010827018709262X]

Structure du chloro-3 méthyl-2 4H-pyrazino[1,2-a]pyrimidinone-4

C. Sablayrolles, J. P. Chapat, B. Ducourant et R. Fourcade



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Acta Cryst. (1987). C43, 1175-1177    [doi:10.1107/S0108270187092618]

Structure of ammonium trichloroacetate-water (1/2·5)

H. Kiriyama, T. Doi and Y. Yamagata



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Acta Cryst. (1987). C43, 1177-1179    [doi:10.1107/S0108270187092606]

Structure of the E isomer of 5-benzylidene-1-methyl-2,4-imidazolidinedione

M. G. B. Drew, K. F. Mok, K. P. Ang and S. F. Tan



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Acta Cryst. (1987). C43, 1179-1182    [doi:10.1107/S010827018709259X]

Substituted cyclopropanes. 1. trans-1,2,3-Tricyanocyclopropane

P. G. Jones and G. Schrumpf



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Acta Cryst. (1987). C43, 1182-1185    [doi:10.1107/S0108270187092588]

Substituted cyclopropanes. 2. cis-1,2,3-Trichlorocyclopropane

G. Schrumpf and P. G. Jones



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Acta Cryst. (1987). C43, 1185-1187    [doi:10.1107/S0108270187092576]

Substituted cyclopropanes. 3. Hexachlorocyclopropane (redetermination)

G. Schrumpf and P. G. Jones



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Acta Cryst. (1987). C43, 1188-1192    [doi:10.1107/S0108270187092564]

Substituted cyclopropanes. 4. cis-1,2,3-Tribromocyclopropane and hexabromocyclopropane

G. Schrumpf and P. G. Jones



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Acta Cryst. (1987). C43, 1192-1195    [doi:10.1107/S0108270187092552]

Diketones from the oxidation of two syn-sesquinorbornene derivatives

W. H. Watson, I. Tavanaiepour, R. P. Kashyap, P. D. Bartlett and R. Banavali



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Acta Cryst. (1987). C43, 1195-1197    [doi:10.1107/S0108270187092540]

Structure of 3-methyladenine hydrochloride

Y. Yamagata and K.-i. Tomita



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Acta Cryst. (1987). C43, 1197-1200    [doi:10.1107/S0108270187092539]

Thermally induced acyl migration in salicylamides. 1. Structures of the reactants, O-acetylsalicylamide and O-benzoylsalicylamide

K. Vyas, V. Mohan Rao and H. Manohar



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Acta Cryst. (1987). C43, 1201-1204    [doi:10.1107/S0108270187092527]

Thermally induced acyl migration in salicylamides. 2. Structures of the products, N-acetylsalicylamide and N-benzoylsalicylamide

K. Vyas, V. Mohan Rao and H. Manohar



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Acta Cryst. (1987). C43, 1204-1206    [doi:10.1107/S0108270187092515]

Structure of dodecyldimethylpropylammonium bromide hemihydrate

T. Taga, K. Machida, N. Kimura, S. Hayashi, J. Umemura and T. Takenaka



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Acta Cryst. (1987). C43, 1206-1209    [doi:10.1107/S0108270187092503]

Structure of 17[alpha]-ethynylestra-1,3,5(10)-trien-3,17[beta]-diol hemihydrate (ethynyl estradiol)

V. J. van Geerestein


short format


metal-organic compounds



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Acta Cryst. (1987). C43, 1209-1211    [doi:10.1107/S0108270187092497]

Structure of trans-dicyanobis(ethylenediamine)cobalt(III) perchlorate

H. Wunderlich



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Acta Cryst. (1987). C43, 1211-1212    [doi:10.1107/S0108270187092485]

Structure of dichlorobis(N-isopropylideneaniline)palladium(II)

W. Clegg, J. Barker and M. Kilner



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Acta Cryst. (1987). C43, 1212-1213    [doi:10.1107/S0108270187092473]

Structure of (benzylideneacetone)tricarbonyliron (monoclinic form)

E. J. M. Hamilton, D. E. Smith and A. J. Welch



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Acta Cryst. (1987). C43, 1214-1215    [doi:10.1107/S0108270187092461]

Structure of tris(acetonitrile)tricarbonyltungsten

E. J. M. Hamilton, D. E. Smith and A. J. Welch



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Acta Cryst. (1987). C43, 1215-1216    [doi:10.1107/S010827018709245X]

[N,N'-Bis(2-aminoethyl)-1,4-diazacycloheptane-N,N',N'',N''']nickel(II) diperchlorate

M. R. Snow and E. R. T. Tiekink



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Acta Cryst. (1987). C43, 1216-1218    [doi:10.1107/S0108270187092448]

Structure of an [eta]2-phosphaalkene nickel complex

A. L. Spek and A. J. M. Duisenberg



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Acta Cryst. (1987). C43, 1218-1219    [doi:10.1107/S0108270187092436]

Structure of vanadyl diformate monohydrate

D. Mootz and R. Seidel


organic compounds



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Acta Cryst. (1987). C43, 1220-1221    [doi:10.1107/S0108270187092424]

Stereochemical studies of oligomers. XIX. 1,5-Pentanediyl bis(p-chlorobenzoate)

G. Bocelli and M.-F. Grenier-Loustalot



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Acta Cryst. (1987). C43, 1221-1223    [doi:10.1107/S0108270187092412]

Stereochemical studies of oligomers. XX. 2,2'-[1,3-Phenylenebis(oxymethylene)]bisoxirane

G. Bocelli and M.-F. Grenier-Loustalot



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Acta Cryst. (1987). C43, 1223-1224    [doi:10.1107/S0108270187092400]

Stereochemical studies of oligomers. XXI. 1,12-Dodecanediyl bis(m-chlorobenzoate)

G. Bocelli and M.-F. Grenier-Loustalot



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Acta Cryst. (1987). C43, 1224-1226    [doi:10.1107/S0108270187092394]

Stereochemical studies of oligomers. XXII. 1,8-Octanediyl bis(p-chlorobenzoate)

G. Bocelli and M.-F. Grenier-Loustalot



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Acta Cryst. (1987). C43, 1226-1228    [doi:10.1107/S0108270187092382]

Structure of ethyl 2-cyanomethyl-1-[beta]-D-arabinofuranosyl-1H-pyrrole-3-carboxylate

S. B. Larson, N. S. Girgis, H. B. Cottam and R. K. Robins



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Acta Cryst. (1987). C43, 1228-1229    [doi:10.1107/S0108270187092370]

9-Acetyloxymethyl-1,3,4-trifluoro-7-methyl-11H-pyrido[4,3-c]benzo[1,2]diazepine

R. G. Pritchard



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Acta Cryst. (1987). C43, 1229-1231    [doi:10.1107/S0108270187092369]

12[alpha]-Hydroxy-3-oxooleanano-28,13-lactone

D. S. Eggleston



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Acta Cryst. (1987). C43, 1231-1233    [doi:10.1107/S0108270187092357]

Polymorphisme de la (-) bromo-10 méthoxycarbonyl-1 nitro-16 aspidospermidine-(2R,7R,16S,20S,21S): structure d`une nouvelle variété

P. Toffoli, N. Rodier, G. Lewin et J. Poisson



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Acta Cryst. (1987). C43, 1233-1235    [doi:10.1107/S0108270187092345]

Structure of a second monoclinic polymorph of triphenylphosphine oxide

A. L. Spek



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Acta Cryst. (1987). C43, 1235-1236    [doi:10.1107/S0108270187092333]

Structure of diazapolycyclic compounds. X. 1,4-Dimethyl-1,4-dihydrobenzo[g]pyridazino[1,2-b]phthalazine-6,13-dione

C. Foces-Foces and F. H. Cano


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