Acta Crystallographica Section C

Crystal Structure Communications

Volume 44, Part 2 (February 1988)



research papers


inorganic compounds



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Acta Cryst. (1988). C44, 207-210    [doi:10.1107/S0108270187009673]

Refinement of three caesium mercury iodides, Cs2Hg3I8.H2O, Cs2HgI4 and Cs3HgI5

R. Sjövall and C. Svensson



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Acta Cryst. (1988). C44, 210-212    [doi:10.1107/S0108270187009533]

Trichlorosulfonium(IV) tetrachloroaurate(III)

P. G. Jones, D. Jentsch and E. Schwarzmann



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Acta Cryst. (1988). C44, 212-216    [doi:10.1107/S0108270187010175]

Crystal structures of two new types of cyclo-tetraphosphates: tetracalcium tetrapotassium tris(cyclo-tetraphosphate) octahydrate and calcium disodium cyclo-tetraphosphate 5.5-hydrate

M. T. Averbuch-Pouchot and A. Durif



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Acta Cryst. (1988). C44, 216-219    [doi:10.1107/S0108270187009338]

Aluminium decavanadate 25-hydrate

G. Punte, B. E. Rivero, G. Rigotti and A. Navaza



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Acta Cryst. (1988). C44, 219-221    [doi:10.1107/S0108270187010230]

Structure of 1,2;1,3;1,4-tri-[mu]-carbonyl-1,2,2,2,3,3,3,4,4,4-decarbonyl-2,3-[mu]-hydrido-tetrahedro-cobalttriruthenium

L. J. Farrugia



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Acta Cryst. (1988). C44, 221-226    [doi:10.1107/S0108270187010357]

ErRh3Si2 and isotypes with an orthorhombic deformation superstructure of the CeCo3B2 type

K. Cenzual, B. Chabot and E. Parthé



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Acta Cryst. (1988). C44, 226-229    [doi:10.1107/S0108270187006516]

Small atomic displacements in the molybdenophosophates AMo2P3O12 (A = K,Rb,Ti)

A. Leclaire and B. Raveau



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Acta Cryst. (1988). C44, 229-232    [doi:10.1107/S0108270187009922]

Structure of hexaaquahydrogen tetrachloroferrate(III) at 210 K by X-ray diffraction

T. Gustafsson



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Acta Cryst. (1988). C44, 232-234    [doi:10.1107/S0108270187009880]

Structure of (Ni,Mg)10Ge3O16

M. E. Fleet and J. Barbier



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Acta Cryst. (1988). C44, 234-236    [doi:10.1107/S0108270187010102]

Affinement sur monocristal de la structure du polytype 2H du séléniure de gallium GaSe forme [beta]

S. Benazeth, Nguyen-Huy Dung, M. Guittard et P. Laruelle


metal-organic compounds



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Acta Cryst. (1988). C44, 237-239    [doi:10.1107/S0108270187009831]

Structure of 1,1,1,1,2,2,2,3,3,3-decacarbonyl-2,3-[mu]-[vinylidenebis(diphenylphosphine)-P,P']-triangulo-triruthenium(0)

M. M. Harding, S. J. Maginn and A. K. Smith



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Acta Cryst. (1988). C44, 239-242    [doi:10.1107/S0108270187009661]

Tris(3-methylpyridinium) decavanadate monohydrate

C. Santiago, A. Arnaiz, L. Lorente, J. M. Arrieta and G. Germain



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Acta Cryst. (1988). C44, 242-245    [doi:10.1107/S0108270187009764]

Structure of binuclear hexaaqua-[mu]-[1,2,4,5-benzenetetracarboxylato(4-)]-bis(ethylenediamine)dinickel(II) tetrahydrate

D. Poleti, D. R. Stojakovic, B. V. Prelesnik and R. M. Herak



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Acta Cryst. (1988). C44, 245-246    [doi:10.1107/S0108270187010126]

Structure of bis(ethylenediamine)isothiocyanatocopper(II) tetrafluoroborate, violet isomer

M. Koman, L. Macasková, G. Ondrejovic, B. Koren, L. Battaglia and A. Corradi



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Acta Cryst. (1988). C44, 247-250    [doi:10.1107/S010827018701103X]

Actinide structural studies. 15. Two 1,10-phenanthroline complexes of uranium(VI)

N. W. Alcock, D. J. Flanders, M. Pennington and D. Brown



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Acta Cryst. (1988). C44, 250-253    [doi:10.1107/S010827018701031X]

Polymeric bis(O-methyldithiocarbonato)lead(II)

E. R. T. Tiekink



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Acta Cryst. (1988). C44, 253-255    [doi:10.1107/S0108270187009934]

Structures of dibromobis(tetrahydroselenophene)mercury(II) and diiodobis(tetrahydroselenophene)mercury(II)

C. Stålhandske and F. Zintl



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Acta Cryst. (1988). C44, 255-257    [doi:10.1107/S0108270187010114]

Structure of dichlorobis(pentane-2,4-dionato)bis(tetrahydrofuran)uranium(IV)

P. Charpin, M. Nierlich, D. Vigner, M. Lance and C. Baudin



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Acta Cryst. (1988). C44, 257-259    [doi:10.1107/S0108270187010783]

N,N-Dimethylformamide-uranium tetrachloride complex: structure of trichloropentakis(N,N-dimethylformamide)uranium(IV) hexachlorouranate(IV)

P. Charpin, M. Nierlich, D. Vigner and H. Marquet-Ellis



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Acta Cryst. (1988). C44, 259-262    [doi:10.1107/S010827018701000X]

Structure of tetrathiafulvalenium bis(5,6-dihydro-1,4-dithiin-2,3-dithiolato)aurate(III), (TTF)[Au(DDDT)2]

U. Geiser, A. J. Schultz, H. H. Wang, M. A. Beno and J. M. Williams



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Acta Cryst. (1988). C44, 263-265    [doi:10.1107/S0108270187010746]

Trichlorobis(diaza-1,4 bicyclo[2.2.2]octane)cuprate(II) d'hydrogène

B. Viossat, P. Khodadad, N. Rodier and Nguyen-Huy Dung



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Acta Cryst. (1988). C44, 265-267    [doi:10.1107/S010827018700996X]

Potassium 4-chloro-1,2-benzoquinone 2-oximate hemihydrate, K(Clqo).1/2H2O

C. Bisi Castellani, O. Carugo and A. Coda



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Acta Cryst. (1988). C44, 267-270    [doi:10.1107/S0108270187009971]

Studies on copper(II) complexes of o-quinone monooximes. 5. Bis(4-chloro-1,2-benzoquinone 2-oximato)(methanol)copper(II), Cu(Clqo)2.MeOH

C. Bisi Castellani, O. Carugo and A. Coda



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Acta Cryst. (1988). C44, 270-272    [doi:10.1107/S0108270187008497]

Structure of potassium hexamethyldisilazide toluene solvate

P. G. Williard


organic compounds



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Acta Cryst. (1988). C44, 272-275    [doi:10.1107/S0108270187008400]

Structure of 1,1'-methylenebis(4,4'-dimethylaminopyridinium) iodide

S. Munavalli, E. J. Poziomek and C. S. Day



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Acta Cryst. (1988). C44, 275-277    [doi:10.1107/S0108270187009211]

Structure of 3-(4-hydroxy-3-methoxyphenyl)-2-propenoic acid (ferulic acid)

M. Nethaji, V. Pattabhi and G. R. Desiraju



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Acta Cryst. (1988). C44, 277-279    [doi:10.1107/S0108270187009016]

X-ray structure of 1,4-bis(diphenylphosphino)butane

A. V. Rivera, D. Gómez C., E. Rodulfo de Gil and T. Suárez



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Acta Cryst. (1988). C44, 279-281    [doi:10.1107/S0108270187009387]

Structure of 3,3-diphenyltetrahydrofuran

B. R. Vincent and T. S. Cameron



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Acta Cryst. (1988). C44, 281-285    [doi:10.1107/S0108270187009612]

Structure of the dipeptide L-prolyl-L-lysine acetate. A new conformation of the lysine side chain

L. Urpí, M. Coll, J. A. Subirana, X. Solans and M. Font-Altaba



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Acta Cryst. (1988). C44, 285-287    [doi:10.1107/S0108270187009867]

Conformation and structure of 9-propylanthracene

G. Schrumpf and P. G. Jones



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Acta Cryst. (1988). C44, 287-289    [doi:10.1107/S0108270187010138]

Inside-protonated 1,8-diazabicyclo[6.4.3]pentadecane picrate

R. W. Alder, A. G. Orpen and J. M. White



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Acta Cryst. (1988). C44, 290-292    [doi:10.1107/S0108270187008412]

Structure of N-methyl-2-pyridineselone

T. Srikrishnan



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Acta Cryst. (1988). C44, 292-294    [doi:10.1107/S0108270187009302]

Structure of (3-isopropyl-1-methyl-4-pyrazolyl)diphenylphosphine oxide

S. Boutiba, A. Kallel, A. Madani, A. Ben Akacha, B. Baccar and I. Pabst



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Acta Cryst. (1988). C44, 294-296    [doi:10.1107/S0108270187009363]

Structure of 2,5-dihydro-4-[(4-methyl-phenyl)amino]-2-oxo-N-phenyl-3-furancarboxamide

P. J. Carroll, R. A. Mack and V. St. Georgiev



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Acta Cryst. (1988). C44, 296-300    [doi:10.1107/S0108270187006590]

Synthesis of cedranoid sesquiterpenes. IV. X-ray characterization of the endo-6-hydroxy-endo-8-methyl and exo-6-hydroxy-exo-8-methyl isomers of methyl 6-hydroxy-4,4,8-trimethyl-3-oxo-cis-bicyclo[3.3.0]octane-1-carboxylate

D. J. Burnell, V. J. Freer, R. S. Grewal, P. C. Hayes, J. F. Sawyer and P. Yates



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Acta Cryst. (1988). C44, 300-303    [doi:10.1107/S0108270187006917]

Structure of N-(2-acetyl-3-benzofuranyl)-p-toluenesulfonamide

F. Bachechi, V. M. Coiro, F. Gatta, G. Settimj and M. Delfini



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Acta Cryst. (1988). C44, 303-306    [doi:10.1107/S0108270187008758]

The structures of polymorph I at 181 K and polymorph II at 297 K of the bis(water-dichloropicric acid)-1,4,7,10,13,16-hexaoxacyclooctadecane complex, 2[H2O.C6(NO2)3Cl2(OH)].(CH2CH2O)6

D. Britton, M. K. Chatooni Jnr and I. M. Kolthoff



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Acta Cryst. (1988). C44, 307-311    [doi:10.1107/S0108270187006905]

Structure of 6-acetoxycoumarin: topochemical photodimerization and analysis of acetoxy...acetoxy interactions in the solid state

G. S. Murthy, V. Ramamurthy and K. Venkatesan



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Acta Cryst. (1988). C44, 311-313    [doi:10.1107/S0108270187009879]

2-Aminopyridinium salicylate

R. W. Gellert and I.-N. Hsu



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Acta Cryst. (1988). C44, 313-315    [doi:10.1107/S0108270187008965]

Structure of 7-chloro-5-(2,6-dichlorophenyl)-1,3-dihydro-2H-1,4-benzodiazepin-2-one

H. J. Kemmish and T. A. Hamor



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Acta Cryst. (1988). C44, 315-317    [doi:10.1107/S0108270187009223]

4,4'-Thiodi([alpha]-toluenethiol)

M. Ratajczak-Sitarz, A. Katrusiak, Z. Kaluski and J. Garbarczyk



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Acta Cryst. (1988). C44, 317-319    [doi:10.1107/S0108270187009600]

Structure of 1,5-diazabicyclo[5.4.0]undecan-6-one

T. A. Olszak, A. M. Brzozowski, M. J. Grabowski, A. Stepien, R. Guryn and Z. Dauter



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Acta Cryst. (1988). C44, 319-321    [doi:10.1107/S0108270187010151]

Structure du (méthyl-1 pipérazinyl-4)-5 pyrido[2,3-b][1,5]benzothiazépine

M. Sbit, L. Dupont, O. Dideberg, J. F. Liégeois et J. Delarge



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Acta Cryst. (1988). C44, 321-324    [doi:10.1107/S0108270187009910]

Structures of two dideoxynucleosides: 2',3'-dideoxyadenosine and 2',3'-dideoxycytidine

J. V. Silverton, F. R. Quinn, R. D. Haugwitz and L. J. Todaro



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Acta Cryst. (1988). C44, 324-326    [doi:10.1107/S0108270187009351]

Structure of 1,5-bis([alpha]-isopropyl-3,4-dimethoxybenzyl)-2,4-dimethoxybenzene

M. C. Natoli, F. Nicolò, G. Bruno, G. Bombieri, L. Ceraulo and L. Lamartina



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Acta Cryst. (1988). C44, 327-329    [doi:10.1107/S0108270187010291]

Conformation of a double dibenzotropone precursor of a bifunctional amitriptyline-type drug: 7,8,15,16-tetrahydrodibenzo[d,d']benzo[1,2-a;4,5-a']dicycloheptene-5,13-dione

C. E. Briant, D. W. Jones, Y. Asscher, D. Avnir and I. Agranat



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Acta Cryst. (1988). C44, 329-332    [doi:10.1107/S0108270187010394]

Structure of 13-ethyl-17[beta]-hydroxy-11-methylene-18,19-dinor-17[alpha]-pregna-4,15-dien-20-yn-3-one (11-methylenegestodene)

V. J. van Geerestein, J. A. Kanters and J. Kroon



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Acta Cryst. (1988). C44, 332-334    [doi:10.1107/S0108270187009004]

Structure of (1[alpha],2[alpha],4[alpha],6[alpha])-3,7-dibenzoyl-3,7-diazatricyclo[4.1.0.02,4]heptane

A. M. Brzozowski, M. J. Grabowski, A. Stepien and Z. Dauter



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Acta Cryst. (1988). C44, 334-337    [doi:10.1107/S0108270187011016]

Structure of tris(2-hydroxyethyl)ammonium 3,5-dinitrobenzoate

G. P. M. van Mier, J. A. Kanters and N. S. Poonia



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Acta Cryst. (1988). C44, 337-340    [doi:10.1107/S0108270187009776]

Studies in nonlinear optical materials: structure of di-2-menthyl 2-(N,N'-dimethyl-2-imidazolidinylidene)malonate monohydrate

D. Kanagapushpam, K. Venkatesan and T. S. Cameron



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Acta Cryst. (1988). C44, 340-342    [doi:10.1107/S0108270187010837]

Structure de la nitro-7 benzoxasélénole-2,1 one-3

M. Sbit, L. Dupont, O. Dideberg et C. Lambert



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Acta Cryst. (1988). C44, 342-347    [doi:10.1107/S0108270187009843]

Small helical aromatic molecules. 1. 5-Propylphenanthrene-4-carboxylic acid (PPC) and 5-propyl-9,10-dihydrophenanthrene-4-carboxylic acid (DPPC)

G. Schrumpf and P. G. Jones



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Acta Cryst. (1988). C44, 347-349    [doi:10.1107/S0108270187009855]

Small helical aromatic molecules. 2. 5[alpha]-([alpha]-Hydroxybenzyl)phenanthrene-4-carbolactone

P. G. Jones and G. Schrumpf



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Acta Cryst. (1988). C44, 350-351    [doi:10.1107/S0108270187010242]

Structure of 2-(2-hydroxyethyl)-1-(2-pyridyl)imidazo[1,5-a]pyridinium perchlorate

S. Brooker and V. McKee



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Acta Cryst. (1988). C44, 352-355    [doi:10.1107/S0108270187009752]

Structure of the designed macrocycle 1,4,11,20-tetraoxa[4]orthobenzeno[2](2,6)pyridino[2]metabenzenophane

K. K. Chacko, G. A. Ruban, K. Aoki and E. Weber



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Acta Cryst. (1988). C44, 355-357    [doi:10.1107/S010827018700595X]

Structure of N-(diethylaminothiocarbonyl)benzamidine

U. Braun, R. Richter, J. Sieler, L. Beyer, I. Leban and L. Golic



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Acta Cryst. (1988). C44, 357-359    [doi:10.1107/S0108270187010850]

Structure of 3-methoxy-2-phenyl-4H-1-benzopyran-4-one (3-methoxyflavone)

J.-C. Wallet, E. M. Gaydou, A. Fadlane and A. Baldy


short format


inorganic compounds



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Acta Cryst. (1988). C44, 360-361    [doi:10.1107/S0108270187010254]

Structure of cis-[PdCl2L] (L = 1,4,7-trithiacyclononane)

A. J. Blake, A. J. Holder, Y. V. Roberts and M. Schröder


metal-organic compounds



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Acta Cryst. (1988). C44, 361-363    [doi:10.1107/S0108270187008771]

Structure of pentacarbonyl-[mu]-[[sigma]:[eta]4-(1-carbonyl-2-phenyl-2-butenyl)]-([eta]5-cyclopentadienyl)diiron(I), [(CO)3Fe{CH3CHC(C6H5)CCO}Fe(CO)2Cp]

M. J. Heeg



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Acta Cryst. (1988). C44, 363-364    [doi:10.1107/S0108270187009727]

Structure of ([eta]5-cyclopentadienyl)(dimethyldithiocarbamato)(triphenylphosphine)ruthenium(II)

A. W. Cordes and M. Draganjac



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Acta Cryst. (1988). C44, 365-367    [doi:10.1107/S0108270187010035]

Structure of [Mg{HO3PCH(C6H5)2}2].8H2O, a layered phosphonate salt

H. Lee, V. M. Lynch, G. Cao and T. E. Mallouk



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Acta Cryst. (1988). C44, 367-369    [doi:10.1107/S0108270187010096]

Structure of a complex of palladium(II) chloride and 5-phenoxy-1-phenyltetrazole co-crystallized with 1,2-dichloroethane solvent

D. J. Chadwick, R. A. W. Johnstone, P. J. Price and M. M. Harding



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Acta Cryst. (1988). C44, 369-370    [doi:10.1107/S0108270187010229]

Structure of bis(tetraphenylphosphonium) oxothiotetra(thiocyanato-N)tungstate(VI) methyl cyanide solvate

C. Potvin, J. M. Manoli, S. Marzak and F. Secheresse



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Acta Cryst. (1988). C44, 371-372    [doi:10.1107/S0108270187010618]

Structure of tetrabromobis(triphenylarsine)osmium(IV)

C. C. Hinckley, M. Matusz and P. D. Robinson



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Acta Cryst. (1988). C44, 372-374    [doi:10.1107/S0108270187010692]

Structure of tetramethylammonium cerium(III) bis(sulfate) trihydrate

I. Leban, A. Arhar, V. Jordanovska and L. Golic


organic compounds



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Acta Cryst. (1988). C44, 374-376    [doi:10.1107/S0108270187009685]

2-(2,5-Dimethoxybenzyl)-3,6-dimethoxy-4-methylbenzonitrile

U. Siriwardane, S. P. Khanapure, S. S. C. Chu and E. R. Biehl



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Acta Cryst. (1988). C44, 376-378    [doi:10.1107/S0108270187010369]

Structure of the ethanol solvate of 13-ethyl-11[beta]-methyl-18-norlynestrenol

V. J. van Geerestein



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Acta Cryst. (1988). C44, 378-379    [doi:10.1107/S0108270187010370]

Structure of 19-nor-17[alpha]-pregna-4,15-dien-20-yn-17[beta]-ol

V. J. van Geerestein and B. R. Leeflang



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Acta Cryst. (1988). C44, 379-381    [doi:10.1107/S0108270187010382]

Structure of 17[beta]-hydroxy-11-methylene-19-nor-17[alpha]-pregna-4,15-dien-20-yn-3-one

V. J. van Geerestein and R. Hendricks



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Acta Cryst. (1988). C44, 381-383    [doi:10.1107/S0108270187010023]

Cycloaddition product from the reaction of benzoquinone and 9-bromoanthracene

W. H. Watson and A. Nagl



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Acta Cryst. (1988). C44, 383-384    [doi:10.1107/S0108270187010977]

Structure of 4-O-ethylascofuranone

Y. Nawata, H. Sasaki, K. Ochi and K. Ando



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Acta Cryst. (1988). C44, 385-386    [doi:10.1107/S0108270187009624]

Structure of 2,3-dihydro-5,6-dimethoxy-3-(o-nitrobenzylidene)benzo[b]thiophen-2-one

G. Salem, A. Terzis and D. Mentzafos



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Acta Cryst. (1988). C44, 386-388    [doi:10.1107/S0108270187010163]

Structure of 9-methoxy-11-demethylellipticine

C. Gansser, C. Viel, Y. Mauguen and G. Tsoucaris



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Acta Cryst. (1988). C44, 388-389    [doi:10.1107/S0108270187009478]

Structure of lumi-arteannuin B

J. L. Flippen-Anderson, R. Gilardi and C. George



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Acta Cryst. (1988). C44, 390-391    [doi:10.1107/S0108270187010217]

Acetyl benzyl disulfide

E. John, J. A. Potenza and H. J. Schugar



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Acta Cryst. (1988). C44, 391-393    [doi:10.1107/S0108270187010333]

4-Methyl-3-{(Z)-methyl[(E)-dimethyl(phenyl)silyl]methylidene}azetidin-2-one: an [alpha]-alkylidene-[beta]-lactam

U. Siriwardane, S. S. C. Chu and J. D. Buynak



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Acta Cryst. (1988). C44, 393-395    [doi:10.1107/S0108270187010011]

7-Chloro-6-oxobicyclo[3.2.0]hept-2-en-5-yl 2,4,6-trimethylbenzoate

W. H. Watson and A. Nagl


short communications



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Acta Cryst. (1988). C44, 395-396    [doi:10.1107/S0108270187010904]

On the structure of Ca8In3

R. E. Marsh and K. M. Slagle


notes and news



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Acta Cryst. (1988). C44, 396    [doi:10.1107/S0108270188099822]

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