Acta Crystallographica Section C

Crystal Structure Communications

Volume 44, Part 6 (June 1988)



research papers


inorganic compounds



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Acta Cryst. (1988). C44, 949-952    [doi:10.1107/S0108270188001143]

Structures of difluorophosphine sulfide at 98 K and difluorophosphine oxide at 158 K

A. J. Blake, E. A. V. Ebsworth and A. J. Welch



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Acta Cryst. (1988). C44, 952-955    [doi:10.1107/S0108270188001659]

Structural characterization of two oxotungsten(IV) complexes, [WOCl(Me2PCH2CH2PMe2)2]ClO4 and [WOCl{Me2PCH2P(S)Me2}2]PF6

F. A. Cotton and R. Llusar



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Acta Cryst. (1988). C44, 955-957    [doi:10.1107/S010827018800191X]

Structure of Sr8PtSi2O14

L. Stenberg



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Acta Cryst. (1988). C44, 958-959    [doi:10.1107/S0108270188002161]

Structure of Er2Ba2Cu1+xPt1-xO8 (x = 0.1)

K. Ukei, T. Shishido and T. Fukuda



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Acta Cryst. (1988). C44, 960-962    [doi:10.1107/S0108270188002215]

The structure of barium perbromate trihydrate Ba(BrO4)2.3H2O

R. E. Gerkin, W. J. Reppart and E. H. Appelman



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Acta Cryst. (1988). C44, 962-965    [doi:10.1107/S010827018800188X]

Structure of calcium zinc tetrabromide pentahydrate

R. Duhlev, I. D. Brown and R. Faggiani



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Acta Cryst. (1988). C44, 965-967    [doi:10.1107/S0108270188001349]

Structures of Rb2[InCl5(H2O)] and Cs2[InCl5(H2O)]

X. Solans, M. C. Moron and F. Palacio


metal-organic compounds



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Acta Cryst. (1988). C44, 967-970    [doi:10.1107/S0108270188001131]

trans-Hexakis(pyrazole)manganese(II) bisperchlorate (1) and trans-dichlorotetrakis(pyrazole)manganese(II) (2)

P. O. Lumme, E. Lindell and I. Mutikainen



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Acta Cryst. (1988). C44, 970-973    [doi:10.1107/S0108270188001830]

The structure of [Au-[mu]-{3,5-(C6H5)2C3HN2}]3Cl2: a trinuclear mixed-valence gold pyrazolate complex

R. G. Raptis, H. H. Murray and J. P. Fackler Jnr



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Acta Cryst. (1988). C44, 973-975    [doi:10.1107/S0108270188000721]

The structure of the tetraphenylarsonium salt of the trichloro(pentane-2,4-dionato)nitrosyltechnetium(II) anion

D. S. Brown, J. L. Newman and J. R. Thornback



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Acta Cryst. (1988). C44, 975-977    [doi:10.1107/S0108270188000885]

Structure of dibromo(thiosemicarbazide)cadmium(II) monohydrate

F. Nicolò, H. El Ghaziri and G. Chapuis



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Acta Cryst. (1988). C44, 978-979    [doi:10.1107/S0108270188001568]

Structure of (methoxymethylethynyl)[tris(p-tolyl)phosphine]gold(I)

G. A. Carriedo, V. Riera, X. Solans and J. Solans



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Acta Cryst. (1988). C44, 979-981    [doi:10.1107/S0108270188001507]

Structure of a dinuclear osmium complex containing a carboxamido and three bromine ligands

K.-L. Lu, Y.-C. Lin, M.-C. Cheng and Y. Wang



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Acta Cryst. (1988). C44, 981-986    [doi:10.1107/S0108270188001520]

Polydentate chelates. 3. Structures of egta4- chelates of manganese(II) and copper(II): Sr[Mn(egta)].7H2O and [Cu2(egta)(OH2)2].2H2O

C. K. Schauer and O. P. Anderson



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Acta Cryst. (1988). C44, 986-990    [doi:10.1107/S010827018800157X]

Structure of monoaquabis(isocyanato)(2,2':6',2''-terpyridyl)nickel(II)

R. Cortés, M. I. Arriortua, T. Rojo, J. L. Mesa, X. Solans and D. Beltran



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Acta Cryst. (1988). C44, 990-992    [doi:10.1107/S0108270188001283]

Structure du trihydrogéno hydroxy-1 ethanedi(phosphonate)-1,1 de rubidium dihydrate

P. Charpin, M. Lance, M. Nierlich, D. Vigner, M.-R. Lee, J.-P. Silvestre et Nguyen Quy Dao



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Acta Cryst. (1988). C44, 992-994    [doi:10.1107/S0108270188002902]

catena-Triaqua-[mu]-[1,3,5-benzenetricarboxylato(2-)]-copper(II)

R. Pech and J. Pickardt



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Acta Cryst. (1988). C44, 994-996    [doi:10.1107/S0108270188001313]

Structure of tetrachlorotris(triphenylphosphine oxide)thorium(IV)

G. Van den Bossche, J. Rebizant, M. R. Spirlet and J. Goffart



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Acta Cryst. (1988). C44, 997-998    [doi:10.1107/S010827018800246X]

Structure of [mu]6-carbido-2,3-[mu]-carbonyl-1,1,1,2,2,3,3,4,4,4,5,5,5-tridecacarbonyl-6-([eta]6-toluene)-octahedro-hexaruthenium(12 Ru-Ru)

L. J. Farrugia



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Acta Cryst. (1988). C44, 999-1001    [doi:10.1107/S0108270188002367]

Crystallographic characterization of [pi]-[Co(bpy)(dien)Cl]Cl2.3H2O

Gh. R. Bhat, K. P. Dubey, B. Segal and C. G. Pierpont



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Acta Cryst. (1988). C44, 1001-1004    [doi:10.1107/S0108270188001842]

Structure of tetracarbonyl[2-([beta]-diphenylphosphinoethyl)pyridine]molybdenum(0)

M. P. Cook, D. G. Van Derveer, L. W. Houk and P. K. Sen Gupta



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Acta Cryst. (1988). C44, 1004-1008    [doi:10.1107/S0108270188001945]

Tris(3-ethylpyridinium) decavanadate monohydrate

J. M. Arrieta, A. Arnaiz, L. Lorente, C. Santiago and G. Germain



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Acta Cryst. (1988). C44, 1008-1011    [doi:10.1107/S010827018800215X]

Structure of bis[1,2-bis(diphenylphosphinoethylene)]iodocobalt(II) tetraphenylborate

A. Radha, M. Seshasayee and P. Kuppusamy


organic compounds



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Acta Cryst. (1988). C44, 1011-1014    [doi:10.1107/S0108270188001192]

The structure of 7,14-di-n-propylacenaphtho[1,2-k]fluoranthene

S. Seth, H. Sur and S. Chakraborty



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Acta Cryst. (1988). C44, 1014-1017    [doi:10.1107/S0108270188000678]

Endoannular reactions and ring-chain tautomerism. Structure of 1-(2-hydroxyethyl)-3-methyl-2,4(1H,3H)-quinazolinedione

F. Mazza, G. Pochetti, F. Pinnen and G. Lucente



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Acta Cryst. (1988). C44, 1017-1020    [doi:10.1107/S0108270188001088]

Structure of (R)-norfenfluramine dichloroacetate

G. Coquerel, C. Mayer and G. Perez



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Acta Cryst. (1988). C44, 1020-1022    [doi:10.1107/S0108270188001519]

Tetrafluorophthalonitrile

D. Britton



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Acta Cryst. (1988). C44, 1022-1024    [doi:10.1107/S0108270188000459]

Structure of 3-O-acetylgibberellin A3

M. B. Hossain, D. van der Helm, R. Sanduja and M. Alam



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Acta Cryst. (1988). C44, 1025-1028    [doi:10.1107/S010827018800040X]

Structure of salicylaldehyde thiosemicarbazone

D. Chattopadhyay, S. K. Mazumdar, T. Banerjee, S. Ghosh and T. C. W. Mak



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Acta Cryst. (1988). C44, 1028-1031    [doi:10.1107/S0108270188001234]

Structure of a synthetic hexahydrobenzofuran subunit, C16H22O7, related to the avermectins

F. Bélanger-Gariépy, D. Dubé, S. Hanessian and F. Brisse



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Acta Cryst. (1988). C44, 1031-1033    [doi:10.1107/S0108270188001684]

Structure of N2-p-nitrophenylbenzamidine

K. Surma, M. Jaskólski, Z. Kosturkiewicz and J. Oszczapowicz



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Acta Cryst. (1988). C44, 1033-1036    [doi:10.1107/S0108270188001350]

Conformational study of optically active oxaziridines. Structures of (I) N-isopropyl-, (II) N-tert-butyl- and (III) N-methylsulfonyldiphenyloxaziridine

G. Bocelli, P. Sgarabotto and F. Ugozzoli



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Acta Cryst. (1988). C44, 1037-1039    [doi:10.1107/S0108270188001593]

A pseudo-centrosymmetric chiral crystal structure: (5S,6S)-5,6-dihydro-5,6-dimethyl-1,3-dithiolo[4,5-b][1,4]dithiin-2-thione

J. D. Wallis and J. D. Dunitz



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Acta Cryst. (1988). C44, 1039-1041    [doi:10.1107/S0108270188001957]

Structure of 2-methoxy-N-(4-nitrobenzylidene)-5-pyridylamine. II. Non-centrosymmetric modification

I. Moustakali-Mavridis and E. Hadjoudis



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Acta Cryst. (1988). C44, 1042-1044    [doi:10.1107/S0108270188000873]

Structure of cyclo(-L-phenylalanyl-N-methyl-L-[alpha]-aminobutyryl-)

M. Gdaniec



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Acta Cryst. (1988). C44, 1044-1046    [doi:10.1107/S0108270188001325]

Structure of 1,4-diaminoanthraquinone dihydrate

S. Kashino, K. Senoo and M. Haisa



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Acta Cryst. (1988). C44, 1047-1049    [doi:10.1107/S0108270188001933]

The structure of ammonium oxalohydroxamate - a monopropellant

A. Sameena Begum, V. K. Jain, S. Ramakumar and C. L. Khetrapal



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Acta Cryst. (1988). C44, 1049-1051    [doi:10.1107/S0108270188001635]

Structure of 2-methylnaphthimidazolium chloride dihydrate

Y. Zhan, Y. Luo, R. J. Barton and B. E. Robertson



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Acta Cryst. (1988). C44, 1051-1054    [doi:10.1107/S0108270188001866]

Structures of two isomeric thiodisaccharides

G. B. Carpenter and H. Kristen



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Acta Cryst. (1988). C44, 1054-1057    [doi:10.1107/S0108270188001726]

Structure of anhydrous octyl [alpha]-D-glucopyranoside. A comparison with its hemi- and monohydrate

H. van Koningsveld, J. C. Jansen and A. J. J. Straathof



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Acta Cryst. (1988). C44, 1057-1059    [doi:10.1107/S0108270188001714]

Structure of N,N-dimethyl-1,4-phenylenediamine

H. Nakai, T. Saito and M. Yamakawa



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Acta Cryst. (1988). C44, 1059-1063    [doi:10.1107/S0108270188000587]

Structure of the quasi-equatorial isomer of 5,11-dinitrohexacyclo[5.4.1.02,6.03,10.04,8.09,12]dodecane and crystal density calculations for several di-, tri- and tetranitro analogs

H. L. Ammon and Z. Du



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Acta Cryst. (1988). C44, 1063-1066    [doi:10.1107/S0108270188000800]

Structure of 1-(4-chlorobenzoyloxy)-4,5-dimethyl-1,2,3-triazole (CBODT)

C. A. Kavounis, A. P. Bozopoulos, C. J. Cheer, P. J. Rentzeperis and A. B. Theocharis



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Acta Cryst. (1988). C44, 1066-1070    [doi:10.1107/S0108270188001908]

Structure of a 3[alpha]-(D-methylglycoside) of 7,8[beta]-epoxysinogenin - a cardioactive steroid

M. Nethaji, V. Pattabhi and E. J. Gabe



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Acta Cryst. (1988). C44, 1070-1076    [doi:10.1107/S0108270188001544]

Détermination structurale du poly{bis[(butoxycarbonylméthylcarbamoyloxy)-4 butyl]-1,2 butène-1 yne-3 ylène} [poly(4BCMU)] par minimisation des energies d'interactions moléculaires

C. Brouty, P. Spinat et A. Whuler



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Acta Cryst. (1988). C44, 1076-1080    [doi:10.1107/S0108270188001878]

Structure of clitocine at 173 K

S. B. Larson, R. J. Moss, G. D. Kini and R. K. Robins



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Acta Cryst. (1988). C44, 1080-1083    [doi:10.1107/S0108270188002173]

Reaction of 3-azidopropanol with tris(dimethylamido)phosphorus and structure of the phosphazide reaction product

C. G. Chidester, J. Szmuszkovicz, D. J. Duchamp, L. G. Laurian and J. P. Freeman



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Acta Cryst. (1988). C44, 1083-1086    [doi:10.1107/S0108270187012721]

Structure of 4-hydroxy-1,2-benzisothiazol-3(2H)-one 1,1-dioxide sodium salt (UH-AF 50 NA) at 123 K based on neutron diffraction data

R. Rudert, J. Buschmann, P. Luger, D. Gregson and G. Trummlitz



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Acta Cryst. (1988). C44, 1086-1089    [doi:10.1107/S0108270188001854]

Two polymorphs of 2-bis[(2-hydroxyphenylmethylene)amino]methylphenol

N. A. R. Nabulsi, F. R. Fronczek and R. D. Gandour



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Acta Cryst. (1988). C44, 1089-1092    [doi:10.1107/S0108270188001532]

Structure de la phase triclinique (phase II) du 4,4' azoxydiphénétole

Ph. Sciau, J. Lapasset et J. Moret



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Acta Cryst. (1988). C44, 1092-1094    [doi:10.1107/S0108270188000381]

Structure and stereochemistry of cacalone acetate, a sesquiterpene

M. Soriano-García, F. Walls, H. Barrios, B. Sánchez-Obregón, B. Ortiz, E. Díaz, R. A. Toscano and F. Yuste



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Acta Cryst. (1988). C44, 1095-1097    [doi:10.1107/S0108270188002860]

1-Methoxy-3-(2-nitro-1-imidazolyl)-2-propanol (misonidazole)

T. C. Jenkins and A. R. Walton



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Acta Cryst. (1988). C44, 1097-1100    [doi:10.1107/S0108270188001970]

Structure of the cis-cisoid-cis isomer of 2,3,11,12-tetra-anisyl-18-crown-6: rel-(2R,3S,11R,12S)-2,3,11,12-tetrakis(4-methoxyphenyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

D. A. Pears, H. Shahriari-Zavareh, J. F. Stoddart, J. Crosby, B. L. Allwood, A. M. Z. Slawin and D. J. Williams



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Acta Cryst. (1988). C44, 1101-1104    [doi:10.1107/S0108270188001982]

A 1:1 adduct between the cis-cisoid-cis isomer of 2,3,11,12-tetra-anisyl-18-crown-6 and ammonia-borane

D. A. Pears, H. Shahriari-Zavareh, J. F. Stoddart, J. Crosby, B. L. Allwood and D. J. Williams



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Acta Cryst. (1988). C44, 1104-1106    [doi:10.1107/S0108270188001994]

Structure of the cis-transoid-cis isomer of 2,3,11,12-tetra-anisyl-18-crown-6: rel-(2R,3S,11S,12R)-2,3,11,12-tetrakis(4-methoxyphenyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

D. A. Pears, H. Shahriari-Zavareh, J. F. Stoddart, J. Crosby, B. L. Allwood and D. J. Williams



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Acta Cryst. (1988). C44, 1106-1109    [doi:10.1107/S0108270188002008]

A 1:2 adduct between the cis-transoid-cis isomer of 2,3,11,12-tetra-anisyl-18-crown-6 and ammonia-borane

D. A. Pears, H. Shahriari-Zavareh, J. F. Stoddart, J. Crosby, B. L. Allwood and D. J. Williams



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Acta Cryst. (1988). C44, 1109-1111    [doi:10.1107/S010827018800201X]

Structure of the trans-cisoid-trans isomer of 2,3,11,12-tetra-anisyl-18-crown-6: rel-(2R,3R,11S,12S)-2,3,11,12-tetrakis(4-methoxyphenyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

D. A. Pears, H. Shahriari-Zavareh, J. F. Stoddart, J. Crosby, B. L. Allwood and D. J. Williams



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Acta Cryst. (1988). C44, 1112-1115    [doi:10.1107/S0108270188002021]

A 1:2 adduct between the trans-cisoid-trans isomer of 2,3,11,12-tetra-anisyl-18-crown-6 and ammonia-borane

D. A. Pears, H. Shahriari-Zavareh, J. F. Stoddart, J. Crosby, B. L. Allwood, A. M. Z. Slawin and D. J. Williams



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Acta Cryst. (1988). C44, 1115-1118    [doi:10.1107/S0108270188002033]

Structure of the dextrorotatory trans-cisoid-trans isomer of 2,3,11,12-tetra-anisyl-18-crown-6: (2R,3R,11R,12R)-2,3,11,12-tetrakis(4-methoxyphenyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

D. A. Pears, H. Shahriari-Zavareh, J. F. Stoddart, J. Crosby, B. L. Allwood and D. J. Williams



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Acta Cryst. (1988). C44, 1118-1121    [doi:10.1107/S0108270188002045]

A 1:1 adduct between the trans-cisoid-trans isomer of 2,3,11,12-tetra-anisyl-18-crown-6 with the (RRRR)-configuration and ammonia-borane

D. A. Pears, H. Shahriari-Zavareh, J. F. Stoddart, J. Crosby, B. L. Allwood and D. J. Williams



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Acta Cryst. (1988). C44, 1122-1124    [doi:10.1107/S0108270188001799]

Structure of 2,2';4,4'-bis(p-phenylenedioxy)bis(2,4,6,6-tetrachloro-1,3,5,2[lambda]5,4[lambda]5,6[lambda]5-triazatriphosphorine)

A. Meetsma, J. C. van de Grampel, K. Brandt and Z. Jedlinski



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Acta Cryst. (1988). C44, 1125-1127    [doi:10.1107/S0108270188001787]

Structure of 8-chloro-2-[(3-furoyl)aminomethyl]-1-methyl-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepine hydrochloride

N. M. Blaton, S. M. Vynckier, C. L. Verlinde, O. M. Peeters and C. J. De Ranter


short format


metal-organic compounds



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Acta Cryst. (1988). C44, 1128-1130    [doi:10.1107/S0108270188001829]

Structures of two acetylacetonate complexes: (I) Sb(acac)Cl4, (II) [NHEt3][Sn(acac)Cl4]

L. Korte, D. Mootz, M. Scherf and M. Wiebcke



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Acta Cryst. (1988). C44, 1130-1132    [doi:10.1107/S0108270188002525]

([eta]-Cyclopentadienyl)[methoxy(methyl)carbene]bis(triphenylphosphine)ruthenium(II) hexafluorophosphate

M. I. Bruce, G. A. Koutsantonis and E. R. T. Tiekink



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Acta Cryst. (1988). C44, 1132-1134    [doi:10.1107/S0108270188001271]

Structure of cis-bis(pentafluorophenyl)bis(triphenylphosphine)palladium(II)

K. Miki, N. Kasai and H. Kurosawa


organic compounds



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Acta Cryst. (1988). C44, 1135-1137    [doi:10.1107/S0108270188001301]

The structures of dimethyl N,N'-[1,1'-p-phenylenebis(1-methylethyl)]dicarbamate (I) and diethyl N,N'-[1,1'-p-phenylenebis(1-methylethyl)]dicarbamate (II)

J. P. Jasinski, C. R. Desper, B. A. Zentner, R. J. Butcher and C. F. Day



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Acta Cryst. (1988). C44, 1137-1139    [doi:10.1107/S010827018800143X]

The structures of dimethyl N,N'-trans-1,4-cyclohexanedicarbamate (I) and diethyl N,N'-trans-1,4-cyclohexanedicarbamate (II)

J. P. Jasinski, C. R. Desper, C. A. Byrne, B. A. Zentner and R. J. Butcher



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Acta Cryst. (1988). C44, 1139-1141    [doi:10.1107/S0108270188002227]

Structure of methyl 8,9-epoxy-5,5-ethylenedioxy-7-oxo-11-methoxytricyclo[7.2.1.04,10]dodec-3-ene-8-carboxylate

A. L. Spek and B. P. van Eijck



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Acta Cryst. (1988). C44, 1141-1143    [doi:10.1107/S0108270188001222]

Methyl 2-[2-(2-hydroxyphenyl)ethyl]benzoate

J. A. Corkern, F. R. Fronczek, R. D. Gandour, K. Guo, M. A. Oliver and S. F. Watkins



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Acta Cryst. (1988). C44, 1143-1144    [doi:10.1107/S0108270188002057]

Structure of 2-chloro-1-(2,4-dihydroxyphenyl)ethanone

P. H. van Rooyen and J. C. Breytenbach



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Acta Cryst. (1988). C44, 1144-1147    [doi:10.1107/S0108270188001611]

The structure of the ethylenediammonium salt of 3-nitro-1,2,4-triazol-5-one, C2H4(NH3)2.2C2N4O3H

D. T. Cromer, J. H. Hall, K.-Y. Lee and R. R. Ryan



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Acta Cryst. (1988). C44, 1147-1148    [doi:10.1107/S0108270188002185]

trans-1,2,5-Triphenylsilacyclopentane

C. L. Barnes, G. L. Larson and S. B. Sandoval



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Acta Cryst. (1988). C44, 1148-1150    [doi:10.1107/S0108270188002197]

trans-1,1,2,5-Tetraphenylsilacyclopentane

C. L. Barnes, G. L. Larson and Y. S. Lee



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Acta Cryst. (1988). C44, 1150-1152    [doi:10.1107/S0108270188001969]

Ethyl 1-trifluoromethylindolizine-3-carboxylate

R. G. Pritchard



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Acta Cryst. (1988). C44, 1152-1153    [doi:10.1107/S0108270188001167]

Structure of 1,7-heptanediamine dihydrochloride

J. Brisson and A. L. Beauchamp


book reviews



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Acta Cryst. (1988). C44, 1153-1154    [doi:10.1107/S0108270188001076]

Crystallographic databases edited by F. H. Allen, G. Gergerhoff and R. Sievers


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