Acta Crystallographica Section C

Crystal Structure Communications

Volume 45, Part 11 (November 1989)



research papers


inorganic compounds



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Acta Cryst. (1989). C45, 1667-1669    [doi:10.1107/S0108270189003343]

Structure of Na2MZr(P2O7)2 (M = Ni and Co)

S. Galí, K. Byrappa and G. S. Gopalakrishna



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Acta Cryst. (1989). C45, 1669-1672    [doi:10.1107/S0108270189003112]

Structure of trigonal thorium molybdate

E. M. Larson, P. G. Eller, T. L. Cremers, R. A. Penneman and C. C. Herrick



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Acta Cryst. (1989). C45, 1672-1674    [doi:10.1107/S0108270189002076]

The structure of Ba4PtO6 from time-of-flight powder neutron diffraction data

A. P. Wilkinson and A. K. Cheetham



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Acta Cryst. (1989). C45, 1674-1677    [doi:10.1107/S010827018900418X]

Structure of CsAlTiO4 - a compound with TiO4 tetrahedra

B. M. Gatehouse



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Acta Cryst. (1989). C45, 1677-1679    [doi:10.1107/S0108270189002830]

Structure of the lanthanum chlorosilicate La3(SiO4)Cl5

P. Gravereau, B. Es-Sakhi and C. Fouassier


metal-organic compounds



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Acta Cryst. (1989). C45, 1679-1683    [doi:10.1107/S0108270189002659]

Dimerer cadmium(II)-komplex mit dihydrazidothiophosphorsäurephenylester als zweizähnigem S,N-chelatligand

U. Engelhardt und C. Renz-Kreikebohm



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Acta Cryst. (1989). C45, 1683-1686    [doi:10.1107/S0108270189002349]

Structure of an acetylcarbonylcyclopentadienyliron complex with a phosphine ligand. I. ([eta]-MeC5H4)Fe(CO)(COMe)(PPh2Et)

H. Y. Liu, Md. M. Rahman, L. L. Koh, K. Eriks, W. P. Giering and A. Prock



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Acta Cryst. (1989). C45, 1686-1689    [doi:10.1107/S0108270189001344]

Structure du [Pd{(C6H5O)2P(O)NP(S)(C6H5O)2}2]

Z. Zák, M. Fofana, J. Kamenícek and T. Glowiak



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Acta Cryst. (1989). C45, 1689-1691    [doi:10.1107/S0108270189002854]

Structure of a polyaminecopper(II) complex

P. Sivý, F. Valach, B. Koren, L. Macásková, F. Pavelcík and J. Sivý



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Acta Cryst. (1989). C45, 1691-1694    [doi:10.1107/S010827018900315X]

Copper 1-aminocyclohexanecarboxylate monohydrate [aquabis(1-aminocyclohexanecarboxylato)copper(II)]; tetra- and pentacoordinate copper

H. M. Haendler



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Acta Cryst. (1989). C45, 1694-1697    [doi:10.1107/S0108270189003124]

Structure of azido(1,4,8,11-tetramethyl-1,4,8,11-tetraazacyclotetradecane)cobalt(II) perchlorate

S. Reimer, M. Wicholas, B. Scott and R. D. Willett



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Acta Cryst. (1989). C45, 1697-1699    [doi:10.1107/S0108270189003598]

Structure of dichlorobis(trimethylphosphine oxide)cobalt(II)

M.-J. Menu, M. Simard, A. L. Beauchamp, H. König, M. Dartiguenave, Y. Dartiguenave and H.-F. Klein



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Acta Cryst. (1989). C45, 1699-1705    [doi:10.1107/S0108270189002829]

Neutron structure refinement of barium oxalate-oxalic acid dihydrate, BaC2O4.H2C2O4.2H2O and of related nonstoichiometric hydrates

O. Chaix-Pluchery, J. C. Mutin, J. Bouillot and J. C. Niepce



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Acta Cryst. (1989). C45, 1705-1707    [doi:10.1107/S0108270189003434]

Structure of bis(benzaldehyde azine)dichloropalladium(II)

C.-F. Chang, C.-H. Cheng, C.-C. Wang and S.-L. Wang



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Acta Cryst. (1989). C45, 1707-1713    [doi:10.1107/S0108270189002994]

Simple, direct synthesis and structure of hexa-[mu]-chloro-tetrakis(1-methylimidazole)-[mu]4-oxo-tetracopper(II)

R. E. Norman, N. J. Rose and R. E. Stenkamp



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Acta Cryst. (1989). C45, 1713-1715    [doi:10.1107/S0108270189003719]

Structure of undecacarbonyl[tris(pentafluorophenyl)phosphine]-triangulo-triosmium, a substituted osmium cluster containing a fluorinated triphenylphosphine ligand

H. G. Ang, W. L. Kwik, W. K. Leong and J. A. Potenza



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Acta Cryst. (1989). C45, 1716-1718    [doi:10.1107/S0108270189002489]

Structure of hexaaquacobalt(II) catena-tetraaqua-[mu]-[1,2,4,5-benzenetetracarboxylato(4-)]-cobaltate(II) 7.36-hydrate

D. Poleti and Lj. Karanovic



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Acta Cryst. (1989). C45, 1718-1721    [doi:10.1107/S0108270189002179]

[Bis-[mu]-iodo-bis(tricarbonylrhenio)-(Re-Re)][[mu]-iodo-bis(tetracarbonylrhenio)-(Re-Re)]indium(III) and bis(pentacarbonylrhenio)(tetracarbonyl-bis-[mu]-iodo-rhenio)indium(III)

H.-J. Haupt and U. Flörke



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Acta Cryst. (1989). C45, 1721-1724    [doi:10.1107/S0108270189003537]

5-[eta]-Benzene-9-hydroxy-9,10-[mu]-triethylphosphinoaurio-5-ruthena-nido-decaborane(11) (dichloromethane solvate), C12H33AuB9OPRu (0.15CH2Cl2)

A. J. McLennan and A. J. Welch



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Acta Cryst. (1989). C45, 1724-1727    [doi:10.1107/S0108270189003318]

Neutron diffraction study of sodium oxalate monoperhydrate at 123 K

B. F. Pedersen and Å. Kvick



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Acta Cryst. (1989). C45, 1727-1730    [doi:10.1107/S0108270189002775]

Tetraphenylphosphonium-hexachlorowolframat(V) und die fehlordnung in tetragonalen EPh4+-salzen mit oktaedrischen anionen

U. Müller und A. El-Kholi



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Acta Cryst. (1989). C45, 1731-1733    [doi:10.1107/S0108270189003756]

Polymeric caesium o-phenylenedioxydiacetate dihydrate

G. Smith, E. J. O'Reilly, C. H. L. Kennard and T. C. W. Mak



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Acta Cryst. (1989). C45, 1733-1736    [doi:10.1107/S0108270189003501]

Structure of [N(C4H9)4]2[Fe(C3H7NO)6][Fe4Br4S4]2

A. C. M. Young, M. A. Walters and J. C. Dewan


organic compounds



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Acta Cryst. (1989). C45, 1736-1738    [doi:10.1107/S0108270189004221]

Structure of ethyl 4-methyl-2-oxo-3-phenyl-2,3-dihydro-5-benzofurancarboxylate

R. Ghosh, P. Roychowdhury and P. Maulik



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Acta Cryst. (1989). C45, 1738-1740    [doi:10.1107/S0108270189003860]

Structure of 1-[(R)-[alpha]-methylbenzylamino]-7-[(R)-[alpha]-methylbenzylimino]-1,3,5-cycloheptatriene, H(CHIRAMT), a ligand used for enantioselective conjugate addition cuprate catalysis

S. G. Bott, K.-H. Ahn and S. J. Lippard



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Acta Cryst. (1989). C45, 1740-1743    [doi:10.1107/S0108270189003744]

Structures of (±)-trans-4-(2,3-dimethoxyphenyl)- (I) and (+)-trans-4-(4-methylphenyl)-2-hydroxy-2-methyl-3,4-dihydro-2H,5H-pyrano[3,2-c][1]benzopyran-5-one (II)

G. Ruggiero, O. Platt Jnr, E. J. Valente and D. S. Eggleston



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Acta Cryst. (1989). C45, 1743-1745    [doi:10.1107/S0108270189003525]

Structure of tris(pentafluorophenyl)phosphine

A. Karipides and C. M. Cosio



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Acta Cryst. (1989). C45, 1746-1748    [doi:10.1107/S0108270189004403]

Room-temperature structure of (±)-methyltrachelogenin

K. Khamlach, R. Dhal, E. Brown, M. Leblanc and G. Ferey



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Acta Cryst. (1989). C45, 1748-1751    [doi:10.1107/S010827018900329X]

Structure of the calcium channel antagonist, nimodipine

S. D. Wang, L. G. Herbette and D. G. Rhodes



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Acta Cryst. (1989). C45, 1751-1753    [doi:10.1107/S0108270189002271]

Structure of N-(2,2-dinitro-1-methylethenyl)-2-bromo-1,1,2-trimethylpropanamine

R. T. Patterson, J. H. Boyer and E. D. Stevens



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Acta Cryst. (1989). C45, 1753-1758    [doi:10.1107/S0108270189003069]

Topochemical studies. XI. Structures of [alpha]-acetylaminocinnamic acid dihydrate, its photodimer and the tetrahydrate of the photodimer

T. Iwamoto, S. Kashino and M. Haisa



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Acta Cryst. (1989). C45, 1758-1760    [doi:10.1107/S0108270189003240]

2-Phenylsparteine

A. Katrusiak, E. Figas, Z. Kaluski and D. Lesiewicz



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Acta Cryst. (1989). C45, 1760-1762    [doi:10.1107/S0108270189003562]

Non-natural 14-hydroxy steroids. I. Methyl 14[beta]-hydroxy-1,7,17-trioxo-5[beta],8[alpha],9[beta]-androstan-10[beta]-oate

A. G. Michel, R. Ruel and N. Michel-Dewez



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Acta Cryst. (1989). C45, 1762-1764    [doi:10.1107/S0108270189003951]

Structure of 2-cyclohexylamino-4,6-dimethoxy-1,3,5-triazine

M. L. Glówka and I. Iwanicka



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Acta Cryst. (1989). C45, 1765-1767    [doi:10.1107/S0108270189003963]

Structure of 2,4,6-trimethoxy-1,3,5-triazine

M. L. Glówka and I. Iwanicka



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Acta Cryst. (1989). C45, 1767-1770    [doi:10.1107/S010827018900260X]

The stereochemistry of the phosphorus-selenium bond. VII. Structure of 5,5-dimethyl-2-(o-nitrophenyl)amino-1,3,2-dioxaphosphorinane 2-selenide

W. M. Wolf and T. J. Bartczak



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Acta Cryst. (1989). C45, 1770-1773    [doi:10.1107/S0108270189002441]

An unusual rearrangement in the boron-trifluoride-promoted reaction of tetracyclo[6.3.0.04,11.05,9]undecane-2,7-dione monoethylene acetal with ethyl diazoacetate

W. H. Watson, A. Nagl, A. P. Marchand and V. Vidyasagar



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Acta Cryst. (1989). C45, 1773-1776    [doi:10.1107/S0108270189002982]

Structure of 3-(4-hydroxy-2-methylphenyl)-3-phenylphthalide

A. Roszak and Z. Skrzat



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Acta Cryst. (1989). C45, 1776-1778    [doi:10.1107/S0108270189003495]

Structure of 4-triphenylmethylthio-2-azetidinone

S. Bando, T. Takano, K. Miyahara, R. Tanaka, T. Nakatsuka and M. Ishiguro



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Acta Cryst. (1989). C45, 1778-1780    [doi:10.1107/S0108270189003288]

The structure of 2,2'-[1,2-ethanediylbis(oxy)]bis(benzenemethanol)

N. A. Bailey, D. E. Fenton, M. G. Williams and D. J. Winter



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Acta Cryst. (1989). C45, 1780-1783    [doi:10.1107/S0108270189003057]

Structural studies of mitomycins. II. Structure of mitomycin A hemihydrate

N. Hirayama and K. Shirahata



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Acta Cryst. (1989). C45, 1783-1787    [doi:10.1107/S0108270189002970]

Structures of colchicine analogues. II. 2',3',4'-Trimethoxybiphenyl-3(and -4)-carboxylic acid methyl esters

M. F. Mackay, L. H. Sands, E. Lacey and P. Burden



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Acta Cryst. (1989). C45, 1788-1792    [doi:10.1107/S0108270189003355]

Structure of a non-planar flavonol, 5,7,2'-trihydroxy-3,6,8,4',5'-pentamethoxyflavone

K. A. Abboud, S. H. Simonsen, T. J. Mabry and N. Fang



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Acta Cryst. (1989). C45, 1792-1794    [doi:10.1107/S010827018900435X]

Structure of the NS-donor ligand 4-(ethylthiomethyl)-5-methylimidazole

E. Bouwman and W. L. Driessen



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Acta Cryst. (1989). C45, 1794-1797    [doi:10.1107/S0108270189003483]

Structure of strychnine hydrochloride sesquihydrate

R. Ghosh, P. Roychowdhury, D. Chattopadhyay and Y. Iitaka



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Acta Cryst. (1989). C45, 1797-1802    [doi:10.1107/S010827018900394X]

Structure and conformational analysis of the opioid antagonist (-)-(1R,5R,9R)-5,9-diethyl-2-(3-furylmethyl)-2'-hydroxy-6,7-benzomorphan (Mr2266)

C. L. Verlinde, N. M. Blaton, O. M. Peeters and C. J. De Ranter



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Acta Cryst. (1989). C45, 1803-1805    [doi:10.1107/S0108270189003732]

Structures of (E,E)-1,1'-ethanediylidenebis(2,3-dihydro-1H-indene), (E,E)-1,1'-ethanediylidenebis(1,2,3,4-tetrahydronaphthalene) and (E,E)-5,5'-ethanediylidenebis(6,7,8,9-tetrahydro-5H-benzocycloheptene)

P. J. Carroll, J. N. Haseltine, R. M. Hochstrasser and A. B. Smith III



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Acta Cryst. (1989). C45, 1805-1808    [doi:10.1107/S0108270189004166]

Structure of dimethyl (1S,3S)-1-methoxycarbonylmethyl-1,2,3,4-tetrahydro-9H-pyrido[3,4-b]indole-1,3-dicarboxylate at 165 K

J. H. Everett, C. D. Reynolds, C. A. Sparks, W. Pangborn, P. Strong, P. D. Bailey, Z. Dauter, M. Helliwell and S. P. Hollinshead


short format


inorganic compounds



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Acta Cryst. (1989). C45, 1808-1809    [doi:10.1107/S0108270189007390]

Structure of Mn2SiS4

J. Fuhrmann and J. Pickardt


metal-organic compounds



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Acta Cryst. (1989). C45, 1810-1811    [doi:10.1107/S0108270189007559]

Trimethylstannyl 2-furancarboxylate

E. R. T. Tiekink, G. K. Sandhu and S. P. Verma



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Acta Cryst. (1989). C45, 1811-1813    [doi:10.1107/S0108270189006840]

Structure of trans-dichlorotetrakis(diphenylphosphine)ruthenium(II) chloroform (1/2)

E. B. McAslan, A. J. Blake and T. A. Stephenson



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Acta Cryst. (1989). C45, 1813-1815    [doi:10.1107/S0108270189007468]

Two crystal modifications of hexamethylcyclotristannatellurane

R. J. Batchelor, F. W. B. Einstein and C. H. W. Jones



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Acta Cryst. (1989). C45, 1815-1817    [doi:10.1107/S0108270189007432]

Nitratobis(triphenylphosphine)silver(I) benzene solvate (1/1)

C. S. W. Harker and E. R. T. Tiekink



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Acta Cryst. (1989). C45, 1817-1818    [doi:10.1107/S010827018900733X]

Structure of bis([mu]-diethyllead)-bis(tetracarbonyliron)

C. Campbell and L. J. Farrugia


organic compounds



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Acta Cryst. (1989). C45, 1819-1820    [doi:10.1107/S0108270189006955]

Structure of a tosyl derivative of morpholine

P. J. Squattrito and A. Clearfield



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Acta Cryst. (1989). C45, 1821-1822    [doi:10.1107/S0108270189003549]

Structure of hexa-2,4-diyne-1,6-diyl bis(3,5-dimethylbenzenesulfonate)

M. J. Barrow, E. A. Blair, A. J. Lough, G. H. W. Milburn and A. R. Werninck



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Acta Cryst. (1989). C45, 1822-1825    [doi:10.1107/S0108270189007596]

Structure of 7-amino-2-chloro[1,3]thiazolo[4,5-d]pyrimidine, an adenine analog

S. B. Larson, J. D. Anderson, H. B. Cottam and R. K. Robins



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Acta Cryst. (1989). C45, 1825-1827    [doi:10.1107/S0108270189007602]

Structure of 5,7-dichloro-2-(N-methylanilino)[1,3]thiazolo[4,5-d]pyrimidine

S. B. Larson, H. B. Cottam and R. K. Robins



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Acta Cryst. (1989). C45, 1827-1829    [doi:10.1107/S0108270189007821]

Structure of the flavone centaureidin

F. R. Fronczek, F. J. Parodi and N. H. Fischer



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Acta Cryst. (1989). C45, 1829-1831    [doi:10.1107/S0108270189007833]

Structure of the guaianolide dehydrocostus lactone

F. R. Fronczek, D. Vargas, F. J. Parodi and N. H. Fischer



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Acta Cryst. (1989). C45, 1831-1832    [doi:10.1107/S0108270189007614]

1-Chloro-3-ethynyl-2,4-dimethoxybenzene

K. L. Evans, F. R. Fronczek and R. D. Gandour



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Acta Cryst. (1989). C45, 1833-1834    [doi:10.1107/S0108270189007389]

Structure of methyl 2-cyano-2-(2-isopropenyl-5-methylcyclohexyl)acetate

J. Antel, G. M. Sheldrick, U. Beifuss and L.-F. Tietze



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Acta Cryst. (1989). C45, 1834-1836    [doi:10.1107/S0108270189007729]

Structure of a 3,4-dihydro-2H-pyran derivative

J. Antel, G. M. Sheldrick, U. Hartfiel and L.-F. Tietze



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Acta Cryst. (1989). C45, 1836-1837    [doi:10.1107/S0108270189006797]

Structure of (3R,6R,7R,11S)-7-acetoxymethyl-5,8,10-trioxa-1-azatricyclo[4.3.2.03,11]undecan-4-one

K. Suwinska, I. Panfil, C. Belzecki and M. Chmielewski



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Acta Cryst. (1989). C45, 1838-1839    [doi:10.1107/S0108270189007146]

Structure of (4S*,6R*)-(8-oxo-3,9-dioxa-1-aza-4-bicyclo[4.3.0]nonanyl)methyl acetate

K. Suwinska, I. Panfil, C. Belzecki and M. Chmielewski


short communications



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Acta Cryst. (1989). C45, 1840    [doi:10.1107/S0108270189005718]

Structure of Na3M3(CO3)5. Corrigendum

R. E. Marsh


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