Acta Crystallographica Section C

Crystal Structure Communications

Volume 46, Part 2 (February 1990)



research papers


inorganic compounds



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Acta Cryst. (1990). C46, 175-177    [doi:10.1107/S0108270189005743]

Neutron diffraction study of the hydrogen-bond system in Cu2K(H3O2)(SO4)2

G. Chevrier, G. Giester, D. Jarosch and J. Zemann



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Acta Cryst. (1990). C46, 177-179    [doi:10.1107/S010827018900627X]

Structure of the trivanadate TlV3O8

R. Benchrifa, M. Leblanc and R. De Pape



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Acta Cryst. (1990). C46, 179-181    [doi:10.1107/S0108270189006190]

Crystal chemistry of cyclo-hexaphosphates. VI. Structure of ammonium cyclo-hexaphosphate tellurate dihydrate

M. T. Averbuch-Pouchot and A. Durif



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Acta Cryst. (1990). C46, 181-186    [doi:10.1107/S0108270189005913]

Structural phase transitions in Chevrel phases containing divalent metal cations. II. Structure refinement of triclinic EuMo6S8 and BaMo6S8 at low temperature

F. Kubel and K. Yvon



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Acta Cryst. (1990). C46, 186-189    [doi:10.1107/S0108270189006128]

Structure investigation by neutron diffraction of deuterated cobalt fluosilicate hexahydrate

G. Chevrier and R. Saint-James



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Acta Cryst. (1990). C46, 190-192    [doi:10.1107/S0108270189006529]

Kalium-dioxonium-hexafluoroaluminat

G. Frenzen and W. Massa


metal-organic compounds



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Acta Cryst. (1990). C46, 192-195    [doi:10.1107/S0108270189005731]

Coordination mode of 4-pyridinecarbaldehyde phenylhydrazone. Structure of dichloro(4-pyridinecarbaldehyde phenylhydrazone)(tri-n-propylphosphine)palladium(II)

G. Bruno, M. Cusumano, A. Giannetto, A. Giuffrida and G. Guglielmo



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Acta Cryst. (1990). C46, 195-197    [doi:10.1107/S0108270189006153]

Structure of di-[mu]-methoxo-bis[dichlorodimethoxomolybdenum(V)]

B. Kamenar, B. Korpar-Colig, M. Penavic and M. Cindric



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Acta Cryst. (1990). C46, 197-201    [doi:10.1107/S0108270189004750]

Structure of tris(thioacetyltrifluoroacetonato)rhodium(III)

L. W. Tari, G. A. Stern, J. B. Westmore and A. S. Secco



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Acta Cryst. (1990). C46, 202-205    [doi:10.1107/S0108270189005883]

Structure of ferrocenium hexafluorophosphate

R. Martinez and A. Tiripicchio



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Acta Cryst. (1990). C46, 205-207    [doi:10.1107/S0108270189005433]

Structures of chromium(III) cyclam complexes. 1. Structure of trans-dicyano(1,4,8,11-tetraazacyclotetradecane)chromium(III) perchlorate

A. M. Hemmings, J. N. Lisgarten, R. A. Palmer and D. M. Gazi



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Acta Cryst. (1990). C46, 208-210    [doi:10.1107/S0108270189005998]

Structure of dichlorobis(3,5-dimethylpyrazole)palladium

C.-H. Cheng, J.-S. Lain, Y.-J. Wu and S.-L. Wang



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Acta Cryst. (1990). C46, 210-213    [doi:10.1107/S0108270189005081]

Structure and pseudosymmetry of tetrabromobis(dimethyl sulfoxide)tin(IV)

M. Gregorkiewitz and D. Tudela



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Acta Cryst. (1990). C46, 213-215    [doi:10.1107/S010827018900555X]

Structure of [Ni(Me8[14]aneC[alpha])](ClO4)2 (Me8[14]ane = 2,5,5,7,9,12,12 14-octamethyl-1,4,8,11-tetraazacyclotetradecane)

G. Ferguson, A. J. Lough and R. Bembi



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Acta Cryst. (1990). C46, 216-218    [doi:10.1107/S010827018900644X]

Bis(thioacetato-S)[tris(2-aminoethyl)amine]cobalt(III) perchlorate

K. Okamoto, T. Konno and J. Hidaka



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Acta Cryst. (1990). C46, 218-220    [doi:10.1107/S0108270189007250]

Structure of tetramethylammonium tetraiodozincate in the monoclinic phase

K. Hasebe, T. Asahi and K. Gesi



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Acta Cryst. (1990). C46, 220-223    [doi:10.1107/S0108270189006207]

Structures of the conducting salts of ethylenedithiotetrathiafulvalene (EDTTTF) and methylenedithiotetrathiafulvalene (MDTTTF): (EDTTTF)I3 and (MDTTTF)I3

A. Hountas, A. Terzis, G. C. Papavassiliou, B. Hilti and J. Pfeiffer



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Acta Cryst. (1990). C46, 224-228    [doi:10.1107/S0108270189006219]

Structures and conductivities of the synthetic metal salts of ethylenedithiotetrathiafulvalene (EDTTTF) and ethylenedithiodiselenadithiafulvalene (EDTDSDTF): 211-(EDTTTF)2IBr2, 211-(EDTDSDTF)2IBr2 and 212-(EDTTTF)2AuBr2

A. Terzis, A. Hountas, G. C. Papavassiliou, B. Hilti and J. Pfeiffer



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Acta Cryst. (1990). C46, 228-231    [doi:10.1107/S0108270189006220]

Structures of the new superconductor (MDTTTF)2AuI2 (Tc = 4.5 K) and the organic metal (EDTTTF)2AuI2 (MDTTTF = methylenedithiotetrathiafulvalene and EDTTTF = ethylenedithiotetrathiafulvalene)

A. Hountas, A. Terzis, G. C. Papavassiliou, B. Hilti, M. Burkle, C. W. Meyer and J. Zambounis



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Acta Cryst. (1990). C46, 231-235    [doi:10.1107/S0108270189005627]

Structures of tetraaquabis(hydroxymethanesulfonato)magnesium(II) and hexaaquaaluminium(III) hydroxymethanesulfonate

T. S. Cameron, W. J. Chute, G. Owen, J. Aherne and A. Linden



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Acta Cryst. (1990). C46, 235-238    [doi:10.1107/S0108270189006426]

Bis-[mu]-[methylenebis(diphenylphosphine)]-dinitratodisilver(I) dichloroform solvate

E. R. T. Tiekink


organic compounds



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Acta Cryst. (1990). C46, 238-240    [doi:10.1107/S0108270189006177]

Structure of cytosinium dihydrogenmonophosphate

M. Bagieu-Beucher



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Acta Cryst. (1990). C46, 240-243    [doi:10.1107/S0108270189005093]

Structure of 2-acetoxy-10-hydroxy-3-methoxy-10-phenyl-9(10H)-anthracenone

A. Roszak and B. Engelen



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Acta Cryst. (1990). C46, 243-246    [doi:10.1107/S0108270189004762]

Structures of two model peptides: N-acetyl-D,L-valine and N-acetyl-L-valyl-L-leucine

P. J. Carroll, P. L. Stewart and S. J. Opella



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Acta Cryst. (1990). C46, 246-248    [doi:10.1107/S0108270189005706]

Structure of 9-chloro-7-(2-fluorophenyl)-5H-pyrimido[5,4-d][2]benzazepine

H. J. Kemmish and T. A. Hamor



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Acta Cryst. (1990). C46, 248-251    [doi:10.1107/S0108270189005925]

Structure of an unexpected dibenz[d, f]azonine from the HBr elimination of N-formyl-N-norbromocodide

H. van Koningsveld, J. T. M. Linders, R. J. Booth, T. S. Lie and L. Maat



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Acta Cryst. (1990). C46, 251-253    [doi:10.1107/S0108270189005640]

Structure of dibromo(2-methoxycyclohexyl)phenyltellurium

R. K. Chadha and T. Nguyen



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Acta Cryst. (1990). C46, 253-256    [doi:10.1107/S0108270189006074]

Formation of diastereoisomeric pinacols via reductive coupling of D3-trishomocubanone

W. H. Watson, A. Nagl, A. P. Marchand and G. M. Reddy



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Acta Cryst. (1990). C46, 256-259    [doi:10.1107/S0108270189006268]

Stereochemistry of rings. XVII. Norbornane derivatives. 1. 2-(p-Methoxyphenyl)-3-phenylbicyclo[2.2.1]heptane (I) and 2-(p-nitrophenyl)-3-phenylbicyclo[2.2.1]heptane (II)

G. Bocelli



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Acta Cryst. (1990). C46, 259-261    [doi:10.1107/S0108270189006189]

Structure of a pyridyl-containing macrobicyclic molecule, potential transition-metal complexing agent and NADH model precursor

J. P. Dutasta, G. Gellon, J. L. Pierre, M. T. Averbuch-Pouchot and A. Durif



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Acta Cryst. (1990). C46, 261-263    [doi:10.1107/S0108270189006049]

Structure of a 1,2,3,5-tetrazin-4-one

K. Yamaguchi, A. Ohsawa, T. Itoh and C. Kawabata



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Acta Cryst. (1990). C46, 263-267    [doi:10.1107/S0108270189005767]

Structure of tetramethyl (2R,3R,11R,12R)-[alpha]-benzyl-1,4,7,10,13,16-hexaoxacyclooctadecane-2,3,11,12-tetra[(2S)-carboxamidoacetate] (an 18-crown-6 derivative)

P. Singh, M. L. Miles and S. Davis



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Acta Cryst. (1990). C46, 267-271    [doi:10.1107/S0108270189005317]

Structure of elsinochrome A

H. J. Mebius, H. Krabbendam and A. J. M. Duisenberg



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Acta Cryst. (1990). C46, 271-273    [doi:10.1107/S0108270189005196]

Zwitterions in crystalline aminophosphonic acids. I. Structure of (2-pyridylmethyl)phosphonic acid

Z. Galdecki and W. M. Wolf



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Acta Cryst. (1990). C46, 274-276    [doi:10.1107/S010827018900630X]

Structure of tris(phenylthio)phosphine

N. Burford, B. W. Royan and P. S. White



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Acta Cryst. (1990). C46, 276-279    [doi:10.1107/S0108270189006256]

Structure of methylenecyclopropane-2-carboxamide by time-of-flight neutron diffraction

A. J. Schultz, D. G. Van Derveer, D. W. Parker and J. E. Baldwin



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Acta Cryst. (1990). C46, 279-281    [doi:10.1107/S0108270189006384]

(Z)-Methyl 2-phenyl-2-(pyrid-4-yl)vinyl sulfoxide

M. Madesclaire, J. Metin, D. Roche and A. Fauve



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Acta Cryst. (1990). C46, 281-286    [doi:10.1107/S0108270189006116]

Structures of benzylammonium hydrogen malonate (I) and 4-picolinium hydrogen malonate (II)

K. Djinovic, L. Golic and I. Leban



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Acta Cryst. (1990). C46, 286-290    [doi:10.1107/S0108270189005755]

Absolute configuration of 1,1'-(1,2-ethanediyl)bis(L-pyroglutamic acid), (S,S)-eddpg

T. J. Emge, L. C. Strickland and C. M. Perkins



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Acta Cryst. (1990). C46, 291-293    [doi:10.1107/S0108270189006591]

Functionalized hydrocarbons with condensed ring skeletons: methyl 1,10-cis-1,2-transoid-2,7-cis-8,14-dioxotricyclo[8.4.0.02,7]tetradecane-1-carboxylate

A. G. Michel, N. Michel-Dewez and R. Ruel



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Acta Cryst. (1990). C46, 293-295    [doi:10.1107/S0108270189006438]

Structure of butyldodecyldimethylammonium bromide monohydrate

T. Taga, Y. Miwa, K. Machida, N. Kimura, S. Hayashi, J. Umemura and T. Takenaka



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Acta Cryst. (1990). C46, 295-298    [doi:10.1107/S010827018900658X]

Structure of 1,4-cubanediyldiammonium bis(trinitromethanide)

H. L. Ammon, C. S. Choi, R. S. Damvarapu, S. Iyer and J. Alster



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Acta Cryst. (1990). C46, 299-301    [doi:10.1107/S0108270189007109]

Structure of 3-(4-nitrobenzoyl)-4-thiazolidinecarboxylic acid ethyl ester

M. T. Averbuch-Pouchot, A. Durif, M. H. Pera and A. Hamri



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Acta Cryst. (1990). C46, 301-303    [doi:10.1107/S0108270189006992]

Structure of tetrahydro-N-methyl-2-(2-pyridinyl)-2-thiophenecarbothioamide (picartamide)

Y. In, Y. Fujimori, H. Ohishi, T. Ishida, M. Inoue, F. Sato, M. Okitsu and T. Ohno



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Acta Cryst. (1990). C46, 303-306    [doi:10.1107/S0108270189006906]

Vernamycin B[alpha]

I. L. Karle and J. L. Flippen-Anderson



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Acta Cryst. (1990). C46, 307-310    [doi:10.1107/S0108270189006578]

Structures of garugamblin-I and garugamblin-II: two natural ansa bridged biaryl ethers

M. Nethaji, V. Pattabhi, H. G. Krishnamurthy and A. C. Talukdar



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Acta Cryst. (1990). C46, 310-313    [doi:10.1107/S0108270189006682]

Structure of quercetin dihydrate

G.-Z. Jin, Y. Yamagata and K. Tomita



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Acta Cryst. (1990). C46, 313-317    [doi:10.1107/S0108270189006785]

Structure of the neuroleptic drug 4-amino-N-1-[(1-ethyl-2-pyrrolidinyl)methyl]-5-(ethylsulfonyl)-2-methoxybenzamide (amisulpride)

H. L. De Winter, C. L. Verlinde, N. M. Blaton, O. M. Peeters and C. J. De Ranter


short format


inorganic compounds



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Acta Cryst. (1990). C46, 317-318    [doi:10.1107/S0108270189006104]

Na2W2O7 (II), a high-pressure phase of disodium ditungstate(VI)

K.-J. Range and H. Haase



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Acta Cryst. (1990). C46, 319-320    [doi:10.1107/S0108270189010395]

Structures of two strong Brønsted acids: (I) fluorosulfuric acid and (II) trifluoromethanesulfonic acid

K. Bartmann and D. Mootz


metal-organic compounds



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Acta Cryst. (1990). C46, 321-322    [doi:10.1107/S0108270189010085]

Structure of potassium (2,2'-bipyridine)tetrachlororuthenate(III)

B. Durham, D. I. Cox, A. W. Cordes and S. Barsoum



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Acta Cryst. (1990). C46, 322-324    [doi:10.1107/S0108270189009807]

Structure of (H4cyclam)4+.ReCl62-.2Cl-.4(CH3)2SO

A. J. Blake, J. A. Greig and M. Schröder



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Acta Cryst. (1990). C46, 324-326    [doi:10.1107/S0108270189010449]

Diaquabis(oxo-5 prolinato)zinc(II)

N. Rodier, R. Ceolin, M. Plat and H. Zumbihl


organic compounds



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Acta Cryst. (1990). C46, 326-327    [doi:10.1107/S010827018900911X]

Structure of a triterpene extracted from Austroplenckia populnea (Celastraceae), methyl-3-oxofriedelan-20[alpha]-oate

A. B. Cota, Y. P. Mascarenhas, G. D. F. Silva and J. R. de Souza



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Acta Cryst. (1990). C46, 328-329    [doi:10.1107/S0108270189009121]

Structure of a triterpene extracted from Austroplenckia populnea (Celastraceae), methyl 3-hydroxy-2-oxofriedelan-3-en-20[alpha]-oate

A. B. Cota, Y. P. Mascarenhas, G. D. F. Silva and J. R. de Souza



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Acta Cryst. (1990). C46, 329-331    [doi:10.1107/S0108270189010048]

Structure of methyl 3-hydroxy-3',3'-dimethylspiro[1,2-benzo-1-cyclohexene-4,1'-cyclopropane]-2'-carboxylate

V. G. Puranik, S. S. Tavale and T. N. Guru Row



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Acta Cryst. (1990). C46, 331-332    [doi:10.1107/S0108270189009613]

2-Ethynyl-1,3-dimethoxybenzene

K. L. Evans, G. W. Horn, F. R. Fronczek, R. D. Gandour and S. F. Watkins



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Acta Cryst. (1990). C46, 333-334    [doi:10.1107/S0108270189009418]

tert-Butyl N-[1-(3-tert-butyl-2-hydroxyphenyl)-1-hydroxy-3-phenyl-2-propyl]carbamate

G. Bocelli and A. Cantoni



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Acta Cryst. (1990). C46, 334-336    [doi:10.1107/S010827018901125X]

Structure of 3[beta]-hydroxy-5-androsten-17-one (DHEA) monohydrate

P. J. Cox, S. M. MacManus, B. C. Gibb, I. W. Nowell and R. A. Howie



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Acta Cryst. (1990). C46, 336-338    [doi:10.1107/S0108270189010073]

Diisopropylammonium chloride

P. Prince, J. A. Miller, F. R. Fronczek and R. D. Gandour



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Acta Cryst. (1990). C46, 338-340    [doi:10.1107/S0108270189009972]

Structure of peperomin B

T.-J. Lee, T.-Y. Lee and C.-M. Chen



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Acta Cryst. (1990). C46, 340-342    [doi:10.1107/S010827018901022X]

Reinvestigation of the structure of hypoxanthinium nitrate monohydrate

H. W. Schmalle, G. Hänggi and E. Dubler



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Acta Cryst. (1990). C46, 342-344    [doi:10.1107/S0108270189009030]

Structure of the lignane (+)-pinoresinol dimethyl ether

M. Vasquez, F. R. Fronczek and N. H. Fischer



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Acta Cryst. (1990). C46, 344-346    [doi:10.1107/S010827018901108X]

Structure of the perchlorate salt of hetisine 13-O-acetate

J. F. Richardson and M. H. Benn



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Acta Cryst. (1990). C46, 346-348    [doi:10.1107/S010827018901070X]

Structure of 3-oxa-1,5-pentanediyl bis(p-toluenesulfonate)

Y. Ferchaux, F. Villain and A. Navaza


short communications



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Acta Cryst. (1990). C46, 348    [doi:10.1107/S0108270189013478]

Structure of recinine. Erratum

M. Soriano-García, M. Jímenez E., R. Reyes Vaca and R. A. Toscano


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