Acta Crystallographica Section C

Crystal Structure Communications

Volume 46, Part 3 (March 1990)



research papers


inorganic compounds



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Acta Cryst. (1990). C46, 349-350    [doi:10.1107/S0108270189007547]

Space-group changes - revised structures of seven compounds

M. Kapon and G. M. Reisner



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Acta Cryst. (1990). C46, 350-354    [doi:10.1107/S0108270189006943]

The structure of hexaaquanickel(II) chlorate

J. C. Gallucci and R. E. Gerkin



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Acta Cryst. (1990). C46, 354-358    [doi:10.1107/S0108270189006803]

Untwinned single crystals of the high-temperature superconductor YBa2Cu3O7-x

K. Brodt, H. Fuess, E. F. Paulus, W. Assmus and J. Kowalewski



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Acta Cryst. (1990). C46, 358-361    [doi:10.1107/S0108270189007249]

Redetermination of the structure of caesium hydrogensulfate

K. Itoh, T. Ukeda, T. Ozaki and E. Nakamura



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Acta Cryst. (1990). C46, 361-363    [doi:10.1107/S0108270189006761]

Hydrogen bonding in barium hydroxide trihydrate by neutron diffraction

H. D. Lutz, T. Kellersohn and T. Vogt



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Acta Cryst. (1990). C46, 363-365    [doi:10.1107/S010827018900750X]

The structure of metastable lithium disilicate, Li2Si2O5

R. I. Smith, R. A. Howie, A. R. West, A. Aragón-Piña and M. E. Villafuerte-Castrejón



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Acta Cryst. (1990). C46, 365-368    [doi:10.1107/S0108270189007936]

Structure du sulfure de thulium et de zinc ZnTm2S4

P. Lemoine, A. Tomas, T. Vovan et M. Guittard



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Acta Cryst. (1990). C46, 368-369    [doi:10.1107/S0108270189007912]

Structure of Na4OI2

H. Sabrowsky, K. Hippler, S. Sitta, P. Vogt and L. Walz



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Acta Cryst. (1990). C46, 370-372    [doi:10.1107/S0108270189005950]

Structure of Ba2Cu(BO3)2

R. W. Smith and D. A. Keszler



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Acta Cryst. (1990). C46, 372-374    [doi:10.1107/S0108270189007948]

Synthèse et structure du borouranate de lithium LiBUO5

M. Gasperin



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Acta Cryst. (1990). C46, 374-377    [doi:10.1107/S0108270189008504]

Structure of [omega]-Ti3Al2.25Nb0.75

C. B. Shoemaker, D. P. Shoemaker and L. A. Bendersky


metal-organic compounds



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Acta Cryst. (1990). C46, 377-379    [doi:10.1107/S0108270189007055]

Structure of bis(acetato)bis(meso-1,2-diphenyl-1,2-ethanediamine)nickel(II) trihydrate, [Ni(C2H3O2)2(C14H16N2)2].3H2O

S. García-Granda, M. R. Díaz, C. Barrio and F. Gómez-Beltrán



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Acta Cryst. (1990). C46, 379-385    [doi:10.1107/S0108270189007092]

Structure and single-crystal conductivity measurements of oxidized 3d metal phthalocyanines. Bis-chloro derivatives of chromium(III), iron(III) and cobalt(III)

B. Moubaraki, M. Ley, D. Benlian and J.-P. Sorbier



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Acta Cryst. (1990). C46, 385-388    [doi:10.1107/S0108270189005251]

Structures of (I) bis[benzyldimethyl(phenyl)ammonium] tetrachloromanganate(II) and (II) bis[benzyldimethyl(phenyl)ammonium] tetrachlorocobaltate(II)

S. Chaudhuri, T. Banerjee, P. N. Roy, G. Bocelli and M. K. Deb Purkayastha



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Acta Cryst. (1990). C46, 388-391    [doi:10.1107/S0108270189006852]

(1,1,4,7,10,10-Hexaphenyl-1,4,7,10-tetraphosphadecane-P,P',P'',P''')platinum(II) bis(tetraphenylborate)

P. Brüggeller and T. Hübner



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Acta Cryst. (1990). C46, 391-394    [doi:10.1107/S0108270189007420]

Structure of iodo-1[kappa]I-[mu]-(O-isopropyl dithiocarbonato-1[kappa]2S,S':2[kappa]S')-bis[(O-isopropyl dithiocarbonato)cadmium] Cd2I(S2COiPr)3

B. F. Abrahams, B. F. Hoskins and G. Winter



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Acta Cryst. (1990). C46, 394-396    [doi:10.1107/S0108270189007924]

Structure of mononuclear bis{aqua[2,2'-(1,3,4-oxadiazole-2,5-diyl)dipyridine-N,N']}copper(II) diperchlorate

J. P. Wignacourt, S. Sueur and M. Lagrenée



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Acta Cryst. (1990). C46, 396-399    [doi:10.1107/S0108270189011248]

Structures of chromium(III) cyclam complexes. 2. Structure of trans-dibromo(1,4,8,11-tetraazacyclotetradecane)chromium(III) bromide

J. N. Lisgarten, R. A. Palmer, A. M. Hemmings and D. M. Gazi



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Acta Cryst. (1990). C46, 399-402    [doi:10.1107/S0108270189007791]

Structures of triaqua[1,2-benzenedicarboxylato(2-)](1,10-phenanthroline)nickel(II) monohydrate (I) and triaqua[1,2-benzenedicarboxylato(2-)](2,2'-dipyridylamine)nickel(II) dihydrate (II)

D. Poleti, D. R. Stojakovic, B. V. Prelesnik and Lj. Manojlovic-Muir



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Acta Cryst. (1990). C46, 402-404    [doi:10.1107/S0108270189008115]

Structure of hexa-[mu]-chloro-[mu]4-oxo-tetrakis[1,2-dimethylimidazolecopper(II)]

A. Erdonmez, J. H. van Diemen, R. A. G. de Graaff and J. Reedijk


organic compounds



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Acta Cryst. (1990). C46, 405-407    [doi:10.1107/S0108270189006499]

Structure of 3-(2-benzimidazolyl)-7-(diethylamino)coumarin

K. Chinnakali, K. Sivakumar and S. Natarajan



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Acta Cryst. (1990). C46, 407-410    [doi:10.1107/S0108270189007134]

Structure of [alpha]-D-N-acetyl-1-O-methylneuraminic acid methyl ester

H. Kooijman, L. M. J. Kroon-Batenburg, J. Kroon, J. N. Breg and J. L. de Boer



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Acta Cryst. (1990). C46, 410-414    [doi:10.1107/S0108270189007626]

Conformational study of 1,3,5-tris(o-chlorophenyl)-1,3,5-triazacyclohexane and 1,3,5-tris(p-chlorophenyl)-1,3,5-triazacyclohexane

A. Bouchemma, P. H. McCabe and G. A. Sim



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Acta Cryst. (1990). C46, 414-417    [doi:10.1107/S0108270189006669]

Structures of (methyl)phenylhydrazone derivatives and their nonlinear optical properties

E. Chiba, K. Tani, M. Shuto, N. Haga and M. Tokonami



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Acta Cryst. (1990). C46, 417-420    [doi:10.1107/S0108270189005524]

Structure of a cyclopropaneaziridine derivative of 1,5-naphthyridine

B. Pniewska, A. Rykowski and R. Anulewicz



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Acta Cryst. (1990). C46, 420-422    [doi:10.1107/S0108270189006359]

Structure du tris(éthylènediammonium) bis(monohydrogénodiphosphate) dihydrate

S. Kamoun, A. Jouini, M. Dabbabi et A. Daoud



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Acta Cryst. (1990). C46, 422-425    [doi:10.1107/S0108270189005949]

Structures of two neolignans

Z.-Y. Zhang, G. J. Palenik, S. K. Chattopadhyay and K. V. Rao



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Acta Cryst. (1990). C46, 425-427    [doi:10.1107/S0108270189007225]

Structure of limonin

K. Takahashi, M. Obayashi and M. Nakatani



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Acta Cryst. (1990). C46, 428-430    [doi:10.1107/S0108270189006451]

Crystallographic studies and physicochemical properties of [pi]-electron compounds. XVII. The structure of p-nitrophenylacetic acid

S. J. Grabowski, T. M. Krygowski, G. Häfelinger and G. Ritter



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Acta Cryst. (1990). C46, 430-432    [doi:10.1107/S0108270189006931]

Structure of 4,4'-dimethylbenzophenone

B. Kojic-Prodic, N. Bresciani-Pahor and D. Horvatic



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Acta Cryst. (1990). C46, 432-435    [doi:10.1107/S0108270189007237]

Structure of diethyl 1-(8-dimethylamino-1-naphthyl)-1H-1,2,3-triazole-4,5-dicarboxylate

Y. Nagawa, M. Goto, K. Honda and H. Nakanishi



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Acta Cryst. (1990). C46, 435-437    [doi:10.1107/S0108270189005858]

Structure of 3-(1-pyridinio)indole-2-thiolate

J. Hasek, K. Huml and L. Kutschabsky



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Acta Cryst. (1990). C46, 437-439    [doi:10.1107/S0108270189006864]

Structure of karanjin

Meena Hariharan and S. S. Rajan



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Acta Cryst. (1990). C46, 439-441    [doi:10.1107/S0108270189007857]

Structure of dicyclopenta[ef,kl]heptalene (azupyrene)

A. G. Anderson Jnr, S. C. Critchlow, L. C. Andrews and R. D. Haddock



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Acta Cryst. (1990). C46, 442-445    [doi:10.1107/S0108270189006530]

Structure of an allylic precursor of higher sugars

Z. Ciunik, H. Paulsen, P. Luger and S. Jarosz



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Acta Cryst. (1990). C46, 445-447    [doi:10.1107/S0108270189006876]

Structure of 3,6,10,12-tetramethylbenzofuro[2,3-b]benzofuran

Meena Hariharan, S. S. Rajan, J. Vijayalakshmi, R. Srinivasan and T. N. Guru Row



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Acta Cryst. (1990). C46, 447-450    [doi:10.1107/S0108270189007705]

Structure of the thromboxane receptor antagonist EP 092

A. McAlpine, L. Sawyer, P. Taylor and A. J. Blake



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Acta Cryst. (1990). C46, 450-453    [doi:10.1107/S0108270189007523]

Structure of 9-chloro-7-(2-chlorophenyl)-3,5-dihydro[1,2,4]triazino[4,3-a][1,4]benzodiazepin-2(1H)-one

H. J. Kemmish and T. A. Hamor



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Acta Cryst. (1990). C46, 453-456    [doi:10.1107/S0108270189007067]

Fumarate de bis{[(1H-benzimidazolyl-1)-3 méthyl-1 propyl][hydroxy-2 (hydroxy-4 méthoxy-3 phényl)-2 éthyl]ammonium} hexahydrate

P. Toffoli, N. Rodier, R. Ceolin, K. Dao Duong et M. Joannic



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Acta Cryst. (1990). C46, 456-458    [doi:10.1107/S0108270189006141]

Structure of N1,N1-(3-oxapentamethylene)-N2-phenylacetamidine

E. Ciszak, M. Jaskólski and Z. Kosturkiewicz



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Acta Cryst. (1990). C46, 459-462    [doi:10.1107/S0108270189007377]

Structure of 5-chloro-2-{3-[(diethylamino)methyl]-5-methyl-4H-1,2,4-triazol-4-yl}benzophenone (I) and of its methylamino analogue (II)

H. J. Kemmish and T. A. Hamor



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Acta Cryst. (1990). C46, 462-465    [doi:10.1107/S0108270189007298]

Crystal studies of acridinium dyes. X. 10-Methyl-9-[2-methyl-4-(1,4,7,10-tetraoxa-13-aza-13-cyclopentadecyl)phenyl]acridinium barium perchlorate acetonitrile (1/1)

L. P. Häming, C. A. Reiss, K. Goubitz and D. Heijdenrijk



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Acta Cryst. (1990). C46, 465-467    [doi:10.1107/S0108270189007328]

Crystal studies of acridinium dyes. XI. 10-Methyl-9-[2-methyl-4-(1,4,7,10-tetraoxa-13-aza-13-cyclopentadecyl)phenyl]acridinium lithium perchlorate

C. A. Reiss, K. Goubitz and D. Heijdenrijk



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Acta Cryst. (1990). C46, 468-470    [doi:10.1107/S0108270189007304]

Crystal studies of musk compounds. I. 4-tert-Butyl-3-methoxy-2,6-dinitrotoluene (musk ambrette)

D. J. A. De Ridder, K. Goubitz and H. Schenk



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Acta Cryst. (1990). C46, 470-472    [doi:10.1107/S0108270189007274]

Structure of benzyl 2-oxo-2,3-dihydro-1,3-benzothiazoleacetate

V. Vrábel, J. Lokaj, E. Kellö, V. Konecný, A. C. Batsanov and Yu. T. Struchkov



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Acta Cryst. (1990). C46, 472-476    [doi:10.1107/S0108270189007365]

Structure of bis(cyclohexylammonium) phosphoenolpyruvate methanol solvate (1/0.5)

A. Weichsel and T. Lis



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Acta Cryst. (1990). C46, 476-478    [doi:10.1107/S0108270189008097]

Structure of methyl (E)-2-cyano-2-(1-phenyl-4,5-dihydro-1H-tetrazol-5-ylidene)acetate

H. Zimmermann, M. Gomm, U. Wirth, M. Fischer, C.-J. Lurz and R. W. Saalfrank



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Acta Cryst. (1990). C46, 479-481    [doi:10.1107/S0108270189008061]

Structure of 1,9:4,10-diethanotriptycene

H. Matsuzawa, K. Kozawa, T. Uchida, H. Akimoto and N. Mori



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Acta Cryst. (1990). C46, 481-483    [doi:10.1107/S0108270189007882]

Structure of a 2-substituted cyclopropane amino acid derivative: 1-hydroxymethyl-5-phenyl-7-oxa-4-azaspiro[2.5]octan-8-one

D. J. Aitken, J. Royer, H.-P. Husson, A. Chiaroni and C. Riche



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Acta Cryst. (1990). C46, 484-486    [doi:10.1107/S0108270189007894]

Structures de l'ebselen (phényl-2 2H-benzisosélénazole-1,2 one-3) (I) et de l'acétonylséléno-2 benzanilide (II)

L. Dupont, O. Dideberg et P. Jacquemin


short format


inorganic compounds



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Acta Cryst. (1990). C46, 487-488    [doi:10.1107/S0108270189012035]

Tm2S3-V, a corundum-type modification of thulium sesquisulfide

K.-J. Range, H. Drexler, A. Gietl, U. Klement and K. G. Lange



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Acta Cryst. (1990). C46, 488-489    [doi:10.1107/S0108270189012047]

Diammonium trimolybdate(VI), (NH4)2Mo3O10

K.-J. Range and A. Fässler


metal-organic compounds



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Acta Cryst. (1990). C46, 490-491    [doi:10.1107/S0108270189011133]

Structure of a tetrahedral NiII dibromo complex with a 6,6'-disubstituted bipyridine

D. W. Evans, G. R. Newkome and F. R. Fronczek



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Acta Cryst. (1990). C46, 492-494    [doi:10.1107/S0108270189011261]

[mu]-([eta]-Diarseno-[mu]-As,[mu]-As')-bis(dicarbonyl-[eta]5-propylcyclopentadienylmolybdenum)(Mo-Mo) and bis-[mu]-([eta]-diarseno-[mu]-As,[mu]-As')-bis(carbonyl-[eta]-cyclopentadienylmolybdenum)(Mo-Mo)

A.-J. DiMaio, C. J. Baldacchini and A. L. Rheingold



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Acta Cryst. (1990). C46, 494-496    [doi:10.1107/S0108270189011376]

Structure of [(1,2,3-[eta])-cyclotridecenyl]bis(triphenylphosphine)rhodium benzene solvate

A. W. Cordes, S. Siegel, S.-T. Lin, L. Martin and M. C. Noble



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Acta Cryst. (1990). C46, 496-498    [doi:10.1107/S0108270189012138]

([eta]2-1,3-Di-tert-butyl-2,5-dioxo-3-cyclopentene-1-carbonitrile)bis(triphenylphosphine)platinum(0)-diethyl ether

A. L. Rheingold, C. J. Baldacchini, P. D. Macklin and G. L. Geoffroy



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Acta Cryst. (1990). C46, 498-500    [doi:10.1107/S0108270189012126]

Carbonyl(2-cyano-3,3-dimethylbutanoic acid-N)([eta]5-cyclopentadienyl)(triphenylphosphine)iron(I) tetrafluoroborate

A. L. Rheingold, C. J. Baldacchini, G. L. Geoffroy and P. D. Macklin



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Acta Cryst. (1990). C46, 500-502    [doi:10.1107/S0108270189010620]

Structure of bis(imidazole)(5,10,15,20-tetraphenylporphinato)iron(III) bis(cis-1,2-dicyanoethylenedithiolato)cuprate(III) tetrakis(tetrahydrofuran) solvate

B. R. Serr, C. E. L. Headford, C. M. Elliott and O. P. Anderson


organic compounds



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Acta Cryst. (1990). C46, 502-504    [doi:10.1107/S0108270189011558]

Methyl 2-[(2,6-dimethoxyphenyl)ethynyl]-3-methoxybenzoate

K. L. Evans, G. W. Horn, F. R. Fronczek and R. D. Gandour



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Acta Cryst. (1990). C46, 504-506    [doi:10.1107/S0108270189011753]

Structure of 1-chloro-3,3,5,5-tetraphenyl-1,3,5,2,4,6-selenadiphosphatriazine

A. W. Cordes, K. Bestari and R. T. Oakley



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Acta Cryst. (1990). C46, 506-508    [doi:10.1107/S0108270189009790]

Structure of 7-methyl-8-thioxo-7,8-dihydroguanosine monohydrate

S. B. Larson, E. M. Henry, G. D. Kini and R. K. Robins



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Acta Cryst. (1990). C46, 508-510    [doi:10.1107/S0108270189011315]

3-Hydroxy-1,3-bis(2-thienyl)prop-2-en-1-one

L. A. M. Baxter, A. J. Blake, G. A. Heath and T. A. Stephenson



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Acta Cryst. (1990). C46, 510-512    [doi:10.1107/S0108270189011091]

The structures of two auxin-like compounds: 1,2-benzisothiazol-3-yl- and 1,2-benzisoxazol-3-ylacetic acid

P. Domiano and C. Branca



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Acta Cryst. (1990). C46, 512-515    [doi:10.1107/S0108270189011741]

Structure of sulfonosine

S. B. Larson, N. B. Hanna, G. R. Revankar and R. K. Robins



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Acta Cryst. (1990). C46, 515-517    [doi:10.1107/S0108270189012175]

Structure of tetrahydrofuniculosin

Y. Nawata, I. Matsuura, K. Ando and Y. Iitaka



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Acta Cryst. (1990). C46, 517-519    [doi:10.1107/S0108270189011583]

5-Hydroxyflavone

M. Shoja



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Acta Cryst. (1990). C46, 519-521    [doi:10.1107/S0108270189006815]

Structure of 3-chloroflavanone

D. W. Tomlin and J. S. Cantrell



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Acta Cryst. (1990). C46, 521-522    [doi:10.1107/S0108270189011595]

The structure of a tetracyclic enone containing the 5-7-6 ring system of the tiglianes

P. Ch. Kierkus, J. H. Rigby and M. J. Heeg


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