Acta Crystallographica Section C

Crystal Structure Communications

Volume 46, Part 7 (July 1990)



research papers


inorganic compounds



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Acta Cryst. (1990). C46, 1185-1188    [doi:10.1107/S0108270189010814]

Structure d'un triarséniate: Na3H2As3O10

A. Driss et T. Jouini



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Acta Cryst. (1990). C46, 1188-1190    [doi:10.1107/S0108270189010759]

Structure of SnMo5O8 containing bioctahedral Mo10 clusters

P. Gougeon, M. Potel and M. Sergent



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Acta Cryst. (1990). C46, 1191-1193    [doi:10.1107/S0108270189011704]

CaCuP2O7: a structure closely related to [alpha]-Ca2P2O7

D. Riou and M. Goreaud



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Acta Cryst. (1990). C46, 1193-1195    [doi:10.1107/S0108270189011303]

Structure of Ta5SnGa2

J. Ye, H. Horiuchi, T. Shishido, K. Ukei and T. Fukuda



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Acta Cryst. (1990). C46, 1195-1197    [doi:10.1107/S0108270189011169]

Structure of V2Sn2Ga

J. Ye, H. Horiuchi, T. Shishido and T. Fukuda



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Acta Cryst. (1990). C46, 1197-1199    [doi:10.1107/S0108270189011820]

Structure of gadolinium monosilicide

D. A. Nagaki and A. Simon



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Acta Cryst. (1990). C46, 1199-1202    [doi:10.1107/S0108270189011029]

Structure and absolute chirality of Rb4LiH3(SO4)4 at 293 K

F. J. Zúñiga, J. Etxebarria, G. Madariaga and T. Breczewski



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Acta Cryst. (1990). C46, 1202-1204    [doi:10.1107/S0108270189011042]

Refinement of the structure of sodium enneagermanate (Na4Ge9O20)

M. E. Fleet



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Acta Cryst. (1990). C46, 1205-1207    [doi:10.1107/S0108270189011418]

Structure de l'oxysulfure d'uranium et de lutécium, (UOS)4LuS

S. Jaulmes, M. Julien-Pouzol, J. Dugué, P. Laruelle, T. Vovan et M. Guittard



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Acta Cryst. (1990). C46, 1207-1209    [doi:10.1107/S0108270189011613]

Structures of two polymorphs of cis-TaBr4(PhPMe2)2

N. Hovnanian, L. G. Hubert-Pfalzgraf and G. Le Borgne


metal-organic compounds



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Acta Cryst. (1990). C46, 1210-1212    [doi:10.1107/S0108270189011297]

Structure of aqua(tetraphenylporphyrinato)zinc(II) a redetermination

A. J. Golder, D. C. Povey, J. Silver and Q. A. A. Jassim



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Acta Cryst. (1990). C46, 1212-1215    [doi:10.1107/S0108270189011571]

Structure of piperazinium tetrachlorocobaltate monohydrate

D. Tran Qui and E. Palacios



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Acta Cryst. (1990). C46, 1215-1217    [doi:10.1107/S0108270189010693]

Structure of dimethyltetramethylenetetrathiafulvalene hexafluoroarsenate: (C12H14S4)2AsF6

T. Granier, B. Gallois, J. Gaultier and J. M. Fabre



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Acta Cryst. (1990). C46, 1217-1220    [doi:10.1107/S0108270189011790]

Structure of a palladium(II) complex with a non-symmetrical tetradentate Schiff base

B. Kratochvíl, M. Nováková, J. Ondrácek, J. Novotný, V. Haber and B. Hájek



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Acta Cryst. (1990). C46, 1220-1223    [doi:10.1107/S0108270189011406]

Synthesis and structure of cytosine dichloride cuprate: direct bonding of copper to cytosine

D. Tran Qui and E. Palacios



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Acta Cryst. (1990). C46, 1223-1226    [doi:10.1107/S0108270189010978]

Structure of the silver salt of N-(p-aminophenylsulfonyl)acetamide (silver sulfacetamide)

M. Ghosh, A. K. Basak and S. K. Mazumdar



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Acta Cryst. (1990). C46, 1226-1228    [doi:10.1107/S0108270189010826]

Structure of dinuclear bis(di-2-pyridylmethanone oximato)copper(II) dihydrate

E. O. Schlemper, J. Stunkel and C. Patterson



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Acta Cryst. (1990). C46, 1228-1231    [doi:10.1107/S010827018901228X]

Structure of 10,11-[mu]-[(triphenylphosphine)aurio]-9-dimethylsulfido-7,8-dicarba-nido-undecaborane(10) methylene chloride solvate

E. J. M. Hamilton and A. J. Welch



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Acta Cryst. (1990). C46, 1231-1233    [doi:10.1107/S0108270189008814]

Dichloro([eta]5-cyclopentadienyl)([eta]5-tris-1,2,4-trimethylsilylcyclopentadienyl)titanium(IV)

C. H. Winter, J. W. Kampf and X.-X. Zhou



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Acta Cryst. (1990). C46, 1234-1236    [doi:10.1107/S0108270189011947]

Structure of chlorotris(1-3-[eta]-1-ethylindenyl)thorium(IV)

M. R. Spirlet, J. Rebizant, S. Bettonville and J. Goffart



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Acta Cryst. (1990). C46, 1236-1238    [doi:10.1107/S0108270189011364]

Structure of a CuI complex with a saturated N2S2 macrocycle

K. P. Balakrishnan, A. Riesen, A. D. Zuberbühler and T. A. Kaden


organic compounds



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Acta Cryst. (1990). C46, 1239-1241    [doi:10.1107/S0108270189010577]

Structure of 2,4-dichlorophenyl 8-oxo-1-azabicyclo[3.3.0]oct-2-ylacetate (endo and exo isomers 92:8)

G. Ferguson, A. J. Lough and A. J. McAlees



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Acta Cryst. (1990). C46, 1241-1244    [doi:10.1107/S0108270189010589]

Structure of N-(2,4-dinitrophenyl)-4-(1-pyrrolyl)pyridinium chloride sesquihydrate

G. Ferguson and A. J. McAlees



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Acta Cryst. (1990). C46, 1244-1248    [doi:10.1107/S0108270189010929]

Structures of leukotriene antagonists: racemic 2-hydroxy-3-[2-(8-phenyloctyl)phenyl]-4-thiaheptanedioic acid, SK&F 103944

D. S. Eggleston, R. F. Hall and J. G. Gleason



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Acta Cryst. (1990). C46, 1248-1251    [doi:10.1107/S0108270189010607]

6-Bromo-2,3-dihydro-5,7-dimethyl-1,4-diazepinium picrate and 6-bromo-2,3-dihydro-1,4-diazepinium picrate

G. Ferguson, M. Parvez, D. Lloyd, H. McNab and D. R. Marshall



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Acta Cryst. (1990). C46, 1252-1254    [doi:10.1107/S0108270189010590]

Structure of 4,4,6-trimethyl-2-(triphenylsiloxy)-1,3,2-dioxaborinane

G. Ferguson, A. J. Lough, J. P. Sheehan and T. R. Spalding



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Acta Cryst. (1990). C46, 1254-1256    [doi:10.1107/S010827018901098X]

Functionalized hydrocarbons with condensed ring skeletons. V. Substituted 1,2-dimethyltricyclo[8.4.0.02,7]tetradec-8-ene

A. G. Michel, P. Giguère, P. Deslongchamps and N. Michel-Dewez



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Acta Cryst. (1990). C46, 1256-1259    [doi:10.1107/S0108270189010644]

Structure of 1-methyl-2,4,4,6-tetraphenyl-1,4-dihydropyridine

J. Hasek and J. Ondrácek



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Acta Cryst. (1990). C46, 1259-1262    [doi:10.1107/S0108270189010656]

Structure of the cyclohexapeptide cleromyrine II trihydrate

J.-P. Declercq, B. Tinant, S. Bashwira and C. Hootelé



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Acta Cryst. (1990). C46, 1262-1264    [doi:10.1107/S0108270189011030]

Structure of the 4-oxo-2-butenoic acid alkyl ester moiety. I. Structures of diethyl 4,4'-(1,4-piperazinediyl)bis(4-oxo-2-butenoate) and dimethyl 4,4'-(2,5-dioxo-1,4-piperazinediyl)bis(4-oxo-2-butenoate)

M. L. Glówka and I. Iwanicka



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Acta Cryst. (1990). C46, 1265-1268    [doi:10.1107/S0108270189011121]

Structures of two tricyclo[5.2.1.02,6]decane derivatives

W. H. Watson, A. Nagl, R. P. Kashyap, A. P. Marchand and V. Vidyasagar



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Acta Cryst. (1990). C46, 1268-1271    [doi:10.1107/S0108270189010012]

Absolute configuration of (-)-4-bromo-N-(cis-2-phenylcycloheptyl)benzamide

L. K. Liem, A. W. Frahm, A. Kirfel and G. Adiwidjaja



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Acta Cryst. (1990). C46, 1271-1273    [doi:10.1107/S0108270189010723]

Structure of dimethyl (±)-1,2,3,4,4a[alpha],4b,9,10-octahydro-6,7-bis(trimethylsilyl)-2[beta],10a[beta]-ethanophenanthrene-12,12-dicarboxylate

J.-P. Gotteland, M. Malacria and R. Faure



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Acta Cryst. (1990). C46, 1273-1275    [doi:10.1107/S0108270189010553]

Structure of 5-hydroxy-2,2-dimethyl-5-phenyl-2,5-dihydrofuran-3-carbonitrile

G. Ferguson, D. McCarthy and F. O'Rourke



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Acta Cryst. (1990). C46, 1276-1279    [doi:10.1107/S0108270189011017]

Structures of two novel heptacyclic compounds: a cage ketone and a cage enone

W. H. Watson, R. P. Kashyap, A. P. Marchand and C. Ren



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Acta Cryst. (1990). C46, 1279-1282    [doi:10.1107/S0108270189011340]

Structure of muscarine chloride

K. Frydenvang and B. Jensen



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Acta Cryst. (1990). C46, 1282-1284    [doi:10.1107/S0108270190001408]

Structure of 3-dimethylamino-2-(2-formyl-3,4-dihydro-1-naphthyl)-N,N-dimethyl-2-propeniminium chloride dihydrate: a Vilsmeier intermediate

A. Koziol, G. J. Palenik, C. M. Marson and A. R. Katritzky



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Acta Cryst. (1990). C46, 1284-1287    [doi:10.1107/S0108270189010541]

Structure of 2,3-dihydro-5-nitro-6-phenyl-1,4-dithiin

G. Ferguson, B. Kaitner and A. D. Brewer



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Acta Cryst. (1990). C46, 1287-1289    [doi:10.1107/S0108270189010565]

Structure of 2,3-dihydro-5-phenyl-1,4-dithiin 1,1,4,4-tetroxide

G. Ferguson, A. J. Lough and A. D. Brewer



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Acta Cryst. (1990). C46, 1289-1293    [doi:10.1107/S0108270189011352]

Structure of 1,3-cyclopentanedione

A. Katrusiak



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Acta Cryst. (1990). C46, 1293-1295    [doi:10.1107/S0108270189011285]

N-Methyl-N'-sulfamidoisothiourea

I. P. Parkin, A. M. Z. Slawin, D. J. Williams and J. D. Woollins



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Acta Cryst. (1990). C46, 1295-1297    [doi:10.1107/S0108270189009522]

Structure of 2-amino-1-(p-methoxyphenyl)-4-imidazolecarbaldehyde

A. López-Castro and E. Moreno



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Acta Cryst. (1990). C46, 1297-1299    [doi:10.1107/S0108270189011467]

The structure of [(4-nitrophenyl)methyl]triphenylphosphonium bromide methanol solvate

P. van der Sluis, K. van der Vlist and H. Krabbendam



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Acta Cryst. (1990). C46, 1300-1303    [doi:10.1107/S0108270189009959]

Structures of two phenyliodonium ylides

N. W. Alcock, A. P. Bozopoulos, E. Hatzigrigoriou and A. Varvoglis



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Acta Cryst. (1990). C46, 1303-1305    [doi:10.1107/S0108270189007900]

Structure of N[alpha]-acetyl-N-methyl-L-tryptophanamide

M. Souhassou, A. Aubry, C. Lecomte and M. Marraud



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Acta Cryst. (1990). C46, 1306-1308    [doi:10.1107/S0108270189011601]

Structure of (+)-(7S,SS)-1,2,3,5,6,7-hexahydro-7-methyl-8-(p-tolylsulfinyl)-5-indolizinone

D. H. Hua, S. N. Bharathi, A. Tsujimoto and P. D. Robinson



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Acta Cryst. (1990). C46, 1308-1312    [doi:10.1107/S0108270189011510]

Structures of colchicine analogues. III. 2-Methoxy-5-(2',3'-dimethoxyphenyl)- and 2-methoxy-5-(3',4'-dimethoxyphenyl)cyclohepta-2,4,6-trien-1-one

R. W. Gable, M. F. Mackay, M. G. Banwell and J. N. Lambert



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Acta Cryst. (1990). C46, 1312-1314    [doi:10.1107/S0108270189010747]

Structure of 3,4-dihydro-3-methyl-1'-phenyl-3',4'-di-p-tolylspiro[naphthalene-2,5'-[2]pyrazoline]-1(2H)one

F. Theobald, N. Rodier, A. Kerbal, K. Tshiamala and B. Laude



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Acta Cryst. (1990). C46, 1314-1318    [doi:10.1107/S0108270189013934]

Chemotactic peptide analogs: conformation of N-formyl-L-methionyl-N2-methyl-L-phenylalanine tert-butyl ester

D. S. Eggleston



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Acta Cryst. (1990). C46, 1318-1324    [doi:10.1107/S0108270189009108]

Structures of two products of arynic condensation of ketone enolates

S. Ianelli, M. Nardelli, D. Belletti, P. Geoffroy, M. C. Carré, A. Mouaddib and P. Caubère


short format


metal-organic compounds



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Acta Cryst. (1990). C46, 1324-1326    [doi:10.1107/S0108270190002074]

Structure of pentacoordinated b-carbonyl-cd-(N-hydroxy-N-nitrosobenzenaminato-O,O')-ae-bis(triphenylphosphine)rhodium(I)

S. S. Basson, J. G. Leipoldt and J. A. Venter



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Acta Cryst. (1990). C46, 1326-1328    [doi:10.1107/S0108270190001093]

cis-Chloro(1-methylcytosine-N3)(N,N,N',N'-tetramethylethylenediamine)platinum(II) perchlorate hemihydrate, cis-[PtCl(C5H7N3O)(C6H16N2)\]ClO4.0.5H2O

H. Preut, G. Frommer and B. Lippert


organic compounds



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Acta Cryst. (1990). C46, 1329-1330    [doi:10.1107/S0108270190002062]

Structure of cyclo(-N-[epsilon]-Boc-L-Lys-L-Pro-)

D. S. Eggleston and K. D. Kopple



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Acta Cryst. (1990). C46, 1330-1332    [doi:10.1107/S0108270190002451]

Structures of two nitro-substituted aryl carbonates

J. A. King Jnr and G. L. Bryant Jnr



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Acta Cryst. (1990). C46, 1332-1334    [doi:10.1107/S010827019000186X]

Structure of [alpha]-truxillamide monohydrate

T. Iwamoto and S. Kashino



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Acta Cryst. (1990). C46, 1334-1336    [doi:10.1107/S0108270190001652]

Structure of verticine N-oxide hydrate

V. Kettmann, I. Masterová and J. Tomko



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Acta Cryst. (1990). C46, 1336-1338    [doi:10.1107/S0108270190001962]

Structure of (1R,5R)-1-p-menth-3-yloxy-2,4-dimethyl-cis-2,4,6,8-tetraazabicyclo[3.3.0]octane-3,7-dione

N. Modric, M. Poje, I. Vickovic and M. Bruvo



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Acta Cryst. (1990). C46, 1338-1340    [doi:10.1107/S0108270190002220]

Structure of 4-piperidone derivatives. II. 2,6-Bis(p-methoxyphenyl)-3,5-dimethyl-4-piperidone

K. Sekar, S. Parthasarathy and T. R. Radhakrishnan



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Acta Cryst. (1990). C46, 1340-1342    [doi:10.1107/S0108270190001810]

Structure of an oxazoylphenyloxazole

H. Beck, G. M. Sheldrick, J. Hege and W. Lüttke



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Acta Cryst. (1990). C46, 1342-1343    [doi:10.1107/S0108270190002542]

Structure of 2-pyridyl 4-nitrobenzoate

M. L. Glówka and I. Iwanicka



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Acta Cryst. (1990). C46, 1343-1344    [doi:10.1107/S0108270190002189]

Structure of p-chlorobenzenesulfonic acid monohydrate

T. Taga and T. Kobayashi



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Acta Cryst. (1990). C46, 1345-1347    [doi:10.1107/S0108270190000427]

Das pyrrolizidinalkaloid otosenin. Erneute kristallstrukturunterschung

H. Wiedenfeld, F. Knoch und E. Röder



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Acta Cryst. (1990). C46, 1347-1349    [doi:10.1107/S010827019000052X]

Structure of trans-13a,21b-dimethoxy-2,3,5,6,8,9,11,12,13a,21b-decahydro-phenanthro[9,10-b][1,4,7,10,13]pentaoxacyclopentadecene

H. Preut and H. G. Thomas



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Acta Cryst. (1990). C46, 1349-1351    [doi:10.1107/S0108270190002281]

Structure of 5-hydroxy-2-methyl-3-[1,2,3,4-tetrahydro-2-(1,4-dihydro-5-hydroxy-2-methyl-1,4-dioxo-3-naphthyl)-5-hydroxy-2-methyl-1,4-dioxo-3-naphthylmethyl]-1,4-naphthoquinone toluene solvate

P. J. Cox and R. A. Howie



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Acta Cryst. (1990). C46, 1351-1353    [doi:10.1107/S0108270190002104]

Structure of (±)-(1R*,4S*,6S*)-1-benzyloxy-4,8,11,11-tetramethyl-6-phenylthiobicyclo[5.3.1]undec-7-en-3-one

V. M. Lynch, T. Tanaka, J. R. Fishpaugh, S. F. Martin and B. E. Davis



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Acta Cryst. (1990). C46, 1353-1355    [doi:10.1107/S0108270190002116]

Structure of (±)-(1S*,3S*)-3-hydroxy-8,11,11-trimethyl-9-oxobicyclo[5.3.1]undec-7-en-1-yl benzoate

V. M. Lynch, J. R. Fishpaugh, S. F. Martin and B. E. Davis


short communications



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Acta Cryst. (1990). C46, 1356-1357    [doi:10.1107/S010827019000021X]

1:1 Molecular complex of acridine with 1,2,4,5-benzenetetracarbonitrile: refinement in space group P\overline{1}

R. E. Marsh



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Acta Cryst. (1990). C46, 1357-1358    [doi:10.1107/S0108270190001433]

Structure of 1,2,5,6-tetramethyltricyclo[3.1.0.02,6]hexane-3,4-dione

A. L. Spek and P. van der Sluis



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Acta Cryst. (1990). C46, 1358    [doi:10.1107/S0108270190005455]

Structure of bis[(-)-menthyl] acetylenedicarboxylate. Erratum

S. V. Evans, J. Trotter and V. C. Yee


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