Acta Crystallographica Section C

Crystal Structure Communications

Volume 46, Part 9 (September 1990)



research papers


inorganic compounds



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Acta Cryst. (1990). C46, 1579-1580    [doi:10.1107/S0108270189011236]

Structure of the heavy-fermion superconductor UBe13

M. W. McElfresh, J. H. Hall, R. R. Ryan, J. L. Smith and Z. Fisk



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Acta Cryst. (1990). C46, 1580-1584    [doi:10.1107/S0108270189013533]

Structure of nickel(II) perbromate hexahydrate at 296 K

J. C. Gallucci, R. E. Gerkin and W. J. Reppart



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Acta Cryst. (1990). C46, 1584-1587    [doi:10.1107/S0108270189013697]

Structure of the sodium ion conductor Na7Fe3(As2O7)4

C. Masquelier, F. d'Yvoire and N. Rodier



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Acta Cryst. (1990). C46, 1587-1590    [doi:10.1107/S0108270190000579]

Die Struktur der eindimensional fehlgeordneten Blei-Vanadiumbronze, [beta]-Pb0,333V2O5

K. Kato, K. Kosuda, T. Koga und H. Nagasawa



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Acta Cryst. (1990). C46, 1590-1592    [doi:10.1107/S0108270189014228]

Structure of K0.5V2O5

Y. Kanke, K. Kato, E. Takayama-Muromachi, M. Isobe and K. Kosuda



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Acta Cryst. (1990). C46, 1592-1596    [doi:10.1107/S0108270190000038]

Structure of nonasodium [alpha]-triniobatopentadecawolframatodiphosphate-acetonitrile-water (1/2/23), Na9[P2W15Nb3O62].2CH3CN.23H2O

R. G. Finke, D. K. Lyon, K. Nomiya and T. J. R. Weakley



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Acta Cryst. (1990). C46, 1596-1597    [doi:10.1107/S0108270190000075]

Structure of RbNaS

K. Hippler, R.-D. Hitzbleck, S. Sitta, P. Vogt, R. Wortmann and H. Sabrowsky



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Acta Cryst. (1990). C46, 1598-1599    [doi:10.1107/S0108270190000014]

Structure of 2H-TaS2

A. Meetsma, G. A. Wiegers, R. J. Haange and J. L. de Boer


metal-organic compounds



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Acta Cryst. (1990). C46, 1600-1603    [doi:10.1107/S0108270189011728]

Structure of a thiolate-bridged polymeric copper(I) compound, catena-(2,9-dimethyl-1,10-phenanthroline)-[mu]-(thiophenolato)-copper(I)

O. P. Anderson, K. K. Brito and S. K. Laird



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Acta Cryst. (1990). C46, 1603-1609    [doi:10.1107/S0108270189012680]

Structures of four- and five-carbon alkyldiammonium tetrachlorocuprate(II) and tetrabromocuprate(II) salts

J. K. Garland, K. Emerson and M. R. Pressprich



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Acta Cryst. (1990). C46, 1609-1612    [doi:10.1107/S0108270189013569]

Structure and conductivity of di[3,4;3'4'-bis(ethylenedithio)-2,2',5,5'-tetrathiafulvalenium] tetrabromomercurate(II)-1,1,2-trichloroethane, (BEDT-TTF)2HgBr4.TCE

X. Bu, P. Coppens and M. J. Naughton



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Acta Cryst. (1990). C46, 1612-1617    [doi:10.1107/S0108270189013624]

Structure and molecular mechanics of ferrirhodin

K. Fidelis, M. B. Hossain, M. A. F. Jalal and D. van der Helm



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Acta Cryst. (1990). C46, 1618-1621    [doi:10.1107/S0108270189013545]

Structure of tris(tetrabutylammonium) hexaisothiocyanatoerbate(III)

L. C. Thompson and L. J. Radonovich



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Acta Cryst. (1990). C46, 1621-1622    [doi:10.1107/S0108270189006086]

Structure of thallium hydrogen phthalate

R. D. Fulton, R. R. Ryan and J. H. Hall



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Acta Cryst. (1990). C46, 1623-1624    [doi:10.1107/S0108270189013776]

Structure of trans-tetrachlorobis(dimethylphenylphosphine)technetium(IV)

F. A. Cotton, C. S. Day, M. P. Diebold and W. J. Roth



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Acta Cryst. (1990). C46, 1624-1627    [doi:10.1107/S0108270189013764]

Structures of two niobium(IV) complexes: [N(C2H5)4]2[NbCl6] and [P(CH3)2(C6H5)H][NbCl5{P(CH3)2(C6H5)\]

F. A. Cotton, M. P. Diebold and W. J. Roth



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Acta Cryst. (1990). C46, 1627-1631    [doi:10.1107/S0108270189013673]

Structures of three bis(3-ethoxy-N-R-salicylideneaminato)nickel(II) complexes (R = H, methyl, ethyl)

B. Kamenar, B. Kaitner, A. Stefanovic and T. N. Waters



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Acta Cryst. (1990). C46, 1631-1633    [doi:10.1107/S0108270189013272]

Structure of bis(dimethylphenylphosphine)(meso-5,10,15,20-tetraphenylporphinato)iron(III) perchlorate

L. Toupet, P. Sodano and G. Simonneaux



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Acta Cryst. (1990). C46, 1633-1635    [doi:10.1107/S0108270189013909]

Diethoxybis(4,4,4-trifluoro-1-phenyl-1,3-butanedionato)titanium(IV)

J. L. Wang, F. M. Miao, X. J. Fan, X. Feng and J. T. Wang



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Acta Cryst. (1990). C46, 1635-1637    [doi:10.1107/S0108270189013752]

Bis(1H+-pyrazinium N4-oxide) dichromate

M. R. Pressprich, R. D. Willett, R. M. Sheets, W. W. Paudler and G. L. Gard



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Acta Cryst. (1990). C46, 1638-1640    [doi:10.1107/S010827018901379X]

Structure of Zn(cyclam)(ClO4)2

T. A. Tyson, K. O. Hodgson, B. Hedman and G. R. Clark



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Acta Cryst. (1990). C46, 1640-1642    [doi:10.1107/S0108270190000129]

Structure of sodium (trimethylenediaminetetraacetato)ferrate(III) trihydrate

K.-I. Okamoto, K. Kanamori and J. Hidaka



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Acta Cryst. (1990). C46, 1642-1645    [doi:10.1107/S0108270189014368]

Structure of [2,6-bis(2-benzimidazolyl)pyridine]dichlorocopper(II) dimethylformamide

G. Bernardinelli, G. Hopfgartner and A. F. Williams



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Acta Cryst. (1990). C46, 1645-1647    [doi:10.1107/S0108270189014186]

Synthesis and structure of cytosine cobalt dichloride

D. Tran Qui and M. Bagieu



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Acta Cryst. (1990). C46, 1648-1650    [doi:10.1107/S0108270189013995]

Structure of cis-diacetylidobis(triethylphosphine)platinum(II)

J. R. Phillips, G. A. Miller and W. C. Trogler



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Acta Cryst. (1990). C46, 1650-1652    [doi:10.1107/S0108270190000580]

Structure of bis[(4,5-[eta])-3,3,6,6-tetramethyl-1-thiacyclohept-4-yne]-bis([mu]-thiophenolato)-dicopper(I)

F. Olbrich, J. Kopf, E. Weiss, A. Krebs and S. Müller



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Acta Cryst. (1990). C46, 1652-1655    [doi:10.1107/S0108270190000555]

Structure of the organic superconductor (DMET)2AuCl2

Y. Ishikawa, K. Saito, K. Kikuchi, I. Ikemoto, K. Kobayashi and H. Anzai


organic compounds



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Acta Cryst. (1990). C46, 1655-1657    [doi:10.1107/S0108270189006542]

Structure of 6-chloro-10-oxabicyclo[5.2.1]decane-2,3-diol

M. L. Rodríguez, C. Ruiz-Pérez, L. Dorta, J. D. Martín, E. Alvarez, E. Manta and D. Zurita



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Acta Cryst. (1990). C46, 1657-1659    [doi:10.1107/S0108270189009443]

Structures of substituted olefins. I. (Z)-2-Nitro-1,2-diphenylvinyl thiocyanate

K. P. Park and J. H. Jeong



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Acta Cryst. (1990). C46, 1659-1661    [doi:10.1107/S0108270190000105]

Structures of substituted olefins. II. 4-(2-Nitro-1,2-diphenylvinyl)morpholine

K. P. Park and J. H. Jeong



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Acta Cryst. (1990). C46, 1661-1663    [doi:10.1107/S0108270189011509]

Ethyl 7-hydroxy-4-coumarinacetate

K. Subramanian, K. Sivakumar, S. Natarajan and S. Parthasarathy



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Acta Cryst. (1990). C46, 1663-1665    [doi:10.1107/S0108270189011522]

7-Hydroxy-4-coumarinacetic acid monohydrate

K. Sivakumar, F. Jesurethinam, K. Subramanian and S. Natarajan



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Acta Cryst. (1990). C46, 1665-1668    [doi:10.1107/S0108270189013454]

Trihydrate structure of a multisubstrate inhibitor of L-DOPA decarboxylase

J. M. Gulbis, M. F. Mackay, M. M. Iles, M. N. Iskander and P. R. Andrews



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Acta Cryst. (1990). C46, 1668-1671    [doi:10.1107/S0108270189013557]

Structure of a photodimer of 3-acetoxy-2-inden-1-one: 9,10-dioxoindano[2,'3':4,3]cyclobuta[1,2-b]indan-4b,4c-diyl diacetate

N. Ramasubbu, K. K. Bhandary, B. S. Joshi, Q. Jiang and S. W. Pelletier



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Acta Cryst. (1990). C46, 1671-1674    [doi:10.1107/S0108270189011868]

Structure of tetramethyl reductic acid (TMRA, 4,4,5,5-tetramethyl-2,3-dihydroxy-2-cyclopenten-1-one), a reductate ligand involved in dioxygen activation by multinuclear iron complexes

X. Feng, S. G. Bott and S. J. Lippard



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Acta Cryst. (1990). C46, 1674-1676    [doi:10.1107/S010827018901187X]

Structure of a 5,6-lactone

V. Geetha and S. S. Rajan



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Acta Cryst. (1990). C46, 1676-1678    [doi:10.1107/S0108270189012412]

Structure of fluorescein dipropionate acetone solvate

L.-F. Wang, X. Wang, Z. Peng, F. He and Q. Wang



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Acta Cryst. (1990). C46, 1679-1681    [doi:10.1107/S0108270189011923]

Structure of N-methyl-D-aspartic acid monohydrate

W. Sawka-Dobrowolska, T. Glowiak, H. Kozlowski and P. Masterlerz



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Acta Cryst. (1990). C46, 1682-1686    [doi:10.1107/S0108270189011789]

2-Benzoylbenzoic acid: structures and hydrogen-bonding patterns of the anhydrous and hydrated forms

R. A. Lalancette, P. A. Vanderhoff and H. W. Thompson



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Acta Cryst. (1990). C46, 1686-1691    [doi:10.1107/S0108270189012400]

6[alpha]- and 6[beta]-Trifluoromethyl-substituted androstenedione

D. S. Eggleston and H. Y. Lan-Hargest



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Acta Cryst. (1990). C46, 1691-1693    [doi:10.1107/S0108270189011935]

Structure of 2-[1-(2-thienyl)ethylideneamino]phenol

W. Sawka-Dobrowolska, Z. Siatecki and J. M. Sobczak



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Acta Cryst. (1990). C46, 1693-1697    [doi:10.1107/S0108270189013910]

Structures of 5-dimethylamino-1-[N-(2,6-dimethylphenyl)benzimidoyl]tetrazole, C18H20N6, and 7,9-dimethyl-5-dimethylamino-2-phenyl-3H-1,3,4-benzotriazepine, C18H20N4

P. F. Lindley, G. V. Boyd and G. A. Nicolaou



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Acta Cryst. (1990). C46, 1697-1700    [doi:10.1107/S0108270189012205]

Structure of ethyl 5-ethoxy-3-phenyl-2-indolecarboxylate

T. N. Chandrakantha, Puttaraja and V. Pattabhi



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Acta Cryst. (1990). C46, 1700-1704    [doi:10.1107/S010827019000018X]

Structure of 5[beta]-dihydrotestosterone

A. W. Roszak and P. W. Codding



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Acta Cryst. (1990). C46, 1704-1707    [doi:10.1107/S0108270189013648]

Structure of delvestine: a norditerpenoid alkaloid from Delphinium vestitum Wall

K. K. Bhandary, N. Ramasubbu, B. S. Joshi, H. K. Desai and S. W. Pelletier



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Acta Cryst. (1990). C46, 1707-1709    [doi:10.1107/S0108270190000452]

Structure of 2-tert-butyl-3-phenyl-2-cyclopropenecarboxylic acid

J. Kopf, G. Starova, V. Plotkin and I. Domnin



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Acta Cryst. (1990). C46, 1709-1711    [doi:10.1107/S0108270189012540]

Structure of 2,4,N-trinitroanilinoacetic acid

K. Vedasankari, G. S. Murthy and M. R. Udupa



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Acta Cryst. (1990). C46, 1712-1715    [doi:10.1107/S0108270190000221]

Structure of 2',6'-dihydroxy-4,4'-dimethoxychalcone

H. W. Schmalle, G. Adiwidjaja, O. H. Jarchow, B. M. Hausen and E. Wollenweber



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Acta Cryst. (1990). C46, 1715-1718    [doi:10.1107/S0108270189014319]

Structure of 2-methoxy-6-nonyl-1,4-benzoquinone, C16H24O3, a synthetic contact allergen related to the naturally occurring primin

G. Ulrich, K. H. Klaska, O. H. Jarchow, H. W. Schmalle, W. A. König, H. Heitsch, R. Rathmann, B. M. Hausen and K.-H. Schulz



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Acta Cryst. (1990). C46, 1718-1720    [doi:10.1107/S010827018901348X]

Structure of 4-(D-galacto-pentaacetoxypentyl)-1-phenylpyrazole

M. J. Diánez and A. López-Castro



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Acta Cryst. (1990). C46, 1720-1723    [doi:10.1107/S0108270189014381]

1-Ethynyl-2,7-dimethoxynaphthalene: an example of hydrogen bonding between an ethynylic hydrogen and a methoxyl oxygen

P. Prince, F. R. Fronczek and R. D. Gandour



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Acta Cryst. (1990). C46, 1723-1725    [doi:10.1107/S0108270190000658]

Structure of N-methylnicotinamide

T. Srikrishnan and R. Parthasarathy



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Acta Cryst. (1990). C46, 1725-1727    [doi:10.1107/S0108270190000543]

Structure of xanthone

S. Onuma, K. Iijima and I. Oonishi



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Acta Cryst. (1990). C46, 1727-1730    [doi:10.1107/S010827019000049X]

Structure of 2,4,4,6-tetraphenyl-4H-pyran

J. Vojtechovský and J. Hasek



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Acta Cryst. (1990). C46, 1730-1732    [doi:10.1107/S0108270190001019]

Structure of a nucleoside analogue, 3'-deoxy-3'-fluorothymidine

D. H. Everaert, O. M. Peeters, N. M. Blaton and C. J. De Ranter


short format


metal-organic compounds



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Acta Cryst. (1990). C46, 1733-1735    [doi:10.1107/S0108270190003377]

Structure du chloro(diméthylsulfoxyde)[oxo-5 prolinato(2-)-O,N]platinate(II) de potassium oxo-5 proline monohydrate

B. Viossat, A. Michelet, P. Khodadad et N. Rodier



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Acta Cryst. (1990). C46, 1735-1737    [doi:10.1107/S0108270189014009]

Structure of chloro[(1,2,3,4,5-[eta])-cyclooctadienyl]hydridobis(triphenylphosphine)rhenium acetone solvate

P. Charpin, M. Nierlich, D. Vigner, M. Lance and M. Ephritikhine



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Acta Cryst. (1990). C46, 1737-1739    [doi:10.1107/S0108270190002773]

Structure of (histamine.2H+)(ZnCl4)

L. B. Cole and E. M. Holt



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Acta Cryst. (1990). C46, 1739-1741    [doi:10.1107/S0108270190004012]

Structure of diaqua[1,6-bis(2-benzimidazolyl)-2,5-dithiahexane]nickel(II) diperchlorate monohydrate

A. Castiñeiras, R. Carballo, W. Hiller and J. Strähle



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Acta Cryst. (1990). C46, 1741-1743    [doi:10.1107/S0108270190004188]

Structure of bis(1,1,1,5,5,5-hexafluoro-2,4-pentanedionato)(2,5,8,11,14-pentaoxapentadecane)barium(II)

P. van der Sluis, A. L. Spek, K. Timmer and H. A. Meinema



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Acta Cryst. (1990). C46, 1743-1745    [doi:10.1107/S0108270190003158]

Structure of bromo(4-iodo-1,2,3,4-tetraphenyl-1,3-butadienyl)diphenyltin(IV)

C. R. A. Muchmore and M. J. Heeg



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Acta Cryst. (1990). C46, 1745-1747    [doi:10.1107/S0108270190004346]

Structure of (3,5,7,13,15,17-hexaethyl-2,8,12,18-tetramethylporphinato)copper(II)

T. Nagata, A. Osuka, K. Maruyama and K. Toriumi


organic compounds



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Acta Cryst. (1990). C46, 1747-1749    [doi:10.1107/S0108270190003444]

N-(Diméthyl-4,6 pyridyl-2) phényl-3 propènamide-(E) hydrate (2/1)

N. Rodier, S. Robert-Piessard et G. Le Baut



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Acta Cryst. (1990). C46, 1749-1751    [doi:10.1107/S0108270190004061]

Structure of a thiadiazole

K. Yamaguchi, A. Ohsawa and C. Kawabata



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Acta Cryst. (1990). C46, 1751-1752    [doi:10.1107/S0108270190004073]

Structure of a pyrazine derivative

K. Yamaguchi, A. Ohsawa and C. Kawabata


short communications



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Acta Cryst. (1990). C46, 1752    [doi:10.1107/S0108270190007648]

Crystal studies of musk compounds. I. 4-tert-Butyl-3-methoxy-2,6-dinitrotoluene (musk ambrette). Erratum

D. J. A. De Ridder, K. Goubitz and H. Schenk


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