Acta Crystallographica Section C

Crystal Structure Communications

Volume 47, Part 3 (March 1991)



research papers


inorganic compounds



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Acta Cryst. (1991). C47, 473-477    [doi:10.1107/S0108270190008575]

Structures of CdSrP2O7 and CdBaP2O7

A. Alaoui El Belghiti, A. Boukhari and E. M. Holt



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Acta Cryst. (1991). C47, 477-479    [doi:10.1107/S0108270190008368]

Structure de LaH(PO3H)2.3H2O

M. Loukili, J. Durand, A. Larbot, L. Cot and M. Rafiq



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Acta Cryst. (1991). C47, 479-483    [doi:10.1107/S0108270190009866]

Structure refinement of monoclinic 12-layer TaNi3 with [beta]-NbPt3 type. New crystallographic descriptions of this type and of the Nb3Rh5 type based on smaller unit cells

J. T. Zhao, L. Gelato and E. Parthé



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Acta Cryst. (1991). C47, 483-486    [doi:10.1107/S0108270190009398]

Structure determination of Ba(OD)Br.2D2O by neutron powder diffraction

T. Kellersohn, K. Beckenkamp, H. D. Lutz and E. Jansen



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Acta Cryst. (1991). C47, 486-489    [doi:10.1107/S0108270190009593]

Structure of trisilylphosphine, P(SiH3)3, at 100 K

A. J. Blake, E. A. V. Ebsworth and S. G. D. Henderson



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Acta Cryst. (1991). C47, 489-492    [doi:10.1107/S0108270190008964]

Structure of photoluminescent polyoxomolybdoeuropate (NH4)12H2[Eu4(MoO4)(H2O)16(Mo7O24)4].13H2O

H. Naruke, T. Ozeki and T. Yamase



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Acta Cryst. (1991). C47, 492-495    [doi:10.1107/S0108270190009623]

Diiodinated derivatives of 1,2-diarsenadecaborane: As2B10H8I2

D. O'Connell, T. R. Spalding and G. Ferguson



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Acta Cryst. (1991). C47, 495-498    [doi:10.1107/S010827019000974X]

Structure of sodium [beta]''-gallate

Y. Michiue, M. Watanabe and Y. Fujiki



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Acta Cryst. (1991). C47, 498-501    [doi:10.1107/S0108270190009532]

Orientational disorder of the nitrite anion in the sodalite Na8[AlSiO4]6(NO2)2

P. Sieger, M. Wiebcke, J. Felsche and J.-C. Buhl



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Acta Cryst. (1991). C47, 501-503    [doi:10.1107/S0108270190009428]

Structure of K3Na[Re2O3(CN)8].2H2O

P. O. Lumme, U. Turpeinen and Z. Stasicka


metal-organic compounds



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Acta Cryst. (1991). C47, 504-507    [doi:10.1107/S0108270190009386]

Structure of cis-diacetonitrile[ferrocenylbis(diphenylphosphine)]rhodium(I) perchlorate acetonitrile solvate

Hong Wang, R. J. Barton and B. E. Robertson



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Acta Cryst. (1991). C47, 507-510    [doi:10.1107/S0108270190008939]

Comparison of two hydrated forms of sodium inosine 5'-monophosphate

M. Sriram, Y.-C. Liaw, Y.-G. Gao and A. H.-J. Wang



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Acta Cryst. (1991). C47, 510-513    [doi:10.1107/S0108270190009192]

Structure of bis(di-2-pyridylamine)copper(I) chloride

G. J. Pyrka, R. J. Seeney and A. A. Pinkerton



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Acta Cryst. (1991). C47, 513-516    [doi:10.1107/S0108270190009714]

Structure of [PhCH2NMe3]2[(B10H12)2Pd] acetonitrile solvate

S. A. Macgregor, J. A. Scanlan, L. J. Yellowlees and A. J. Welch



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Acta Cryst. (1991). C47, 516-519    [doi:10.1107/S0108270190009659]

Structure of di-[mu]-bromo-(tetrabromo-1[kappa]4Br)bis(N,N-dimethylselenourea-2[kappa]2Se)ditellurium(II,IV)-acetonitrile-methanol (2/3/1)

H. M. K. K. Pathirana, J. H. Reibenspies, E. A. Meyers and R. A. Zingaro



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Acta Cryst. (1991). C47, 519-522    [doi:10.1107/S010827019000960X]

Structure of bis(2,2'-bipyridine)dichlororhodium(III) chloride dihydrate

P. Lahuerta, J. Latorre, R. Martínez-Máñez, S. García-Granda and F. Gómez-Beltrán



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Acta Cryst. (1991). C47, 522-525    [doi:10.1107/S0108270190008459]

Structures of [1,3-bis(diphenylphosphino)propane]tetracarbonylmolybdenum(0) (1) and [1,4-bis(diphenylphosphino)butane]tetracarbonylmolybdenum(0) (2)

C.-H. Ueng and G.-Y. Hwang



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Acta Cryst. (1991). C47, 525-528    [doi:10.1107/S0108270190009283]

Structures of (2-cyanoethyl)(3-cyanopyridine)bis[dimethylglyoximato(1-)]cobalt(III) monohydrate (I) and (4-aminopyridine)(2-cyanoethyl)bis[dimethylglyoximato(1-)]cobalt(III) (II)

A. Sekine, Y. Ohashi and K. Hori



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Acta Cryst. (1991). C47, 528-531    [doi:10.1107/S0108270190009271]

Structure of zinc(II) (RS)-1-isopropyl citrate tetrahydrate

S. Tsuji, T. Shibata, Y. Ito, S. Fujii and K. Tomita



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Acta Cryst. (1991). C47, 531-533    [doi:10.1107/S0108270190009581]

Structures of two Zn2+ complexes with two tetraaza macrocyclic tetraacetates

A. Riesen, M. Zehnder and T. A. Kaden



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Acta Cryst. (1991). C47, 533-536    [doi:10.1107/S0108270190009908]

Structure of a monocyclopentadienyl niobium(III) phosphine adduct

A. Zaki, L. G. Hubert-Pfalzgraf and L. Toupet



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Acta Cryst. (1991). C47, 536-539    [doi:10.1107/S0108270190009635]

Tricarbonyl[(1,2,3,4-[eta])-2,3-dimethylbutadiene]cobalt acetonitriletrichloroferrate(1-)

S. A. Macgregor, L. J. Yellowlees and A. J. Welch



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Acta Cryst. (1991). C47, 539-541    [doi:10.1107/S0108270190009507]

Structure of bis(1,5-cyclooctadiene)rhodium(I) hexacarbonyl-tri-[mu]-chloro-dirhenate(I)

N. C. Baenziger, E. A. Mottel and J. R. Doyle



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Acta Cryst. (1991). C47, 541-544    [doi:10.1107/S0108270190009337]

Simple oxygen bridged TiIV dimer: structure of [Ti([mu]-O)(OC6H3-2,6Pri2)2(NC5H4-4NC4H8)]2

J. E. Hill, P. E. Fanwick and I. P. Rothwell



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Acta Cryst. (1991). C47, 544-547    [doi:10.1107/S0108270190009611]

Structure of [[mu]-hexamethylenebis(diphenylphosphine)-P,P']bis[di-[mu]-carbonyl-nonacarbonyl-triangulo-triiron(3 Fe-Fe)] {[Fe3(CO)11]Ph2P(CH2)3}2

G. Ferguson, R. Hourihane and T. R. Spalding



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Acta Cryst. (1991). C47, 547-550    [doi:10.1107/S0108270190009465]

Structure of imidazolium hexachlorotantalate(V)

G. Levasseur and A. L. Beauchamp


organic compounds



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Acta Cryst. (1991). C47, 550-553    [doi:10.1107/S0108270190006394]

Structures of the tetrafluoroborate salts of triphenylcarbenium ions with one and with two 4-methoxy substituents: stable carbocations

C. Bleasdale, W. Clegg, S. B. Ellwood and B. T. Golding



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Acta Cryst. (1991). C47, 553-555    [doi:10.1107/S0108270190005686]

2,6-Dimethoxy-3-nitrobenzoic acid. A hydrogen-bonded chain structure

G. M. Frankenbach, D. Britton and M. C. Etter



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Acta Cryst. (1991). C47, 556-561    [doi:10.1107/S0108270190006242]

Structures of N-acetylbenzamide, N-propionylbenzamide and N-butyrylbenzamide and analysis of imide hydrogen-bond patterns

M. C. Etter, D. Britton and S. M. Reutzel



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Acta Cryst. (1991). C47, 561-563    [doi:10.1107/S0108270190005078]

1,2,3,3,8-Pentamethyl-5-trifluoromethyl-2,3-dihydro-1H-pyrrolo[2,3-g]quinolin-7(8H)-one

K. Chinnakali, K. Sivakumar, S. Natarajan, N. K. McGuire and A. Clearfield



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Acta Cryst. (1991). C47, 563-566    [doi:10.1107/S0108270190006175]

Structure of an unusually non-polar hydroxy ether

M. M. Olmstead, M. E. Price, J. Strutzel and N. E. Schore



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Acta Cryst. (1991). C47, 566-569    [doi:10.1107/S0108270190006540]

Structures of two isomeric dihydropyridine derivatives with S substituents: solid-state allyl migration

T. P. E. Auf der Heyde, H.-B. Bürgi and V. E. Shklover



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Acta Cryst. (1991). C47, 570-573    [doi:10.1107/S0108270190005868]

Structure of bis[{3-[(4-acetyl-2-propoxymethyl)phenoxy]-2-hydroxypropyl}(isopropyl)ammonium] fumarate

V. Kettmann, J. Dillinger and R. Cizmáriková



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Acta Cryst. (1991). C47, 573-577    [doi:10.1107/S0108270190005133]

Lattice inclusion compounds of gossypol. Structure of the 2:3 gossypol-benzaldehyde coordinatoclathrate

M. Gdaniec, B. T. Ibragimov and S. A. Talipov



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Acta Cryst. (1991). C47, 577-580    [doi:10.1107/S0108270190006576]

Structure and conformation of the 1:1 molecular complex sulfaproxyline-caffeine

M. Ghosh, A. K. Basak, S. K. Mazumdar and B. Sheldrick



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Acta Cryst. (1991). C47, 580-584    [doi:10.1107/S0108270190005418]

Structure of an adenine tetrafluoroborate salt

A. C. M. Young, J. C. Dewan and A. J. Edwards



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Acta Cryst. (1991). C47, 584-587    [doi:10.1107/S0108270190007016]

Pyramidalization in a hexachloronorbornadiene derivative

W. H. Watson, R. P. Kashyap and B. F. Plummer



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Acta Cryst. (1991). C47, 587-590    [doi:10.1107/S0108270190006850]

Strained heterocyclic systems. 18. Structure of 1,2,3-methylidyne-2,3-dihydro-1H-cyclopenta[b]quinoxaline

K. M. Gigstad, J. S. Ricci Jnr, J. H. Markgraf, M. Christl and A. Kraft



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Acta Cryst. (1991). C47, 590-592    [doi:10.1107/S0108270190006655]

Structure of 2-phenyl-1,2,3-triazolo[4,5-e][1,2,3,4]tetrazine at 153 K

K. Yamaguchi, T. Kaihoh, T. Itoh and A. Ohsawa



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Acta Cryst. (1991). C47, 592-594    [doi:10.1107/S010827019000676X]

Structure of 3-acetoxyindole

D. K. Chakraborty, A. Mukhopadhyay and S. K. Talapatra



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Acta Cryst. (1991). C47, 594-596    [doi:10.1107/S0108270190006783]

Structure of (+)-[S-(E)]-N-([alpha]-methylbenzylidene)-p-toluenesulfinamide

P. D. Robinson, D. H. Hua, J. S. Chen and S. Saha



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Acta Cryst. (1991). C47, 596-599    [doi:10.1107/S010827019000717X]

Structure of a charge-transfer complex, dithieno[3,4-b:3',4'-d]thiophene-tetracyanoquinodimethane (DTT1-TCNQ)

M. Catellani and W. Porzio



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Acta Cryst. (1991). C47, 599-602    [doi:10.1107/S0108270190006023]

Azoles. 29. Structure of the molecular complex of 3,5-dinitroindazole with piperazine and water (2/1/2)

A. Gzella and U. Wrzeciono



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Acta Cryst. (1991). C47, 602-604    [doi:10.1107/S0108270190007545]

Structure du chlorhydrate de (diméthylamino méthyl)-2 acrylophénone

C. Follet-Houttemane, J. P. Wignacourt, J. C. Boivin, I. Lesieur et D. Lesieur



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Acta Cryst. (1991). C47, 604-606    [doi:10.1107/S0108270190007235]

Structural studies of mitomycins. V. Structure of mitomycin H

N. Hirayama



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Acta Cryst. (1991). C47, 606-608    [doi:10.1107/S0108270190007569]

X-ray structure of the pyrethroid insecticide {1R-[1[alpha](S*),2[alpha]]}-2-(2,2-dichlorovinyl)-3,3-dimethylcyclopropanecarboxylic acid cyano(3-phenoxyphenyl)methyl ester (RU 24501)

F. Baert and A. Guelzim



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Acta Cryst. (1991). C47, 608-611    [doi:10.1107/S0108270190006990]

Structure of 5-methoxy-3-(1-methylethoxy)-1-phenyl-N-(1H-tetrazol-5-yl)-1H-indole-2-carboxamide-diethylamine, a potential anti-allergy agent

M. Parvez, P. C. Unangst, D. T. Connor and M. D. Mullican



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Acta Cryst. (1991). C47, 611-613    [doi:10.1107/S0108270190007004]

Structure of 3-(1-methylethoxy)-7-phenyl-N-(1H-tetrazol-5-yl)-2-benzofurancarboxamide, a potential anti-allergy agent

M. Parvez, P. C. Unangst, D. T. Connor and M. D. Mullican



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Acta Cryst. (1991). C47, 613-616    [doi:10.1107/S010827019000796X]

Structure and absolute configuration of an antihistaminic drug, clemastine hydrogen fumarate

M. Parvez and M. A. Wendling



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Acta Cryst. (1991). C47, 616-618    [doi:10.1107/S0108270190007909]

Structures of 2-chloro-4-cyclohexylamino-6-methoxy-1,3,5-triazine and 2-chloro-4-methoxy-6-piperidino-1,3,5-triazine

M. L. Glówka and I. Iwanicka



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Acta Cryst. (1991). C47, 618-620    [doi:10.1107/S0108270190007922]

Structure of the 4-oxo-2-butenoic acid alkyl ester moiety. II. Structure of dimethyl 4,4'-(methylhydrazo)bis(4-oxo-2-butenoate)

M. L. Glówka, I. Iwanicka and L. Najman



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Acta Cryst. (1991). C47, 620-623    [doi:10.1107/S0108270190007739]

Structure of 8-chloro-6-(2-chlorophenyl)-2H,4H-[1,2,3]triazolo[5,4-d][2]benzazepinium methanesulfonate methanol solvate

H. J. Kemmish and T. A. Hamor



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Acta Cryst. (1991). C47, 623-626    [doi:10.1107/S0108270190007296]

Structure of a photoresponsive crown ether, 21-(4'-methoxyphenylazo)-1,4,7,14,23-pentaoxa[7.2.2]orthometaorthobenzenophane

H. L. Ammon and S. Shinkai



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Acta Cryst. (1991). C47, 627-629    [doi:10.1107/S0108270190007387]

Strained chlorocarbons. Structure of perchlorotoluene, the simplest perchloroarylalkane

J. Rius, C. Miravitlles, J. Castañer and J. Riera



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Acta Cryst. (1991). C47, 629-632    [doi:10.1107/S0108270190007399]

Structure and NMR spectra of N-[2-([alpha]-hydrazonobenzyl)-3-benzofuranyl]-p-toluenesulfonamide

F. Bachechi, V. M. Coiro, M. Delfini and G. Settimj



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Acta Cryst. (1991). C47, 632-634    [doi:10.1107/S0108270190008241]

Structure of 4'-butyl-2,3,5,6-tetrafluorobiphenyl-4-carbonitrile

L. D. Field, T. W. Hambley and G. K. Pierens



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Acta Cryst. (1991). C47, 634-636    [doi:10.1107/S0108270190007661]

Structure of (E)-1,2-dimesitylvinylene bis(mesitylenecarboxylate)

M. L. C. E. Kouwijzer, B. P. van Eijck and W. J. Muizebelt


short format


inorganic compounds



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Acta Cryst. (1991). C47, 637-638    [doi:10.1107/S0108270190009763]

Structure of triammonium hexahydrogenhexamolybdorhodate(III) hexahydrate

Y. Ozawa, Y. Hayashi and K. Isobe



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Acta Cryst. (1991). C47, 638-640    [doi:10.1107/S0108270190009039]

Structure of caesium selenate

F. J. Zúñiga, T. Breczewski and A. Arnaiz


metal-organic compounds



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Acta Cryst. (1991). C47, 640-641    [doi:10.1107/S0108270190009404]

Structure of di-[mu]-chloro-bis[dicarbonylrhodium(I)]

L. Walz and P. Scheer



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Acta Cryst. (1991). C47, 642-643    [doi:10.1107/S0108270190009313]

Barium D-glucose 6-phosphate heptahydrate: new diffractometer data

T. Lis



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Acta Cryst. (1991). C47, 643-645    [doi:10.1107/S0108270190009556]

Structure of ([mu]-sulfur dioxide)bis(dicarbonylcyclopentadienyliron) hydrate

A. W. Cordes, E. F. Askew, D. R. Tyler and T. W. Koenig



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Acta Cryst. (1991). C47, 645-648    [doi:10.1107/S0108270190009970]

Structures of two bis(ethylenedithio)tetrathiafulvalene hexamolybdate and hexatungstate salts: (BEDT-TTF)2M6O19, M = Mo, W

S. Triki, L. Ouahab, D. Grandjean and J. M. Fabre



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Acta Cryst. (1991). C47, 648-650    [doi:10.1107/S0108270190009684]

[(C5Me5)(Et2NCS2)Rh([mu]-Ph2PCH2CH2PPh2)Rh(Et2NCS2)(C5Me5)]2+.2BPh4-

A. J. Blake, J. D. Fotheringham, T. A. Stephenson, S. G. Hambling and L. Sawyer



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Acta Cryst. (1991). C47, 650-651    [doi:10.1107/S0108270190009441]

A vanadyl complex of a tetradentate ligand featuring a cis-N2S2 donor ligand set

D. Farchione, A. G. Wedd and E. R. T. Tiekink



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Acta Cryst. (1991). C47, 651-654    [doi:10.1107/S0108270190009544]

Structure of di[(carbonyl)(chloro)(1,4,7-triazacyclononane)(triphenylphosphine)osmium(II)] tetrachlorozincate(II)

P. D. Robinson, I. A. Ali and C. C. Hinckley



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Acta Cryst. (1991). C47, 654-655    [doi:10.1107/S0108270190009374]

Structure of dibromobis(triphenylarsine oxide)nickel(II), NiBr2(Ph3AsO)2

E. E. Castellano, G. Oliva and J. Zukerman-Schpector



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Acta Cryst. (1991). C47, 655-657    [doi:10.1107/S010827019000988X]

Structure of a bis{[(2,3-[eta],[kappa]P')-1,2-diphospha-2-propene]nickel

M. Nieger, G. Bruder and R. Appel



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Acta Cryst. (1991). C47, 657-659    [doi:10.1107/S0108270190009350]

Vaska's compound - dichloromethane solvate (1/2)

A. J. Blake, E. A. V. Ebsworth, H. M. Murdoch and L. J. Yellowlees



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Acta Cryst. (1991). C47, 659-661    [doi:10.1107/S0108270190009477]

The structure of a complex containing a chelating S32- ligand: [(C5Me5)2TiS3]

A. Shaver, J. M. McCall, P. H. Bird and U. Siriwardane



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Acta Cryst. (1991). C47, 661-662    [doi:10.1107/S0108270190009787]

A dimeric stannoxane structure: [Sn2(Cl)(O)(OH)(C6H5)4]2.2C3H7NO

E. R. T. Tiekink


organic compounds



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Acta Cryst. (1991). C47, 662-664    [doi:10.1107/S0108270190009143]

Structure of 1,4,5,8,9,10-hexabromo-11,11-dimethoxytricyclo[6.2.1.02,7]undeca-4,9-diene-3,6-dione

C. L. Picou, S. R. Homer, R. A. Breyer, L. W. Reichel, G. W. Griffin and E. D. Stevens



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Acta Cryst. (1991). C47, 664-666    [doi:10.1107/S0108270190008253]

Structure of 7-methoxy-5H-dibenz[c,e]azepine

H. Preut, R. Röhrkasten and R. P. Kreher



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Acta Cryst. (1991). C47, 666-668    [doi:10.1107/S0108270190008599]

Synthesis of a 2-oxabrendane derivative via reaction of endo-5-acetyl-7,7-dimethoxynorborn-2-ene with N-bromosuccinimide

W. H. Watson, R. P. Kashyap, A. P. Marchand and V. Vidyasagar



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Acta Cryst. (1991). C47, 668-670    [doi:10.1107/S0108270190009027]

Structure of ethyl 4-oxo-1,2,3,4-tetrahydrocinnoline-2-acetate

M. L. Glówka, I. Iwanicka and A. Stanczak



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Acta Cryst. (1991). C47, 670-672    [doi:10.1107/S0108270190009842]

Structure of 10,11-dihydro-5,10-ethano-5H-dibenzo[a,d]cycloheptan-11-one

K. A. Abboud, S. H. Simonsen, C. S. Tyllick and R. M. Roberts



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Acta Cryst. (1991). C47, 672-674    [doi:10.1107/S0108270190009921]

Structure of 10,11-dihydro-5,10-ethano-5H-dibenzo[a,d]cycloheptene

K. A. Abboud, S. H. Simonsen, C. S. Tyllick and R. M. Roberts



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Acta Cryst. (1991). C47, 674-676    [doi:10.1107/S0108270190008885]

2-Amino-4-methyl-5-phenylthiophene-3-carboxamide

P. S. Joseph, S. Selladurai, S. Kannan and V. Parthasarathi



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Acta Cryst. (1991). C47, 676-678    [doi:10.1107/S0108270190009003]

Structure of 2-hydroxy-2-phenyl-2-phthalidylacetophenone

L. Malpezzi



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Acta Cryst. (1991). C47, 678-680    [doi:10.1107/S0108270190009015]

Structure of a nucleoside analogue: 3'-azido-5-chloro-2',3'-dideoxyuridine

D. H. Everaert, O. M. Peeters, N. M. Blaton, C. J. De Ranter, A. Van Aerschot and P. Herdewijn



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Acta Cryst. (1991). C47, 680-682    [doi:10.1107/S0108270190009751]

Structural studies of mitomycins. VI. Structure of mitiromycin monohydrate

N. Hirayama, M. Kohno, E. Shimizu and M. Kasai



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Acta Cryst. (1991). C47, 682-684    [doi:10.1107/S0108270190009155]

Structure of cholest-5-en-3-one

P. Grochulski, Z. Wawrzak and Z. Galdecki



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Acta Cryst. (1991). C47, 684-686    [doi:10.1107/S0108270190009775]

Structure of an ascochlorin derivative (AS-6)

Y. Nawata, I. Matsuura, T. Hosokawa, M. Sawada and K. Ando



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Acta Cryst. (1991). C47, 686-687    [doi:10.1107/S0108270190009416]

Triethylammonium 3,3,6,6-tetrathioxocyclodi(phosphadithianate) at 178 K

P. G. Jones and A. Weinkauf



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Acta Cryst. (1991). C47, 687-689    [doi:10.1107/S0108270190009088]

Structure of cholest-5-en-4-one

Z. Wawrzak, P. Grochulski and Z. Galdecki



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Acta Cryst. (1991). C47, 689-691    [doi:10.1107/S0108270190009362]

Structure of 6[beta],6'[beta]-bi(7[alpha]-allyl-3-oxo-4-estren-17[beta]-yl acetate)

W. L. Duax, J. F. Griffin, P. D. Strong, B. Miller and D. N. Kirk


short communications



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Acta Cryst. (1991). C47, 692    [doi:10.1107/S010827019001410X]

Structure of (chloranilato)bis(tri-m-tolylphosphine)palladium(II). Erratum

R. F. Johnston, P. K. Sen Gupta, M. B. Ossain, R. van der Helm, W.-Y. Jeong and R. A. Holwerda


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