Acta Crystallographica Section C

Crystal Structure Communications

Volume 47, Part 4 (April 1991)



research papers


inorganic compounds



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Acta Cryst. (1991). C47, 693-696    [doi:10.1107/S0108270190011052]

Structure of a dititanodecatungstophosphate

T. Ozeki and T. Yamase



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Acta Cryst. (1991). C47, 696-698    [doi:10.1107/S010827019001040X]

Structure of LaCuO3 by powder neutron diffraction

D. B. Currie and M. T. Weller



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Acta Cryst. (1991). C47, 698-701    [doi:10.1107/S0108270190011477]

Structure cristalline de Cs2TiO(P2O7)

J. Protas, B. Menaert, G. Marnier et B. Boulanger


metal-organic compounds



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Acta Cryst. (1991). C47, 701-703    [doi:10.1107/S0108270190007946]

Structure of 2-carboxypyridinium trichloro(dimethyl sulfoxide)platinate(II)

A. Cantoni, A. Tiripicchio, M. Tiripicchio Camellini and G. Annibale



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Acta Cryst. (1991). C47, 703-705    [doi:10.1107/S0108270190007582]

Structure of dichlorobis(p-phenoxyphenyl)tellurium(IV)

M. de Matheus, L. Torres, J. F. Piniella, J. L. Briansó and C. Miravitlles



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Acta Cryst. (1991). C47, 706-708    [doi:10.1107/S0108270190010009]

Structure of [bis(diphenylphosphino-P,P')methanide]tetrakis(phenyl isocyanide)iron(II) perchlorate 0.37-pyridine solvate

J. M. Rubio González, J. Ruiz, S. García Granda and J. Fayos



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Acta Cryst. (1991). C47, 708-711    [doi:10.1107/S0108270190010010]

Structure of 2,2'-[5-(2-aminoethyl)-1-hydroxy-2,5,8-triazanon-3-ene-1,9-diyl]bis(pyridine N-oxide)nickel hexafluorophosphate monohydrate, [Ni(C18H26N6O3)]2+.2PF6-.H2O: a novel tripodal nickel(II) complex with three inequivalent arms

S.-H. Gou, X.-Z. You, Z. Xu, S.-X. Liu and C.-C. Lin



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Acta Cryst. (1991). C47, 711-714    [doi:10.1107/S0108270190010277]

Structure of (isothiocyanato)[3,3,9,9-tetramethyl-4,8-diazaundecane-2,10-dione dioximato(1-)]copper(II) monohydrate

T.-J. Lee, T.-Y. Lee, C.-S. Chung and Y.-M. Wang



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Acta Cryst. (1991). C47, 714-716    [doi:10.1107/S0108270190010319]

Transition-metal complexes with hydrazides and hydrazones. II. The structure of aqua(4-methyl-1-naphth-1-yl-2,3-diaza-1,3,5-heptatriene-1,6-diolato)copper(II)

R. Fazlic, V. Divjakovic, V. M. Leovac and S. Yu. Chundak



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Acta Cryst. (1991). C47, 716-719    [doi:10.1107/S0108270190010320]

Structure of acetonitrile(dichloro)(phenyl)bis(triphenylstibine)rhodium(III)

R. Cini, G. Giorgi and E. Periccioli



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Acta Cryst. (1991). C47, 719-722    [doi:10.1107/S0108270190010265]

(1,3-Diamino-2-propanol-N,N')diiodoplatinum(II) and (1,3-diamino-2-propanol-N,N')dichloroplatinum(II)

A. Oksanen, R. Kivekäs, P. Lumme and T. Laitalainen



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Acta Cryst. (1991). C47, 722-725    [doi:10.1107/S0108270190010423]

Synthesis and structure of (CH3)2AsC(CF3)=C(CF3)As(CH3)2W(CO)2Br2P(C6H5)3

S. K. Manocha, L. M. Mihichuk, R. J. Barton and B. E. Robertson



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Acta Cryst. (1991). C47, 725-728    [doi:10.1107/S0108270190010514]

Structures of [cis-1,2-bis(diphenylphosphino)ethylene]tetracarbonylmolybdenum(0) (1) and bis[cis-1,2-bis(diphenylphosphino)ethylene]dicarbonylmolybdenum(0) (2)

C.-H. Ueng and L.-C. Leu



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Acta Cryst. (1991). C47, 728-730    [doi:10.1107/S0108270190010459]

Structure of sodium hydrogen glutarate dihydrate

A. L. Macdonald, P. Morrison, A. Murray and A. A. Freer



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Acta Cryst. (1991). C47, 730-732    [doi:10.1107/S0108270190010642]

Structure of a 4:1 adduct of cadmium(II) chloride with 15-crown-5 ether

A. Hazell and R. G. Hazell



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Acta Cryst. (1991). C47, 732-737    [doi:10.1107/S0108270190010575]

Structures of trans-[TcCl4{P(CH3)(C6H5)2}2], [TcCl4{P(C2H5)3}2] and [P(C2H5)3H][TcCl5{P(C2H5)3}]

F. D. Rochon, R. Melanson and P.-C. Kong



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Acta Cryst. (1991). C47, 738-740    [doi:10.1107/S0108270190011027]

Structure du perrhenate de triphényl-2,3,5 tétrazolium

M. Predota, V. Petrícek, Z. Zák, T. Glowiak et J. Novotný



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Acta Cryst. (1991). C47, 740-743    [doi:10.1107/S0108270190010976]

Synthesis and structure of ammonium isoorotate monohydrate and bis(isoorotato)manganese(II) dihydrate

G. Maistralis, N. Katsaros, D. Mentzafos and A. Terzis



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Acta Cryst. (1991). C47, 743-745    [doi:10.1107/S0108270190010964]

Structure of homochiral carbonylchloro(3-trifluoroacetylcamphorato)platinum(II)

P. Scheer, V. Schurig, L. Walz and H. G. von Schnering



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Acta Cryst. (1991). C47, 745-747    [doi:10.1107/S0108270190011210]

Structure of a five-coordinate copper(II) hexaaza macrotricyclic complex: chloro(1,3,6,9,11,14-hexaazatricyclo[12.2.1.16,9]octadecane)copper(II) perchlorate

J. Kim, M. P. Suh and W. Shin



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Acta Cryst. (1991). C47, 747-750    [doi:10.1107/S0108270190011118]

Structure of trans-dichlorotetrakis(dimethyl sulfoxide)rhodium(III) tetrafluoroborate

M. Calligaris, P. Faleschini and E. Alessio



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Acta Cryst. (1991). C47, 750-752    [doi:10.1107/S0108270190011337]

New precursors in the chemistry of IVB transition metal alkoxides. III. Synthesis and structure of Zr2Co2([mu]3-OC3H7)2([mu]2-OC3H7)4(OC3H7)4(acetylacetone)2

R. Schmid, A. Mosset and J. Galy



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Acta Cryst. (1991). C47, 752-754    [doi:10.1107/S0108270190011222]

Quasi-one-dimensional structure of cis-dichlorobis(2,6-dimethylphenyl isocyanide)palladium(II), [Pd{2,6-(CH3)2C6H3NC}2Cl2]

M. Drouin, D. Perreault, P. D. Harvey and A. Michel



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Acta Cryst. (1991). C47, 754-757    [doi:10.1107/S0108270190011726]

Structure of 1% copper(II)-doped dichlorobis(1,2-dimethylimidazole)zinc(II)

P. K. Bharadwaj, H. J. Schugar and J. A. Potenza


organic compounds



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Acta Cryst. (1991). C47, 757-759    [doi:10.1107/S0108270190005698]

Structure and absolute configuration of (23R)-6[alpha]-chloro-5[beta]-17[beta]-dihydroxy-12[beta]-methoxy-1-oxo-12,22-epoxyergosta-2,24-dien-23,26-olide, a new withanolide from Jaborosa magellanica

M. Parvez, V. Fajardo and M. Shamma



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Acta Cryst. (1991). C47, 759-761    [doi:10.1107/S0108270190007673]

Structure of 6,7-dihydro-2-phenyl-5H-2a[lambda]4-thia-3-selena-1,2-diazacyclopent[cd]indene

D. G. Billing, D. C. Levendis and D. H. Reid



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Acta Cryst. (1991). C47, 762-764    [doi:10.1107/S0108270190007958]

Charge-transfer complex of 2,2',5,5'-tetrathiafulvalene and p-benzoquinone

G. M. Frankenbach, M. A. Beno and J. M. Williams



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Acta Cryst. (1991). C47, 764-768    [doi:10.1107/S0108270190006588]

Solid-state stereochemistry of Diels-Alder adducts between a bicyclic cyclohexadienone derivative and [alpha]-acyloxyacrylonitrile

A. G. Michel, G. Boulay, N. Michel-Dewez, M. Drouin, L. Ruest and P. Deslongchamps



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Acta Cryst. (1991). C47, 768-771    [doi:10.1107/S0108270190007557]

Structure of two pyrethroid insecticides: acrynathryn (RU 38702) and a derivative (RU 38181)

F. Baert, A. Guelzim and G. Germain



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Acta Cryst. (1991). C47, 771-775    [doi:10.1107/S0108270190007284]

Structures of two conformationally defined phenylethanolamines: exo-1,4-epoxy-2-formamido-1,2,3,4-tetrahydro-8-trifluoromethylnaphthalene and exo-1,4-epoxy-2-formamido-1,2,3,4-tetrahydro-6-trifluoromethylnaphthalene

G. L. Grunewald, M. S. S. Palanki and F. Takusagawa



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Acta Cryst. (1991). C47, 775-777    [doi:10.1107/S0108270190007533]

Structure of 3-(bromoacetyl)coumarin

K. T. Vasudevan, Puttaraja and M. V. Kulkarni



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Acta Cryst. (1991). C47, 777-779    [doi:10.1107/S0108270190008022]

Structure of the aglycone ethyl ether of jasminin

K. Takahashi, T. Kamikawa, M. Asaka and M. Fukuyo



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Acta Cryst. (1991). C47, 779-781    [doi:10.1107/S0108270190008149]

Structure of 4,7-diacetoxy-12,15-difluorohexacyclo[8.6.0.02,15.03,8.09,12.011,16]hexadeca-3,5,7-triene-13,14-dicarboxylic anhydride

M. Kimura, H. Okamoto, S. Morosawa and S. Kashino



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Acta Cryst. (1991). C47, 782-787    [doi:10.1107/S0108270190008277]

Absolute configurations of three ent-beyerene derivatives

K. A. Abboud, S. H. Simonsen, E. F. Lee and T. J. Mabry



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Acta Cryst. (1991). C47, 787-790    [doi:10.1107/S010827019000806X]

Structure of two polymorphs of 2-methyl-3,4'-bipyridin-6(1H)-one

V. Cody and A. Wojtczak



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Acta Cryst. (1991). C47, 790-793    [doi:10.1107/S0108270190008290]

Structure of a new dammarane-type triterpene from Gynostemma pentaphyllum (Thurb.) Makino

M. F. Mackay, J.-X. Wei and Y.-G. Chen



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Acta Cryst. (1991). C47, 793-797    [doi:10.1107/S0108270190008356]

Crystal structure and photochemistry of a methyl phenyl diester derivative of dibenzobarrelene

J. Trotter and F. C. Wireko



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Acta Cryst. (1991). C47, 797-800    [doi:10.1107/S0108270190008514]

Structure of solanid-4-en-6-one

S. Stankovic, D. Miljkovic, K. Gasi, C. Mészáros, F. Ugozzoli and G. Calestani



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Acta Cryst. (1991). C47, 800-803    [doi:10.1107/S0108270190008587]

Structures of three complexes with the host diaza-18-crown-6

W. H. Watson, A. Nagl and R. P. Kashyap



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Acta Cryst. (1991). C47, 804-807    [doi:10.1107/S0108270190008447]

Structure of 5-amino-1-diphenylmethylimidazole-4-carboxamide

T. Banerjee, P. Roychowdhury, D. Chattopadhyay, S. Ray, G. Chatterjee, S. Kashino and M. Haisa



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Acta Cryst. (1991). C47, 807-810    [doi:10.1107/S0108270190008988]

Structure of 8-dimethylamino-1-dimethylammonionaphthalene hydrogen squarate

J. A. Kanters, A. Schouten, J. Kroon and E. Grech



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Acta Cryst. (1991). C47, 810-812    [doi:10.1107/S0108270190008897]

Structure of lantadene A, the major triterpenoid of Lantana camara, red variety

V. Pattabhi, N. Sukumar and O. P. Sharma



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Acta Cryst. (1991). C47, 813-817    [doi:10.1107/S0108270190008563]

Five 8,11-substituted pentacyclo[5.4.0.02,6.03,10.05,9]undecanes

J. L. Flippen-Anderson, C. George, R. Gilardi, W. W. Zajac Jnr, T. R. Walters, A. Marchand, P. R. Dave and B. E. Arney Jnr



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Acta Cryst. (1991). C47, 817-824    [doi:10.1107/S010827019000899X]

Structures of three photochromic compounds and three non-photochromic derivatives; the effect of methyl substituents

W. Clegg, N. C. Norman, T. Flood, L. Sallans, W. S. Kwak, P. L. Kwiatkowski and J. G. Lasch



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Acta Cryst. (1991). C47, 824-827    [doi:10.1107/S0108270190008952]

Huperzine A - a potent acetylcholinesterase inhibitor of use in the treatment of Alzheimer's disease

S. J. Geib, W. Tückmantel and A. P. Kozikowski



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Acta Cryst. (1991). C47, 827-829    [doi:10.1107/S0108270190009180]

Structures of N-substituted 1,2-oxazines. I. A monocyclic derivative, 2-(tert-butylthio)-3-(3,6-dihydro-2H-1,2-oxazin-2-yl)acrylonitrile

B. Tinant and J. P. Declercq



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Acta Cryst. (1991). C47, 829-832    [doi:10.1107/S0108270190008940]

Structure of (±)-aminoglutethimide

P. Van Roey, K. A. Bullion, Y. Osawa and D. G. Braun



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Acta Cryst. (1991). C47, 832-835    [doi:10.1107/S0108270190008976]

Structure of the modified nucleoside 2,3'-dideoxy-3'-fluorocytidine

H. L. De Winter, N. M. Blaton, O. M. Peeters, C. J. De Ranter, A. Van Aerschot and P. Herdewijn



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Acta Cryst. (1991). C47, 835-837    [doi:10.1107/S0108270190010526]

Structure of 1-(2-deoxy-[beta]-D-ribopyranosyl)-5-iodouracil

H. L. De Winter, N. M. Blaton, O. M. Peeters, C. J. De Ranter, A. Van Aerschot and P. Herdewijn



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Acta Cryst. (1991). C47, 838-842    [doi:10.1107/S0108270190010538]

Structures of 1-(2,3-dideoxy-erythro-[alpha]-D-hexopyranosyl)thymine and the 1-(2,3-dideoxy-erythro-[beta]-D-hexopyranosyl)thymine.dioxane complex

H. L. De Winter, N. M. Blaton, O. M. Peeters, C. J. De Ranter, A. Van Aerschot and P. Herdewijn



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Acta Cryst. (1991). C47, 842-845    [doi:10.1107/S0108270190008630]

Three stereoisomeric methyl 8-bromo-2,3-diphenyl-2,3,3a,9b-tetrahydro-1H,4H-[1]benzopyrano[4,3-b]pyrrole-2-carboxylates

I. Ueda, N. Marubayashi, K. Ueno and O. Tuge



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Acta Cryst. (1991). C47, 845-848    [doi:10.1107/S010827019000912X]

Structure of 3-benzoyl-2-phenylquinoxaline 1,4-dioxide

Yi Wang, Hanqing Wang and Qiguang Wang


short format


inorganic compounds



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Acta Cryst. (1991). C47, 849-850    [doi:10.1107/S0108270190010666]

Redetermination of the structure of PNb9O25

A. Benabbas, M. M. Borel, A. Grandin, A. Leclaire and B. Raveau



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Acta Cryst. (1991). C47, 850-852    [doi:10.1107/S0108270190011362]

Structure of Tl2SnTe5

V. Agafonov, B. Legendre, N. Rodier, J. M. Cense, E. Dichi and G. Kra


metal-organic compounds



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Acta Cryst. (1991). C47, 852-854    [doi:10.1107/S010827019001054X]

cis-Bis(1-methylcytosine-[kappa]N)(N,N,N',N'-tetramethylethylenediamine-[kappa]2N,N')platinum(II) diperchlorate monohydrate

H. Preut, G. Frommer and B. Lippert



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Acta Cryst. (1991). C47, 854-856    [doi:10.1107/S0108270190010241]

Structure of tris([eta]5-cyclopentadienyl)uranium iodide

J. Rebizant, M. R. Spirlet, C. Apostolidis and B. Kanellakopulos



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Acta Cryst. (1991). C47, 856-858    [doi:10.1107/S0108270190010022]

Structure of 2,3,4-[mu]3-chloro-1,2,3;1,3,4;1,2,4-tri-[mu]3-sulfido-tris[(triphenylphosphine)copper](sulfidotungsten)(3 Cu-W).0.5-propanol

N. Zhu, Jianhui Wu and X. Wu



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Acta Cryst. (1991). C47, 858-860    [doi:10.1107/S0108270190010873]

Structure of pentacarbonyl(morpholine-[kappa]N)chromium(0)

M. L. Rodriguez, I. Brito, F. V. Rodriguez-Romero, V. Manriquez, G. González and C. Díaz



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Acta Cryst. (1991). C47, 860-862    [doi:10.1107/S0108270190010812]

Structure of ([eta]5-cyclopentadienyl)([eta]6-p-isopropylnitrobenzene)iron(II) trifluoroacetate at 198 K

K. A. Abboud, S. H. Simonsen, A. Piórko and R. G. Sutherland



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Acta Cryst. (1991). C47, 862-864    [doi:10.1107/S0108270190010708]

Structure of dicarbonyl(dimethylphosphonate)iodo([eta]5-pentamethylcyclopentadienyl)rhenium(II)

F. W. B. Einstein, C. E. F. Rickard, H. Klahn and C. Leiva



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Acta Cryst. (1991). C47, 864-866    [doi:10.1107/S010827019001099X]

Structure of di-[mu]-chloro-bis[trichlorobis(tetrahydrofuran)uranium(IV)]

J. Rebizant, M. R. Spirlet, C. Apostolidis, G. Van den Bossche and B. Kanellakopulos



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Acta Cryst. (1991). C47, 866-869    [doi:10.1107/S010827019001085X]

Structure of aqua-hexakis([mu]2-benzoato)-bis(methanol)-[mu]3-oxo-triiron(III) benzoate ethanol methanol solvate

V. M. Lynch, J. W. Sibert, J. L. Sessler and B. E. Davis



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Acta Cryst. (1991). C47, 869-871    [doi:10.1107/S0108270190011349]

The 1/2 complex of mercury(II) trifluoroacetate and pyridine N-oxide

J. Halfpenny and R. W. H. Small



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Acta Cryst. (1991). C47, 871-872    [doi:10.1107/S0108270190010988]

Bis(acetato)(4-benzyl-1,7-diphenyl-2,4,6-triazahepta-2,5-diene-[kappa]2N2,N6)copper(II)

S. W. Breuer and R. W. H. Small



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Acta Cryst. (1991). C47, 872-874    [doi:10.1107/S0108270190011064]

Structure of di(quinoxalinium) tetrachlorocobaltate(II) monohydrate

S. Lindroos and P. Lumme



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Acta Cryst. (1991). C47, 874-876    [doi:10.1107/S0108270190011179]

Chloro(tri-tert-butylphosphino-C,P)(tricyclohexylphosphine)platinum(II)

D. F. Mullica, E. L. Sappenfield and D. H. Leschnitzer



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Acta Cryst. (1991). C47, 876-878    [doi:10.1107/S0108270190011088]

Structure of a heptanuclear tungsten-copper complex, (Ph4P)2[Cu5W2O2S6(S2CNEt2)3].DMF

R. Cao, X. Lei and H. Liu



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Acta Cryst. (1991). C47, 878-880    [doi:10.1107/S0108270190011428]

Chloro[tris(m-tolyl)phosphine]gold(I)

C. S. W. Harker and E. R. T. Tiekink


organic compounds



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Acta Cryst. (1991). C47, 880-882    [doi:10.1107/S0108270190010605]

Structure of cis-9,10-dibenzyl-9,10-dihydroanthracene at 193 K

K. A. Abboud, S. H. Simonsen, R. S. Prasad and R. M. Roberts



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Acta Cryst. (1991). C47, 882-884    [doi:10.1107/S0108270190010034]

Structure de la benzoyl-6 dihydro-2,3 benzothiazole-1,3 one-2

C. Follet-Houttemane, J. C. Boivin, J. P. Bonte and D. Lesieur



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Acta Cryst. (1991). C47, 884-886    [doi:10.1107/S0108270190009726]

Structure of bis[bis(trimethylsilyl)methylene]methoxyphosphorane

N. Burford, J. D. McInnis, M. J. Schriver and R. D. Rogers



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Acta Cryst. (1991). C47, 886-888    [doi:10.1107/S0108270190010460]

Structure of diethyl 2,6-dimethyl-4-[5-(4-methylphenyl)-2-furyl]-1,4-dihydropyridine-2,5-dicarboxylate

J. Lokaj, V. Vrábel, P. Sivý, V. Kettmann, D. Ilavský and J. Jecný



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Acta Cryst. (1991). C47, 888-890    [doi:10.1107/S010827019000991X]

Structure of 3,5-dihydrobenz[f]indolizin-3-one

J. Lamiot, F. Baert, A. Guelzim, D. Barbry, D. Couturier, B. Rigo and E. Tulier



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Acta Cryst. (1991). C47, 890-893    [doi:10.1107/S0108270190010344]

Structure of (4RS)-6,7-dimethoxy-4-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

B. Stensland, P.-E. Werner, D. Mondeshka, I. Angelova and C. Ivanov



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Acta Cryst. (1991). C47, 893-895    [doi:10.1107/S0108270190010186]

[2-(1-Aza-4,7,10-trioxacyclododecyl)ethyl]dimethylammonium iodide. An intramolecular trifurcated hydrogen bond

P. Prince, S. F. Watkins, F. R. Fronczek, R. D. Gandour, B. D. White and G. W. Gokel



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Acta Cryst. (1991). C47, 895-898    [doi:10.1107/S0108270190010198]

Two polymorphs of 3,5-dinitrobenzoic acid

P. Prince, F. R. Fronczek and R. D. Gandour



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Acta Cryst. (1991). C47, 898-902    [doi:10.1107/S0108270190010551]

Structure of nucleoside analogues 3'-fluoro-2',3'-dideoxyuridine, 3'-fluoro-2',3'-dideoxy-5-bromouridine and 3'-azido-2',3'-dideoxy-5-bromouridine

D. H. Everaert, O. M. Peeters, N. M. Blaton, C. J. De Ranter, A. Van Aerschot and P. Herdewijn



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Acta Cryst. (1991). C47, 903-904    [doi:10.1107/S0108270190009830]

Structure of N1,N1,N3,N3-tetramethyl-[alpha],[alpha]1-diselenobisformamidinium bromide

H. M. K. K. Pathirana, J. H. Reibenspies, E. A. Meyers and R. A. Zingaro



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Acta Cryst. (1991). C47, 904-906    [doi:10.1107/S0108270190010654]

Structure of (E,E)-bis(2-acetoxy-1-iodo-2-phenylvinyl) disulfide

A. Frost Jensen and R. G. Hazell



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Acta Cryst. (1991). C47, 906-908    [doi:10.1107/S0108270190010332]

Structure of calliterpenone hemihydrate

W. H. Wong, C. Wei, S. E. Loke and T. C. W. Mak



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Acta Cryst. (1991). C47, 908-910    [doi:10.1107/S0108270190010617]

Structure of (±)-7(S)-16-deformyl-21-oxogeissoschizine-oxindole

V. M. Lynch, M. Mortimore, S. F. Martin and B. E. Davis



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Acta Cryst. (1991). C47, 910-912    [doi:10.1107/S0108270190011039]

Structure of a key intermediate in the asymmetric synthesis of (+)-KDO

V. M. Lynch, P. W. Zinke, S. F. Martin and B. E. Davis


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