Acta Crystallographica Section C

Crystal Structure Communications

Volume 48, Part 5 (May 1992)



research papers


inorganic compounds



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Acta Cryst. (1992). C48, 769-771    [doi:10.1107/S0108270191011915]

Structure of lithium tetrafluoroindate

P. Gravereau, J. P. Chaminade, T. Gaewdang, J. Grannec, M. Pouchard and P. Hagenmuller



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Acta Cryst. (1992). C48, 771-773    [doi:10.1107/S0108270191011599]

Structure of europium zirconium selenide, EuZrSe3

A. Mar and J. A. Ibers



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Acta Cryst. (1992). C48, 774-776    [doi:10.1107/S0108270191012532]

Structure du sulfure de manganèse et d'ytterbium Mn2/3Yb7/3S4

P. Lemoine, A. Tomas et M. Guittard



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Acta Cryst. (1992). C48, 776-779    [doi:10.1107/S0108270191012003]

Structure of cobalt sulfate tetrahydrate

T. Kellersohn


metal-organic compounds



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Acta Cryst. (1992). C48, 779-782    [doi:10.1107/S0108270191011460]

Synthesis and structure determination of SrCa(edta).5H2O

M. I. Arriortua, M. Insausti, M. K. Urtiaga, J. Vía and T. Rojo



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Acta Cryst. (1992). C48, 782-785    [doi:10.1107/S0108270191011824]

Dicarbonyl([eta]5-cyclopentadienyl)(triphenylphosphite)[(triphenylphosphonio)methanide]molybdenum p-toluenesulfonate

D. H. Gibson, J. F. Richardson and J. O. Franco



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Acta Cryst. (1992). C48, 785-788    [doi:10.1107/S010827019101185X]

Structure of bis(4-nitro-1,2-catecholato)oxotechnetium(V)

F. D. Rochon, R. Melanson and P.-C. Kong



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Acta Cryst. (1992). C48, 788-792    [doi:10.1107/S0108270191011769]

Structure of NiII, PdII and PtII complexes with the bidentate ligand 2,11-bis(diethylphosphinomethyl)benzo[c]phenanthrene

F. Bachechi and L. Zambonelli



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Acta Cryst. (1992). C48, 793-795    [doi:10.1107/S0108270191012301]

Magnesium formate-urea (1/2)

K. Yamagata, N. Achiwa, M. Hashimoto, N. Koyano, Ridwan, Y. Iwata and I. Shibuya



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Acta Cryst. (1992). C48, 795-798    [doi:10.1107/S0108270191011903]

Structure of 1,2,3-tris(dimethylamino)cyclopropenylium hexachloroniobate(V) and hexachlorotantalate(V)

H. N. Schäfer, H. Burzlaff, A. M. H. Grimmeiss and R. Weiss



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Acta Cryst. (1992). C48, 798-802    [doi:10.1107/S0108270191012568]

Structures of methyl- and benzyl([eta]1-azaferrocene)cobaloximes

M. Cesario, C. Giannotti, J. Guilhem and J. Zakrzewski



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Acta Cryst. (1992). C48, 802-806    [doi:10.1107/S0108270191012325]

Two different (croconato)(2,2':6',2''-terpyridyl)copper(II) complexes in one single crystal: structure of [Cu(C15H11N3)(H2O)(C5O5)][Cu(C15H11N3)(C5O5)\].4H2O

M. Aguiló, X. Solans, I. Castro, J. Faus and M. Julve



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Acta Cryst. (1992). C48, 806-811    [doi:10.1107/S0108270191011848]

Structures of Pd[(PPh2)2(NMe)]Cl2, Pt[(PPh2)2(NMe)]Cl2 and Pt[(PPh2)2(NMe)](CN)2

C. S. Browning, D. H. Farrar and D. C. Frankel



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Acta Cryst. (1992). C48, 811-814    [doi:10.1107/S010827019101199X]

An organometallic cyanine: [mu]-1,3,5-heptatriene-1,7-diylidene-bis[[mu]2-carbonyl-dicarbonylbis([eta]5-cyclopentadienyl)diiron] tetrafluoroborate

W. P. Schaefer, J. M. Spotts and S. R. Marder



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Acta Cryst. (1992). C48, 814-817    [doi:10.1107/S0108270191012830]

Structure of bromodicyano(2,2':6',2''-terpyridine)gold(III)

V. Ferretti, P. Gilli, V. Bertolasi, G. Marangoni, B. Pitteri and G. Chessa



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Acta Cryst. (1992). C48, 817-821    [doi:10.1107/S010827019100999X]

meso-(1,1,4,7,10,10-Hexaphenyl-1,4,7,10-tetraphosphadecane-P,P',P'',P''')platinum(II) bis(tetraphenylborate)

P. Brüggeller, H. Nar and A. Messerschmidt


organic compounds



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Acta Cryst. (1992). C48, 821-824    [doi:10.1107/S010827019101154X]

Structure of guanidinium hydrogen acetylenedicarboxylate, CH6N3+.C4HO4-

I. Leban and A. Rupnik



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Acta Cryst. (1992). C48, 824-826    [doi:10.1107/S0108270191012131]

Bond length and reactivity. Structure of the diphenyl phosphate ester of 2,6-dichlorobenzyl alcohol

P. G. Jones, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 826-829    [doi:10.1107/S0108270191012143]

Bond length and reactivity. Structure of 2-endo-bornyl p-toluenesulfonate

P. G. Jones, K. Schmidt-Bäse, M. R. Edwards and A. J. Kirby



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Acta Cryst. (1992). C48, 829-832    [doi:10.1107/S0108270191012155]

Bond length and reactivity. Structures of the triphenylmethyl ether and the 4-nitrobenzoate ester of anti-7-norbornenol

P. G. Jones, A. J. Kirby and J. M. Percy



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Acta Cryst. (1992). C48, 832-834    [doi:10.1107/S0108270191012167]

Bond length and reactivity. Structure of 2-phenylethyl p-toluenesulfonate

A. J. Kirby, J. K. Parker and P. R. Raithby



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Acta Cryst. (1992). C48, 835-837    [doi:10.1107/S0108270191012179]

Bond length and reactivity. The effect of [beta]-fluorine. Structures of the 4-nitrophenyl ether and the 4-nitrobenzoate ester of 2-fluoro-2-phenylethanol

P. G. Jones, A. Dölle, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 838-841    [doi:10.1107/S0108270191012180]

Bond length and reactivity. The effect of [beta]-fluorine. Structures of the 4-methyl-, 4-chloro- and 4-nitrobenzenesulfonate esters of 2-fluoro-2-phenylethanol

P. G. Jones, A. Dölle, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 841-844    [doi:10.1107/S0108270191012192]

Bond length and reactivity. The effect of [beta]-fluorine. Structures of the 4-nitrobenzenesulfonate esters of 2-fluoroethanol and 2,2,2-trifluoroethanol

P. G. Jones, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 844-847    [doi:10.1107/S0108270191012209]

Bond length and reactivity. Structures of the 4-phenylbenzoate esters of cis- and trans-4-tert-butylcyclohexanol

P. G. Jones, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 847-849    [doi:10.1107/S0108270191012210]

Bond length and reactivity. Structure of the 4-phenylbenzoate ester of trans-3-tert-butylcyclohexanol

P. G. Jones, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 849-851    [doi:10.1107/S0108270191012222]

Bond length and reactivity. Structures of the methanesulfonate esters of cis- and trans-4-tert-butylcyclohexanol

P. G. Jones, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 852-855    [doi:10.1107/S0108270191012234]

Bond length and reactivity. The effect of [beta]-fluorine. Structures of the 4-phenylbenzoate, the diphenyl phosphate and the 2-naphthalenesulfonate esters of trans-2-fluorocyclohexanol

P. G. Jones, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 855-858    [doi:10.1107/S0108270191012246]

Bond length and reactivity. The effect of [beta]-fluorine. Structures of the 4-phenylbenzoate and methanesulfonate esters of trans,cis-4-tert-butyl-2-fluorocyclohexanol

P. G. Jones, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 859-864    [doi:10.1107/S0108270191012258]

Bond length and reactivity. The effect of [beta]-fluorine. Structures of the 9-(9-phenylxanthenyl) ether, and the 4-phenylbenzoate, diphenyl phosphate and methanesulfonate esters of cis,trans-4-tert-butyl-2-fluorocyclohexanol

P. G. Jones, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 864-866    [doi:10.1107/S010827019101226X]

Bond length and reactivity. The effect of [beta]-fluorine. Structure of the methanesulfonate ester of trans,trans-5-tert-butyl-2-fluorocyclohexanol

P. G. Jones, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 866-868    [doi:10.1107/S0108270191012271]

Bond length and reactivity. The effect of [beta]-silicon. Structure of the 4-phenylbenzoate ester of 2-trimethylsilylethanol

M. J. Doyle, A. J. Kirby, J. M. Percy and P. R. Raithby



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Acta Cryst. (1992). C48, 868-871    [doi:10.1107/S0108270191012283]

Bond length and reactivity. The effect of [beta]-silicon. Structure of the 3,5-dinitrobenzoate ester of trans-2-(dimethylphenylsilyl)cyclohexanol

P. G. Jones, A. J. Kirby and J. K. Parker



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Acta Cryst. (1992). C48, 871-873    [doi:10.1107/S0108270190007934]

Structure of N2-(3,5-dichlorophenyl)-4-(4-hydroxy-2-methoxyphenyl)-1-piperazinecarboxamidine monohydrate

D. P. Elder, I. A. Selby, R. O. Gould and P. Taylor



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Acta Cryst. (1992). C48, 873-876    [doi:10.1107/S0108270191011897]

Methyl 4,6-O-benzylidene-2-deoxy-2-C-(1,2:3,4-di-O-isopropylidene-L-glycero-D-galacto-hexopyranos-6-yl)-[alpha]-D-arabino-hexopyranosid-3-ulose monohydrate

Z. Ciunik, P. Luger and K.-L. Yu



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Acta Cryst. (1992). C48, 876-878    [doi:10.1107/S0108270191011150]

Structures of sobrerol enantiomers and racemates. II. (±)-trans-5-Hydroxy-[alpha],[alpha],4-trimethyl-3-cyclohexene-1-methanol (racemic trans-sobrerol)

G. Giuseppetti, C. Tadini and G. P. Bettinetti



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Acta Cryst. (1992). C48, 878-883    [doi:10.1107/S0108270191012489]

Structures of a partially deuterated sodium trihydrogen dimalonate and sodium hydrogen malonate (a reinvestigation) at 120 K

N. Kalsbeek



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Acta Cryst. (1992). C48, 883-885    [doi:10.1107/S0108270191011782]

Structure of (Z,Z)-3,11-diiodo-N,N-ditosyl-1,9-diazacyclohexadeca-3,11-diene

M. Anderson, T. Gallagher, M. F. Mahon, K. C. Molloy and R. Shaw



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Acta Cryst. (1992). C48, 885-887    [doi:10.1107/S0108270191011605]

Spiro[(2,3-époxycyclohexane)-1:4'-(2',3'-dihydro-8'-méthoxybenzo-4H-pyranne)]

N. Rodier, Y. M. Zhang et J. Mayrargue



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Acta Cryst. (1992). C48, 887-891    [doi:10.1107/S0108270191011186]

Structure of 1,1-dichloro-2-(4-methoxyphenyl)-2,3-diphenylcyclopropane

L. Du, M. B. Hossain, X. Ji, D. van der Helm, R. A. Magarian and B. W. Day



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Acta Cryst. (1992). C48, 891-894    [doi:10.1107/S0108270191011241]

Structure of asperketal B

X. Ji, D. van der Helm, J. Shin and W. Fenical



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Acta Cryst. (1992). C48, 894-897    [doi:10.1107/S0108270191011885]

Structures of 2,2'-polymethylene-1,1'-biisoquinolinium dibromides

Y. Mori, Y. Matsuyama, S. Yamada and K. Maeda



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Acta Cryst. (1992). C48, 897-899    [doi:10.1107/S0108270191012337]

The first structure of a benzo[b][1,4]diazocine

J. D. Wallis



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Acta Cryst. (1992). C48, 900-902    [doi:10.1107/S0108270191011800]

Refined molecular structure of tetrabenzo[de,hi,op,st]pentacene

A. Izuoka, K. Wakui, T. Fukuda, N. Sato and T. Sugawara



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Acta Cryst. (1992). C48, 902-905    [doi:10.1107/S0108270191011836]

Studies on nonlinear optical materials: structure of diphenylmethyl (Z)-1-(1-methylthio-2-nitrovinyl)tetrahydropyrrole-2-carboxylate

N. S. Begum and K. Venkatesan



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Acta Cryst. (1992). C48, 905-907    [doi:10.1107/S0108270191012556]

Structure of 1-acetylthymine

L. W. Tari and A. S. Secco


short format


inorganic compounds



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Acta Cryst. (1992). C48, 908-909    [doi:10.1107/S0108270191008260]

Structure of bromopentacarbonylrhenium(I)

L. C. Porter, A. H. Reid and J. P. Fackler Jnr


metal-organic compounds



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Acta Cryst. (1992). C48, 909-912    [doi:10.1107/S0108270191011289]

Structure of [(1,2-[eta]2)-1,3,5,7-cycloheptatetraene]bis(triphenylphosphine)platinum(0)

K. A. Abboud, Z. Lu and W. M. Jones



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Acta Cryst. (1992). C48, 912-913    [doi:10.1107/S0108270191011940]

Structure of 1,2,3-tris(dimethylamino)cyclopropenylium hexachloroantimonate(V)

H. N. Schäfer, H. Burzlaff, A. M. H. Grimmeiss and R. Weiss



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Acta Cryst. (1992). C48, 913-915    [doi:10.1107/S0108270191012611]

Structure of di-[mu]-chloro-bis[1,3-bis(di-tert-butylphosphino)propaneplatinum(II)] tetrafluoroborate 0.8-dichloromethane solvate

S. A. Litster, L. Mole, A. D. Redhouse and J. L. Spencer



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Acta Cryst. (1992). C48, 915-917    [doi:10.1107/S0108270191011551]

Structure of tris(dicyclohexylphenylphosphine)gold(I) perchlorate

J. A. Muir, S. I. Cuadrado and M. M. Muir



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Acta Cryst. (1992). C48, 917-919    [doi:10.1107/S0108270191012039]

Two new crystal morphologies for tetraphenyldibismuthine, Bi2Ph4

K. H. Whitmire and J. M. Cassidy



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Acta Cryst. (1992). C48, 919-921    [doi:10.1107/S0108270191011757]

Structure of 2-chloroimidazolium aquatrichlorocuprate(II)

G. Valle and R. Ettorre



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Acta Cryst. (1992). C48, 921-923    [doi:10.1107/S0108270191012635]

Structure of tetracarbonyl[(2,3,7,8,12,13,17,18-octaethylporphinato)germanio(IV)]iron

A. Habbou, C. Lecomte and J. M. Barbe


organic compounds



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Acta Cryst. (1992). C48, 923-925    [doi:10.1107/S0108270191010727]

Structure of (2R,4R,5R)-2-chloro-3-isopropyl-4-methyl-5-phenyl-1,3,2-oxazaphospholidine 2-oxide

P. D. Robinson, D. H. Hua and D. Roche



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Acta Cryst. (1992). C48, 925-929    [doi:10.1107/S0108270191011721]

Structures of a pair of diastereomeric salts of ephedrine and dichloro-substituted cyclic phosphoric acid

H. J. Bruins Slot, F. J. J. Leusen, A. D. van der Haest and F. van Bolhuis



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Acta Cryst. (1992). C48, 929-930    [doi:10.1107/S010827019101171X]

Structure of 2,3,4,5-tetra-O-acetyl-6-amino-6-deoxy-D-mannonolactam

J. Ondrácek, J. Novotný, K. Kefurt and J. Havlícek



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Acta Cryst. (1992). C48, 931-932    [doi:10.1107/S0108270191011666]

Structure of 4-bromo-13[alpha]-methyl-13a[alpha]H-tetrahydropseudocoptisin

A. M. Atkinson and D. Rogers



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Acta Cryst. (1992). C48, 932-934    [doi:10.1107/S0108270191012015]

6,6''-Dibromo-4'-phenyl-2,2':6',2''-terpyridine

E. C. Constable, F. K. Khan, V. E. Marquez and P. R. Raithby



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Acta Cryst. (1992). C48, 934-936    [doi:10.1107/S0108270191011496]

Structure of octabenzone

I. Brito, F. Cataldo, L. Astudillo and P. Rivera



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Acta Cryst. (1992). C48, 936-938    [doi:10.1107/S0108270191011277]

Methyl 8-[(2,6-dimethoxyphenyl)ethynyl]-7-methoxy-2-naphthoate

P. Prince, K. L. Evans, F. R. Fronczek and R. D. Gandour



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Acta Cryst. (1992). C48, 938-940    [doi:10.1107/S0108270191012544]

Structure of 2-cyanobenzophenone

H. Preut, T. Kolev, I. Juchnovski and P. Bleckmann



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Acta Cryst. (1992). C48, 940-942    [doi:10.1107/S0108270191011939]

Structure of xanthoherquein tetraacetate

J. Trotter



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Acta Cryst. (1992). C48, 942-943    [doi:10.1107/S0108270191012672]

Structure of [Ni(OH2)2(NH2CH2CH2CH2NH2)2][picrate]2

W. Clegg, P. K. Bharadwaj and S. Mandal



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Acta Cryst. (1992). C48, 944-945    [doi:10.1107/S0108270191011575]

Structure of isocorypalmine

B. Ribár, P. Radivojevic, O. Gasic, I. Kanyó and L. Golic



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Acta Cryst. (1992). C48, 945-947    [doi:10.1107/S0108270191011587]

Structure of isocorydine

B. Ribár, D. Lazar, O. Gasic, I. Kanyó and P. Engel



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Acta Cryst. (1992). C48, 947-949    [doi:10.1107/S0108270191011678]

Structure of 3,3-diethyl-1,2-diphenyl-1,4,2-diazaphospholidine-5-one 2-oxide

X. L. Liu, M. Sun, F. M. Miao, K. S. Feng and R. Y. Chen



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Acta Cryst. (1992). C48, 949-951    [doi:10.1107/S0108270191012453]

Structure of a dibenzo[d,d']benzo[1,2-b:4,3-b']dithiophene (DBBDT) complex with 7,7,8,8-tetracyano-p-quinodimethane (TCNQ)

N. Thorup, M. Hjorth, J. Larsen and K. Bechgaard



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Acta Cryst. (1992). C48, 952-953    [doi:10.1107/S0108270191012507]

Non-steroidal anti-inflammatory drugs. I. Structure of (E)-2,6-di-tert-butyl-4-[2-(2-thienyl)ethenyl]phenol

K. Ravikumar



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Acta Cryst. (1992). C48, 953-955    [doi:10.1107/S0108270191011617]

Structure of (3R,6S,12bR)-6-cyanomethyl-3-ethyl-2-oxo-1,2,3,4,7,7a,12a,12b-octahydro-6H-indolo[2,3-a]quinolizine

L. F. Delboni and G. Oliva



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Acta Cryst. (1992). C48, 955-957    [doi:10.1107/S0108270191012295]

Structure of di-O-methylscandenin: a complex 4-hydroxy-3-phenylcoumarin derivative

S. Mehdi and K. Ravikumar



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Acta Cryst. (1992). C48, 957-959    [doi:10.1107/S0108270191012064]

Structure of (E)-4-hydroxyiminomethyl-1-(p-methoxyphenyl)imidazole

J. D. Martin-Ramos, M. D. Reinoso and A. Navarrete



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Acta Cryst. (1992). C48, 959-961    [doi:10.1107/S0108270191014105]

Structure of 5-phenyldibenzophosphole

E. C. Alyea, G. Ferguson and J. F. Gallagher



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Acta Cryst. (1992). C48, 961-963    [doi:10.1107/S0108270191012623]

N-(4-Chlorobenzylidene)-2-(4-imidazolyl)ethylamine

G. Bocelli and A. Cantoni


regular structural papers


organic compounds



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Acta Cryst. (1992). C48, 964-965    [doi:10.1107/S0108270192002269]

2-Methyl-4,6-diphenyl-1,2,3-triazinium iodide

K. Yamaguchi, T. Itoh, M. Okada and A. Ohsawa



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Acta Cryst. (1992). C48, 965-969    [doi:10.1107/S0108270192000921]

Unusual conformation of (R,R)-N,N,N',N'-tetramethyltartramide (I) and its O,O'-dibenzoyl derivative (II)

U. Rychlewska


metal-organic compounds



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Acta Cryst. (1992). C48, 969-972    [doi:10.1107/S0108270192001781]

Structure of aqua[N,N'-ethylenebis(N-carbamoylmethylglycinato)]copper(II) dihydrate

B. C. Noll and R. A. Marusak


short communications



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Acta Cryst. (1992). C48, 972    [doi:10.1107/S010827019200266X]

Structure of MgCl2.NH4Cl.6H2O: amplification and apology

R. E. Marsh


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