Acta Crystallographica Section C

Crystal Structure Communications

Volume 48, Part 9 (September 1992)



research papers


inorganic compounds



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Acta Cryst. (1992). C48, 1569-1571    [doi:10.1107/S0108270192001379]

Structure of ferroelastic K3H(SeO4)2

M. Ichikawa, S. Sato, M. Komukae and T. Osaka



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Acta Cryst. (1992). C48, 1571-1574    [doi:10.1107/S0108270192001094]

A neutron powder diffraction study of HIO3 and DIO3

K. Ståhl and M. Szafranski



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Acta Cryst. (1992). C48, 1574-1576    [doi:10.1107/S010827019200146X]

Structure of pentaamminechlororuthenium(III) bisulfate tetrahydrate

E. John, H. J. Schugar and J. A. Potenza



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Acta Cryst. (1992). C48, 1576-1578    [doi:10.1107/S0108270191013549]

A new type of borate double salt: structure of LiBa2B5O10

Q. Huang, S. Lu, G. Dai and J. Liang


metal-organic compounds



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Acta Cryst. (1992). C48, 1579-1582    [doi:10.1107/S0108270192000982]

Structure of [mu]-(tetraphthalato)-bis[N,N'-ethylenebis(salicylaldiminato)iron(III)]

M. Dusek, V. Petrícek, J. Kamenícek and Z. Sindelár



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Acta Cryst. (1992). C48, 1582-1584    [doi:10.1107/S0108270192001008]

A platinum chloro (fluoroaryl)phosphine complex

W. P. Schaefer, D. K. Lyon, J. A. Labinger and J. E. Bercaw



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Acta Cryst. (1992). C48, 1585-1587    [doi:10.1107/S0108270192001082]

Structure of the dinuclear copper(II) compound of N,N,N',N'-tetrakis[2-(3,5-dimethyl-1-pyrazolyl)ethyl]-1,2-ethylenediamine (tped), [Cu2(tped)(H2O)2(NO3)2](NO3)2.2CH3OH

W. L. Driessen, W. G. Haanstra and J. Reedijk



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Acta Cryst. (1992). C48, 1587-1590    [doi:10.1107/S0108270192001318]

Structure of methylbis(salicylaldoximato-O1,N)gallium(III)

S. J. Rettig, A. Storr and J. Trotter



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Acta Cryst. (1992). C48, 1590-1594    [doi:10.1107/S010827019200129X]

Structures of aqua and pyridine adducts of dimeric copper(II) 2-chlorobenzoate

T. Kawata, S. Ohba, T. Tokii, Y. Muto and M. Kato



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Acta Cryst. (1992). C48, 1594-1597    [doi:10.1107/S0108270192001331]

Structure of the clathrate compound tris(2,4-pentanedionato)iron(III)-trans-1,2-dichloroethene (1/1)

L. Pang, R. C. Hynes and M. A. Whitehead



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Acta Cryst. (1992). C48, 1597-1599    [doi:10.1107/S0108270192001288]

Structure of a 1:1 addition compound of mercuric bromide with 3-methyl-4-nitropyridine 1-oxide

S.-Z. Hu, D.-S. Shi, S.-X. Li and Y.-C. Yang



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Acta Cryst. (1992). C48, 1600-1603    [doi:10.1107/S0108270192001513]

Bis(4,5-dimethylimidazol-2-ylidene)gold(I) chloride hydrate: an unexpected product from the reaction of tris(4,5-dimethylimidazol-2-yl)phosphine and tetrachloroauric acid

J. F. Britten, C. J. L. Lock and Z. Wang



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Acta Cryst. (1992). C48, 1603-1606    [doi:10.1107/S010827019200163X]

Structure of trimethylplatinum(IV) with a tripod ligand

R. E. Marsh, W. P. Schaefer, D. K. Lyon, J. A. Labinger and J. E. Bercaw



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Acta Cryst. (1992). C48, 1606-1609    [doi:10.1107/S0108270191007552]

Structure of the nickel(II) and copper(II) complexes of 3-hydroxy-6-methylpyridine-2-thione

J. A. Boyko, W. F. Furey Jnr and R. A. Lalancette



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Acta Cryst. (1992). C48, 1610-1612    [doi:10.1107/S0108270192001628]

Cp,Cp*-dimethyltantalum triflate

W. P. Schaefer, R. W. Quan and J. E. Bercaw



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Acta Cryst. (1992). C48, 1612-1614    [doi:10.1107/S0108270192001549]

Structure of [mu]-chloro-bis{bis[2-(2-pyridyl)ethylamine-N,N']copper(II)} trishexafluorophosphate

E. H. Alilou, M. Giorgi, M. Pierrot and M. Reglier


organic compounds



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Acta Cryst. (1992). C48, 1614-1616    [doi:10.1107/S0108270192001732]

3,3,6,9,9-Pentamethyl-2,10-diazabicyclo[4.4.0]dec-1-ene hydrogen trifluoroacetate

D. Patel, D. S. Brown and J. R. Traynor



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Acta Cryst. (1992). C48, 1616-1619    [doi:10.1107/S0108270192000544]

Structure of N,N-di-tert-butyloxycarbonyl-glycine N'-methoxy-N'-methylamide

J. Lubkowski, L. Lankiewicz and Z. Kosturkiewicz



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Acta Cryst. (1992). C48, 1619-1622    [doi:10.1107/S0108270192000209]

Structure of ethyl 2-(2-amino-3-ethoxycarbonyl-4H-chromen-4-yl)-2-cyanoacetate

M. K. Kokila, K. A. Nirmala, Puttaraja, M. V. Kulkarni and N. C. Shivaprakash



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Acta Cryst. (1992). C48, 1622-1624    [doi:10.1107/S0108270192000738]

A chiral N-crontonyloxazolidinone Diels-Alder adduct

R. E. Marsh, W. P. Schaefer, P. J. Kukkola and A. G. Myers



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Acta Cryst. (1992). C48, 1624-1626    [doi:10.1107/S0108270192001215]

Structure of 1,2,3,5,6,7-hexahydro-1,5:3,7-dimethano-4-benzoxonin-3,5-diol monohydrate

R. Bishop, D. C. Craig and M. L. Scudder



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Acta Cryst. (1992). C48, 1627-1630    [doi:10.1107/S0108270192001446]

Crystal structure of a calcium channel antagonist: 4-(2,4-dichlorophenyl)-N,N,N',N'-tetraethyl-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxamide

S. Mehdi and K. Ravikumar



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Acta Cryst. (1992). C48, 1630-1633    [doi:10.1107/S0108270192000994]

Structure of 5[beta],10[alpha],10[beta]-triethylthebaine hydrochloride

R. H. Woudenberg, T. S. Lie, H. van Koningsveld and L. Maat



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Acta Cryst. (1992). C48, 1633-1635    [doi:10.1107/S0108270192001458]

Acenaphtho[1,2-a]acenaphthylene at 178 K

P. G. Jones, P. Bubenitschek, G. M. Sheldrick and G. Dyker



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Acta Cryst. (1992). C48, 1635-1637    [doi:10.1107/S0108270192001471]

Structure of racemic (±)-6,8-dimethyl-6,12-methano-6H,12H,13H-[1]benzopyran[4,3-d][1,3]benzodioxocin-13-one

E. J. Valente, G. Ruggiero and D. S. Eggleston



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Acta Cryst. (1992). C48, 1638-1641    [doi:10.1107/S010827019200101X]

Synthesis and structure of the picrate salt of 2,2'-bis[2N-(1,1,3,3-tetramethylguanidino)]biphenyl

P. Pruszynski, K. T. Leffek, B. Borecka and T. S. Cameron



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Acta Cryst. (1992). C48, 1641-1645    [doi:10.1107/S0108270192001185]

Structures of 1,1'-dicyanobicyclopentyl, 1,1'-dicyanobicyclohexyl and 1,1'-dicyanobicycloheptyl

L. L. Koh, H. H. Huang and K. Y. Sim



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Acta Cryst. (1992). C48, 1645-1648    [doi:10.1107/S0108270192001070]

Structure of N-tert-butyloxycarbonyl-[alpha]-aminoisobutyryl-DL-pipecolyl-[alpha]-aminoisobutyric acid methyl ester

R. Bardi, A. M. Piazzesi, M. Crisma, C. Toniolo, M. Sukumar and P. Balaram


short format


inorganic compounds



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Acta Cryst. (1992). C48, 1648-1650    [doi:10.1107/S0108270192001173]

Structure of tetrachlorophosphonium hexafluoroantimonate

H. Preut, D. Lennhoff and R. Minkwitz



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Acta Cryst. (1992). C48, 1650-1652    [doi:10.1107/S0108270192000611]

Structure of aluminium disodium trihydrogenbis(diphosphate)

S. Galí, A. Cárdenas, K. Byrappa and G. S. Gopalakrishna


metal-organic compounds



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Acta Cryst. (1992). C48, 1652-1654    [doi:10.1107/S0108270192000635]

Structural investigations of nickel(II) complexes. X. Tris(3,5-dimethylpiperidine)bis(isothiocyanato)nickel(II), [Ni(NCS)2(3,5-diMepip)3]

M. Koman, E. Jóna and E. Durcanská



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Acta Cryst. (1992). C48, 1654-1655    [doi:10.1107/S0108270192000647]

Structure of a dinuclear nickel compound, Ni2(PPh3)2(SC3H6S)2

R. Cao, Z. Huang, X. Lei, B. Kang, M. Hong and H. Liu



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Acta Cryst. (1992). C48, 1655-1657    [doi:10.1107/S0108270192000684]

Structure of the condensation product formed by pyrrolidine, acetonitrile and copper(I) iodide

X. Bao and E. M. Holt



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Acta Cryst. (1992). C48, 1657-1658    [doi:10.1107/S0108270192000945]

Structure of triphenyltin glyoxalate O-methyloxime

K. M. Lo, S. W. Ng, C. Wei and V. G. Kumar Das



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Acta Cryst. (1992). C48, 1658-1660    [doi:10.1107/S0108270192001240]

Structure of [IrCl2(CO)(PEt3)2(SOCl)]

A. J. Blake, R. W. Cockman and E. A. V. Ebsworth



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Acta Cryst. (1992). C48, 1660-1661    [doi:10.1107/S0108270192001689]

Structure of pentakis(N,N-dimethylformamide)dioxouranium(VI) tetrafluoroborate

L. Deshayes, N. Keller, M. Lance, M. Nierlich and D. Vigner



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Acta Cryst. (1992). C48, 1661-1663    [doi:10.1107/S010827019200132X]

Structure of [1,3-bis(diphenylphosphino)propane]([eta]5-cyclopentadienyl)hydridoruthenium(II)

S. A. Litster, A. D. Redhouse and S. J. Simpson



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Acta Cryst. (1992). C48, 1663-1665    [doi:10.1107/S0108270191015111]

Rhodium(I)-cyclooctadiene (cod) complexes with the N-donor ligands 1,8-diazabicyclo[5.4.0]undec-7-ene (dbu) and 1,5-diazabicyclo[4.3.0]non-5-ene (dbn)

U. Flörke, U. Ortmann and H.-J. Haupt



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Acta Cryst. (1992). C48, 1665-1666    [doi:10.1107/S0108270192001896]

Structure of chlorodioxotetrakis(tetrahydrofuran)uranium(VI) pentachloro(tetrahydrofuran)uranate(IV)

M. Noltemeyer, J. W. Gilje and H. W. Roesky



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Acta Cryst. (1992). C48, 1667-1669    [doi:10.1107/S0108270192001574]

Structure of diaqua[tris(3-aminopropyl)amine]cobalt(III) aquatetrakis(trifluoromethanesulfonato)sodate(I) monohydrate

G. H. Rawji and V. M. Lynch


organic compounds



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Acta Cryst. (1992). C48, 1670-1671    [doi:10.1107/S010827019101497X]

Structure of tris(phenylseleno)phosphine

N. L. Keder, R. K. Shibao and H. Eckert



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Acta Cryst. (1992). C48, 1671-1673    [doi:10.1107/S0108270191015068]

Structure of 3,3-bis(2-imidazolyl)propionic acid monohydrate

B. Gimeno, L. Soto, A. Sancho, F. Dahan and J.-P. Legros



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Acta Cryst. (1992). C48, 1673-1675    [doi:10.1107/S0108270191015147]

Structure of tert-butylammonium hexachlorotellurate(IV)

H. Ishida and S. Kashino



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Acta Cryst. (1992). C48, 1675-1677    [doi:10.1107/S0108270192000453]

1,3,7,9-Tetra-tert-butyl-2,2,8,8-tetramethyl-5,10-diphenyl-1,3,5,7,9,10-hexaaza-2,8-disila-4,6-digermadispiro[3.1.3.1]decane

H. Preut, B. Klein and W. P. Neumann



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Acta Cryst. (1992). C48, 1677-1679    [doi:10.1107/S010827019200043X]

Structure of a twisted styrylbenzothiazole, 2-([alpha]-acetoxy-2-chloro-5-nitrostyryl)benzothiazole

J. A. Muir, O. Cox, L. A. Bernard and M. M. Muir



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Acta Cryst. (1992). C48, 1679-1680    [doi:10.1107/S0108270192000696]

Structure of 3-nitrato-1-nitroazetidine

R. Gilardi, C. George and J. L. Flippen-Anderson



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Acta Cryst. (1992). C48, 1680-1681    [doi:10.1107/S0108270192000702]

Structure of 1,1,3,3-tetranitrocyclobutane

R. Gilardi, C. George and J. L. Flippen-Anderson



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Acta Cryst. (1992). C48, 1682-1683    [doi:10.1107/S010827019100375X]

Structure of 3-amino-5-nitro-1,2,4-triazole

E. Garcia and K.-Y. Lee



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Acta Cryst. (1992). C48, 1683-1685    [doi:10.1107/S0108270191003773]

Structure of the hydrazinium salt of 3-amino-5-nitro-1,2,4-triazole

E. Garcia, K.-Y. Lee and C. B. Storm



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Acta Cryst. (1992). C48, 1685-1686    [doi:10.1107/S0108270192000775]

Structure of 4,5-di-O-acetyl-6-S-acetyl-2,3-di-S-ethyl-2,3,6-trithio-D-allose diethyl dithioacetal

V. Divjakovic, D. Miljkovic, S. Lajsic and U. Klement



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Acta Cryst. (1992). C48, 1687-1689    [doi:10.1107/S0108270192001197]

Structure of 5-(2-hydroxyethoxy)-6-[1-(4-methoxyphenyl)ethyl]-1,3-benzodioxole

F. V. Sicheri, W. B. Derry, R. S. Gupta and D. S.-C. Yang



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Acta Cryst. (1992). C48, 1689-1690    [doi:10.1107/S0108270192000878]

syn-2-Benzyl-1,3-dithiane 1-oxide

J. Barkley, M. M. Harding, B. M. Kariuki, E. S. Namwindwa and P. C. B. Page



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Acta Cryst. (1992). C48, 1690-1692    [doi:10.1107/S0108270192001227]

Structure of the 1:1 complex formed by triphenylphosphine oxide and 4-nitrophenol

R. M. Fuquen and J. R. Lechat



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Acta Cryst. (1992). C48, 1692-1694    [doi:10.1107/S0108270192001057]

Structure of 2,5:3,4-dianhydro-D-altritol

J. G. Garcia, R. J. Voll, F. R. Fronczek and E. S. Younathan



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Acta Cryst. (1992). C48, 1694-1695    [doi:10.1107/S0108270192000957]

Structure of 1H-isoindole-1,3(2H)-dione (phthalimide)

S. W. Ng



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Acta Cryst. (1992). C48, 1695-1698    [doi:10.1107/S0108270192001033]

Structure of a densely oxygenated carbocycle

K. A. Abboud, E. J. Enholm and A. Trivellas



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Acta Cryst. (1992). C48, 1698-1699    [doi:10.1107/S0108270192001367]

Structure of 3-methoxytyramine perchlorate

N. Okabe and S. Mori



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Acta Cryst. (1992). C48, 1699-1701    [doi:10.1107/S0108270192000933]

Structure of an acetone solvate of 7,9-diacetyl-2,5-dinitro-2,5,7,9-tetraazabicyclo[4.3.0]nonane

C. George, R. Gilardi and J. L. Flippen-Anderson



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Acta Cryst. (1992). C48, 1701-1703    [doi:10.1107/S0108270192001586]

2-Chloro-2'-methoxyacetophenone and 2-chloro-4'-methoxyacetophenone

K. L. Evans, F. R. Fronczek and R. D. Gandour



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Acta Cryst. (1992). C48, 1703-1705    [doi:10.1107/S0108270192001045]

Structure of a tricyclic subunit of manzamine A

V. M. Lynch, Y. Liao, S. F. Martin and B. E. Davis



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Acta Cryst. (1992). C48, 1705-1707    [doi:10.1107/S0108270192001380]

Structure of mepirizole.H(mepirizole) hexafluorophosphate

L. Soto, J. Garcia-Lozano, M. Martinez, F. Dahan and J.-P. Legros


regular structural papers


inorganic compounds



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Acta Cryst. (1992). C48, 1708-1709    [doi:10.1107/S0108270192005559]

Pentacarbonyliodomanganese(I)

A. J. Blake, B. F. G. Johnson and A. Sieker



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Acta Cryst. (1992). C48, 1709-1710    [doi:10.1107/S010827019200581X]

A new modification of Hg[Mn(CO)5]2

U. Flörke and H.-J. Haupt


organic compounds



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Acta Cryst. (1992). C48, 1710-1712    [doi:10.1107/S010827019200605X]

trans-1,3-Bis(diphenylphosphinoyl)cyclohexane

M. Morooka, T. Hashimoto, H. Maeta, T. Matsumoto, K. Suzuki and S. Ohba



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Acta Cryst. (1992). C48, 1712-1713    [doi:10.1107/S0108270192006437]

Structure of oxatomide monohydrate: an anti-allergic drug

M. L. Raves, J. A. Kanters and J. P. Tollenaere



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Acta Cryst. (1992). C48, 1714-1715    [doi:10.1107/S0108270192005456]

Structure of 6-hydroxyflavone

J. Seetharaman and S. S. Rajan



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Acta Cryst. (1992). C48, 1715-1717    [doi:10.1107/S0108270192006887]

1,4-Dibenzoylbenzene

T. Kolev, H. Preut, P. Bleckmann and I. Juchnovski



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Acta Cryst. (1992). C48, 1717-1718    [doi:10.1107/S0108270192006723]

Structure of 1,4,7,10-tetraazacyclododecane trihydrate

J. H. Reibenspies



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Acta Cryst. (1992). C48, 1718-1720    [doi:10.1107/S0108270192006334]

1-Benzenesulfonyl-3-methyl-2-oxo-2,3-dihydroindol-3-yl acetate

D. A. Grossie and D. M. Ketcha



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Acta Cryst. (1992). C48, 1720-1722    [doi:10.1107/S0108270192005316]

Structure du 2[alpha],3[alpha],7[alpha],13[alpha]-diépoxyhimachalane

A. Chiaroni, C. Riche, A. Benharref, A. Chekroun et J.-P. Lavergne



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Acta Cryst. (1992). C48, 1722-1727    [doi:10.1107/S0108270192005699]

Enantiomerically pure [alpha]-haloketals: structure and conformation of (2'S,4'R,5'R)-dimethyl 2'-halo-1',2',3',4'-tetrahydrospiro[1,3-dioxolane-2,1'-naphthalene]-4,5-dicarboxylates (halo = Cl, Br, I)

S. Ianelli, M. Nardelli, C. Giordano, L. Coppi and A. Restelli



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Acta Cryst. (1992). C48, 1727-1730    [doi:10.1107/S0108270192005328]

Structure and conformation of 1'-phenylindan-2-spiro-4'-piperidin-1-one

S. Ianelli, M. Nardelli, D. Belletti, B. Jamart-Grégoire, H. Forconi and P. Caubère



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Acta Cryst. (1992). C48, 1730-1733    [doi:10.1107/S0108270192005420]

Structure and conformation of cis,anti,cis-4b,4c,8b,9,10,10a-hexahydro-4b-hydroxybenzo[3,4]cyclobuta[1,2-a]biphenylene-4-carbaldehyde

S. Ianelli, M. Nardelli, D. Belletti, B. Jamart-Grégoire, M. A. Zouaoui and P. Caubère



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Acta Cryst. (1992). C48, 1734-1737    [doi:10.1107/S0108270192005912]

Structure and conformation of cis-9a-methoxy-1,2,3,4,4a,9a-hexahydrofluoren-9-one oxime

S. Ianelli, M. Nardelli, D. Belletti, B. Jamart-Grégoire and P. Caubère



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Acta Cryst. (1992). C48, 1737-1739    [doi:10.1107/S0108270192004608]

Structure of a novel carbapenem antibiotic, meropenem

K. Yanagi, Y. Takeuchi and M. Sunagawa


letters to the editor



pdf version free

Acta Cryst. (1992). C48, 1740    [doi:10.1107/S0108270192007169]

Non-conventional settings of crystal structures

K. Lukaszewicz


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