Acta Crystallographica Section C

Crystal Structure Communications

Volume 48, Part 10 (October 1992)



research papers


inorganic compounds



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Acta Cryst. (1992). C48, 1741-1744    [doi:10.1107/S0108270192002099]

Structure of CuZr2(PO4)3 by X-ray and neutron powder diffraction

I. Busserau, M. S. Belkhiria, P. Gravereau, A. Boireau, J. L. Soubeyroux, R. Olazcuaga and G. Le Flem



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Acta Cryst. (1992). C48, 1744-1747    [doi:10.1107/S0108270192002129]

A niobium silicophosphate belonging to the niobium phosphate bronze series: K4Nb8P4SiO34

A. Leclaire, M. M. Borel, J. Chardon, A. Grandin and B. Raveau



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Acta Cryst. (1992). C48, 1747-1749    [doi:10.1107/S0108270192001963]

Structure refinement of the semi-metallic oxide SrTl2O4: a neutron diffraction study

C. Michel, M. Hervieu, V. Caignaert and B. Raveau



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Acta Cryst. (1992). C48, 1749-1751    [doi:10.1107/S0108270192000192]

Redetermination of the structure of potassium tetranitropalladate(II)

A. J. Blake, R. O. Gould, B. F. G. Johnson and E. Parisini


metal-organic compounds



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Acta Cryst. (1992). C48, 1751-1754    [doi:10.1107/S0108270192001860]

Structure of bis(thiourea)gold(I) bromide, [Au{SC(NH2)2}2]Br

L. C. Porter, J. P. Fackler Jnr, J. Costamagna and R. Schmidt



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Acta Cryst. (1992). C48, 1754-1756    [doi:10.1107/S0108270192000040]

Structures of chromium(III) cyclam complexes. 3. Structure of trans-dichloro(1,4,8,11-tetraazacyclotetradecane)chromium(III) bromide

C. G. Dealwis, R. W. Janes, R. A. Palmer, J. N. Lisgarten, D. Maes, C. D. Flint and D. M. Gazi



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Acta Cryst. (1992). C48, 1756-1759    [doi:10.1107/S0108270192000039]

Structures of chromium(III) cyclam complexes. 4. Structure of trans-bromochloro(1,4,8,11-tetraazacyclotetradecane)chromium(III) bromide displaying structural enantiomorphism with the dibromo complex

T. K. Chattopadhyay, R. A. Palmer, J. N. Lisgarten, L. Wyns and D. M. Gazi



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Acta Cryst. (1992). C48, 1759-1761    [doi:10.1107/S0108270192001744]

Structure of a tetrahedral niobium oxo compound [Nb(OC6H3Ph2-2,6)3(O)]

J. S. Yu, P. E. Fanwick and I. P. Rothwell



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Acta Cryst. (1992). C48, 1761-1764    [doi:10.1107/S0108270192001975]

Structure of bis(hexafluoroacetylacetonato)bis(triphenylphosphine oxide)nickel(II)

J. R. Polam and L. C. Porter



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Acta Cryst. (1992). C48, 1764-1767    [doi:10.1107/S0108270192001884]

Structure of [mu]-dioxane-bis[(ethanol)bis(hexafluoroacetylacetonato)nickel(II)]

R. R. Romero, F. Cervantes-Lee and L. C. Porter



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Acta Cryst. (1992). C48, 1767-1771    [doi:10.1107/S0108270192002397]

Structures of racemic and meso (5,7,7,12,14,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene)nickel(II) perchlorate

D. J. Szalda and E. Fujita



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Acta Cryst. (1992). C48, 1771-1773    [doi:10.1107/S0108270192002038]

Structure of a permethylcyclopentadienyl-[mu]-tetramethylcyclopentadienylmethylene scandium dimer

S. Hajela, W. P. Schaefer and J. E. Bercaw



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Acta Cryst. (1992). C48, 1773-1776    [doi:10.1107/S0108270192001987]

A silicon-bridged bis(substituted Cp) yttrium complex

R. E. Marsh, W. P. Schaefer, E. B. Coughlin and J. E. Bercaw



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Acta Cryst. (1992). C48, 1776-1778    [doi:10.1107/S0108270192002026]

A bis(pyrazolyl)(bipyridyl)platinum complex

W. P. Schaefer, W. B. Connick, V. M. Miskowski and H. B. Gray



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Acta Cryst. (1992). C48, 1779-1782    [doi:10.1107/S0108270192002671]

Tetrabromo(1,4,7,10,13,16-hexathiacyclooctadecane)dimercury(II)

M. Herceg and D. Matkovic-Calogovic



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Acta Cryst. (1992). C48, 1782-1785    [doi:10.1107/S010827019200235X]

Structure of [Ca(triethylene glycol)2]Cl2.4H2O

R. D. Rogers and A. H. Bond



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Acta Cryst. (1992). C48, 1785-1788    [doi:10.1107/S0108270192000568]

Mixed chelate complexes. III. Structures of (L-alaninato)(aqua)(2,2'-bipyridine)copper(II) nitrate monohydrate and aqua(2,2'-bipyridine)(L-tyrosinato)copper(II) chloride trihydrate

X. Solans, L. Ruíz-Ramírez, A. Martínez, L. Gasque and R. Moreno-Esparza


organic compounds



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Acta Cryst. (1992). C48, 1788-1791    [doi:10.1107/S0108270192001537]

4-Iodo-2,2,6,6-tetramethylheptane-3,5-dione

S. Sans-Lenain, A. Reynes and A. Gleizes



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Acta Cryst. (1992). C48, 1791-1794    [doi:10.1107/S0108270192001550]

Stereochemical investigation of 2,3,4,6-tetra-O-acetyl-1-S-benzhydroximoyl-[alpha]-D-glucopyranose

V. Durier, H. Driguez, P. Rollin, E. Duee and G. Buisson



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Acta Cryst. (1992). C48, 1794-1798    [doi:10.1107/S0108270192001604]

Structures and absolute configurations of enantiomers of two local anaesthetics: (2S)-1-methyl- and (2R)-1-butyl-2',6'-pipecoloxylidide hydrochlorides

I. Csöregh



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Acta Cryst. (1992). C48, 1798-1801    [doi:10.1107/S0108270192001719]

Structure of 3-(p-chlorophenyl)-1-phenyl-1,3-propanedione enol

P. Gilli, V. Ferretti, V. Bertolasi and G. Gilli



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Acta Cryst. (1992). C48, 1801-1804    [doi:10.1107/S0108270192001641]

A urea with non-planar nitrogen-bonding geometry

A. C. Regan, J. D. Wallis and D. C. Povey



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Acta Cryst. (1992). C48, 1804-1806    [doi:10.1107/S0108270192001562]

Structure du chlorhydrate de (1R,2S)(3-hydroxy-3-m-hydroxyphényl-2-propyl)triméthylammonium monohydrate

L. Dupont, O. Dideberg, M. C. Pardon et J. L. Piette



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Acta Cryst. (1992). C48, 1806-1808    [doi:10.1107/S0108270192001823]

Structure of the lactonic adduct from 2-hydroxypinan-3-one and glycine

J. Lapasset, A. El Marini, M. L. Roumestant, Y. Vidal and P. Viallefont



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Acta Cryst. (1992). C48, 1808-1810    [doi:10.1107/S0108270192002002]

Structure du 2,3-dihydro-3-(2-hydroxyéthylthio)benzo[b]thiophène 1-oxyde, C10H12O2S2

D. Ginderow, J.-P. Mornon, I. Erdelmeier, P. Dansette et D. Mansuy



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Acta Cryst. (1992). C48, 1810-1815    [doi:10.1107/S0108270192001999]

Structure and conformation of photosynthetic pigments and related compounds. 4. Two crystal forms of a chlorin - rhodochlorin XV dimethyl ester

M. O. Senge, K. Ruhlandt-Senge and K. M. Smith



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Acta Cryst. (1992). C48, 1815-1818    [doi:10.1107/S0108270192002014]

Structure of sp-9-hydroxy-9-pivaloylfluorene, product of base-catalyzed autoxidation of ap-9-pivaloylfluorene

C. Y. Meyers, J. L. Tunnell, P. D. Robinson, D. H. Hua and S. Saha



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Acta Cryst. (1992). C48, 1819-1821    [doi:10.1107/S0108270192004463]

Structure of (E)-4-benzoylbutyramide oxime

J. K. Maurin, I. C. Paul and D. Y. Curtin



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Acta Cryst. (1992). C48, 1821-1823    [doi:10.1107/S010827019200458X]

Structure of 3-benzoylbenzamide oxime

J. K. Maurin, I. C. Paul and D. Y. Curtin



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Acta Cryst. (1992). C48, 1823-1827    [doi:10.1107/S0108270192001859]

Structures of two bufadienolides: telocinobufagin (3[beta],5[beta]-dihydroxy-5[beta],14[beta]-bufa-20,22-dienolide) monohydrate and 14[alpha]-artebufogenin (3[beta]-hydroxy-15-oxo-5[beta],14[alpha]-bufa-20,22-dienolide)

G. Argay, A. Kálmán, B. Ribár, D. Zivanov-Stakic and S. Vladimirov



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Acta Cryst. (1992). C48, 1827-1830    [doi:10.1107/S0108270192001677]

Structure of the antipsychotic drug 3-{2-[4-(6-fluoro-1,2-benzisoxazol-3-yl)-1-piperidinyl]ethyl}-2,9-dimethyl-4H-pyrido[1,2-a]pyrimidin-4-one (ocaperidone)

W. I. Jottier, H. L. De Winter, O. M. Peeters, N. M. Blaton and C. J. De Ranter


short format


inorganic compounds



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Acta Cryst. (1992). C48, 1831-1832    [doi:10.1107/S0108270192002270]

Refinement of the structure of boroleucite, K(BSi2O6)

D. Miklos, L. Smrcok, S. Durovic, D. Gyepesová and M. Handlovic


metal-organic compounds



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Acta Cryst. (1992). C48, 1832-1834    [doi:10.1107/S0108270192002191]

Carbonyl(1-methyl-[eta]5-cyclopentadienyl)bis(triphenylphosphine)manganese dichloromethane solvate

A. L. Rheingold, C. B. White, B. S. Haggerty, M. R. Terry and G. L. Geoffroy



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Acta Cryst. (1992). C48, 1834-1835    [doi:10.1107/S0108270192001793]

Structure of [2-(chlorodimethylstannyl)ethyl]diphenylphosphine selenide

H. Preut, B. Godry and T. N. Mitchell



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Acta Cryst. (1992). C48, 1836-1837    [doi:10.1107/S0108270192001872]

Dichlorotetrakis(pyridine)nickel(II)

R. E. Bachman, K. H. Whitmire, S. Mandal and P. K. Bharadwaj



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Acta Cryst. (1992). C48, 1837-1839    [doi:10.1107/S0108270192002385]

Structure of the [mu]-azido-dichloro([eta]5-methylcyclopentadienyl)titanium(IV) dimer

K. Kirschbaum and D. M. Giolando



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Acta Cryst. (1992). C48, 1839-1841    [doi:10.1107/S0108270192001306]

Structure of triphenyltin chloride-triphenylphosphine oxide (1/1) complex

S. W. Ng and V. G. Kumar Das



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Acta Cryst. (1992). C48, 1841-1842    [doi:10.1107/S0108270192002105]

Carbonatobis(1,10-phenanthroline)cobalt(III) perchlorate

C. A. McAuliffe, R. G. Pritchard, M. R. Bermejo, A. Garcia-Vazquez, A. Macias, J. Sanmartín, J. Romero and A. Sousa



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Acta Cryst. (1992). C48, 1843-1844    [doi:10.1107/S0108270192002488]

Structure of bis(trifluoracetamidinium) di-[mu]-chloro-hexachlorodioxodimolybdate(V)

R. Herbst-Irmer and E. Egert



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Acta Cryst. (1992). C48, 1844-1846    [doi:10.1107/S0108270192002439]

Tri-[mu]-chloro-bis(1,4,7-trithiacyclononane)dinickel(II) tetrafluoroborate acetonitrile solvate

A. J. Blake, M. A. Halcrow and M. Schröder


organic compounds



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Acta Cryst. (1992). C48, 1846-1848    [doi:10.1107/S0108270192001161]

Structure of ethyl 8,9-dimethoxy-3-(4-methoxyphenyl)-10b-methyl-1-phenyl-4,5,6,10b-tetrahydro-1,2,4-triazolo[3,4-a]isoquinoline-5-carboxylate

F. Theobald, N. Rodier, K. Moustaid and B. Laude



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Acta Cryst. (1992). C48, 1848-1851    [doi:10.1107/S0108270192001239]

Ethanol complex of 1,3-diethoxy-p-tert-butylcalix[4]arene

K.-E. Bugge, W. Verboom, D. N. Reinhoudt and S. Harkema



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Acta Cryst. (1992). C48, 1851-1853    [doi:10.1107/S0108270192001021]

Structure du 8-chloro-11-(4-méthylpipérazin-1-yl)dibenzo[b,f]-1,4-thiazépine

L. Dupont, O. Dideberg, J. F. Liégeois et J. Delarge



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Acta Cryst. (1992). C48, 1853-1855    [doi:10.1107/S0108270191013410]

Structure of xindongnin B

J.-L. Wang, L.-J. Zhang, F.-M. Miao, H.-D. Sun and Y.-H. Gong



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Acta Cryst. (1992). C48, 1855-1857    [doi:10.1107/S0108270192001409]

Absolute configuration of (-)-[alpha]-acetylmethadol hydrochloride

J. L. Flippen-Anderson and C. F. George



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Acta Cryst. (1992). C48, 1857-1859    [doi:10.1107/S0108270192001598]

Structure of 3,6-diacetyl-8-benzoylantakyatriol

P. W. Baures, M. Miski and D. S. Eggleston



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Acta Cryst. (1992). C48, 1859-1862    [doi:10.1107/S0108270192000623]

Structure of 7-diethylamino-4-trifluoromethylcoumarin

K. Chinnakali, K. Sivakumar and S. Natarajan



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Acta Cryst. (1992). C48, 1862-1864    [doi:10.1107/S0108270191014658]

Structure of 3-tert-butyl-1-[(4-chlorophenyl)sulfonyl]-1-methylurea

M. Ghosh, A. K. Das, S. K. Mazumdar and G. Bocelli



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Acta Cryst. (1992). C48, 1864-1866    [doi:10.1107/S0108270192001951]

Structure of corydaline

B. Ribár, D. Lazar, P. Radivojevic, P. Engel, O. Gasic and I. Kanyó



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Acta Cryst. (1992). C48, 1866-1868    [doi:10.1107/S0108270192002051]

Structure of cis,cis-4,6-diphenyl-2-(2-propenyl)-1,3-dioxa-2-phosphorinane 2-oxide

D. H. Hua, D. Roche, S. N. Bharathi, X. Wu and P. D. Robinson



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Acta Cryst. (1992). C48, 1868-1870    [doi:10.1107/S0108270192001902]

Structure of a p-nitrobenzoyl praziquantel analogue

R. A. Toscano, M. Rubio, R. Cetina and B. M. Pérez-Ibarra



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Acta Cryst. (1992). C48, 1870-1872    [doi:10.1107/S010827019200204X]

Structure of 10-acetyloxy-10-methyl-9(10H)-anthracenone

T.-Y. Lin, Y.-L. Mao and C.-M. Chuo



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Acta Cryst. (1992). C48, 1872-1873    [doi:10.1107/S0108270192001707]

Structure of 8,10-diacetyl-2,4,6-trinitro-2,4,6,8,10-pentaazabicyclo[5.3.0]decane

R. Gilardi, J. L. Flippen-Anderson and C. F. George



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Acta Cryst. (1992). C48, 1874-1876    [doi:10.1107/S0108270192002282]

Structure of a bicyclic guanidinium nitrite salt

A. Meetsma, E. van Aken and H. Wynberg



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Acta Cryst. (1992). C48, 1876-1878    [doi:10.1107/S0108270192002427]

Structure of 1,1-dibromo-2-phenylseleno-3-p-tolylcyclopropane

J. Zukerman-Schpector, E. E. Castellano, J. V. Comasseto and H. A. Stefani



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Acta Cryst. (1992). C48, 1878-1880    [doi:10.1107/S0108270192002336]

Structure of a chiral intermediate in the synthesis of (+)-19-epiajmalicine

V. M. Lynch, J. W. Corbett, S. F. Martin and B. E. Davis



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Acta Cryst. (1992). C48, 1880-1881    [doi:10.1107/S0108270192002324]

2-Menthyl (2-hydroxyphenyl)glycolate

G. Bocelli and A. Cantoni



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Acta Cryst. (1992). C48, 1882-1884    [doi:10.1107/S0108270192002312]

Structure of tris(5-acetyl-3-thienyl)methane-n-hexane (3/1) inclusion compound

H. M. Roos and J. L. M. Dillen



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Acta Cryst. (1992). C48, 1884-1886    [doi:10.1107/S0108270192001756]

N,N-Diethyl-6-(hydroxyimino)-[alpha]-methyl-1-cyclohexene-1-acetamide

P. J. S. S. van Eijk, W. Verboom, D. N. Reinhoudt and S. Harkema



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Acta Cryst. (1992). C48, 1886-1887    [doi:10.1107/S0108270192001768]

N,N-Diethyl-2-[2-(hydroxyimino)cyclohexylidine]propanamide

P. J. S. S. van Eijk, W. Verboom, D. N. Reinhoudt and S. Harkema


regular structural papers


metal-organic compounds



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Acta Cryst. (1992). C48, 1888-1894    [doi:10.1107/S0108270192005808]

Dimeric nickel(II) carboxylates and a silanecarboxylate: [Ni(Me3CCOO)2(2,5-lutidine)]2, [Ni(MePh2CCOO)2(quinoline)]2.2CHCl3, [Ni(Me2PhCCOO)2(quinoline)]2, [Ni(Me3CCOO)2(2-ethylpyridine)]2, [Ni(Me3CCOO)2(2-picoline)]2 and [Ni(MePh2SiCOO)2(Ph3P)]2

M. Morooka, S. Ohba, M. Nakashima, T. Tokii, Y. Muto, M. Kato and O. W. Steward



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Acta Cryst. (1992). C48, 1894-1896    [doi:10.1107/S0108270192007236]

Structure of [2-(fluorodimethylstannyl)ethyl]diphenylphosphine oxide

H. Preut, B. Godry and T. Mitchell



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Acta Cryst. (1992). C48, 1896-1898    [doi:10.1107/S0108270192006103]

Structure of a dichromium(II) complex with bridging betaine ligands, [Cr2(O2CCH2NMe3)4(OH2)2][ZnCl4]2.2H2O

W. Clegg, B. P. Straughan and A. R. Yusoff


organic compounds



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Acta Cryst. (1992). C48, 1898-1900    [doi:10.1107/S0108270192005997]

Structure of 2-[(4-methylphenylimino)methyl]-1-nitrobenzene

G.-Y. Yeap, H.-K. Fun, S.-B. Teo and S.-G. Teoh



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Acta Cryst. (1992). C48, 1900-1902    [doi:10.1107/S0108270192006449]

Structure of an oxonium salt crystal complex

O. Simonsen



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Acta Cryst. (1992). C48, 1902-1904    [doi:10.1107/S0108270192006425]

Structure of a polydentate alkoxide ligand, cis-tetrahydroxytetramethylcyclobutane

M. M. Olmstead, J. L. Hobbs and R. P. Planalp



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Acta Cryst. (1992). C48, 1904-1906    [doi:10.1107/S0108270192006127]

Structure of the allene C39H32P22+.2CF3O3S-

A. Bram, H. Burzlaff, D. Hadawi and H.-J. Bestmann



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Acta Cryst. (1992). C48, 1906-1908    [doi:10.1107/S0108270192005754]

2S-[2[alpha],3[alpha],3a[beta],6[beta](R*),7[alpha],7a[alpha]]}-6-(3-Benzyloxy-2-propyl)-2-hydroxy-2,3,7-trimethylhexahydro-4H-furo[3,2-c]pyran-4-one, a rearrangement product of pyranone derivatives in the tirandamycin A series

M. Parvez, M.-T. Lin and P. DeShong



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Acta Cryst. (1992). C48, 1908-1909    [doi:10.1107/S0108270192007340]

1,8-Dichloro-5-oxa-10-azatricyclo[5.3.1.03,8]undecan-9-one: structure of a hydrolysed Diels-Alder addition product

M. G. Barlow, R. G. Pritchard, L. Sibous and A. E. Tipping



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Acta Cryst. (1992). C48, 1909-1911    [doi:10.1107/S0108270192008199]

Oxonium (R)-O-acetylmandelate

G. Ferguson, J. F. Gallagher, R. Fullwood and D. Parker


short communications



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Acta Cryst. (1992). C48, 1912    [doi:10.1107/S0108270192007984]

Structure of an adduct between diammonium dihydrogendiphosphate and telluric acid: 2(NH4)2H2P2O7.Te(OH)6. Erratum

M. T. Averbuch-Pouchot and A. Durif


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