Acta Crystallographica Section C

Crystal Structure Communications

Volume 48, Part 11 (November 1992)



research papers


inorganic compounds



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Acta Cryst. (1992). C48, 1913-1915    [doi:10.1107/S0108270192002300]

Structure of PbV2P2O10

A. Grandin, J. Chardon, M. M. Borel, A. Leclaire and B. Raveau



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Acta Cryst. (1992). C48, 1915-1917    [doi:10.1107/S0108270192003214]

Structure of La4Mo2O11 containing isolated Mo2O10 cluster units

P. Gall and P. Gougeon



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Acta Cryst. (1992). C48, 1917-1920    [doi:10.1107/S0108270192002919]

Structure of potassium hexarhenium nonabromide pentasulfide: KRe6S5Br9

A. Slougui, A. Perrin and M. Sergent


metal-organic compounds



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Acta Cryst. (1992). C48, 1920-1923    [doi:10.1107/S0108270192002750]

Structures of some quasi-two-dimensional molecular conductors. I. Structure of [kappa]-tetrakis(3,4-methylenedithio-2,2',5,5'-tetrathiafulvalen)ium tetracyanoplatinate dihydrate: [kappa]-(MDTTTF)4Pt(CN)4(H2O)2

M. Fettouhi, L. Ouahab, D. Grandjean, G. Mousdis and P. Delhaes



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Acta Cryst. (1992). C48, 1923-1926    [doi:10.1107/S0108270192002634]

Structure of bis[[mu]-4-amino-3,5-bis(aminomethyl)-1,2,4-triazole-N',N1,N2,N'']-bis[diaquacopper(II)] bis(sulfate) tetrahydrate

P. J. van Koningsbruggen, J. G. Haasnoot, R. A. G. de Graaff, J. Reedijk and S. Slingerland



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Acta Cryst. (1992). C48, 1926-1929    [doi:10.1107/S0108270192003056]

Structure of the hydrogen-bond-rich dinickel(II) complex of N,N',N'',N'''-tetrakis(2-aminoethyl)-1,1,2,2-ethanetetraamide

S. Zhu, Q. Luo, M. Shen and L. Huang



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Acta Cryst. (1992). C48, 1929-1931    [doi:10.1107/S0108270191000550]

Etude structurale du dihydrate de l'hexafluorostannate de triméthylammonium

A. Taha, B. Liautard et W. Granier



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Acta Cryst. (1992). C48, 1931-1933    [doi:10.1107/S0108270192003354]

Structure of trans-diiodobis(methyl phenyl telluride)platinum(II)

W. Levason, M. Webster and C. J. Mitchell



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Acta Cryst. (1992). C48, 1933-1936    [doi:10.1107/S0108270192003263]

Structure of copper(II) salicylates: bis(3-pyridylmethanol)bis(salicylato)copper(II)

N. N. Hoang, F. Valach, L. Macásková and M. Melník



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Acta Cryst. (1992). C48, 1936-1939    [doi:10.1107/S0108270192003457]

Structure of a one-dimensional Br-bridged PtII-PtIV mixed-valence complex, catena-poly[bis(ethylenediamine)platinum(II,IV)-[mu]-bromo bis(hydrogensulfate)]

N. Matsushita, T. Taga and I. Tsujikawa


organic compounds



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Acta Cryst. (1992). C48, 1940-1945    [doi:10.1107/S0108270192001811]

Effect of the protonation and of the ortho substitution on the structure of aryliminophosphoranes

A. L. Llamas-Saiz, C. Foces-Foces, J. Elguero, P. Molina, M. Alajarín and A. Vidal



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Acta Cryst. (1992). C48, 1945-1948    [doi:10.1107/S010827019200221X]

Methyl 2,4-dideoxy-6,7,8,9,10-penta-O-acetyl-D-glycero-[alpha]-D-gluco-decapyranosid-3-ulose

Z. Ciunik, P. Luger, H.-W. Hagedorn and R. Brossmer



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Acta Cryst. (1992). C48, 1948-1951    [doi:10.1107/S0108270192002233]

Structure of an anti-aldol addition product of benzaldehyde and a pseudoephedrine-derived O-silyl ketene N,O-acetal

R. E. Marsh, W. P. Schaefer, K. L. Widdowson and A. G. Myers



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Acta Cryst. (1992). C48, 1951-1954    [doi:10.1107/S0108270192002257]

Structure of thiamine bromide sesquihydrate

N.-H. Hu and S.-L. Zhang



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Acta Cryst. (1992). C48, 1954-1957    [doi:10.1107/S010827019200252X]

Structure of (17[alpha])-androstano[3,4-c][1,2,5]oxadiazole-17-ol (HS963)

D. Maes, P. Fiddelaers, L. Wyns, J. Lisgarten, D. Lisgarten and R. Palmer



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Acta Cryst. (1992). C48, 1957-1960    [doi:10.1107/S0108270192002294]

Structure of an adenine-hydrogen peroxide adduct

M. A. Serra, B. K. Dorner and M. E. Silver



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Acta Cryst. (1992). C48, 1960-1965    [doi:10.1107/S0108270192002361]

Structure of p-hydroxybenzoic acid and p-hydroxybenzoic acid-acetone complex (2/1)

E. A. Heath, P. Singh and Y. Ebisuzaki



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Acta Cryst. (1992). C48, 1965-1968    [doi:10.1107/S0108270192001690]

Structure of the white-line-inducing principle isolated from Pseudomonas reactans

F. Han, R. J. Mortishire-Smith, P. B. Rainey and D. H. Williams



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Acta Cryst. (1992). C48, 1969-1971    [doi:10.1107/S0108270192002245]

Structures of two crystal forms of the host-guest complex between trans-3,3'-bis(diphenylhydroxymethyl)azobenzene and acetone

K. Hamada, M. Oh-hira, T. Fujiwara and F. Toda



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Acta Cryst. (1992). C48, 1971-1975    [doi:10.1107/S0108270192003226]

Structure of 2,3-naphthalenedicarboxylic acid

L. J. Fitzgerald and R. E. Gerkin



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Acta Cryst. (1992). C48, 1975-1980    [doi:10.1107/S0108270192002373]

Structure of 9-epiquinine hydrochloride dihydrate versus antimalarial activity

J. M. Karle and I. L. Karle



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Acta Cryst. (1992). C48, 1980-1981    [doi:10.1107/S0108270192002154]

Structure of pentacyclo[8.5.0.02,7.04,13.05,1]pentadeca-8,14-diene-3,6-dione

M. Nethaji, V. Pattabhi and S. Harikrishna Reddy



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Acta Cryst. (1992). C48, 1982-1984    [doi:10.1107/S0108270192003445]

Structure of the charge-transfer complex of (DBTTF)(BTDA-TCNQ)

K. Iwasaki, T. Ida, A. Kawamoto, A. Ugawa, Y. Yamashita, K. Yakushi and T. Suzuki



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Acta Cryst. (1992). C48, 1985-1988    [doi:10.1107/S0108270192003329]

Structures of the isomeric triazene 1-oxides 3-(4-ethoxycarbonylphenyl)-1-methyltriazene 1-oxide (1) and 3-(2-ethoxycarbonylphenyl)-1-methyltriazene 1-oxide (2)

K. Vaughan, L. M. Cameron, S. Christie and M. J. Zaworotko



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Acta Cryst. (1992). C48, 1988-1991    [doi:10.1107/S0108270192003251]

Intramolecular interactions in 3,3'-dinitro-2,2'-bipyridine

C. R. Rice, J. D. Wallis and D. C. Povey



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Acta Cryst. (1992). C48, 1991-1994    [doi:10.1107/S0108270192002853]

Structure and conformation of N-(4-methyl-2-pyridyl)-p-chlorophenylsuccinimide

J. Karolak-Wojciechowska, W. Kwiatkowski, Z. Karczmarzyk, A. Zejc and J. Obniska



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Acta Cryst. (1992). C48, 1994-1996    [doi:10.1107/S0108270192002798]

Structure of a phenylhydrazone of diacetone protected 3-keto-glucose

C. Y. Qing, D. de Wit, F. van Rantwijk, H. van Koningsveld and L. Maat



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Acta Cryst. (1992). C48, 1996-2000    [doi:10.1107/S0108270192003482]

Structures of 4[beta]-(nitromethyl)-2[alpha],6[alpha]-diphenyl-4[alpha]-piperidinol and 4[beta]-(nitromethyl)-2[beta],6[beta]-diphenyl-4[alpha]-piperidinol

P. Singh, S. G. Levine and K. Kasdorf



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Acta Cryst. (1992). C48, 2000-2002    [doi:10.1107/S010827019200307X]

Structure of wigandol

R. A. Toscano, L. Quijano, F. Gómez, G. García-Pérez and T. Rios



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Acta Cryst. (1992). C48, 2002-2004    [doi:10.1107/S0108270192002518]

Triphenylphosphine oxide hydrogen bromide

H. P. Lane, C. A. McAuliffe and R. G. Pritchard



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Acta Cryst. (1992). C48, 2004-2007    [doi:10.1107/S0108270192003330]

Structure of N-(2-dimethylaminoethyl)phenothiazine-1-carboxamide hydrochloride

J. Christiansen, G. R. Clark, W. A. Denny and B. D. Palmer



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Acta Cryst. (1992). C48, 2007-2009    [doi:10.1107/S0108270192002865]

Structure of the 1:2 adduct of meso-2,3-dimercaptosuccinic acid and N,N-dimethylformamide

G. J. Pyrka, N. Scott and Q. Fernando



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Acta Cryst. (1992). C48, 2009-2013    [doi:10.1107/S0108270192003378]

Structures of two crystalline modifications of lapachol

I. K. Larsen, L. A. Andersen and B. F. Pedersen



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Acta Cryst. (1992). C48, 2013-2016    [doi:10.1107/S0108270192003858]

Structure of N,N',N''-triphenylbiuret

O. Carugo, G. Poli and L. Manzoni



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Acta Cryst. (1992). C48, 2016-2019    [doi:10.1107/S0108270192002701]

Structural aspects of the 6,11-dihydro-11-oxodibenz[b,e]oxepin skeleton

E. S. Matsuzawa, N. Hirayama, E. Ohshima and H. Obase


short format


inorganic compounds



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Acta Cryst. (1992). C48, 2020-2021    [doi:10.1107/S0108270192003433]

Redetermination of decacarbonyl di-[mu]4-sulfido-tetracobalt

K. M. Mackay, B. K. Nicholson and M. L. van Tiel


metal-organic compounds



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Acta Cryst. (1992). C48, 2021-2023    [doi:10.1107/S0108270192002695]

Structure of monosodium N1-(4,6-dimethyl-2-pyrimidyl)sulfanilamidate dihydrate

S. S. Hannan and A. N. Talukdar



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Acta Cryst. (1992). C48, 2023-2025    [doi:10.1107/S0108270192001495]

Bis-adducts of trimethylaluminium and trimethylgallium with N,N,N',N'-tetramethylethylenediamine

J. J. Byers, W. T. Pennington and G. H. Robinson



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Acta Cryst. (1992). C48, 2025-2026    [doi:10.1107/S0108270192002609]

Structure of triphenyltin 2-(4-pyridylthio)acetate

S. W. Ng and V. G. Kumar Das



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Acta Cryst. (1992). C48, 2027-2029    [doi:10.1107/S0108270192002622]

Structure of sodium (7-amino-2,3-dihydro-5-oxo-5H-thiazolo[3,2-a]pyrimidin-6-yl)sulfamate trihydrate

P. Pecorari, M. Rinaldi and L. Antolini



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Acta Cryst. (1992). C48, 2029-2031    [doi:10.1107/S0108270192003275]

Penta[bis(5-oxoprolinato)platinate(II) d'ammonium] monohydrate

P. Khodadad and N. Rodier


organic compounds



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Acta Cryst. (1992). C48, 2032-2033    [doi:10.1107/S0108270192002440]

3-Methyl-2-thioxo-6-trifluoromethyl-2,3-dihydro-4(1H)-pyrimidinone

B. Tinant, J. Feneau-Dupont, J.-P. Declercq, F. Evariste and H. G. Viehe



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Acta Cryst. (1992). C48, 2033-2035    [doi:10.1107/S010827019200249X]

4',6,7-Trimethoxyisoflavone

M. Shoja



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Acta Cryst. (1992). C48, 2035-2036    [doi:10.1107/S0108270192002221]

Structure of a cinnamic acid derivative

M. Dyrbusch and E. Egert



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Acta Cryst. (1992). C48, 2036-2039    [doi:10.1107/S0108270192002403]

Structures of two acylpyridinium salts and one simple pyridinium salt

G. L. Bryant Jnr and J. A. King Jnr



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Acta Cryst. (1992). C48, 2039-2040    [doi:10.1107/S0108270192002749]

anti-2-Methyl-1,3-dithiane 1,1,3-trioxide

J. Barkley, I. M. Dodd, M. M. Harding, E. S. Namwindwa and P. C. B. Page



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Acta Cryst. (1992). C48, 2040-2042    [doi:10.1107/S0108270192002567]

Structure of tetrafluoroisophthalonitrile

D. Britton



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Acta Cryst. (1992). C48, 2042-2043    [doi:10.1107/S0108270192001483]

2-{[(o-Hydroxyphenyl)imino]methyl}pyridine

L. B. Orr Jnr, E. J. Parsons and W. T. Pennington



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Acta Cryst. (1992). C48, 2044-2045    [doi:10.1107/S0108270192003160]

Structure of an epoxytetradecahydropyrene

M. Nieger and E. Egert



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Acta Cryst. (1992). C48, 2045-2047    [doi:10.1107/S0108270192002944]

2,11-Dithia[3.3]metacyclophane-9-carboxylic acid

W. Assenmacher, M. Jansen, R. Güther and F. Vögtle



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Acta Cryst. (1992). C48, 2047-2049    [doi:10.1107/S0108270192003081]

Structure of phenylazocarboxamide

N. Okabe and H. Kisaichi



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Acta Cryst. (1992). C48, 2049-2051    [doi:10.1107/S0108270192002683]

Structure of the cation radical salt 3,8-dimethoxy-1,6-dithiapyrenium hexafluorophosphate

N. Thorup, P. Frederiksen and K. Bechgaard



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Acta Cryst. (1992). C48, 2051-2053    [doi:10.1107/S0108270192003500]

(5[alpha],6[alpha],7[alpha],11[beta])-[Delta]13,14-Sophocarpine monohydrate

M. A. Khan, G. E. Burrows and E. M. Holt



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Acta Cryst. (1992). C48, 2053-2054    [doi:10.1107/S0108270192002415]

Structure cristalline d'un N-azaarylphtalimide à activité anti-inflammatoire, le 2-(4,6-diméthylpyridin-2-yl)-2,3-dihydro-1H-isoindole-1,3-dione

N. Rodier, J.-M. Robert, D. Leblois et G. Le Baut



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Acta Cryst. (1992). C48, 2055-2057    [doi:10.1107/S0108270192002786]

Structure of ibogaine

M. Soriano-García



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Acta Cryst. (1992). C48, 2057-2058    [doi:10.1107/S0108270192002592]

Structure of 2-[1-(2-carboxyethyl)ethylidene]hydrazinecarbothioamide

S. W. Ng



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Acta Cryst. (1992). C48, 2058-2060    [doi:10.1107/S0108270192002774]

1,3-Dinitropyrrolo[1,2-b]isoquinoline-5,10-dione

M.-H. Du and P. B. Hitchcock



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Acta Cryst. (1992). C48, 2060-2061    [doi:10.1107/S0108270192003524]

Structure of 1-[3-(1,1-dimethylethyl)-2-hydroxy-6-methylphenyl]-1-propanone

C. Bois and R. Martin


regular structural papers


inorganic compounds



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Acta Cryst. (1992). C48, 2062-2064    [doi:10.1107/S010827019200461X]

Structure of KY0.95Er0.05F4

Y. Le Fur, N. M. Khaidukov and S. Aléonard



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Acta Cryst. (1992). C48, 2064-2065    [doi:10.1107/S0108270192007303]

Structure of LaPd2In

B. Xue, H. Schwer and F. Hulliger



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Acta Cryst. (1992). C48, 2066-2067    [doi:10.1107/S0108270192006784]

Structure of Ba0.84Rb3Nb8P5O34

C. Gueho, M. M. Borel, A. Grandin, A. Leclaire and B. Raveau



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Acta Cryst. (1992). C48, 2067-2069    [doi:10.1107/S0108270192007534]

Ba15Al13.4Ga14.5, a disordered structure derived from Sr5Al9

M. L. Fornasini and M. Pani



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Acta Cryst. (1992). C48, 2069-2071    [doi:10.1107/S0108270192005006]

Structure of phase III of (NH4)3H(SeO4)2

A. Pietraszko, K. Lukaszewicz and M. A. Augustyniak


metal-organic compounds



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Acta Cryst. (1992). C48, 2071-2073    [doi:10.1107/S0108270192006917]

Metallointercalators: structure of rac-bis(ethylenediamine)(9,10-phenanthrenequinone diimine)rhodium(III) tribromide trihydrate

W. P. Schaefer, A. H. Krotz, L. Y. Kuo, T. P. Shields and J. K. Barton



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Acta Cryst. (1992). C48, 2073-2075    [doi:10.1107/S0108270192007212]

Structure of trans-dichloro(dimethylsulfoxide)(piperidine)platinum(II)

K. Lövqvist and Å. Oskarsson


organic compounds



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Acta Cryst. (1992). C48, 2075-2078    [doi:10.1107/S0108270192006115]

Regioselective pyrazine ring reduction of 4-(quinoxalin-2-yl)-1,3-dithiole-2-thione

R. L. Beddoes, J. R. Russell, C. D. Garner and J. A. Joule



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Acta Cryst. (1992). C48, 2078-2080    [doi:10.1107/S0108270192006164]

Structure of a `hypervalent' linear bis(phthalimidato)bromate(I) complex

M. Elding, A.-K. Larsson, G. Svensson, J. Albertsson and L. Eberson



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Acta Cryst. (1992). C48, 2080-2082    [doi:10.1107/S0108270192007455]

Structure of an intermediate in the synthesis of corymbolone

E. E. Castellano, J. Zukerman-Schpector, H. M. C. Ferraz, A. J. C. de Souza and B. S. M. Tenius



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Acta Cryst. (1992). C48, 2082-2085    [doi:10.1107/S0108270192006450]

D-Secoestrone derivatives. II. 16-Cyano-3-methoxy-16,17-secoestra-1,3,5(10)-trien-17-yl p-toluenesulfonate

S. Stankovic, A. Stefanovic, M. Bruvo and A. Altomare



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Acta Cryst. (1992). C48, 2085-2088    [doi:10.1107/S0108270192008333]

Structures of bis(dialkylthiophosphoryl) disulfides, [R2P(S)]2S2, R = Me, iPr, and the question of P-S [pi] bonding

A. C. Gallacher and A. A. Pinkerton



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Acta Cryst. (1992). C48, 2088-2090    [doi:10.1107/S010827019200814X]

Ethyl (2R,3R,SR)-3-(ethoxycarbonyloxy)-2-[1-(p-tolylsulfinyl)cyclopropyl]-1-pyrrolidinecarboxylate

P. D. Robinson, D. H. Hua, X. Wu, S. W. Miao and M. Meled



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Acta Cryst. (1992). C48, 2090-2092    [doi:10.1107/S0108270192006851]

Structure of an 11-membered cyclic silyl enol ether from condensation of methacrolein and a pseudoephedrine-derived O-silyl ketene N,O-acetal

W. P. Schaefer, V. Subramanian and A. G. Myers



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Acta Cryst. (1992). C48, 2092-2094    [doi:10.1107/S0108270192007030]

endo-2-Phenyl-exo-3,4,5-trithiatricyclo[5.2.1.02,6]decane exo-4-oxide

W. H. Watson, M. Krawiec, T. Ghosh and P. D. Bartlett



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Acta Cryst. (1992). C48, 2094-2096    [doi:10.1107/S0108270192006802]

Diammonium cyclopropane-1,1-dicarboxylate

P. Bréhin, J. Kozelka and C. Bois



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Acta Cryst. (1992). C48, 2096-2098    [doi:10.1107/S010827019200828X]

Structure of the 1:1 complex of 6,6'-diquinolyl ether with 5,5-diethylbarbituric acid

H. Liu, X. Wang and X. Zhang



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Acta Cryst. (1992). C48, 2098-2100    [doi:10.1107/S0108270192007339]

(E)-Methyl 2-phenyl-2-(3-pyridyl)vinyl sulfide

J. Metin, D. Roche, H. Veschambre and M. Madesclaire


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