Acta Crystallographica Section C

Crystal Structure Communications

Volume 49, Part 2 (February 1993)



research papers


inorganic compounds



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Acta Cryst. (1993). C49, 205-207    [doi:10.1107/S0108270192005481]

Structure of wadalite Ca6Al5Si2O16Cl3

K. Tsukimura, Y. Kanazawa, M. Aoki and M. Bunno



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Acta Cryst. (1993). C49, 207-209    [doi:10.1107/S0108270192006486]

A new layered ZnIn2S4-(IIIa) polytype: structure of FeCr0.8Ga1.2Se4

H. D. Lutz and T. Stingl



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Acta Cryst. (1993). C49, 209-211    [doi:10.1107/S0108270192004888]

Structure of lithium copper pyrophosphate

M. R. Spirlet, J. Rebizant and M. Liegeois-Duyckaerts



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Acta Cryst. (1993). C49, 211-214    [doi:10.1107/S0108270192006383]

Structure of strontium lithium indium pyroborate, Sr2LiInB4O10

K. I. Schaffers and D. A. Keszler



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Acta Cryst. (1993). C49, 214-216    [doi:10.1107/S0108270192003706]

Thermal effects in the structure of potassium perrhenate

R. J. C. Brown, B. M. Powell and S. N. Stuart


metal-organic compounds



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Acta Cryst. (1993). C49, 216-219    [doi:10.1107/S0108270192005948]

Structure of triphenyltin 2-[2-bromo-4-(dimethylamino)phenylazo]benzoate

B. C. Das, G. Biswas, B. B. Maji, K. L. Ghatak, S. N. Ganguly, Y. Iitaka and A. Banerjee



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Acta Cryst. (1993). C49, 219-221    [doi:10.1107/S0108270192007108]

Structure of monoclinic zinc n-butanoate

J. Blair, R. A. Howie and J. L. Wardell



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Acta Cryst. (1993). C49, 222-224    [doi:10.1107/S010827019200622X]

Structure of bis[tris(2-aminoethanethiolato)cobalt(III)-[mu]-S,[mu]-S',[mu]-S'']nickel(II) chloride trihydrate

T. Konno, K. Okamoto and J. Hidaka



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Acta Cryst. (1993). C49, 224-226    [doi:10.1107/S0108270192004992]

Structure of trans-bis[1,2-bis(dimethylphosphino)ethane]dibromoiron(II)

L. D. Field, T. W. Hambley and B. C. K. Yau



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Acta Cryst. (1993). C49, 226-228    [doi:10.1107/S0108270192006413]

Structure of bis[ferrocenyl(p-tolyl)methyl] ether

D. Matkovic-Calogovic, V. Rapic and S. Kovac



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Acta Cryst. (1993). C49, 229-231    [doi:10.1107/S0108270192006401]

Determination of the absolute configuration of sodium (-)589-bis(N-methyliminodiacetato)cobaltate(III) trihydate

Y. Yamasaki, T. Kurisaki, T. Yamaguchi and H. Wakita



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Acta Cryst. (1993). C49, 231-233    [doi:10.1107/S0108270192005444]

Structure of bis(tetramethylammonium) hexachlororhenate(IV)

R. Loris, D. Maes, J. N. Lisgarten, M. Bettinelli and C. Flint



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Acta Cryst. (1993). C49, 233-236    [doi:10.1107/S0108270192006395]

Structure of hexa-[mu]-acetato-1[kappa]3O:2[kappa]3O';2[kappa]3O:3[kappa]3O'-bis(1,10-phenanthroline)-1[kappa]2N1,N10;2[kappa]2N1,N10-trimanganese(II)

K. Tsuneyoshi, H. Kobayashi and H. Miyamae



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Acta Cryst. (1993). C49, 236-238    [doi:10.1107/S0108270192007133]

Structure of chloro([alpha],[beta],[gamma],[delta]-tetraphenylporphinato)manganese(III) toluene solvate

R. S. Armstrong, G. J. Foran and T. W. Hambley



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Acta Cryst. (1993). C49, 238-241    [doi:10.1107/S0108270192005985]

cis-[Diaquabis(1-aminocyclohexanecarboxylato)nickel(II)]-water (1/1)

H. M. Haendler



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Acta Cryst. (1993). C49, 241-244    [doi:10.1107/S010827019200489X]

Structure of sodium 6-hydroxy-2-methyl-3-thioxo-2H-1,2,4-triazin-5(4H)-onate 1.25-hydrate

M. Valencic, L. Golic, M. Japelj and A. Stefanic



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Acta Cryst. (1993). C49, 244-246    [doi:10.1107/S0108270192006218]

Synthesis and structure of diaquabis(glycolato-O,O'')germanium(IV)

H.-C. Chiang, M.-H. Wang and C.-H. Ueng


organic compounds



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Acta Cryst. (1993). C49, 246-250    [doi:10.1107/S0108270192003470]

Structure of (+)-(5R,6R)-5-chloro-6-methoxy-5,6-dihydro-1-(2',3'-didehydro-2',3'-dideoxy-[beta]-D-glycero-2-enopentofuranosyl)thymine

H. Blanchard, M. N. G. James, R. Kumar, L. I. Wiebe and E. E. Knaus



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Acta Cryst. (1993). C49, 250-253    [doi:10.1107/S0108270192005766]

Structure of the anthracycline antibiotic aranciamycin

K. Schmidt-Bäse, M. Noltemeyer, E. Egert, E. Eigelt and A. Zeeck



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Acta Cryst. (1993). C49, 253-257    [doi:10.1107/S0108270192006097]

Structures of 1,2,3,4-benzenetetracarboxylic acid and 1,2,3,5-benzenetetracarboxylic acid dihydrate

C. Barrio, S. García-Granda and F. Gómez-Beltrán



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Acta Cryst. (1993). C49, 257-261    [doi:10.1107/S0108270192006838]

Ketone pyramidalization in a tetracyclic perpendicular enone derivative

B. A. Lloyd, C. Ericson, A. M. Arif and E. L. Allred



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Acta Cryst. (1993). C49, 261-263    [doi:10.1107/S010827019200684X]

A twisted pentacyclic ketone derivative

B. A. Lloyd, A. M. Arif, E. L. Allred, A. Patton and T. R. Sharp



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Acta Cryst. (1993). C49, 264-267    [doi:10.1107/S0108270192006875]

Structure of a powerful mutagenic compound; 6-methoxy-2-nitronaphtho[1,8-bc]pyran

J. P. Bideau, M. Cotrait, J. P. Buisson and P. Demerseman



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Acta Cryst. (1993). C49, 267-270    [doi:10.1107/S0108270192005602]

Structure of benzo[a]phenothiazine pentachlorotellurate(IV)

K. Kozawa and T. Uchida



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Acta Cryst. (1993). C49, 270-273    [doi:10.1107/S0108270192003007]

Structure of 3-methoxy-6[alpha],17[beta]-dihydroxyestra-1,3,5(10)-trien-7-one oxime

B. Ribár, S. Stankovic, C. Mészáros, D. Miljkovic, V. Pejanovic and J. Petrovic



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Acta Cryst. (1993). C49, 273-275    [doi:10.1107/S0108270192005134]

Structure of a steriod fungal metabolite

P. Dastidar, T. Joseph, K. M. Madyastha and T. N. Guru Row



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Acta Cryst. (1993). C49, 275-278    [doi:10.1107/S0108270192006954]

Structures of sobrerol enantiomers and racemates. III. (±)-cis-5-Hydroxy-[alpha],[alpha],4-trimethyl-3-cyclohexene-1-methanol (racemic cis-sobrerol)

G. Giuseppetti, C. Tadini and G. P. Bettinetti



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Acta Cryst. (1993). C49, 278-282    [doi:10.1107/S0108270192007856]

Structure and conformation of 3-(dibenzylamino)phenylacetonitrile

S. Ianelli, M. Nardelli, D. Belletti, B. Jamart-Grégoire, A. Zouaoui and P. Caubère



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Acta Cryst. (1993). C49, 282-285    [doi:10.1107/S0108270192006711]

Structure of amprolium hydrochloride

W. Shin and D. Oh



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Acta Cryst. (1993). C49, 285-288    [doi:10.1107/S0108270192005572]

Molecular co-crystals of carboxylic acids. 10. Structure of the 1:1 adduct of triphenylphosphine oxide with (pentachlorophenoxy)acetic acid

D. E. Lynch, G. Smith, K. A. Byriel and C. H. L. Kennard



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Acta Cryst. (1993). C49, 288-292    [doi:10.1107/S0108270192007029]

Structure of 4-[4'-(dimethylamino)phenylazo]phenyl acrylate (1) and 4-[4'-(dimethylamino)phenylazo]phenyl methacrylate (2)

A. Meetsma, T. S. Boer, H. J. Haitjema and Y. Y. Tan



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Acta Cryst. (1993). C49, 292-294    [doi:10.1107/S0108270192007807]

Structure of (4-bromophenyl)propiolic acid and its unusual hydrogen-bonding pattern

B. S. Goud and G. R. Desiraju



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Acta Cryst. (1993). C49, 294-298    [doi:10.1107/S0108270192006905]

Structure of benfotiamine hemihydrate

W. Shin, S. W. Cho and C. H. Chae



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Acta Cryst. (1993). C49, 298-300    [doi:10.1107/S0108270192006929]

2,2,6,6-Tetramethylpiperidine-1-oxyl-4-yl [alpha]-D-glucopyranoside

A. Hempel, N. Camerman, S. J. Hamodrakas, F. P. Ottensmeyer, A. Troganis, C. I. Stassinopoulou and A. Camerman



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Acta Cryst. (1993). C49, 300-303    [doi:10.1107/S010827019200893X]

Structure of debrisoquinium sulfate

P. A. Bates, S. A. Islam and M. J. E. Sternberg



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Acta Cryst. (1993). C49, 303-307    [doi:10.1107/S0108270192007996]

Structures of derivatives of the Diels-Alder adduct 1,4,4a,5,8,8a,9a,10a-octahydro-1,4:5,8-dimethano-9,10-anthraquinone

G. Alex, S. Srinivasan, R. Bakthavatchalam, S. R. Ramadas and B. Varghese



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Acta Cryst. (1993). C49, 307-310    [doi:10.1107/S0108270192008965]

The absolute configuration of (+)-2-benzyl-2-[N-([alpha]-phenylethyl)amino]cyclohexanone hydrochloride

R. Platzbecker, G. Will, K. Hümmer, E. Weckert, G. Lauktien and A. W. Frahm



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Acta Cryst. (1993). C49, 310-313    [doi:10.1107/S0108270192008515]

Structure of 1,1,1,7,7,7-hexafluoro-2,6-dihydroxy-2,6-bis(trifluoromethyl)-4-heptanone

J. J. Vittal and C. J. Willis


short format


inorganic compounds



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Acta Cryst. (1993). C49, 314-316    [doi:10.1107/S0108270192005687]

Reinvestigation of the structure of [Y(H2O)5(NO3)2][Y(H2O)2(NO3)4]

B. Ribár, A. Kapor, B. Scott and R. D. Willett



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Acta Cryst. (1993). C49, 316-318    [doi:10.1107/S0108270192006504]

Caesium nitrate (II) at 296 K

D. Pohl and T. Gross


metal-organic compounds



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Acta Cryst. (1993). C49, 318-320    [doi:10.1107/S0108270192007017]

Structure of tetrakis(dimethylammonium) chloride hexachlorobismuthate(III), {[(CH3)2NH2]+}4.Cl-.[BiCl6]3-

E. Herdtweck and U. Kreusel



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Acta Cryst. (1993). C49, 320-321    [doi:10.1107/S0108270192007054]

Structure of the thallium-rich complex [(Tl18-crown-6)4CuBr4][TlBr4]2

I. A. Kahwa, D. Miller, M. Mitchel and F. R. Fronczek



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Acta Cryst. (1993). C49, 322-324    [doi:10.1107/S0108270192006085]

Structure redetermination of carbonatobis(ethlenediamine)cobalt(III) chloride

S. García-Granda, V. Calvo-Pérez and F. Gómez-Beltrán



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Acta Cryst. (1993). C49, 324-326    [doi:10.1107/S0108270192006474]

Structure of diaqua[1,8-bis(2-pyridyl)-3,6-dithiaoctane-N,N',S,S']nickel(II) diperchlorate at 243 K

E. Bermejo, A. Castiñeiras, R. Domínguez, J. Strähle and W. Hiller



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Acta Cryst. (1993). C49, 327-328    [doi:10.1107/S0108270192006498]

Bis[bis(triphenylphosphine)iminium] decacarbonyldimolybdenum(Mo-Mo)

R. E. Bachman and K. H. Whitmire


organic compounds



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Acta Cryst. (1993). C49, 329-330    [doi:10.1107/S0108270192003974]

Structure of 4-(3,4-dihydroxyphenyl)-5-(O-[beta]-D-galactopyranosyl)-7-methoxycoumarin trihydrate

M. Soriano-García, R. V. Iribe, S. Mendoza-Díaz, M. del Rayo Camacho and R. Mata



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Acta Cryst. (1993). C49, 331-333    [doi:10.1107/S0108270192002737]

Structure of the highly crowded alkyne di[tris(trimethylsilyl)methyl]acetylene and the octasilane hexakis(trimethylsilyl)disilane

F. R. Fronczek and P. D. Lickiss



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Acta Cryst. (1993). C49, 333-336    [doi:10.1107/S0108270192005596]

Structures of benzo[a]phenothiazine and benzo[c]phenothiazine

S. Yoshida, H. Matsuzawa, K. Kozawa and T. Uchida



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Acta Cryst. (1993). C49, 336-338    [doi:10.1107/S0108270192004761]

Structure of (S,S)-(E)-3-(2-butenoyl)-2,4-bis(phenylmethyl)oxazolidine

G. L. Hardgrove Jnr, J. S. Clark, R. M. Hanson and A. Q. Thieu



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Acta Cryst. (1993). C49, 338-340    [doi:10.1107/S0108270192005675]

Structure of 6-(3,3-dimethyl-2-oxo-2,3-dihydro-5-furanyl)-2-pyridone at 145 K

E. Maverick, J. Chiefari and D. A. Lightner



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Acta Cryst. (1993). C49, 341-343    [doi:10.1107/S010827019200595X]

Structure of the germacrane furanosesquiterpenoid linderane

K. Okada and H. Koyama



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Acta Cryst. (1993). C49, 343-345    [doi:10.1107/S010827019200444X]

Structure of 3-benzoylamino-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydrocoumarin

I. Leban, M. Kocevar and B. Vercek



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Acta Cryst. (1993). C49, 345-347    [doi:10.1107/S0108270192006073]

Structure of tri-p-tolylphosphine oxide hemihydrate, P(p-C6H4CH3)3O.1/2H2O

M. R. Churchill, R. F. See, S. L. Randall and J. D. Atwood



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Acta Cryst. (1993). C49, 347-350    [doi:10.1107/S0108270192006024]

Low-temperature structures of cis-4-tert-butylcyclohexyl p-nitrobenzoate (1) and trans-4-tert-butylcyclohexyl p-nitrobenzoate (2)

J. M. White and G. B. Robertson



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Acta Cryst. (1993). C49, 350-351    [doi:10.1107/S0108270192005535]

Structure of 4'-dimethylamino-4-methyl-4-azastilbenium p-toluenesulfonate hydrate

G. L. Bryant Jnr, C. P. Yakymyshyn and K. R. Stewart



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Acta Cryst. (1993). C49, 351-354    [doi:10.1107/S0108270192006760]

Structure of 17-(3-oxazolin-4-yl)androsta-4,16-dien-3-one

A. Meetsma, D. van Leusen and A. M. van Leusen



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Acta Cryst. (1993). C49, 354-355    [doi:10.1107/S0108270192005614]

1,3-Dicyanomethylhexahydropyrimidine

M. Shoja and S. Saba



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Acta Cryst. (1993). C49, 355-357    [doi:10.1107/S0108270192006176]

Structure of orthorhombic triphenylphosphine oxide: a redetermination at room temperature

J. A. Thomas and T. A. Hamor



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Acta Cryst. (1993). C49, 357-359    [doi:10.1107/S010827019200670X]

5,7-Dihydroxy-2-(2,3,4-trimethoxyphenyl)-4H-1-benzopyran-4-one (5,7-dihydroxy-2',3',4'-trimethoxyflavone)

J.-C. Wallet, A. Wojtczak, V. Cody, N. Galitsky and E. M. Gaydou



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Acta Cryst. (1993). C49, 359-360    [doi:10.1107/S0108270192006899]

Structure of 1,3-di-tert-butyl-2,4-dichloro-2,4-bis[1-(trimethylsilyl)vinyl]-1,3-diaza-2,4-disilacyclobutane

N. Auner, E. Herdtweck and E. Penzenstadler


regular structural papers


inorganic compounds



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Acta Cryst. (1993). C49, 361-363    [doi:10.1107/S0108270192009466]

Ammonium cyclo-octaphosphate-telluric acid dihydrate adduct

M.-T. Averbuch-Pouchot and A. Durif



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Acta Cryst. (1993). C49, 363-365    [doi:10.1107/S0108270192009399]

Structure of a new sodium thiosulfate hydrate

W. Hesse, B. Leutner, K.-H. Böhn and N. P. C. Walker


metal-organic compounds



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Acta Cryst. (1993). C49, 365-368    [doi:10.1107/S0108270192010552]

Structure du bis([pi]-allylhimachalène)-[alpha],[alpha]-dichlorodipalladium

A. Chiaroni, C. Riche, L. El Firdoussi, A. Benharref and A. Karim



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Acta Cryst. (1993). C49, 368-370    [doi:10.1107/S0108270192008928]

Structure of [N-(2-mercaptophenyl)-4-oxo-2-pentylideneaminato-N,O,S]diphenyltin(IV)

R. C. Okechukwu, H.-K. Fun, S.-G. Teoh, S.-B. Teo and K. Chinnakali



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Acta Cryst. (1993). C49, 370-372    [doi:10.1107/S0108270192009326]

Structure of [Cu(CN)(py)2]

M. M. Olmstead, G. Speier and L. Szabó



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Acta Cryst. (1993). C49, 372-374    [doi:10.1107/S0108270192009478]

Structure of aquabis(2,2'-bipyridyl)zinc(II) diperchlorate

M. Liu and S. K. Arora



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Acta Cryst. (1993). C49, 374-376    [doi:10.1107/S0108270192010631]

Dimanganese octacarbonyl compounds with bridging cyclohexylphosphanes

U. Flörke and H.-J. Haupt



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Acta Cryst. (1993). C49, 376-377    [doi:10.1107/S0108270192009533]

trans-Dichlorobis(1,3-dihydrobenzo[c]thiophene-S)platinum(II)

M. Parvez, J. F. Fait, P. D. Clark and C. G. Jones



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Acta Cryst. (1993). C49, 378-381    [doi:10.1107/S0108270192005924]

Two iron-tricarbonyl complexes with substituted bicyclo[2.2.2]octadienes

H. Irngartinger, T. Oeser and C.-M. Köhler



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Acta Cryst. (1993). C49, 381-383    [doi:10.1107/S0108270192009934]

Structure of [Fe(C16H14ClNO4)(CO)3]

J.-C. Wang, C.-H. Sun, G.-Z. Yang, F. R. Fronczek and S. F. Watkins



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Acta Cryst. (1993). C49, 383-385    [doi:10.1107/S0108270192009545]

mer-Trichlorotris(2,3-dihydrobenzo[b]thiophene-S)rhodium(III)

M. Parvez, J. F. Fait, P. D. Clark and C. G. Jones


organic compounds



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Acta Cryst. (1993). C49, 385-387    [doi:10.1107/S0108270192008497]

Structure of 6-methyl-2-oxabicyclo[4.3.0]non-4-ene-3,8-dione

J. Zukerman-Schpector, R. C. Boscaini, J. T. B. Ferreira and F. A. Marques



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Acta Cryst. (1993). C49, 387-388    [doi:10.1107/S0108270192009193]

Structure of (E)-1-(4-methoxyphenyl)-2-nitropropene

D. Boys, V. Manríquez and B. K. Cassels



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Acta Cryst. (1993). C49, 388-391    [doi:10.1107/S010827019200920X]

Structure of ethyltriphenylphosphonium triiodide, [P(C2H5)(C6H5)3]I3

S. Bélanger and A. L. Beauchamp



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Acta Cryst. (1993). C49, 391-392    [doi:10.1107/S0108270192009120]

Structure of 1-deoxycastanospermine

L. L. Koh, C.-K. Lee, K. Y. Sim and J. Zhu



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Acta Cryst. (1993). C49, 393-394    [doi:10.1107/S0108270192009715]

Structure of 2,2,4,4,6-pentaphenyl-2,4,1,3,5-diphosphatriazine; a six-membered P2N3C ring

V. Chandrasekhar, T. Chivers and M. Parvez



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Acta Cryst. (1993). C49, 394-398    [doi:10.1107/S0108270192009685]

Structures of (E,E)-o-nitroacetophenone azine (I), (E,Z)-o-nitroacetophenone azine (II) and (E,E)-o-nitrobenzaldehyde azine (III)

L.-Y. Hsu, C. E. Nordman and D. H. Kenny



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Acta Cryst. (1993). C49, 398-400    [doi:10.1107/S0108270192009375]

Structure of dibenzofuran-d8, C12D8O, at 173 K

L. J. Fitzgerald, J. C. Gallucci and R. E. Gerkin



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Acta Cryst. (1993). C49, 400-402    [doi:10.1107/S0108270192010175]

Structure of 1,2,2,3,3,4,4,5-octamethyl-6,7,8-trioxabicyclo[3.2.1]octane

L. B. Jerzykiewicz, D. Dziewonska-Baran, J. Baran and T. Lis



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Acta Cryst. (1993). C49, 402-404    [doi:10.1107/S0108270192010485]

Structure of 1,3-xylyl-(18-crown-5)-ammonium catecholborate (1/1)

R. Goddard, C. M. Niemeyer and M. T. Reetz



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Acta Cryst. (1993). C49, 404-406    [doi:10.1107/S0108270192009089]

Structure of 1:1 clathrate between tris(2,3-naphthalenedioxy)cyclotriphosphazene and p-xylene

K. Kubono, N. Asaka, S. Isoda, T. Kobayashi and T. Taga



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Acta Cryst. (1993). C49, 406-408    [doi:10.1107/S0108270192009442]

Structure of 2-phenylacetophenone

T. P. Rieker, C. Haltiwanger, K. Eidman, D. W. Walba, N. A. Clark and A. C. Larson



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Acta Cryst. (1993). C49, 408-410    [doi:10.1107/S0108270192010023]

Structure of Z-L-([alpha]Me)Phe-(L-Ala)2-OMe monohydrate

G. Valle, F. Formaggio, M. Crisma, C. Toniolo and J. Kamphuis



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Acta Cryst. (1993). C49, 410-413    [doi:10.1107/S0108270192009491]

Tricyclo[9.3.0.03,7]tetradec-3-ene-5,10-dione (I), tetracyclo[9.3.0.01,5.05,9]tetradecane-2,7-dione (II) and cis-cisoid-cis-2,9-epoxy-9-methyltricyclo[9.3.0.04,8]tetradecan-2-ol (III)

T. Kawata, M. Okuda, S. Ohba, M. Umehara, H. Honnami and S. Hishida



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Acta Cryst. (1993). C49, 413-416    [doi:10.1107/S0108270192009831]

Structure of a 6-(tetrahydroxybutyl)-substituted pteridine

R. L. Beddoes, J. R. Russell, C. D. Garner and J. A. Joule


short communications



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Acta Cryst. (1993). C49, 416    [doi:10.1107/S0108270192008667]

Über die Fehlordnung von Triethylammoniumchlorid

I. Sens und U. Müller



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Acta Cryst. (1993). C49, 417    [doi:10.1107/S0108270192013106]

Structure of the white-line-inducing principle isolated from Pseudomonas reactans. Erratum.

F. Han, R. J. Mortishire-Smith, P. B. Rainey and D. H. Williams


international union of crystallography



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Acta Cryst. (1993). C49, 418-423    [doi:10.1107/S0108270193000800]

`How does my CIF become a printed paper?'



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Acta Cryst. (1993). C49, 424    [doi:10.1107/S0108270193099809]

Access to CIFs archived in Chester


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