Acta Crystallographica Section C

Crystal Structure Communications

Volume 49, Part 4 (April 1993)



research papers


inorganic compounds



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Acta Cryst. (1993). C49, 645-647    [doi:10.1107/S0108270192008217]

Structure of lithium catena-poly[3,4-dihydroxopentaborate-1:5-[mu]-oxo]

A. Cárdenas, J. Solans, K. Byrappa and K. V. K. Shekar



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Acta Cryst. (1993). C49, 647-650    [doi:10.1107/S0108270192006371]

Alkaline-earth beryllium borate CaBeB2O5

K. I. Schaffers and D. A. Keszler



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Acta Cryst. (1993). C49, 650-652    [doi:10.1107/S0108270192010849]

Redetermination of tristrontium uranate(VI). A Rietveld refinement of neutron powder diffraction data

D. J. W. IJdo



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Acta Cryst. (1993). C49, 652-654    [doi:10.1107/S0108270192010850]

Ba2Ce3/4SbO6, a Rietveld refinement of neutron powder diffraction data

D. J. W. IJdo and R. B. Helmholdt



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Acta Cryst. (1993). C49, 654-656    [doi:10.1107/S0108270192010874]

Pb3U11O36, a Rietveld refinement of neutron powder diffraction data

D. J. W. IJdo



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Acta Cryst. (1993). C49, 657-659    [doi:10.1107/S0108270192010643]

Structure of the fully ferroelectric/fully ferroelastic orthorhombic room-temperature phase of iron iodine boracite, Fe3B7O13I

F. Kubel and A.-M. Janner



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Acta Cryst. (1993). C49, 659-663    [doi:10.1107/S0108270192011533]

Structure of Ce16Mo21O56 containing single Mo atoms and isolated Mo10 clusters

P. Gall and P. Gougeon


metal-organic compounds



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Acta Cryst. (1993). C49, 663-666    [doi:10.1107/S0108270192011557]

Structure of [Ru2Cl4(Me2SO)5]

M. Calligaris, P. Faleschini and E. Alessio



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Acta Cryst. (1993). C49, 666-668    [doi:10.1107/S0108270192009880]

Structure of a nickel(II) complex of the deprotonated anion of 3,6,6,9-tetramethyl-4,8-diaza-3,8-undecadiene-2,10-dione dioxime

T.-H. Lu, F. Tseng, H. Luh and C.-S. Chung



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Acta Cryst. (1993). C49, 668-671    [doi:10.1107/S0108270192008837]

Structure of dipiperidinium catena-poly[nickel-tri-[mu]-chloro(1-)] chloride

M. R. Bond and R. D. Willett



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Acta Cryst. (1993). C49, 671-674    [doi:10.1107/S010827019200934X]

Structure of trans-[Re(CO)4(PPh3)I]

W. L. Ingham, D. G. Billing, D. C. Levendis and N. J. Coville



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Acta Cryst. (1993). C49, 674-677    [doi:10.1107/S0108270192004505]

Synthesis and structure of (acetato-O,O')(perchlorato-O)(2,2':6'2''-terpyridine-N,N',N'')copper(II)

M. C. Muñoz, R. Ruiz, M. Julve, F. Lloret and X. Solans



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Acta Cryst. (1993). C49, 677-680    [doi:10.1107/S0108270192010813]

Structure of [W2([mu]-C2){OC(CH3)3}6]: a dimetallabutadiyne

T. M. Gilbert and R. D. Rogers



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Acta Cryst. (1993). C49, 680-682    [doi:10.1107/S0108270192010436]

Diphenylphosphinoferrocene

J. A. Adeleke and L.-K. Liu



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Acta Cryst. (1993). C49, 682-684    [doi:10.1107/S0108270192009363]

Structure of the 2-pyridylhydrazone of ferrocenecarbaldehyde

A. Houlton, M. T. Ahmet, J. R. Miller, J. Silver and E. Slade



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Acta Cryst. (1993). C49, 684-687    [doi:10.1107/S0108270192005961]

Bis[2-(4-ethoxyphenyltelluro)ethyl]amino-N,Te,Te'}chloroplatinum(II) chloride trichloromethane monohydrate

J. E. Drake, J. H. E. Bailey, A. K. Singh and V. Srivastava


organic compounds



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Acta Cryst. (1993). C49, 688-690    [doi:10.1107/S0108270192009351]

Structure of dichloro(pentabenzylcyclopentadienyl)phosphine

H. Schumann, F. H. Görlitz and M. Schäfers



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Acta Cryst. (1993). C49, 690-693    [doi:10.1107/S0108270192010916]

Structure of 4-carboxy-2-nitrobenzeneboronic acid

S. Soundararajan, E. N. Duesler and J. H. Hageman



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Acta Cryst. (1993). C49, 693-695    [doi:10.1107/S0108270192011326]

Structure of 4(5)-nitroimidazole at 100 K

H. L. De Bondt, E. Ragia, N. M. Blaton, O. M. Peeters and C. J. De Ranter



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Acta Cryst. (1993). C49, 696-705    [doi:10.1107/S0108270192010758]

Structure of phosphoglycolate (PG) in different ionization states. Structure of phosphoglycolic acid (H3PG) and its salts: KH2PG, NaH2PG, K3H3(PG)2, Na2HPG.0.5H2O, Na5H(PG)2.4H2O and Na3PG.4H2O

T. Lis



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Acta Cryst. (1993). C49, 705-710    [doi:10.1107/S0108270192012125]

Structure of 1,2-diphenylcarbaborane, 1,2-Ph2-1,2-closo-C2B10H10

Z. G. Lewis and A. J. Welch



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Acta Cryst. (1993). C49, 710-714    [doi:10.1107/S0108270192012137]

Structures of [HNEt3]+ and [Me3NCH2C6H5]+ salts of [7,8-Ph2-7,8-nido-C2B9H10]-

J. Cowie, D. J. Donohoe, N. L. Douek and A. J. Welch



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Acta Cryst. (1993). C49, 715-718    [doi:10.1107/S0108270192012149]

Structure of 7,8-Ph2-10-endo-PPh3Hg-7,8-nido-C2B9H9 methylene chloride solvate

Z. G. Lewis and A. J. Welch



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Acta Cryst. (1993). C49, 718-721    [doi:10.1107/S0108270192011193]

Molecular co-crystals of carboxylic acids. 11. Structure of the 1:1 adduct of triphenylphosphine oxide with (3,4-dichlorophenoxy)acetic acid

D. E. Lynch, G. Smith, K. A. Byriel and C. H. L. Kennard



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Acta Cryst. (1993). C49, 721-723    [doi:10.1107/S0108270192009028]

Polymorphism in dethoxyprone, a steroidal anaesthetic. I. Structure of 11[alpha]-dimethylamino-2[beta]-ethoxy-3[alpha]-hydroxy-5[alpha]-pregnan-20-one (dethoxyprone form I)

R. A. Palmer, H. T. Palmer, J. N. Lisgarten and R. Lancaster



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Acta Cryst. (1993). C49, 724-729    [doi:10.1107/S0108270192010187]

(4S,7R)-7,8,8-Trimethyl-4,5,6,7-tetrahydro-4,7-methano-1H(2H)-indazole (campho[2,3-c]pyrazole): comparison between the X-ray structure and carbon-13 NMR data in the solid state

A. L. Llamas-Saiz, C. Foces-Foces, I. Sobrados, J. Elguero and W. Meutermans



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Acta Cryst. (1993). C49, 729-731    [doi:10.1107/S0108270192009181]

Structure of (4[alpha])-13-hydroxykaur-16-en-18-oic acid (steviol) methanol solvate

A. M. G. Dias Rodrigues, R. H. de Almeida Santos and J. R. Lechat



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Acta Cryst. (1993). C49, 731-735    [doi:10.1107/S0108270192012253]

Structures of Diels-Alder mono-adducts of 4-phenyl- or 4-methyl-1,2,4-triazolidine-3,5-dione with 11-substituted-1,6-methano[10]annulene

P. Ashkenazi and M. Kaftory



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Acta Cryst. (1993). C49, 735-738    [doi:10.1107/S0108270192009910]

2,2'-Bis(acetamido)biphenyl

J. P. Reboul, G. Pèpe, D. Siri, Y. Oddon, C. Caranoni, H. Rahal, J. C. Soyfer and J. Barbe



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Acta Cryst. (1993). C49, 738-741    [doi:10.1107/S0108270192004530]

Structure of MAP:MNA, the 1:1 adduct between (R)-methyl 2-(2,4-dinitroanilino)propanoate (MAP) and 2-methyl-4-nitroaniline (MNA), a new nonlinear optical crystal

R. M. Metzger, J. L. Atwood, W.-J. Lee, S. M. Rao, R. B. Lal and B. H. Loo



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Acta Cryst. (1993). C49, 741-744    [doi:10.1107/S010827019201062X]

Structure and crystal packing of the antibacterial drug 1-{[(5-nitro-2-furanyl)methylene]amino}-2,4-imidazolidinedione (nitrofurantoin)

V. Bertolasi, P. Gilli, V. Ferretti and G. Gilli



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Acta Cryst. (1993). C49, 744-747    [doi:10.1107/S010827019201179X]

Structure of N-hexadecylpyridinium chloride monohydrate

H. H. Paradies and F. Habben



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Acta Cryst. (1993). C49, 747-749    [doi:10.1107/S0108270192005651]

Structure of 5-benzoyl-1-[4-(dimethylamino)phenylmethyleneamino]-4-phenyl-1H-pyrimidin-2-one

M. Akkurt and W. Hiller


short format


metal-organic compounds



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Acta Cryst. (1993). C49, 749-751    [doi:10.1107/S0108270192008011]

Structures of trimethyloxosulfonium salts. VII. The dichromate: [(CH3)3SO]2Cr2O7

M. Jannin, R. Puget, C. de Brauer and R. Perret



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Acta Cryst. (1993). C49, 751-752    [doi:10.1107/S0108270192008308]

Structure of potassium tribromo(diethyl sulfoxide)platinate(II)

V. K. Belsky, V. E. Konovalov and V. Yu. Kukushkin



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Acta Cryst. (1993). C49, 753-754    [doi:10.1107/S0108270192008862]

Structure of bis(2-methoxycarbonylethyl-C',O)tin dichloride

S. W. Ng



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Acta Cryst. (1993). C49, 754-756    [doi:10.1107/S0108270192008874]

Structure of bis(triphenyltin) succinate-[bis(triphenyltin) succinate bis(N,N-dimethylformamide)] (1/1)

S. W. Ng and V. G. Kumar Das



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Acta Cryst. (1993). C49, 756-758    [doi:10.1107/S0108270192007765]

Bis(tetrabutylammonium) nonadecaoxohexamolybdenum(VI): a second polymorph

A. L. Rheingold, C. B. White, B. S. Haggerty and E. A. Maatta



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Acta Cryst. (1993). C49, 758-760    [doi:10.1107/S0108270192009843]

Structure of tribenzyl(thiocyanato-N)(triphenylarsine oxide-O)tin

S. W. Ng and V. G. Kumar Das



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Acta Cryst. (1993). C49, 760-763    [doi:10.1107/S0108270192009569]

Structure of ([eta]4-1,5-cyclooctadiene)(1-ferrocenyl-1,3-butanedionato-[kappa]2O,O')rhodium(I)

J. C. Swarts, T. G. Vosloo, J. G. Leipoldt and G. J. Lamprecht


organic compounds



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Acta Cryst. (1993). C49, 763-765    [doi:10.1107/S0108270192009570]

Structure of 5-benzylamino-1-methyl-4-nitroimidazole

H. L. De Bondt, N. M. Blaton, O. M. Peeters and C. J. De Ranter



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Acta Cryst. (1993). C49, 765-766    [doi:10.1107/S0108270192007145]

Structure of 11-(4-bromophenyl)-1,2,3,4,5,6-hexahydro-1,6-methano-1,6-benzodiazocine

M. Dunaj-Jurco, D. Miklos and J. Jendrichovský



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Acta Cryst. (1993). C49, 767-768    [doi:10.1107/S0108270192007625]

Tetra-n-propyl-1,2-dithioxodi-[lambda]5-phosphane

R. Sillanpää, Ö. Ergin and S. Çelebi



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Acta Cryst. (1993). C49, 768-770    [doi:10.1107/S0108270192009806]

Structure of ethyl 2-(3-methyl-1,2,4-oxadiazol-5-yl)-2-phenylhydrazonoethanoate

R. Bardi, A. M. Piazzesi and A. Del Pra



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Acta Cryst. (1993). C49, 770-772    [doi:10.1107/S0108270192009557]

Structure of a 2'-oxo-8.1'-neolignan

D. L. Galinis, D. C. Swenson and D. F. Wiemer



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Acta Cryst. (1993). C49, 772-774    [doi:10.1107/S010827019200965X]

1,1,4-Trimethylsilacyclohexan-4-ol

A. Negron, C. L. Barnes and J. A. Soderquist



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Acta Cryst. (1993). C49, 774-776    [doi:10.1107/S0108270192006644]

Structure of galphimine B

R. A. Toscano, A. Ortega, E. Maldonado, R. Gaviño, X. Lozoya and J. Tortoriello



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Acta Cryst. (1993). C49, 776-778    [doi:10.1107/S0108270192010655]

Structure of a coupled carbohydrate and terpene

K. A. Abboud, S. Jiang and E. J. Enholm



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Acta Cryst. (1993). C49, 779-781    [doi:10.1107/S0108270192010618]

Structure of 1H-indazole-3-carboxylic acid

F. Benetollo and A. Del Pra


regular structural papers


inorganic compounds



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Acta Cryst. (1993). C49, 782-784    [doi:10.1107/S010827019201148X]

Refinement of the structure of Tl2AlF5.H2O

M. Molinier and W. Massa



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Acta Cryst. (1993). C49, 784-786    [doi:10.1107/S0108270192010588]

Mercury(II) arsenate, a graphtonite-type structure

A.-K. Larsson, S. Lidin, C. Stålhandske and J. Albertsson



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Acta Cryst. (1993). C49, 786-788    [doi:10.1107/S0108270192010904]

A new one-dimensional compound: synthesis and structure of InNb3(Se2)6

S. Deng, H. Zhuang, Jinshun Huang and Jingling Huang


metal-organic compounds



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Acta Cryst. (1993). C49, 788-790    [doi:10.1107/S0108270192012058]

Structure of 1-benzhydryl-4-(2-benzoylethyl)piperazinium tetrachlorocuprate(II) hydrate

J. Macícek, J. Tcholakova and M. Parvanova



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Acta Cryst. (1993). C49, 791-793    [doi:10.1107/S0108270192010576]

1-(N,N-Dimethylferrocenylmethylamine)-2-methyl-3-(trimethylsilyl)-2,3-dicarba-1-plumba-closo-heptaborane(6)

H. Zhang, L. Jia and N. S. Hosmane



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Acta Cryst. (1993). C49, 793-796    [doi:10.1107/S0108270192010229]

A diphenylformamidinate-bridged terpyridineplatinum(II) dimer

J. A. Bailey, V. M. Miskowski and H. B. Gray



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Acta Cryst. (1993). C49, 796-799    [doi:10.1107/S0108270192010564]

Structure of [1,9-bis(2-pyridyl)-2,5,8-triazanonane]zinc(II) tetrachlorozincate(II)

M. E. Sosa-Torres, V. M. Ugalde-Saldívar, M. J. Rosales-Hoz and R. A. Toscano



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Acta Cryst. (1993). C49, 799-801    [doi:10.1107/S010827019201117X]

Tetrachlorobis(2-pyridone)-bis([mu]2-2-pyridone)-dicopper

A. J. Blake and R. E. P. Winpenny



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Acta Cryst. (1993). C49, 801-803    [doi:10.1107/S0108270192011089]

Structure of [3,10-dimethyl-4,9-diaza-3,9-dodecadiene-2,11-dione dioximato(1-)](isothiocyanato)copper(II)

T. H. Tahirov, T.-H. Lu, H. Luh and C.-S. Chung



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Acta Cryst. (1993). C49, 803-805    [doi:10.1107/S010827019201237X]

N2-[2,2-Bis(diphenylphosphino)ethyl]-N1,N1-dimethylethane-1,2-diamine}-1[kappa]2P,P':2[kappa]2N1,N2-tetracarbonyl-1[kappa]4C-dichloro-2[kappa]2Cl-molybdenumzinc(II), a bimetal complex with a hetero-bifunctional ligand

U. Flörke and H.-J. Haupt



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Acta Cryst. (1993). C49, 805-808    [doi:10.1107/S0108270192011223]

2-[eta]3-Allyl-1,1,1-tricarbonyl-[mu]-([eta]1:[eta]6-diphenylmethyl)chromiumpalladium(Pd-Cr) at 130 K

V. N. Kalinin, I. A. Cherepanov, S. K. Moiseev, F. M. Dolgushin, A. I. Yanovsky and Yu. T. Struchkov



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Acta Cryst. (1993). C49, 808-810    [doi:10.1107/S0108270192010825]

Barium bis(trimethylacetate)-18-crown-6 (1/1)

A. L. Rheingold, C. B. White, B. S. Haggerty, P. Kirlin and R. A. Gardiner


organic compounds



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Acta Cryst. (1993). C49, 810-813    [doi:10.1107/S0108270192011442]

3,4,5-Trihydroxybenzohydroxamic acid monohydrate, a ribonucleotide reductase inhibitor

B. B. Nielsen and I. K. Larsen



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Acta Cryst. (1993). C49, 813-815    [doi:10.1107/S0108270192010898]

Isopropylammonium dihydrogenmonophosphate and isopropylammonium monohydrogenphosphite

M.-T. Averbuch-Pouchot



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Acta Cryst. (1993). C49, 815-818    [doi:10.1107/S0108270192010771]

Structures of glycinium phosphite and glycylglycinium phosphite

M.-T. Averbuch-Pouchot



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Acta Cryst. (1993). C49, 818-820    [doi:10.1107/S010827019201134X]

X-ray structure of a new pyrethroid, RU 52259

F. Hamzaoui, J. Lamiot and F. Baert



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Acta Cryst. (1993). C49, 820-824    [doi:10.1107/S0108270192011545]

Structures of tribenzylmethanol and 1,2,3-triphenyl-2-propanol

G. Ferguson, J. F. Gallagher, C. Glidewell, D. C. Liles and C. M. Zakaria



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Acta Cryst. (1993). C49, 824-825    [doi:10.1107/S0108270192011788]

Structure of (+)-(S)-5-phenyl-5-ethylhydantoin

G. Coquerel, M. N. Petit and F. Robert



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Acta Cryst. (1993). C49, 826-828    [doi:10.1107/S0108270192011156]

Structure of a tricyclo[3.2.1.02,7]octene derivative: a double bridged central ring in an octahydrobenz[g]-3-nitroindole

A. Meetsma, R. ten Have, F. R. Leusink and A. M. van Leusen



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Acta Cryst. (1993). C49, 828-830    [doi:10.1107/S0108270192011399]

Structure du (2S,6'R)-2-amino-2-(1,2:3,4-di-O-isopropylidène-[alpha]-D-galactopyranos-6-yl)acétate de méthyle

A. Chiaroni, C. Riche, E. M. El Hadrami, J.-P. Lavergne et P. Viallefont



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Acta Cryst. (1993). C49, 831-833    [doi:10.1107/S0108270192010606]

Structure of 1,3-bis(1-pyrenyl)hexamethyltrisilane

L. Van Meervelt



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Acta Cryst. (1993). C49, 833-834    [doi:10.1107/S0108270192010886]

Structure of the photostable form of p-nitrocinnamic acid

Y. Kageyama, T. Iwamoto, M. Haisa and S. Kashino



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Acta Cryst. (1993). C49, 834-837    [doi:10.1107/S0108270192011302]

2-Amino-5-nitropyridinium monohydrogenphosphite

J. Pecaut and M. Bagieu-Beucher



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Acta Cryst. (1993). C49, 837-841    [doi:10.1107/S0108270192012216]

A twist-boat 1,3,5-triaryl-1,3,5-triazacyclohexane: X-ray analysis of the inclusion compound formed between 1,3,5-tris(p-nitrophenyl)-1,3,5-triazacyclohexane and pyridine

D. Adam, P. H. McCabe, G. A. Sim and A. Bouchemma



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Acta Cryst. (1993). C49, 841-843    [doi:10.1107/S0108270192010540]

5-(3-Iodophényl)-2,3-dihydro-5-hydroxy-5H-imidazo[2,1-a]isoindole

N. Rodier, V. Agafonov, J. M. Cense, E. Galinier, J. E. Ombetta, Y. Frangin et D. Guilloteau



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Acta Cryst. (1993). C49, 844-846    [doi:10.1107/S0108270192011387]

Etude de la regio et de la stéréospecificité de l'addition du phénylnitriloxyde au 3-methyl-2-benzylidene indan-1-one. Structure de l'adduit obtenu

L. Toupet, R. Chekti, M. Soufiaoui et R. Carrie



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Acta Cryst. (1993). C49, 846-848    [doi:10.1107/S0108270192011880]

Structure of dimethyl 9-chloro-9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboxylate

J. Trotter and V. C. Yee


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