Acta Crystallographica Section C

Crystal Structure Communications

Volume 49, Part 6 (June 1993)



research papers


inorganic compounds



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Acta Cryst. (1993). C49, 1039-1041    [doi:10.1107/S0108270193000058]

Structure of sodium tetrahydroxyborate

L. J. Csetenyi, F. P. Glasser and R. A. Howie


metal-organic compounds



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Acta Cryst. (1993). C49, 1041-1044    [doi:10.1107/S0108270192012836]

Structure of catena-poly[tris(pyridine)copper-[mu]-{N-(2-hydroxyiminopropionyl)-L-methioninato(1-)-O'',N':O}] nitrate ethanol solvate

I. O. Fritsky, R. D. Lampeka, V. Kh. Kravtsov and Y. A. Simonov



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Acta Cryst. (1993). C49, 1044-1046    [doi:10.1107/S0108270192011958]

Structures of triphenylantimony(V) dibromide and dichloride

M. J. Begley and D. B. Sowerby



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Acta Cryst. (1993). C49, 1047-1049    [doi:10.1107/S0108270192005122]

Structure of tetrakis([mu]-acetato-5[kappa]O:[kappa]O')-bis(2-cyano-[kappa]N-guanidine)dicopper(II)

M. J. Begley, P. Hubberstey, P. H. Spittle and P. H. Walton



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Acta Cryst. (1993). C49, 1049-1052    [doi:10.1107/S0108270192013192]

Structure of bis(2,2'-bipyrimidine-N,N')dichlorocobalt(II), [Co(bpm)2Cl2]

G. De Munno, F. Nicolò and M. Julve



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Acta Cryst. (1993). C49, 1052-1056    [doi:10.1107/S0108270193001076]

A novel type of two-dimensional pattern of association of mixed-valence dimers in the structures of two cation radical salts of thieno- and selenolo[3,4-d]-1,3-dithiol-2-ylidene and a monovalent hexanuclear chalcohalide rhenium cluster anion

J.-C. Gabriel, I. Johannsen, P. Batail and C. Coulon



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Acta Cryst. (1993). C49, 1056-1059    [doi:10.1107/S0108270193000903]

Structure of [FeH(N2){(H5C2)2PCH2CH2P(C2H5)2}2]BPh4

I. E. Buys, L. D. Field, T. W. Hambley and A. E. D. McQueen



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Acta Cryst. (1993). C49, 1059-1061    [doi:10.1107/S0108270193000551]

Structure of diaquadibromobis(tetrahydrofuran)dilithium-tetrakis(methyleneoxydiphenylphosphinato)dimercury(II), [Hg(Br){CH2P(O)Ph2}2Li(H2O)(C4H8O)]2

R. A. Kresinski and J. P. Fackler Jnr



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Acta Cryst. (1993). C49, 1061-1063    [doi:10.1107/S0108270193000630]

Structure of dicarbonyl([eta]5-pentamethylcyclopentadienyl)iridium

J. Chen, L. M. Daniels and R. J. Angelici



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Acta Cryst. (1993). C49, 1063-1066    [doi:10.1107/S0108270193002033]

Structure of cis-(1,2-ethanediamine)(1,4,8,11-tetraazacyclotetradecane)chromium(III) perchlorate

K. A. Beveridge, D. Heyd and A. D. Kirk



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Acta Cryst. (1993). C49, 1066-1068    [doi:10.1107/S010827019300157X]

Tetrakis(2-chlorobenzyl)lead

U. Fahrenkampf, M. Schürmann and F. Huber



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Acta Cryst. (1993). C49, 1068-1070    [doi:10.1107/S0108270193001568]

Structure of tetrabutylammonium bis[benzene-1,2-dithiolato(2-)]oxorhenate(V)

R. Hübener and U. Abram


organic compounds



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Acta Cryst. (1993). C49, 1070-1072    [doi:10.1107/S0108270192012290]

Structure of N-(2-aminophenyl)-N'-methylurea

B. J. Jean-Claude, J. F. Britten and G. Just



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Acta Cryst. (1993). C49, 1072-1075    [doi:10.1107/S010827019300023X]

Structure of tris(2,4,6-trimethoxyphenyl)phosphine oxide hydrate

P. A. Chaloner, R. M. Harrison and P. B. Hitchcock



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Acta Cryst. (1993). C49, 1075-1077    [doi:10.1107/S0108270192013441]

Thiophene chalcone

Z. Li and G. Su



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Acta Cryst. (1993). C49, 1078-1080    [doi:10.1107/S0108270192012976]

Structure of linuron, 3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea

H. Cadiergue, G. Pèpe, J. P. Astier, R. Boistelle and J. F. Fiard



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Acta Cryst. (1993). C49, 1080-1082    [doi:10.1107/S0108270192012939]

Structure of cis-1-{2-[(2-butoxy)phenylcarbamoyloxy]cycloheptylmethyl}piperidinium chloride

V. Kettmann, J. Sivý, E. Fresová and F. Gregán



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Acta Cryst. (1993). C49, 1082-1087    [doi:10.1107/S0108270192013325]

Structures of three electron donor-acceptor complexes of dibenz[a,h]anthracene (DBA)

D. E. Zacharias



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Acta Cryst. (1993). C49, 1087-1092    [doi:10.1107/S0108270192009922]

The monoclinic phase of the 2/1 inclusion compound between deoxycholic acid and o-xylene

S. Cerrini, G. Pochetti, F. Gallese and E. Possagno



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Acta Cryst. (1993). C49, 1092-1094    [doi:10.1107/S0108270192012642]

Mesoionic compounds. 4. Structure of 1,4,5-triphenyl-1,2,4-triazolium-3-thiolate

K.-K. Cheung, A. Echevarria, S. Galembeck, M. A. M. Maciel, J. Miller, V. M. Rumjanek and A. M. Simas



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Acta Cryst. (1993). C49, 1095-1097    [doi:10.1107/S0108270193002094]

Structure of a dideoxynucleoside active against the HIV (AIDS) virus

J. M. Gulbis, M. F. Mackay, G. Holan and S. M. Marcuccio



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Acta Cryst. (1993). C49, 1098-1103    [doi:10.1107/S0108270192012927]

Structures of some methylenecyclobutanols and transposed derivatives

S. Ianelli, M. Nardelli, D. Belletti, B. Jamart-Grégoire, N. Brosse and P. Caubère



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Acta Cryst. (1993). C49, 1104-1107    [doi:10.1107/S010827019300071X]

Two structures involved in the separation of the enantiomeric pair of 2,2'-spirobi[indan]-1,1'-dione

B. B. Iversen, E. R. Møller, L. Krogh, M. F. Holm, E. Dynesen, F. K. Larsen and R. G. Hazell



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Acta Cryst. (1993). C49, 1107-1111    [doi:10.1107/S0108270192011168]

Structure of 4-iodo-trans-cinnamic acid and a study of carboxyl group disorder

B. S. Goud, S. S. Pathaneni and G. R. Desiraju



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Acta Cryst. (1993). C49, 1111-1113    [doi:10.1107/S0108270192003937]

Structure of 1-amino-3-(methylthio)propylphosphonic acid

W. Sawka-Dobrowolska, E. Matczak-Jon and L. Dembkowski



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Acta Cryst. (1993). C49, 1113-1116    [doi:10.1107/S010827019201059X]

(3R,6R)-3,4-Dimethyl-1,4-diazabicyclo[4.4.0]decane-2,5-dione

M. Verbruggen, A. T. H. Lenstra, F. Reyniers and F. Borremans


short format


metal-organic compounds



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Acta Cryst. (1993). C49, 1117-1120    [doi:10.1107/S0108270193000836]

Structures of ortho-metalated [2-(p-tolyl)pyridine]iridium(III) complexes

F. O. Garces, K. Dedeian, N. L. Keder and R. J. Watts



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Acta Cryst. (1993). C49, 1120-1121    [doi:10.1107/S0108270192012903]

Structure of bis[(bipyridyl)dicyanatocopper(II)](Cu-Cu)

M. Kabesová, V. Jorík and M. Dunaj-Jurco



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Acta Cryst. (1993). C49, 1121-1123    [doi:10.1107/S0108270193001830]

Bis[bis(triphenylphosphine)iminium] dodecacarbonylhexanickelate

R. E. Bachman and K. H. Whitmire


organic compounds



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Acta Cryst. (1993). C49, 1123-1125    [doi:10.1107/S0108270192011077]

Structure of 17[beta]-acetoxy-18-methyl-1-thia-A-norestra-3,9(10),11-trien-2-one

K. Okada and H. Koyama



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Acta Cryst. (1993). C49, 1125-1127    [doi:10.1107/S0108270193001763]

1-[3-(3,4-Methylenedioxyphenoxy)propyl]-4-phenylpiperazine monohydrochloride

K. Okamoto, S. Fujii and K. Tomita



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Acta Cryst. (1993). C49, 1127-1128    [doi:10.1107/S0108270193001088]

Structure of 2,2-bis(3,5-di-tert-butylphenyl)propane-2',2''-dithiol

W. Hiller and W. Rundel



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Acta Cryst. (1993). C49, 1129-1130    [doi:10.1107/S0108270193001799]

Structure of 2-selenoxoperhydro-2H-thieno[3,4-d][1,3]dithiole 5,5-dioxide

E. Molins, J. Veciana and C. Miravitlles


regular structural papers


inorganic compounds



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Acta Cryst. (1993). C49, 1131-1133    [doi:10.1107/S0108270192012599]

Distrontium nickel orthophosphate

B. Elbali, A. Boukhari, E. M. Holt and J. Aride



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Acta Cryst. (1993). C49, 1133-1135    [doi:10.1107/S0108270192012368]

Structure of hexagonal V3S4 determined at three different temperatures

W. Bensch and J. Koy



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Acta Cryst. (1993). C49, 1135-1137    [doi:10.1107/S010827019201285X]

A new type of one-dimensional compound: structure of Nb4(Te2)4Te4I

S. Deng, H. Zhuang, C. Lu, Jinshun Huang and Jingling Huang


metal-organic compounds



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Acta Cryst. (1993). C49, 1138-1140    [doi:10.1107/S0108270192012897]

Tris[(1,2,3-[eta])-1-ethylindenyl]methylthorium(IV)

M. R. Spirlet, J. Rebizant, S. Bettonville and J. Goffart



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Acta Cryst. (1993). C49, 1140-1142    [doi:10.1107/S0108270192013015]

Structure of [Cu2(dmpe)3Cl2]n.2CH2Cl2

J. H. Reibenspies, D. J. Darensbourg and E. M. Longridge



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Acta Cryst. (1993). C49, 1142-1146    [doi:10.1107/S0108270192012575]

Structures of the monoclinic form of Ph3PAuRuRh3(CO)12 (I) and its cubic form with Ru3(CO)12 (II)

J. Pursiainen, T. A. Pakkanen, M. Ahlgrén and J. Valkonen



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Acta Cryst. (1993). C49, 1146-1148    [doi:10.1107/S0108270192012666]

Structure of trans-[Rh(PPh3)2(CO)(OH2)][ClO4].CH2Cl2

R. J. Cross, A. R. Kennedy, L. Manojlovic-Muir and K. W. Muir



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Acta Cryst. (1993). C49, 1148-1150    [doi:10.1107/S0108270192012484]

Di-[mu]-nitrato-bis[bis(triphenylphosphine)silver(I)], [(Ph3P)2AgNO3]2, at 178 K

P. G. Jones



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Acta Cryst. (1993). C49, 1150-1152    [doi:10.1107/S0108270192012605]

Structure of sodium hydrogen (+)-tartrate monohydrate

R. C. Bott, D. S. Sagatys, D. E. Lynch, G. Smith and C. H. L. Kennard



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Acta Cryst. (1993). C49, 1152-1154    [doi:10.1107/S0108270192012496]

Structure of di-2-pyridyl ketone-hydrate platinum(II) chloride tetrahydrate

S. O. Sommerer and K. A. Abboud



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Acta Cryst. (1993). C49, 1154-1156    [doi:10.1107/S0108270192012435]

Redetermination of the structure of polymeric carboxyethylgermanium sesquioxide

Z.-X. Xie, S.-Z. Hu, Z.-H. Chen, S.-A. Li and W.-P. Shi



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Acta Cryst. (1993). C49, 1156-1158    [doi:10.1107/S0108270192011570]

Structure of CdCl2.C3H7NO2

K. I. Schaffers and D. A. Keszler



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Acta Cryst. (1993). C49, 1158-1160    [doi:10.1107/S0108270193000447]

Structure of monomeric hydrated manganese(III) tetra(4-N-methylpyridyl)porphyrin pentachloride

S. Prince, F. Körber, P. R. Cooke, J. R. Lindsay Smith and M. A. Mazid



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Acta Cryst. (1993). C49, 1160-1163    [doi:10.1107/S0108270192013246]

Structure of (2,4-pentanedionato-O,O')bis(phenyl 3,3',5,5'-tetra-tert-butyl-1,1'-biphenyl-2,2'-diyl phosphite-P)rhodium

A. Meetsma, T. Jongsma, G. Challa and P. W. N. M. van Leeuwen



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Acta Cryst. (1993). C49, 1163-1169    [doi:10.1107/S0108270192012265]

Structures of two cobalt(III) sepulchrate complexes

A. Bacchi, F. Ferranti and G. Pelizzi



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Acta Cryst. (1993). C49, 1169-1171    [doi:10.1107/S0108270192011855]

Structure of di-[mu]-chloro-bis[bis(triphenylphosphine)palladium(II)] bis(tetrafluoroborate) acetone solvate dihydrate

S. Ganguly, E. M. Georgiev, J. T. Mague and D. M. Roundhill



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Acta Cryst. (1993). C49, 1171-1173    [doi:10.1107/S0108270192012514]

Structure of pentaaqua(L-serine)holmium(III) trichloride

T. Glowiak and C. N. Dao



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Acta Cryst. (1993). C49, 1173-1175    [doi:10.1107/S0108270192012150]

Structures of the cadmium halide complexes [{CdCl2(dmso)(MeOH)}n] and [{CdBr2(dmso)(MeOH)}n] with coordinated dimethyl sulfoxide and methanol

M. Nieuwenhuyzen, W. T. Robinson and C. J. Wilkins



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Acta Cryst. (1993). C49, 1176-1178    [doi:10.1107/S0108270192011697]

Structure of cis-[1,2-bis(dicyclohexylphosphino)ethane-P,P']dichloroplatinum(II) chloroform solvate

J. T. Mague, M. J. Fink and C. A. Recatto


organic compounds



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Acta Cryst. (1993). C49, 1178-1180    [doi:10.1107/S0108270192012630]

Interactions of thiamine with anions. Structure of thiamine dithiocyanate

N.-H. Hu and S.-L. Zhang



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Acta Cryst. (1993). C49, 1180-1182    [doi:10.1107/S0108270192013076]

Non-steroidal anti-inflammatory drugs. II. Structure of (E)-2,6-di-tert-butyl-4-[2-(4-fluorophenyl)ethenyl]phenol

K. Ravikumar



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Acta Cryst. (1993). C49, 1182-1184    [doi:10.1107/S010827019201309X]

Structure of N-(2-hydroxyethyl)ethylenediaminetriacetic acid

V. Kettmann, J. Lokaj, C. Ducamp-Sanguesa, M. Figlarz and M. Touboul



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Acta Cryst. (1993). C49, 1184-1187    [doi:10.1107/S0108270192013313]

Structure of the bis(7,7,8,8-tetracyano-p-quinodimethane)-4-(benzylmethylaminomethyl)-2,2',5,5'-tetrathiafulvalene charge-transfer complex

S. Triki, L. Ouahab, D. Grandjean, J. Garin, S. Uriel and J. M. Fabre



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Acta Cryst. (1993). C49, 1187-1189    [doi:10.1107/S0108270192013222]

Structures of 3,4-dimethyl-2,2',5,5'-tetrathiafulvalene perrhenate, (DMTTF)ReO4, and 3',4'-dimethyl-3,4-tetramethylene-2,5-dithia-2',5'-diselenafulvalene hexafluorophosphate, (CHDTDMDSF)PF6

A. Mhanni, L. Ouahab, D. Grandjean, J. Amouroux and J. M. Fabre



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Acta Cryst. (1993). C49, 1189-1192    [doi:10.1107/S0108270192013283]

Structure of anthracenediylidene-bis(1,3-dithiole)-tetracyanoquinodimethane-bis(cyanoformyl)phenyl-malononitrile ylide monohydrate: (Ext-TTF2+).TCNQ.(Y-)2.(H2O)

S. Triki, L. Ouahab, D. Lorcy and A. Robert



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Acta Cryst. (1993). C49, 1192-1195    [doi:10.1107/S0108270192013568]

Structures of the 1:1 and 2:1 adducts of (+)-(S)-[2.2]paracyclophane-4-carboxylic acid and (-)-ephedrine

P. G. Jones, D. Döring, T. Laue and H. Hopf



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Acta Cryst. (1993). C49, 1195-1197    [doi:10.1107/S0108270192010527]

(-)-(S)-[alpha]-Phenylethylammonium (-)-(R)-[2.2]paracyclophane-4-carboxylate

P. G. Jones, T. Laue and H. Hopf



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Acta Cryst. (1993). C49, 1197-1199    [doi:10.1107/S0108270193000277]

Structure of [alpha]-tetrachlorothiophene 1,1-dioxide at 150 K

G. Douglas, C. S. Frampton and K. W. Muir



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Acta Cryst. (1993). C49, 1199-1201    [doi:10.1107/S0108270192013003]

Structure of a chiral monocyclic phosphonamide

K. J. Koeller, N. P. Rath and C. D. Spilling



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Acta Cryst. (1993). C49, 1201-1203    [doi:10.1107/S0108270192012915]

Structure of endo-(5R*,6R*,10R*,11S*)-10-(tert-butyldimethylsiloxy)-5,6,10,11-tetrahydro-5-hydroxy-4,11-dimethoxy-7,7,9-trimethyl-6,10-methano-(7H)-benzocyclononene-8-carbaldehyde

S. Kamei, A. Uchida, Y. Ohashi, M. Seto, K. Morihira, Y. Horiguchi and I. Kuwajima



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Acta Cryst. (1993). C49, 1203-1205    [doi:10.1107/S0108270192012940]

Structure of a triazaoxabicyclodecatriene derivative

P. Beltrame, G. Gelli, E. Cadoni, M. M. Carnasciali, M. Pani and A. Mugnoli



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Acta Cryst. (1993). C49, 1205-1207    [doi:10.1107/S010827019300006X]

Structure of photochromic spiroxazines. II. 1',3',3'-Trimethylspiro{anthra[2,1-f][1,4]benzoxazine-2,2'-indoline}-7,12-dione

R. Millini, G. Del Piero, P. Allegrini, V. Malatesta and G. Castaldi



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Acta Cryst. (1993). C49, 1207-1209    [doi:10.1107/S0108270192013374]

[beta]-Homopipitzolone

E. Huipe-Nava, V. A. Igonin, S. V. Lindeman, Yu. T. Struchkov, V. Mendoza, E. Garcia G. and J. A. Guzman



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Acta Cryst. (1993). C49, 1209-1211    [doi:10.1107/S0108270192013271]

Structure of 4-nitrobenzyl N-(4-nitrobenzyloxy)trifluoroacetimidate

D. M. Brown, P. K. T. Lin and L. Van Meervelt



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Acta Cryst. (1993). C49, 1211-1215    [doi:10.1107/S0108270192013453]

Orthorhombic form of thiopurinol: 1,5-dihydro-4H-pyrazolo[3,4-d]pyrimidine-4-thione

P. Singh and L. G. Pedersen



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Acta Cryst. (1993). C49, 1215-1218    [doi:10.1107/S0108270193000034]

Structure of 1,3,5-trichloro-2,4,6-trinitrobenzene

F. Gerard, A. Hardy and A. Becuwe



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Acta Cryst. (1993). C49, 1218-1220    [doi:10.1107/S0108270193000095]

Structure of cis-4-cyclohexene-1,2-dicarboxylic acid

H. Küppers and S. A. Kim



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Acta Cryst. (1993). C49, 1220-1222    [doi:10.1107/S0108270192012824]

N,N'-Dimethylcryptand[2.2.2] diiodide

N. Korber and M. Jansen



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Acta Cryst. (1993). C49, 1222-1224    [doi:10.1107/S0108270192013210]

(R)-2-Bromo-1,4-butanedioic acid

J. F. Britten, H. E. Howard-Lock, D. Leblanc and C. J. L. Lock



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Acta Cryst. (1993). C49, 1224-1227    [doi:10.1107/S0108270193000083]

(+)-(R)- and racemic forms of 2,2'-dihydroxy-1,1'-binaphthyl

K. Mori, Y. Masuda and S. Kashino



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Acta Cryst. (1993). C49, 1227-1230    [doi:10.1107/S0108270193000186]

Structure of 6-O-methylerythromycin A (clarithromycin)

H. Iwasaki, Y. Sugawara, T. Adachi, S. Morimoto and Y. Watanabe



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Acta Cryst. (1993). C49, 1230-1232    [doi:10.1107/S0108270192012769]

Structure of a pyrano[2,3-b]indolizine

A. Kakehi, K. Kitajima, S. Ito and N. Takusagawa



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Acta Cryst. (1993). C49, 1232-1234    [doi:10.1107/S0108270193000071]

Structure of the [gamma] phase of erucic acid

F. Kaneko, K. Yamazaki, M. Kobayashi, Y. Kitagawa, Y. Matsuura, K. Sato and M. Suzuki



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Acta Cryst. (1993). C49, 1234-1237    [doi:10.1107/S0108270193000113]

Structure of a coupled carbohydrate and terpene

K. A. Abboud, S. Jiang and E. J. Enholm



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Acta Cryst. (1993). C49, 1237-1238    [doi:10.1107/S0108270193000496]

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