Acta Crystallographica Section C

Crystal Structure Communications

Volume 49, Part 7 (July 1993)



research papers


metal-organic compounds



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Acta Cryst. (1993). C49, 1243-1246    [doi:10.1107/S0108270193002999]

Structure of trimethyltelluronium bis(4,5-dimercapto-1,3-dithiole-2-thionato)aurate(III)

K. Swaminathan, P. J. Carroll, Kochurani, H. B. Singh and H. D. Bhargava



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Acta Cryst. (1993). C49, 1246-1248    [doi:10.1107/S0108270193002471]

Structure of a platinum(II) complex of levamisole

G. M. Arvanitis, M. E. Berardini, G. N. Parkinson and B. S. Schneider



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Acta Cryst. (1993). C49, 1249-1251    [doi:10.1107/S0108270193001404]

A polymeric copper(II) complex with 2,2'-bipyridine and 1,2-benzenedicarboxylate(2-)

D. Poleti, Lj. Karanovic and B. V. Prelesnik



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Acta Cryst. (1993). C49, 1252-1255    [doi:10.1107/S0108270193001416]

Structure of aquachloro[tris(2-aminoethyl)amine]nickel(II) chloride monohydrate

A. Marzotto, D. A. Clemente and G. Valle



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Acta Cryst. (1993). C49, 1255-1258    [doi:10.1107/S0108270193002100]

A new tetranuclear iron(III) complex with an [Fe4O2] core: synthesis, structure and Mössbauer studies of [Fe4([mu]3-O)2([mu]-O2CCH3)6Cl2(3-Mepy)4].CH3C=N (3-Mepy = 3-methylpyridine)

L. Wu, M. Pressprich, P. Coppens and M. J. DeMarco



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Acta Cryst. (1993). C49, 1259-1262    [doi:10.1107/S010827019300321X]

Structures of trans-[TcCl4{P(CH3)3}2] and [P(C7H7)3{C(CH3)2CH2COCH3}]2[TcCl6]

F. D. Rochon and R. Melanson



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Acta Cryst. (1993). C49, 1262-1264    [doi:10.1107/S0108270193002239]

Structure of [mu]6-carbido-undecacarbonyldi([mu]3-sulfido)(triphenylphosphine)-triprismo-hexacobalt

G. Gervasio and R. Rossetti


short format


metal-organic compounds



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Acta Cryst. (1993). C49, 1265-1267    [doi:10.1107/S0108270193001970]

Structures of cis- and trans-bis(ethylenediamine)(isothiocyanato)(thiosulfato)cobalt(III)

K. Tang, M. E. Kastner, J. N. Cooper, M. Kanaskie and A. Monoski


regular structural papers


inorganic compounds



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Acta Cryst. (1993). C49, 1268-1270    [doi:10.1107/S0108270192013143]

Refinement of the structure of Sr2RuO4 with 100 and 295 K X-ray data

L. Walz and F. Lichtenberg



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Acta Cryst. (1993). C49, 1270-1271    [doi:10.1107/S0108270192013131]

Structure cristalline du sulfure d'ytterbium et d'indium: Yb4/3In4/3S4

A. Likforman et M. Guittard



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Acta Cryst. (1993). C49, 1271-1275    [doi:10.1107/S0108270192013465]

Structure of hexaaquacobalt(II) perbromate

A. C. Blackburn and R. E. Gerkin



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Acta Cryst. (1993). C49, 1275-1277    [doi:10.1107/S0108270193000460]

Structure du monophosphate synthétique de cuivre et de sodium

A. Kawahara, T. Kageyama, I. Watanabe et J. Yamakawa


metal-organic compounds



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Acta Cryst. (1993). C49, 1277-1280    [doi:10.1107/S0108270193001155]

Bis(tetraphenylarsonium) aquatetra(cyano-C)nitridorhenate(V) pentahydrate

J. F. Britten, C. J. L. Lock and Y. Wei



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Acta Cryst. (1993). C49, 1280-1283    [doi:10.1107/S0108270192013180]

Structures of amino(triphenyl)phosphonium bromide and amino(triphenyl)phosphonium hexachloroantimonate

E. Pohl, H. J. Gosink, R. Herbst-Irmer, M. Noltemeyer, H. W. Roesky and G. M. Sheldrick



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Acta Cryst. (1993). C49, 1283-1284    [doi:10.1107/S0108270193001301]

Structure of potassium silanolate at 153 K

F. Pauer and G. M. Sheldrick



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Acta Cryst. (1993). C49, 1284-1286    [doi:10.1107/S0108270193000228]

Structure of a phenyl dioxocyclam nickel complex

P. Chinn, D. H. Busch and N. W. Alcock



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Acta Cryst. (1993). C49, 1287-1294    [doi:10.1107/S0108270193000411]

Structures of tetrapotassium, tetrarubidium and tetracaesium 1,4,5,8-naphthalenetetracarboxylate hexahydrates

L. J. Fitzgerald, J. C. Gallucci and R. E. Gerkin



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Acta Cryst. (1993). C49, 1294-1296    [doi:10.1107/S010827019300037X]

catena-Poly[silver(I)-[mu]-(cyano-C:N)-cis-bis(2,2'-bipyridine-N,N')copper(II)-[mu]-(cyano-N:C)] dicyanoargentate(I) monohydrate

J. Cernák, F. Gérard and J. Chomic



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Acta Cryst. (1993). C49, 1297-1298    [doi:10.1107/S0108270193000022]

Isotypie entre les structures cristallines des tétrakis([mu]-acétato)bis(méthanol) dicuivre(II) et de dirhodium(II)

V. Noinville, B. Viossat et Nguyen-Huy Dung



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Acta Cryst. (1993). C49, 1298-1300    [doi:10.1107/S0108270193001209]

Structure of dibromobis(2-chloroimidazole)copper(II)

G. Valle, A. Sánchez González and R. Ettorre



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Acta Cryst. (1993). C49, 1300-1303    [doi:10.1107/S010827019201360X]

Hexaaquadisodium hexakis(tetramethylammonium) bis[bis(3-acetylamino-4-hydroxyphenylarsonato)aquaoctadecaoxohexamolybdate] decahydrate: [Na2(H2O)6][(CH3)4N]6[Mo6(C8H8AsNO5)2O18(H2O)\]2.10H2O

X.-Z. You, H.-L. Li, K.-B. Yu and L. Li



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Acta Cryst. (1993). C49, 1303-1307    [doi:10.1107/S0108270192012952]

Structures of hexachloroniobate(V) salts of the 1-methylimidazole/1-methylimidazolium and 2-methylimidazolium cations

B. Therrien and A. L. Beauchamp



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Acta Cryst. (1993). C49, 1307-1309    [doi:10.1107/S0108270192012812]

Structure of [As(C6H5)4]2[Sn{Se2C=C(CN)2}3]

D. Gruss and H.-U. Hummel



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Acta Cryst. (1993). C49, 1309-1311    [doi:10.1107/S0108270192013337]

Structure of bis-[mu]-[(trimethylsilylmethanolato-O)-bis(trimethylsilylmethyl)gallium] and bis-[mu]-[(trimethylsilylmethanolato-O)-bis(trimethylsilylmethyl)indium]

U. Dembowski, T. Pape, R. Herbst-Irmer, E. Pohl, H. W. Roesky and G. M. Sheldrick



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Acta Cryst. (1993). C49, 1311-1315    [doi:10.1107/S0108270192012691]

CuII and PdII complexes of 3-hydroxy-1,3-bis(2-thienyl)prop-2-en-1-one

L. A. M. Baxter, A. J. Blake, R. O. Gould, G. A. Heath and T. A. Stephenson



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Acta Cryst. (1993). C49, 1315-1317    [doi:10.1107/S0108270192013489]

(1,1-Cyclobutanedicarboxylato-O,O')bis(trimethylphosphine-P)platinum(II) monohydrate

Y. Suzuki, T. K. Miyamoto and H. Ichida



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Acta Cryst. (1993). C49, 1317-1318    [doi:10.1107/S0108270192013490]

(Oxalato-O,O')bis(trimethylphosphine)platinum(II)

Y. Suzuki, T. K. Miyamoto and H. Ichida



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Acta Cryst. (1993). C49, 1318-1320    [doi:10.1107/S0108270192013507]

[SP-4-2]-Dinitratobis(trimethylphosphine)platinum(II)

Y. Suzuki, T. K. Miyamoto and H. Ichida



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Acta Cryst. (1993). C49, 1320-1322    [doi:10.1107/S0108270193000010]

[mu]-Hydroxo diplatinum(II) complex containing bridging cyclometallated 1,3-bis(diphenylphosphino)propane as the tetrafluoroborate salt

M. A. Bennett, D. E. Berry, K. A. Beveridge, J. Browning and M. P. Russow



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Acta Cryst. (1993). C49, 1322-1324    [doi:10.1107/S010827019300085X]

Structure of the trigonal phase of bis(methinyltricobaltenneacarbonyl), [CCo3(CO)9]2

U. Geiser and A. M. Kini



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Acta Cryst. (1993). C49, 1325-1328    [doi:10.1107/S0108270193000770]

Structures of nickel(II) bis- and trisphosphine diisothiocyanate complexes

B. Juma, F. R. Fronczek and G. G. Stanley



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Acta Cryst. (1993). C49, 1328-1330    [doi:10.1107/S0108270192012745]

Structure of bis(diethyldithiocarbamato)diiodotellurium(IV)

R. K. Kumar, G. Aravamudan, M. R. Udupa, M. Seshasayee and T. A. Hamor



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Acta Cryst. (1993). C49, 1330-1333    [doi:10.1107/S0108270193000848]

Bis(4-hydroxymethyl-1,5-dimethylimidazole-N3)gold(I) chloride

C. J. L. Lock and Z. Wang



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Acta Cryst. (1993). C49, 1333-1335    [doi:10.1107/S0108270193000733]

(tert-Butyl isocyano-C)(carbonyl)([eta]5-cyclopentadienyl)(triphenylphosphine-P)ruthenium(II) hexafluorophosphate

S. J. Simpson



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Acta Cryst. (1993). C49, 1335-1336    [doi:10.1107/S0108270193000368]

Structure of guanidinium hexafluorogallate, [C(NH2)3]3GaF6

H. Maluszynska



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Acta Cryst. (1993). C49, 1336-1339    [doi:10.1107/S0108270193000940]

Structure of dipotassium trans-diaquabis(oxalato-O,O')nickelate(II)-water (1/4)

P. Román, C. Guzmán-Miralles and A. Luque



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Acta Cryst. (1993). C49, 1339-1342    [doi:10.1107/S0108270193000642]

A highly solvated zinc(II) tetrakis(pentafluorophenyl)-[beta]-octabromoporphyrin

R. E. Marsh, W. P. Schaefer, J. A. Hodge, M. E. Hughes, H. B. Gray, J. E. Lyons and P. E. Ellis Jnr



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Acta Cryst. (1993). C49, 1342-1345    [doi:10.1107/S0108270193000587]

Copper(II) tetrakis(pentafluorophenyl)-[beta]-octachloroporphyrin

W. P. Schaefer, J. A. Hodge, M. E. Hughes, H. B. Gray, J. E. Lyons, P. E. Ellis Jnr and R. W. Wagner



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Acta Cryst. (1993). C49, 1345-1347    [doi:10.1107/S0108270192013349]

Trimeric bis(cyclopentadienyl)oxozirconium(IV) benzene solvate

O. A. Mikhailova, M. H. Minacheva, V. V. Burlakov, V. B. Shur, A. P. Pisarevsky, A. I. Yanovsky and Yu. T. Struchkov



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Acta Cryst. (1993). C49, 1347-1350    [doi:10.1107/S0108270193000332]

Cobaltocenium bis[(4,5-dimercapto-S4,S5)-1,3-dithiole-2-thionato]nickelate

Q. Fang, X.-Z. You, J.-H. Cai and M.-Y. He



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Acta Cryst. (1993). C49, 1350-1352    [doi:10.1107/S0108270193000289]

Structure of tricarbonyltris(diphenylphosphine)molybdenum(0) hexane solvate: fac-[Mo(CO)3(PPh2H)3] . 0.25C6H14

G. R. Willey, M. L. Butcher, M. T. Lakin and G. W. Downs



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Acta Cryst. (1993). C49, 1352-1354    [doi:10.1107/S0108270192013386]

cis-1-Ferrocenyl-2-(2-nitrophenyl)ethylene

Z. V. Todres, A. I. Yanovsky, D. S. Ermekov and Yu. T. Struchkov



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Acta Cryst. (1993). C49, 1354-1357    [doi:10.1107/S0108270193000381]

Structure of [(2S,4R)-[gamma]-hydroxynorvalinato][(2R,4S)-[gamma]-hydroxynorvalinato]copper(II)

A. Deljac, B. Kaitner, S. I. Kirin and E. Mestrovic



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Acta Cryst. (1993). C49, 1357-1359    [doi:10.1107/S010827019300109X]

Structure of [di-tert-butyl(dimethoxy)salen]cobalt(II)

W. Hiller, A. Nishinaga, T. Tsutsui and A. Rieker



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Acta Cryst. (1993). C49, 1359-1361    [doi:10.1107/S0108270193000484]

Structure of the monomethylgallium derivative of TMTAA (dibenzotetramethyltetraaza[14]annulene)

N. W. Alcock, N. C. Blacker, W. Errington and M. G. H. Wallbridge



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Acta Cryst. (1993). C49, 1361-1363    [doi:10.1107/S010827019300054X]

Structures of chromium(III) cyclam complexes. 5. Structure of trans-dichloro(1,4,8,11-tetraazacyclotetradecane)chromium(III) isothiocyanate

J. Bouckaert, D. Maes, J. N. Lisgarten, T. K. Chattopadhyay, R. A. Palmer, M. A. Mazid and D. M. Gazi



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Acta Cryst. (1993). C49, 1363-1365    [doi:10.1107/S010827019201299X]

Structure of dicarbonylbis-([mu]-3,5-dimethylpyrazolyl)-bis(4-tolyl diphenylphosphinite)diiridium(I)-dichloromethane (1/1)

R. S. Farid, L. M. Henling and H. B. Gray



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Acta Cryst. (1993). C49, 1365-1367    [doi:10.1107/S0108270193000617]

Structure of [N,N'-o-phenylenebis(salicylideneaminato)]iron(III) chloride as a five-coordinate monomer

A. Elmali, Y. Elerman, I. Svoboda and H. Fuess



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Acta Cryst. (1993). C49, 1367-1369    [doi:10.1107/S0108270193000526]

Redetermination of the structure of [mu]6-acetonato-1:2:3[kappa]3C1;4:5:6[kappa]3C3-bis[nonacarbonyl-1[kappa]3C,2[kappa]3C,3[kappa]3C-triangulo-tricobalt(3 Co-Co)] at 128 K

G. H. Worth, B. H. Robinson and J. Simpson



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Acta Cryst. (1993). C49, 1370-1372    [doi:10.1107/S0108270193000046]

Diamminechloro(5-oxoprolinato)platine(II)

B. Viossat, P. Khodadad and N. Rodier



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Acta Cryst. (1993). C49, 1372-1373    [doi:10.1107/S0108270193001878]

Redetermination of tetraphenyllead

H. Preut and F. Huber


organic compounds



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Acta Cryst. (1993). C49, 1373-1376    [doi:10.1107/S0108270193001003]

Structure of a keto derivative of 9,11-dihydrogracilin A

R. Puliti, A. Fontana, G. Cimino, C. A. Mattia and L. Mazzarella



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Acta Cryst. (1993). C49, 1376-1378    [doi:10.1107/S010827019201357X]

Structure of the benzo-15-crown-5-3,5-dinitrobenzoic acid-water (1/1/1) complex

A. Schouten, J. A. Kanters and N. S. Poonia



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Acta Cryst. (1993). C49, 1378-1380    [doi:10.1107/S0108270193000629]

Structure of (S)-(+)-ibuprofen

A. A. Freer, J. M. Bunyan, N. Shankland and D. B. Sheen



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Acta Cryst. (1993). C49, 1380-1384    [doi:10.1107/S0108270193000265]

Synthesis and structure of new families of potential antitumor or antiviral agents. I. 4b,6a,10b,10c-Tetrahydrobenzo[3,4]cyclobuta[1,2-a]biphenylene-4b,6a-diyl diacetate

S. Ianelli, M. Nardelli, D. Belletti, B. Jamart-Grégoire, A. Mouaddib and P. Caubère



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Acta Cryst. (1993). C49, 1384-1388    [doi:10.1107/S0108270192012782]

Synthesis and structure of new families of potential antitumor or antiviral agents. II. 1-(p-Toluenesulfonyloxy)-3,4:7,8-dibenzotricyclo[3.3.2.02,6]decane

S. Ianelli, M. Nardelli, D. Belletti, B. Jamart-Grégoire, A. Zouaoui and P. Caubère



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Acta Cryst. (1993). C49, 1388-1392    [doi:10.1107/S0108270193000319]

Synthesis and structure of strained polycyclic cyclobutane-containing derivatives

S. Ianelli, M. Nardelli, D. Belletti, B. Jamart-Grégoire, N. Brosse and P. Caubère



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Acta Cryst. (1993). C49, 1393-1396    [doi:10.1107/S0108270193000605]

Three monofluorinated small molecules: ortho-fluorophenylglycine, methyl 4-(fluorocarbonyl)benzoate and 16[alpha]-fluoro-[alpha]-estradiol 3-methyl ether

J. H. Burns and E. W. Hagaman



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Acta Cryst. (1993). C49, 1396-1398    [doi:10.1107/S0108270193000654]

Structure of 4-[(3-methoxyphenylimino)methyl]phenol

G.-Y. Yeap, S.-B. Teo, H.-K. Fun and S.-G. Teoh



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Acta Cryst. (1993). C49, 1398-1401    [doi:10.1107/S0108270193000393]

Structure of diiodide salts of N-heteroaromatic dications

Y. Mori, Y. Matsuyama, J. Suzuki, Y. Ishii, S. Yamada and K. Maeda



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Acta Cryst. (1993). C49, 1401-1402    [doi:10.1107/S0108270193000976]

Structure of 2-ethyl-2-nitroindan-1,3-dione

J. G. Garcia, J. D. Enas, E. Chang and F. R. Fronczek



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Acta Cryst. (1993). C49, 1402-1404    [doi:10.1107/S0108270193000198]

Structure of 1-phenylsemicarbazide

N. Okabe



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Acta Cryst. (1993). C49, 1404-1406    [doi:10.1107/S0108270193000241]

Structure of 1,4-diethyl-3,5-dimethoxy-1,4-dihydrobenzoic acid

M. Soriano-García, R. V. Iribe, A. L. Silva and L. A. Maldonado



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Acta Cryst. (1993). C49, 1406-1409    [doi:10.1107/S0108270193000320]

The asymmetric Michael process involving chiral imines: structure of (±)-p-nitrobenzyl 2-(2,2-dimethyl-1-phenylpropylamino)-1-cyclopentene-1-carboxylate

A. Chiaroni, C. Riche, A. Guingant and J. d'Angelo



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Acta Cryst. (1993). C49, 1409-1410    [doi:10.1107/S0108270193001660]

Structure of 1,3-bis(triphenylphosphonium)acetone bis(trifluoromethanesulfonate)

A. Bram, H. Burzlaff, D. Hadawi and H.-J. Bestmann



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Acta Cryst. (1993). C49, 1410-1412    [doi:10.1107/S0108270192013581]

Structure of 2-([alpha]-hydroxybenzyl)-8-methyl-8-azabicyclo[3.2.1]octan-3-one

J. Li, J. W. Quail, G. Z. Zheng and M. Majewski



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Acta Cryst. (1993). C49, 1413-1414    [doi:10.1107/S0108270193000678]

Structure of 8-(dicyclopropylmethyl)-1,3-dipropylxanthine

N. Hirayama, Y. Nagahara, J. Shimada and F. Suzuki


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