Acta Crystallographica Section C

Crystal Structure Communications

Volume 49, Part 9 (September 1993)



research papers


inorganic compounds



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Acta Cryst. (1993). C49, 1555-1559    [doi:10.1107/S0108270193004767]

Structure of [alpha]-dicalcium silicate hydrate

T. Yano, K. Urabe, H. Ikawa, T. Teraushi, N. Ishizawa and S. Udagawa



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Acta Cryst. (1993). C49, 1559-1561    [doi:10.1107/S0108270193003634]

Structure of Ag3Cu12Y5, a new ternary compound

L. Zeng, D. Li and Y. Zhuang


metal-organic compounds



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Acta Cryst. (1993). C49, 1561-1564    [doi:10.1107/S0108270193004275]

Isostructural trigonal-bipyramidal CuII and nominally 1% CuII-doped ZnII complexes with N5 ligation

R. T. Stibrany, J. A. Potenza and H. J. Schugar


organic compounds



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Acta Cryst. (1993). C49, 1564-1566    [doi:10.1107/S0108270193005062]

Redetermination of the structure of phenanthridine

W. A. Brett, P. Rademacher and R. Boese



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Acta Cryst. (1993). C49, 1566-1568    [doi:10.1107/S0108270193005074]

Structure of 1,3,6,8-tetrahydrodithieno[3,4-a:3',4'-c]benzene

W. A. Brett, P. Rademacher and R. Boese



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Acta Cryst. (1993). C49, 1568-1571    [doi:10.1107/S0108270193004123]

Structure of the product from a novel cyclization reaction involving a C(6)-substituted uridine analog

B. Wang, F. Takusagawa, M. P. Mertes and K. Bowman-James


regular structural papers


inorganic compounds



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Acta Cryst. (1993). C49, 1572-1574    [doi:10.1107/S0108270193002082]

Structure of NaSr4[EuW10O36].34.5H2O

T. Yamase, T. Ozeki and K. Ueda



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Acta Cryst. (1993). C49, 1574-1577    [doi:10.1107/S0108270193002070]

Structure of K3Na4H2[SmW10O36].22H2O

T. Ozeki and T. Yamase



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Acta Cryst. (1993). C49, 1577-1580    [doi:10.1107/S0108270193003300]

Structure of K3Na4H2[GdW10O36].21H2O

T. Yamase and T. Ozeki



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Acta Cryst. (1993). C49, 1580-1584    [doi:10.1107/S0108270193001532]

Structure of La5Mo32O54 containing trans bicapped Mo8 octahedral clusters and tricluster Mo7-Mo10-Mo7 chain fragments

P. Gall, L. Toupet and P. Gougeon



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Acta Cryst. (1993). C49, 1584-1585    [doi:10.1107/S0108270193002380]

Structure of UOSe

M. F. Mansuetto, S. Jobic, H. P. Ng and J. A. Ibers



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Acta Cryst. (1993). C49, 1585-1588    [doi:10.1107/S0108270193002379]

Structure of Ba4NaSb3O12 by neutron powder diffraction

K. P. Reis and A. J. Jacobson



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Acta Cryst. (1993). C49, 1588-1589    [doi:10.1107/S0108270193003038]

The KInTe2 structure revisited

Y.-C. Hung and S.-J. Hwu


metal-organic compounds



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Acta Cryst. (1993). C49, 1589-1591    [doi:10.1107/S0108270193001969]

Structure of dimeric dichloro(4,4'-dimethyl-2,2'-bipyridine)copper(II) hemihydrate

O. González Q., A. M. Atria, E. Spodine, J. Manzur and M. T. Garland



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Acta Cryst. (1993). C49, 1591-1594    [doi:10.1107/S0108270193001295]

Structure of dimethyl(phenyl)phosphonium tris(1,2-benzenedithiolato)tungsten(V)

T. E. Burrow, R. H. Morris, A. Hills, D. L. Hughes and R. L. Richards



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Acta Cryst. (1993). C49, 1594-1596    [doi:10.1107/S0108270193001283]

Structure of [(C2H5)2NH2]3BiCl6

S. Jarraya, A. B. Salah, A. Daoud, W. Rothammel and H. Burzlaff



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Acta Cryst. (1993). C49, 1596-1598    [doi:10.1107/S0108270193002124]

Structure of [NH3(C2H5)]2[Hg(CN)2Cl2]

R. Zouari, A. B. Salah, A. Daoud, W. Rothammel and H. Burzlaff



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Acta Cryst. (1993). C49, 1598-1602    [doi:10.1107/S0108270193002215]

A monodentate 1,3-diphenyl-2-triazeno terpyridineplatinum(II) complex

J. A. Bailey, V. J. Catalano and H. B. Gray



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Acta Cryst. (1993). C49, 1602-1603    [doi:10.1107/S0108270193002707]

Chloro(dimethylphenylphosphine)gold(I)

P. D. Cookson and E. R. T. Tiekink



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Acta Cryst. (1993). C49, 1603-1606    [doi:10.1107/S0108270193002604]

Structure of ([eta]5-cyclopentadienyl)bis(dimethylphenylphosphine)palladium(II) perchlorate

L. Manojlovic-Muir, R. J. Cross and R. W. Hoyle



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Acta Cryst. (1993). C49, 1607-1609    [doi:10.1107/S0108270193002148]

Structure of [mu]-oxo-bis[trichloro(2,2-diisobutyl-1,3-dimethoxypropane-O,O')titanium(IV)]

E. Iiskola, A. Pelkonen, H. J. Kakkonen, M. Ahlgrén, T. A. Pakkanen and J. Pursiainen



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Acta Cryst. (1993). C49, 1609-1611    [doi:10.1107/S0108270193004494]

Niobium 1,4-diazabutadiene derivatives. Structure of ([eta]5-Cp)NbCl2(tBuNCHCHNtBu)

L. G. Hubert-Pfalzgraf, A. Zaki and L. Toupet



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Acta Cryst. (1993). C49, 1611-1614    [doi:10.1107/S0108270193000691]

Structure of the dimeric complex of iron(III) chloride with pyridoxine

V. Kh. Sabirov, M. A. Porai-Koshitz and Yu. T. Struchkov



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Acta Cryst. (1993). C49, 1614-1616    [doi:10.1107/S0108270193002288]

Structure of an iridium complex of 1,1'-bisdiphenylphosphinoferrocene

R. B. Bedford, P. A. Chaloner and P. B. Hitchcock



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Acta Cryst. (1993). C49, 1616-1619    [doi:10.1107/S0108270193001581]

Ferrocenyl ligands. Part 4. Structure of [1,1'-bis(diphenylphosphino)-3,3'-bis(trimethylsilyl)ferrocene]dichlorocobalt

M. T. Ahmet, R. A. Brown, R. M. G. Roberts, J. R. Miller, J. Silver and A. Houlton



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Acta Cryst. (1993). C49, 1619-1621    [doi:10.1107/S0108270193002483]

Structure of Ru4(CO)8(O2CCH2CH=CH2)4(NMe3)2

J. H. Reibenspies, B. Fontal and D. J. Darensbourg



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Acta Cryst. (1993). C49, 1621-1623    [doi:10.1107/S0108270193002847]

catena-Poly[{aqua(cyanoacetato-[kappa]O)(N,N-dimethylformamide-[kappa]O)neodymium}-di-[mu]-cyanoacetato-[kappa]O,[kappa]O':[kappa]O'] monohydrate

P. Starynowicz



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Acta Cryst. (1993). C49, 1623-1625    [doi:10.1107/S0108270193002173]

Structure of a V2Cu2S4 cubane-like cluster (Et4N)2[V2Cu2S4(S2CNMe2)2(SPh)2]

Y. Yang and Q. Liu



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Acta Cryst. (1993). C49, 1625-1627    [doi:10.1107/S0108270193002562]

Ring cleavage of imidazole to oxamide by reaction with dioxygen in the presence of a CuI-amine complex. Structure of [mu]-oxamidato-bis[(1,4,7-trimethyl-1,4,7-triazacyclononane)copper(II)] triiodide iodide

U. Flörke, H.-J. Haupt, I. Karpenstein and P. Chaudhuri



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Acta Cryst. (1993). C49, 1627-1629    [doi:10.1107/S0108270193003233]

2-[2,2-Bis(diphenylphosphanyl)ethylsulfanyl]phenylamine (NSPP), a new hetero-bifunctional ligand and its PdCl2 complex

U. Flörke and H.-J. Haupt



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Acta Cryst. (1993). C49, 1630-1632    [doi:10.1107/S0108270193003129]

Structure of the ion-pair charge-transfer complex (methylviologen)2+[Pd(mnt)2]2-

M. Lemke, F. Knoch and H. Kisch


organic compounds



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Acta Cryst. (1993). C49, 1632-1636    [doi:10.1107/S0108270193001180]

The optical resolution of bicyclo[2.2.1]hept-5-ene-2-cyanohydrins using brucine - a crystallographic and molecular-mechanics study

A. A. Pinkerton, P.-A. Carrupt, F. Claret and P. Vogel



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Acta Cryst. (1993). C49, 1637-1638    [doi:10.1107/S010827019300188X]

Structure of 2,7,7-trimethyl-5,6,7,8-tetrahydro-4H-furo[3,2-c]azepine-4-thione

M. Soriano-García, E. Cortés C., E. Cortés R., J. G. Avila Z. and A. Domínguez T.



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Acta Cryst. (1993). C49, 1638-1640    [doi:10.1107/S0108270193001374]

Structure of a 2-arylquinoline dimer, a compound with a new ring system

H. L. Ammon and T. L. Reid



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Acta Cryst. (1993). C49, 1641-1643    [doi:10.1107/S0108270193001489]

Structure of 2-methoxycarbonyl-1,4-dinitrocubane

H. L. Ammon and A. Bashir-Hashemi



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Acta Cryst. (1993). C49, 1643-1646    [doi:10.1107/S0108270193001271]

Phosphor(V)-Hydrazin-Sauerstoff-Achtring mit Boot-Sessel-Konformation

U. Engelhardt and B. Stromburg



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Acta Cryst. (1993). C49, 1646-1649    [doi:10.1107/S0108270193001313]

Structures of 3-hydroxy-1-(2-methoxyethyl)-2-methyl-4-pyridinone, its hydrochloride and 1-ethyl-3-hydroxy-2-methyl-4-pyridinone hydrochloride hydrate

G. Xiao, D. van der Helm, F. H. Goerlitz, R. C. Hider and P. S. Dobbin



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Acta Cryst. (1993). C49, 1649-1652    [doi:10.1107/S0108270193001593]

Structure of a 6-tetrahydroxybutyl-substituted 5,6,7,8-tetrahydropteridine

R. L. Beddoes, J. R. Russell, C. D. Garner and J. A. Joule



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Acta Cryst. (1993). C49, 1652-1654    [doi:10.1107/S0108270193001544]

Tetra(n-butyl)ammonium trifluoromethanesulfonate

A. J. Blake, C. Radek and M. Schröder



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Acta Cryst. (1993). C49, 1654-1655    [doi:10.1107/S0108270193001684]

Structure of (±)-1[beta]-tert-butoxy-3a[alpha],4[beta],5,6,7,7a-hexahydro-7a[beta]-methyl-5-oxo-4[alpha]-indancarboxylic acid methyl ester at 153 K

E. Pohl, R. Herbst-Irmer, G. M. Sheldrick, S. van Hommelen and U. Groth



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Acta Cryst. (1993). C49, 1656-1657    [doi:10.1107/S010827019300277X]

3-Amino-1-propylammonium perchlorate: an extensively hydrogen-bonded system

N. Aurangzeb, C. A. McAuliffe, R. G. Pritchard, M. Watkinson, A. Garcia-Deibe, A. Sousa and M. R. Bermejo



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Acta Cryst. (1993). C49, 1657-1659    [doi:10.1107/S010827019300229X]

Structures of the Diels-Alder reaction products of thymoquinone and 1-vinylcyclohexene. I. 2-Isopropyl-5-methyltricyclo[8.4.0.02,7]tetradeca-4,9-diene-3,6-dione

J. Iulek, J. Zukerman-Schpector, T. J. Brocksom and F. Silva Jnr



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Acta Cryst. (1993). C49, 1659-1661    [doi:10.1107/S0108270193002422]

1,5-Dihydro-3-(4,7-dihydro-1,3-dioxepin-2-yl)-8-methyl-3H-[1,3]dioxepino[5,6-c]pyridinium-9-ol maleate

M. Vinkovic, M. Dumic and B. Kamenar



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Acta Cryst. (1993). C49, 1661-1663    [doi:10.1107/S0108270193002185]

1-Methanesulfonyl-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine

M. Vinkovic, M. Dumic and B. Kamenar



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Acta Cryst. (1993). C49, 1663-1665    [doi:10.1107/S0108270193002616]

Benzyl 2-[(2R,SS)-2-(benzylaminosulfinyl)-4-oxoazetidin-1-yl]-3-methylbut-2-enoate

M. Vinkovic, J. J. Herak and B. Kamenar



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Acta Cryst. (1993). C49, 1665-1667    [doi:10.1107/S0108270193002458]

Structure of an antimalarial alkaloid, jatrorrhizine

R. Ghosh, K. Mukherjee, P. Roychowdhury and D. L. Klayman



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Acta Cryst. (1993). C49, 1667-1670    [doi:10.1107/S0108270193000782]

5,10,15,20-Tetrakis(p-chlorophenyl)porphyrin

T. Hökelek, D. Ülkü, N. Gündüz, M. Hayvali and Z. Kiliç



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Acta Cryst. (1993). C49, 1670-1673    [doi:10.1107/S0108270193002367]

Structure of 5-[1-(diaminomethylenehydrazono)ethyl]-4-methyl-2-methylthiopyrimidine

A. Cousson, F. Nectoux, B. Bachet, B. Kokel and M. Hubert-Habart



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Acta Cryst. (1993). C49, 1673-1676    [doi:10.1107/S010827019300246X]

Structure of a 1:1 complex between L-Asp-L-Phe and L-His-Gly

C. H. Görbitz and M. C. Etter



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Acta Cryst. (1993). C49, 1677-1678    [doi:10.1107/S010827019300304X]

Structure of iproniazid phosphate

N. Okabe, H. Fukuda and T. Nakamura



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Acta Cryst. (1993). C49, 1678-1680    [doi:10.1107/S0108270193002550]

Structure of 2,4-dinitrophenylhydrazine

N. Okabe, T. Nakamura and H. Fukuda



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Acta Cryst. (1993). C49, 1680-1683    [doi:10.1107/S0108270193002677]

Cyclobutane structures fused to a 13-membered ring

K. Yamaguchi, K. Takeda, A. Shimotani and E. Yoshii



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Acta Cryst. (1993). C49, 1683-1685    [doi:10.1107/S0108270193002744]

Non-natural 14-hydroxy steroids. III. (±)-Methyl 17[beta]-benzoyloxy-14[beta]-hydroxy-3[beta]-isopropenyl-1,7-dioxo-5[beta]-androstan-19-oate

A. G. Michel and M. Drouin



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Acta Cryst. (1993). C49, 1685-1688    [doi:10.1107/S0108270193002987]

Structure of 3-epiryanodol: a heptahydro diterpene

A. G. Michel and M. Drouin



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Acta Cryst. (1993). C49, 1688-1691    [doi:10.1107/S0108270193003130]

Structures of the natural alkaloids vincadifformine and 8-oxotabersonine

G. Palmisano and T. Pilati



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Acta Cryst. (1993). C49, 1691-1693    [doi:10.1107/S0108270193002410]

Structure of (±)-tetrahydropalmatine

B. Ribár, D. Lazar, O. Gasic, I. Kanyó, Y. A. Simonov and V. Kh. Kravtsov



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Acta Cryst. (1993). C49, 1693-1694    [doi:10.1107/S0108270193002896]

2-Methyl-4-oxo-3H,5H-6-imidazo[3,4-b][1,2,4]triazepinecarbonitrile: condensation product of a [beta]-keto ester with 1,5-diamino-4-imidazolecarbonitrile under basic conditions

B. L. Booth, R. G. Pritchard, A. P. Freitas and M. F. J. R. P. Proença



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Acta Cryst. (1993). C49, 1695-1696    [doi:10.1107/S0108270193002938]

Ethyl 3-(5-amino-4-cyano-1-imidazolyl-amino)-2-butenoate: an example of a combined inter- and intramolecular bifurcated hydrogen bond

B. L. Booth, R. G. Pritchard, A. P. Freitas and M. F. J. R. P. Proença



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Acta Cryst. (1993). C49, 1696-1698    [doi:10.1107/S0108270193002902]

1,3,5-Triacetyl-2,4,6-triphenylbenzene: a sterically hindered molecule

B. L. Booth, R. G. Pritchard and J. Taylor-Gomes



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Acta Cryst. (1993). C49, 1698-1700    [doi:10.1107/S0108270193002240]

Structure of 3-{2-[4-(6-fluoro-1,2-benzisoxazol-3-yl)piperidino]ethyl}-6,7,8,9-tetrahydro-2-methyl-4H-pyrido[1,2-a]pyrimidin-4-one (risperidone)

O. M. Peeters, N. M. Blaton and C. J. De Ranter



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Acta Cryst. (1993). C49, 1700-1702    [doi:10.1107/S0108270193002690]

Structure of a 4-phenyl-1,4-dihydropyridine derivative containing a nitrooxyalkyl ester at the 3-position

T. Ogawa, K. Matsumoto, K. Hatayama and K. Kitamura


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