Acta Crystallographica Section C

Crystal Structure Communications

Volume 49, Part 10 (October 1993)



research papers


metal-organic compounds



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Acta Cryst. (1993). C49, 1703-1706    [doi:10.1107/S0108270193002537]

Structures of the nitroimidazole platinum group metal complexes cis-amminedibromo[1-({[(2-hydroxyethyl)amino]carbonyl}methyl)-2-nitroimidazole]platinum(II) and trans-dichlorobis(1-hydroxyethyl-2-methyl-5-nitroimidazole)palladium(II)

F. D. Rochon, R. Melanson and N. Farrell



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Acta Cryst. (1993). C49, 1706-1713    [doi:10.1107/S0108270193004597]

A comparison of the inner coordination spheres of a series of nickel(II) macrocyclic imine ethers

D. J. Macchia, W. F. Furey Jnr and R. A. Lalancette



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Acta Cryst. (1993). C49, 1714-1716    [doi:10.1107/S0108270193006584]

Structure of chloro[1,1,1-tris(diphenylphosphinomethyl)ethane]copper(I)

D. J. Fife, H. J. Mueh and C. F. Campana


organic compounds



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Acta Cryst. (1993). C49, 1716-1719    [doi:10.1107/S0108270193005980]

Structure of [3,5-(C6H5)2C3H2N2]4. A 3,5-diphenylpyrazole tetramer linked by hydrogen bonds

R. G. Raptis, R. J. Staples, C. King and J. P. Fackler Jnr


short format


organic compounds



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Acta Cryst. (1993). C49, 1720-1721    [doi:10.1107/S0108270193003956]

Structure of (E)-3-bromo-4-nitro-4-phenyl-3-buten-2-one

H.-J. Ha, K. P. Park and J. H. Jeong



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Acta Cryst. (1993). C49, 1722-1723    [doi:10.1107/S0108270193005463]

Piperidine nitroxide radicals with heterocyclic ring substituents. I. Structure of 4-hydroxy-2,2,6,6-tetramethyl-4-(2-pyridylmethyl)piperidine 1-oxide

T. A. Olszak, M. J. Grabowski and K. Gwozdzinski


regular structural papers


inorganic compounds



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Acta Cryst. (1993). C49, 1724-1727    [doi:10.1107/S0108270193003373]

Thallium(I) selenate

J. Fábry and T. Breczewski


metal-organic compounds



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Acta Cryst. (1993). C49, 1727-1730    [doi:10.1107/S0108270193002112]

Structure of a citrate double salt: potassium dihydrogen citrate-lithium potassium hydrogen citrate monohydrate

D. E. Zacharias and J. P. Glusker



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Acta Cryst. (1993). C49, 1730-1732    [doi:10.1107/S0108270193001477]

Structure of dipotassium hydrogen citrate

D. E. Zacharias and J. P. Glusker



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Acta Cryst. (1993). C49, 1732-1735    [doi:10.1107/S0108270193000964]

Structure of strontium citrate pentahydrate

D. E. Zacharias and J. P. Glusker



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Acta Cryst. (1993). C49, 1735-1737    [doi:10.1107/S0108270193002781]

Diphenylbis(2-pyridinethiolato)tin(IV)

R. Schmiedgen, F. Huber and H. Preut



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Acta Cryst. (1993). C49, 1737-1739    [doi:10.1107/S0108270193003105]

Structure of dioxo[N,N,N',N'-tetrakis(2-pyridylmethyl)ethylenediamine]vanadium(V) chloride monohydrate, [VO2(tpen)]Cl.H2O

A. Neves, M. Hörner, H. Fenner and J. Strähle



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Acta Cryst. (1993). C49, 1739-1741    [doi:10.1107/S0108270193003853]

Tetramethylarsonium pentachlorodicuprate(II)

K. Murray and R. D. Willett



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Acta Cryst. (1993). C49, 1741-1743    [doi:10.1107/S0108270193003075]

Heptacarbonylbis(triphenylphosphine)bis([mu]3-tellurium)-triiron

A. L. Rheingold, R. L. Ostrander and P. Mathur



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Acta Cryst. (1993). C49, 1743-1747    [doi:10.1107/S0108270193003051]

Copper(II) and nickel(II) octabromo-tetrakis(pentafluorophenyl)porphyrin complexes

L. M. Henling, W. P. Schaefer, J. A. Hodge, M. E. Hughes, H. B. Gray, J. E. Lyons and P. E. Ellis Jnr



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Acta Cryst. (1993). C49, 1747-1749    [doi:10.1107/S010827019300280X]

Structure of (2,5,8,11,14-pentaazapentadecane)copper(II) diperchlorate monohydrate

T.-H. Lu, T. H. Tahirov, C.-K. Bin, C.-D. Hsiao, Y.-L. Liu, J.-C. Lee and C.-S. Chung



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Acta Cryst. (1993). C49, 1749-1753    [doi:10.1107/S0108270193003026]

Preparation of chiral tricarbonyl([eta]6-arene)chromium(0) complexes derived from (S)-2-indolinecarboxylic acid

S. B. Heaton, G. B. Jones and W. T. Pennington



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Acta Cryst. (1993). C49, 1753-1756    [doi:10.1107/S010827019300232X]

Tetraphenylphosphonium salts of 2-telluro-5-methylthiophene and its mercury(II) metal complex

J. Zhao, J. W. Kolis and W. T. Pennington



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Acta Cryst. (1993). C49, 1756-1761    [doi:10.1107/S0108270193002859]

Structures of bis(di-2-pyridylamine)dinitratocopper(II) and bis(acetato)bis(di-2-pyridylamine)copper(II) monohydrate

M. C. Muñoz, J. M. Lázaro, J. Faus and M. Julve



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Acta Cryst. (1993). C49, 1761-1762    [doi:10.1107/S010827019300318X]

Structure of the copper(II) complex isonicotinic acid

N. Okabe, T. Nakamura and H. Fukuda



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Acta Cryst. (1993). C49, 1762-1764    [doi:10.1107/S0108270193003002]

Structure of [Ru([eta]6-C7H8)(acetylacetonato)Cl]

J. G. Toerien and J. L. M. Dillen



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Acta Cryst. (1993). C49, 1764-1766    [doi:10.1107/S0108270193003452]

Structure of ([eta]5-cyclopentadienyl)[1-(2-quinoxalinyl)ethene-1,2-dithiolato]cobalt(III), [([eta]5-C5H5)Co{S2C2H(2-quinoxalinyl)}]

E. M. Armstrong, M. S. Austerberry, R. L. Beddoes, M. Helliwell, J. A. Joule and C. D. Garner



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Acta Cryst. (1993). C49, 1766-1767    [doi:10.1107/S0108270193003889]

The Pbca polymorph of dichloro([eta]4-1,5-cyclooctadiene)palladium(II)

R. Kumar, A. W. Maverick, F. R. Fronczek, J. R. Doyle, N. C. Baenziger and M. A. M. Howells



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Acta Cryst. (1993). C49, 1767-1770    [doi:10.1107/S0108270193003518]

Bis([mu]-benzoato-[kappa]O:[kappa]O')-bis[(benzoato-[kappa]2O,O')(N,N-dimethylformamide-[kappa]O)dioxouranium(VI)]

A. Navaza, M. G. Iroulart, M. Nierlich, M. Lance and J. Vigner



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Acta Cryst. (1993). C49, 1770-1773    [doi:10.1107/S0108270193003919]

Structure and bonding in [TaCl4(C5H5N)2]

G. J. Miller, J. Lin and V. Young Jnr



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Acta Cryst. (1993). C49, 1773-1775    [doi:10.1107/S0108270193002926]

Structure of trans-carbonyl(thiocyanato-N)bis(triethylphosphine)rhodium(I)

A. J. Blake, E. A. V. Ebsworth and P. G. Watson


organic compounds



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Acta Cryst. (1993). C49, 1775-1777    [doi:10.1107/S0108270193002689]

8-(N,N-Di-p-toluenesulfonylamino)quinoline

S. F. Lincoln, I. B. Mahadevan, E. R. T. Tiekink and A. D. Ward



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Acta Cryst. (1993). C49, 1777-1779    [doi:10.1107/S0108270193002768]

N-(2-Chloro-6-methylphenyl)-6-methyl-3-pyridinecarboxamide hydrate: an anticonvulsant drug exhibiting solid-state rotational disorder

R. A. Palmer, N. Puddle and J. N. Lisgarten



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Acta Cryst. (1993). C49, 1779-1781    [doi:10.1107/S0108270193001659]

Structure of 5,7-dinitro-2,1,3-benzoxadiazol-4-yl phenyl diketone

M. Ramm, J. Kind and H.-J. Niclas



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Acta Cryst. (1993). C49, 1781-1783    [doi:10.1107/S0108270193001611]

Structure of 5,10-dihydro-3-phenylimino-1,2,4-thiaselenazolo[4,5-b][2,4]benzodiazepine

D. G. Billing, J. C. A. Boeyens, W. Haag, L.-L. Lai and D. H. Reid



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Acta Cryst. (1993). C49, 1783-1786    [doi:10.1107/S0108270193001647]

6,6a,7,11b-Tetrahydro-6a-methyl-5-phenyl-5,7-methano-5H-benzo[c]fluorene and 9-methyl-1,3,9-triphenylfluorene

D. W. Sullins, E. M. Holt and E. J. Eisenbraun



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Acta Cryst. (1993). C49, 1786-1789    [doi:10.1107/S0108270193002136]

X-ray diffraction analysis of two hexahydropyrido[2,1-b][1,3,4]oxadiazines: evidence for the effect of steric congestion on anion formation at the aminonitrile centre

A. Chiaroni, C. Riche, L. Guerrier, J. Royer, D. S. Grierson and H.-P. Husson



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Acta Cryst. (1993). C49, 1789-1792    [doi:10.1107/S0108270193003464]

[beta]-Cytidine, C9H13N3O5

D. L. Ward



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Acta Cryst. (1993). C49, 1792-1793    [doi:10.1107/S0108270193002276]

Structure of 1-benzoyl-4,4,5,5-tetramethyl-2-phenylimidazoline hydrate

J. L. Flippen-Anderson, W. W. Zajac, J. H. Buzby and T. R. Walters



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Acta Cryst. (1993). C49, 1793-1796    [doi:10.1107/S010827019300366X]

Structures of the bis(diarylthiophosphoryl) disulfides [Ph2P(S)]2S2 and [(PhO)2P(S)]2S2 and the question of P-S [pi] bonding

A. C. Gallacher and A. A. Pinkerton



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Acta Cryst. (1993). C49, 1796-1799    [doi:10.1107/S0108270192012794]

18-Crown-6-bis(methyl 10-camphorsulfonate) (1/2)

R. Chênevert, R. Gagnon and F. Bélanger-Gariépy



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Acta Cryst. (1993). C49, 1799-1801    [doi:10.1107/S010827019300263X]

Structure of an [alpha]-(methyldiphenylsilyl)-[gamma]-lactone

T. J. Delord, F. R. Fronczek, R. M. Betancourt de Perez and G. L. Larson



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Acta Cryst. (1993). C49, 1801-1802    [doi:10.1107/S0108270193003440]

Structure of (3R*,6S*)-3,6-bis(methoxymethoxy)-2,2,7,7-tetramethyl-4-octene

T. Nemoto, Y. Ohashi, M. Arai and E. Nakamura



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Acta Cryst. (1993). C49, 1802-1804    [doi:10.1107/S0108270193003968]

Structure of endo-(5S*,6S*,11R*,12R*)-5,6,11,12-tetrahydro-5,6-dihydroxy-4,11,12-trimethoxy-9,13,13-trimethyl-6,10-methano-8(7H)-benzocyclodecenone

S. Kamei, Y. Sakai, Y. Ohashi, K. Tsuruta, Y. Horiguchi and I. Kuwajima



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Acta Cryst. (1993). C49, 1804-1806    [doi:10.1107/S0108270193003658]

Quinuclidine-trifluoromonoborane: a (1/1) Lewis base-Lewis acid complex

R. E. Banks, M. K. Besheesh, R. G. Pritchard and I. Sharif



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Acta Cryst. (1993). C49, 1806-1807    [doi:10.1107/S0108270193003646]

N-Fluoroquinuclidinium trifluoromethanesulfonate (triflate): a novel electrophilic fluorinating agent

R. E. Banks, R. G. Pritchard and I. Sharif



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Acta Cryst. (1993). C49, 1808-1809    [doi:10.1107/S0108270193003117]

5-Methoxy-3,3a,8,8a-tetrahydro-1H-cyclopenta[a]inden-2-one

R. Aebi, R. Buechel, H.-B. Bürgi, M. Foertsch and P. Venugopalan



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Acta Cryst. (1993). C49, 1810-1811    [doi:10.1107/S0108270193003014]

9,9,10,10-Tetrafluoro-1,3,5,7-tetrathio-2,4,6,8-tetraaoxa-1,3,5,7-tetraphosphatricyclo[3.3.1.13,7]decane, P4O4(CF2)2S4: a cage structure related to P4O6

P. G. Jones and A. Weinkauf



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Acta Cryst. (1993). C49, 1811-1813    [doi:10.1107/S0108270193002914]

Structure of 2,3-diphenyl-2-norbornene: comparison with data for a cis-stilbene

R. L. Beddoes, A. A. Gorman and S. P. McNeeney



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Acta Cryst. (1993). C49, 1813-1818    [doi:10.1107/S0108270193003695]

Structures of 1,1-diphenyl-2-aza-1,3-butadienes. I. 3-Cyano-4-(n-methoxyphenyl)-1,1-diphenyl-2-aza-1,3-butadienes (n = 2, 3, 4)

O. Angelova, J. Macícek and V. Dryanska



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Acta Cryst. (1993). C49, 1818-1821    [doi:10.1107/S0108270193003166]

Structures of 1,1-diphenyl-2-aza-1,3-butadienes. II. 3-Cyano-4-(n-fluorophenyl)-1,1-diphenyl-2-aza-1,3-butadienes (n = 2, 4)

J. Macícek, O. Angelova and V. Dryanska



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Acta Cryst. (1993). C49, 1821-1823    [doi:10.1107/S0108270193003178]

Structures of 1,1-diphenyl-2-aza-1,3-butadienes. III. 3-Cyano-4-(4-cyanophenyl)-1,1-diphenyl-2-aza-1,3-butadiene

O. Angelova, J. Macícek and V. Dryanska



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Acta Cryst. (1993). C49, 1823-1824    [doi:10.1107/S0108270193002963]

Structure of a 2-acylindan-1-one

J. G. Garcia, J. D. Enas and F. R. Fronczek



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Acta Cryst. (1993). C49, 1824-1826    [doi:10.1107/S0108270193003336]

Structure of 23,24-dinor-5[alpha]-cholan-12-one

K. Decanniere, D. Maes, J. N. Lisgarten, I. Zegers and M. Biesemans



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Acta Cryst. (1993). C49, 1826-1828    [doi:10.1107/S0108270193003683]

2-Amino-2-carboxyethylphosphinic acid monohydrate

C. H. W. Schwalbe, S. Freeman and M. DasGupta



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Acta Cryst. (1993). C49, 1828-1830    [doi:10.1107/S0108270193002975]

Functionalized hydrocarbons with condensed ring skeletons. XIV. A dioxotricyclo[8.4.0.02,7]tetradec-6-ene

A. G. Michel and M. Drouin



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Acta Cryst. (1993). C49, 1830-1833    [doi:10.1107/S0108270193002756]

Functionalized hydrocarbons with condensed ring skeletons. XV. A (methoxymethoxymethyl)tricyclo[9.4.0.02,8]pentadec-9-ene

A. G. Michel and M. Drouin



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Acta Cryst. (1993). C49, 1833-1834    [doi:10.1107/S0108270193002732]

Ethynylenebis(2-methoxybenzene)

D. S. Davis, F. R. Fronczek and R. D. Gandour



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Acta Cryst. (1993). C49, 1834-1837    [doi:10.1107/S0108270193003932]

Structure of (-)-muscarone iodide

K. Frydenvang and B. Jensen



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Acta Cryst. (1993). C49, 1837-1840    [doi:10.1107/S0108270193003944]

Structure determinations of (dl)-trans-3-hydroxy-5-iodomethyl-2,2-diphenyltetrahydrofuran and (dl)-trans-N,N,N-trimethyl-(3-hydroxy-2,2-diphenyltetrahydro-5-furyl)methylammonium iodide

K. Frydenvang



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Acta Cryst. (1993). C49, 1840-1844    [doi:10.1107/S0108270193002446]

Structure of the charge-transfer complexes 2,4,5,7-tetranitro-9-fluorenone-1-ethylnaphthalene (1/1) (I) and 2,4,5,7-tetranitro-9-fluorenone-3,6-dimethylphenanthrene (1/1) (II)

S. L. Baldwin and R. G. Baughman



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Acta Cryst. (1993). C49, 1844-1845    [doi:10.1107/S0108270193003762]

Structure of hydralazine hydrochloride

N. Okabe, H. Fukuda and T. Nakamura



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Acta Cryst. (1993). C49, 1845-1848    [doi:10.1107/S0108270193002331]

Structure of cyclo-1,1',4,4'-bis(1,1,3,3-tetramethyl-1,3-disiloxanediyl)dibenzene

K. A. Abboud, D. W. Smith Jnr and K. B. Wagener



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Acta Cryst. (1993). C49, 1848-1850    [doi:10.1107/S0108270193002343]

Structure of a phosphazene-aniline compound

K. A. Abboud, L. A. Villanueva and J. M. Boncella



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Acta Cryst. (1993). C49, 1850-1852    [doi:10.1107/S0108270193004202]

Structures of endo- and exo-3-acetoxy-2,4-diethoxy-6-(2-oxo-1,3-oxazolidin-3-ylcarbonyl)-3,4-dihydro-2H-pyran

E. Pohl, R. Herbst-Irmer, M. Noltemeyer, C. Schneider and L. F. Tietze



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Acta Cryst. (1993). C49, 1852-1854    [doi:10.1107/S0108270193004317]

Structure of methyltris(2,4,6-trimethoxyphenyl)phosphonium iodide ethanol solvate

P. A. Chaloner, R. M. Harrison and P. B. Hitchcock



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Acta Cryst. (1993). C49, 1854-1857    [doi:10.1107/S0108270193003750]

Three isomers of tricyclo[10.3.0.04,9]pentadecane-2,10-dione, (I), (II) and (III), and cis-cisoid-cis-9-hydroxy-9-methyltricyclo[9.3.0.03,7]tetradecan-2-one, (IV)

T. Kawata, S. Ohba, M. Umehara and H. Honnami



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Acta Cryst. (1993). C49, 1857-1859    [doi:10.1107/S0108270193004135]

Structure of a bis-spiroacetal, cis-14-phenylsulfonyl-1,7,9-trioxadispiro[5.1.5.3]hexadecane

E. N. Baker, M. A. Brimble, G. E. Norris, J. W. Quail and C. A. Rush



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Acta Cryst. (1993). C49, 1859-1862    [doi:10.1107/S0108270193003865]

Structures of two hexacyclic cage diketone monoacetals

J. M. Coxon, S. T. Fong, P. J. Steel, S. G. Bott, A. P. Marchand and U. R. Zope



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Acta Cryst. (1993). C49, 1862-1865    [doi:10.1107/S0108270193003907]

8-Pentacyclo[6.3.0.02,6.03,10.05,9]undec-3'-yl-exo-pentacyclo[5.4.0.02,6.03,10.05,9]undecane

W. H. Watson, R. P. Kashyap, A. P. Marchand and M. N. Deshpande



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Acta Cryst. (1993). C49, 1865-1866    [doi:10.1107/S0108270193004470]

3,7-Diphenyl-5,6;10,11-dibenzotricyclo[7.2.1.03,8]dodeca-5,7,10-trien-4-one

R. P. Kashyap, W. H. Watson, M. Balci and Y. Taskesenligil



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Acta Cryst. (1993). C49, 1867-1868    [doi:10.1107/S0108270193003610]

(Benzoylmethyl)(3-hydroxypropyl)dimethylammonium bromide

V. E. Keblys, J. G. Garcia, R. D. Gandour, F. R. Fronczek and S. F. Watkins



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Acta Cryst. (1993). C49, 1868-1871    [doi:10.1107/S0108270193003713]

Structure of 6-fluoro-1,2,3,4,7,12-hexahydro-7-methyl-12-methylenebenz[a]anthracene

J. C. Gallucci, P. K. Sharma, S. D. Black, S. J. Rinderle and D. T. Witiak



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Acta Cryst. (1993). C49, 1871-1873    [doi:10.1107/S0108270193002525]

Delnuttaline, (6[beta],9[beta],13[beta])-13-acetoxy-6,9-dihydroxyhetisan-2-one

M. Parvez, Y. Bai, F. Sun and M. H. Benn


short communications



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Acta Cryst. (1993). C49, 1873    [doi:10.1107/S0108270193008248]

Structures of the 1:1 and 2:1 adducts of (+)-(S)-[2.2]paracyclophane-4-carboxylic acid and (-)-ephedrine. Erratum

P. G. Jones, D. Döring, T. Laue and H. Hopf


international union of crystallography



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Acta Cryst. (1993). C49, 1874    [doi:10.1107/S0108270193099779]

Commission on Journals. Section Editors for Acta Crystallographica


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