Acta Crystallographica Section C

Crystal Structure Communications

Volume 50, Part 2 (February 1994)


Cover illustration Cover illustration: trans-1,2,3-Tris(3-thenoyl)cyclopropane, see Saba, pages 271-274.

international union of crystallography



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Acta Cryst. (1994). C50, 145-159    [doi:10.1107/S0108270194099816]

Notes for Authors


inorganic compounds



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Acta Cryst. (1994). C50, 160-161    [doi:10.1107/S0108270193008637]

Refinement of hexagonal BaTiO3

J. Akimoto, Y. Gotoh and Y. Oosawa



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Acta Cryst. (1994). C50, 161-164    [doi:10.1107/S0108270193008972]

Structural reinvestigation of Ba3Zr2S7 by single-crystal X-ray diffraction

B.-H. Chen, B. Eichhorn and W. Wong-Ng



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Acta Cryst. (1994). C50, 164-166    [doi:10.1107/S0108270193007802]

Silver insertion mode in [beta]-AgxV2O5 tunnel structure

E. Déramond, J.-M. Savariault and J. Galy



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Acta Cryst. (1994). C50, 166-168    [doi:10.1107/S0108270193006705]

Structure du sulfur d'ytterbium, Yb2S3

Z. El Fadli, P. Lemoine, M. Guittard and A. Tomas


metal-organic compounds



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Acta Cryst. (1994). C50, 169-171    [doi:10.1107/S0108270193007851]

2,2'-Ethylenebis([eta]5-indenyl)TiCl2

S. Parkin, S. R. Hitchcock, H. Hope and M. H. Nantz



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Acta Cryst. (1994). C50, 171-173    [doi:10.1107/S0108270193007140]

Tetra(N-methylimidazol)-kupfer(II)-bis(triiodid) [Cu(C4H6N2)4](I3)2

K.-F. Tebbe and S. Nafepour



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Acta Cryst. (1994). C50, 173-175    [doi:10.1107/S0108270193009229]

Bis(2-ethoxycarbonylamino-6-methylpyridine N-oxide)copper(II)

D. X. West, E. J. Zaluzec and S. F. Pavkovic



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Acta Cryst. (1994). C50, 175-178    [doi:10.1107/S0108270193007322]

Polyol metal complexes. V. Structure of (2,2'-bipyridyl-[kappa]2N,N')[meso-oxolane-3,4-diolato(2-)-[kappa]2O,O']palladium(II) 6.5-hydrate

M. Achternbosch and P. Klüfers



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Acta Cryst. (1994). C50, 178-180    [doi:10.1107/S0108270193011680]

Disodium bis(o-chloranilato)uranyl(VI) hexahydrate

A. Bram, G. Bruederl, H. Burzlaff, J. Lange, W. Rothammel, R. Spengler, M. I. Karayannis and P. G. Veltsistas



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Acta Cryst. (1994). C50, 180-181    [doi:10.1107/S0108270193006882]

trans-Dichlorobis(metronidazole)palladium(II), [PdCl2(C6H9N3O3)2]

H. L. De Bondt, N. M. Blaton, O. M. Peeters and C. J. De Ranter



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Acta Cryst. (1994). C50, 181-185    [doi:10.1107/S0108270193007711]

Zinc(II) bis(phosphoglycolate) dihydrate and calcium bis(phosphoglycolate) dihydrate

T. Lis



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Acta Cryst. (1994). C50, 185-188    [doi:10.1107/S0108270193006092]

Dicalcium 1,4,5,8-naphthalenetetracarboxylate pentahydrate

L. J. Fitzgerald and R. E. Gerkin



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Acta Cryst. (1994). C50, 188-190    [doi:10.1107/S0108270193006791]

trans-Bisaquabis[1,2-bis(diphenylphosphino)ethane]technetium(I) tetraphenylborate

R. Hübener, U. Abram and W. Hiller



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Acta Cryst. (1994). C50, 191-193    [doi:10.1107/S0108270193007279]

Bis(tri-n-butylphosphino)gold(I) tetraphenylborate

R. J. Staples, J. P. Fackler Jnr, M. N. I. Khan and R. E. P. Winpenny



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Acta Cryst. (1994). C50, 193-195    [doi:10.1107/S010827019300664X]

Hybrid ligands. Structure of a palladium(II) complex containing a pyrazolol-derived phosphine ligand, [(o-C6H4CH2NMe2)Pd(Ph2P{\bridge{C\db C(O)N(Ph)N\db C}{33mm}(Me)})]

D. Matt, J.-C. Guillemin, R. Ziessel, F. Balegroune and D. Grandjean



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Acta Cryst. (1994). C50, 196-198    [doi:10.1107/S0108270193007371]

Tetrakis(isopropylammonium) [beta]-octamolybdate(VI)

J. M. Gutiérrez-Zorrilla, T. Yamase and M. Sugeta



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Acta Cryst. (1994). C50, 198-200    [doi:10.1107/S0108270193007127]

Bridged bis(dicarbadodecaborane)cobalt(III)

I. Císarová, K. Malý and L. Hummel



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Acta Cryst. (1994). C50, 200-202    [doi:10.1107/S0108270193007735]

Tribenzylammonium dibenzylammonium tetrachlorocuprate

G.-F. Zeng, M. Qin, Y.-H. Lin and S.-Q. Xi



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Acta Cryst. (1994). C50, 202-203    [doi:10.1107/S0108270193007231]

trans-Dichloro[(2RS,5RS,9SR,12RS)-2,5,9,12-tetraazatridecane]cobalt(III) perchlorate, [CoCl2(C9H24N4)]ClO4

T.-H. Lu, C.-Y. Lai and C.-S. Chung



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Acta Cryst. (1994). C50, 204-206    [doi:10.1107/S010827019300722X]

A dinuclear copper(II) complex of deprotonated N,N'-bis(N-propylglycyl)ethylenediamine

T. H. Tahirov, T.-H. Lu, K. Shu, C.-S. Chung, C.-C. Huang and Y.-S. Hong



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Acta Cryst. (1994). C50, 206-209    [doi:10.1107/S0108270193007310]

Tris(2-pyridinethiolato)(p-tolyl)tin(IV), [Sn(C5H4NS)3(C7H7)]

M. Schürmann and F. Huber



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Acta Cryst. (1994). C50, 209-211    [doi:10.1107/S0108270193006237]

Synthèse et structure du tétrachloroplatinate(II) de pyrido[2,3-h]pyrrolo[1,2-a]quinoxalinium monohydrate, [C14H11N3][PtCl4].H2O

B. Viossat, Nguyen-Huy Dung, J. C. Daran et J. C. Lancelot



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Acta Cryst. (1994). C50, 211-214    [doi:10.1107/S0108270193007309]

Dichloro(2,5-diphényl-3,4-di-2-pyridyl-1H-pyrrole-N,N')cobalt(II)

B. Viossat, Nguyen-Huy Dung, J. Lehuede et J. M. Vierfond



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Acta Cryst. (1994). C50, 214-217    [doi:10.1107/S0108270193007759]

[2,3-Bis(3,4-dimethoxyphenyl)-3-oxopropanalato-O,O']difluoroboron(III)

R. Stomberg, S. Li and K. Lundquist



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Acta Cryst. (1994). C50, 217-219    [doi:10.1107/S0108270193007553]

cis-Dichloro[1,2-bis(dicyclohexylphosphino)ethane]palladium(II)

S. Ganguly, J. T. Mague and D. M. Roundhill



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Acta Cryst. (1994). C50, 219-221    [doi:10.1107/S0108270193007292]

3,3'-Dimethyl-4,4'-diphenyl-2,2',5,5'-tetrathiafulvalenium hexamolybdate, 2(C20H16S4+)[Mo6O19]2-

S. Triki, L. Ouahab and J. M. Fabre



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Acta Cryst. (1994). C50, 221-224    [doi:10.1107/S0108270193009205]

Barium (cryptand 222B)Cl2.6H2O

W. A. Pettit and N. C. Baenziger



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Acta Cryst. (1994). C50, 224-226    [doi:10.1107/S0108270193008273]

1,1'-Bis(diphenylphosphine oxide)ferrocene dihydrate

V. Munyejabo, M. Postel, J. L. Roustan and C. Bensimon



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Acta Cryst. (1994). C50, 226-227    [doi:10.1107/S0108270193008054]

Di-[mu]-fluoro-bis[bis(dimethyl sulfoxide)trifluorozirconium(IV)]

N. W. Alcock, W. Errington, S. L. Golby, S. M. C. Patterson and M. G. H. Wallbridge



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Acta Cryst. (1994). C50, 227-229    [doi:10.1107/S0108270193007760]

Dimeric [mu]-hydroxy-diphenyl(trichloroacetato)tin

N. W. Alcock and S. M. Roe



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Acta Cryst. (1994). C50, 229-231    [doi:10.1107/S0108270193008297]

Tris(2-methoxyphenyl)tin iodide

R. A. Howie, J.-N. Ross, J. L. Wardell and J. N. Low



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Acta Cryst. (1994). C50, 231-233    [doi:10.1107/S010827019300825X]

[(C5H5N)2H]3[PW12O40]

M. Hashimoto and M. Misono



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Acta Cryst. (1994). C50, 233-238    [doi:10.1107/S0108270193007929]

C-H...I- interactions in ferrocene derivatives: structures of (Ferrocenylmethyl)triphenylphosphonium iodide and 1,1'-ferrocenediylbis(methyltriphenylphosphonium iodide) dichloromethane solvate (1/1)

C. Glidewell, C. M. Zakaria, G. Ferguson and J. F. Gallagher


organic compounds



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Acta Cryst. (1994). C50, 239-245    [doi:10.1107/S0108270193006997]

Three substituted 3-amino-2-benzoylaminopropenoic acid derivatives

K. Djinovic-Carugo, L. Golic, I. Leban, J. Svete, B. Stanovnik, M. Tisler and C. Tate



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Acta Cryst. (1994). C50, 245-247    [doi:10.1107/S010827019300736X]

Double-layered polytypic structure of the B form of octadecanoic acid, C18H36O2

F. Kaneko, H. Sakashita, M. Kobayashi, Y. Kitagawa, Y. Matsuura and M. Suzuki



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Acta Cryst. (1994). C50, 247-250    [doi:10.1107/S0108270193007243]

Double-layered polytypic structure of the E form of octadecanoic acid, C18H36O2

F. Kaneko, H. Sakashita, M. Kobayashi, Y. Kitagawa, Y. Matsuura and M. Suzuki



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Acta Cryst. (1994). C50, 250-252    [doi:10.1107/S0108270193006808]

Structure of the tripeptide amide H-L-Pro-L-Leu-L-Pro-NH2, a dopamine receptor modulating agent

B. Di Blasio, F. Nastri, M. Saviano, E. Benedetti, M. Crisma, C. Toniolo and R. L. Johnson



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Acta Cryst. (1994). C50, 252-254    [doi:10.1107/S0108270193011916]

2-[(5-Phenyl-2,3-dihydro-6H-1,3,4-thiadiazin-2-ylidene)amino]-3-pyridinol

J. Macícek, O. Angelova, V. Kalcheva and M. Tosheva



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Acta Cryst. (1994). C50, 254-255    [doi:10.1107/S0108270193007437]

4,4'-Difluorobenzophenone

S. J. Maginn and R. J. Davey



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Acta Cryst. (1994). C50, 255-259    [doi:10.1107/S0108270193006146]

Substitution effects on the structure of o-aryliminophosphoranes

A. L. Llamas-Saiz and C. Foces-Foces



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Acta Cryst. (1994). C50, 259-260    [doi:10.1107/S0108270193008261]

(22R)-3[beta]-tert-Butyldimethylsilyloxy-22-methylchola-5,23-diene

A. Uchida, Y. Ohashi, M. Arai and E. Nakamura



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Acta Cryst. (1994). C50, 260-263    [doi:10.1107/S010827019300678X]

2-(4-Pentanoyloxyphenyl)-6-pentanoyloxybenzoxazole

R. Centore



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Acta Cryst. (1994). C50, 263-265    [doi:10.1107/S0108270193008212]

1,3,5-Triethyl-1,3,5-triazine-2,4,6(1H,3H,5H)-trione, C9H15N3O3

M. J. Hornish and W. Watt



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Acta Cryst. (1994). C50, 265-267    [doi:10.1107/S0108270193006821]

Crystal studies of musk compounds. V. Structure of 1-(1,2,6,7,8,8a-hexahydro-3,6,6,8a-tetramethylacenaphthylen-4-yl)ethan-1-one

D. J. A. De Ridder, K. Goubitz and H. Schenk



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Acta Cryst. (1994). C50, 267-269    [doi:10.1107/S0108270193008170]

2,2'-Biadamantane

K. Mielke, J. L. Fry, D. C. Finnen and A. A. Pinkerton



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Acta Cryst. (1994). C50, 269-271    [doi:10.1107/S0108270193003592]

Structure du 5-méthyl-2-thioxo-1,2,3,4-tétrahydro-7H-pyrano[2,3-d]pyrimidine-4,7-dione méthanol solvaté, C8H6N2O3S.CH4O

B. Viossat, Nguyen-Huy Dung, A. Tomas, A. Esanu et A. Rolland



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Acta Cryst. (1994). C50, 271-274    [doi:10.1107/S0108270193008820]

Synthesis and structure of trans-1,2,3-tris(3-thenoyl)cyclopropane

A. Saba



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Acta Cryst. (1994). C50, 274-276    [doi:10.1107/S0108270193009266]

Structure of a model for the aranorosin nucleus

R. C. Haltiwanger, D. S. Eggleston, A. McKillop, R. J. K. Taylor, R. J. Watson and N. Lewis



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Acta Cryst. (1994). C50, 276-278    [doi:10.1107/S0108270193008881]

Dimethyl 9-[(S)-(-)-N-acetylalanyloxy]methyl-9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboxylate

P. R. Pokkuluri and J. Trotter



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Acta Cryst. (1994). C50, 278-281    [doi:10.1107/S0108270193009060]

Structure of a mixed crystal of [alpha]- and [beta]-pipitzol (1:1), C15H20O3.C15H20O3

S. V. Evans, V. C. Yee, M. Garcia-Garibay and J. Trotter



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Acta Cryst. (1994). C50, 281-283    [doi:10.1107/S0108270193008893]

Structure of a cyclopropapentalene photolysis product of a dibenzobarrelene ester lactone

P. R. Pokkuluri and J. Trotter



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Acta Cryst. (1994). C50, 283-284    [doi:10.1107/S0108270193010157]

Potential [beta]-blockers. I. 2-tert-Butyl-1,2,3,4-tetrahydro-4,6,8-trihydroxyisoquinolinium sulfate dihydrate

T. A. Olszak, M. J. Grabowski and E. Brzezinska



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Acta Cryst. (1994). C50, 284-286    [doi:10.1107/S0108270193010145]

2H-1-Benzopyrans. I. (E)-4-Chloro-2-[dimethoxyphosphoryl(dimethoxyphosphoryloxy)methylene]-2H-1-benzopyran

T. A. Olszak, A. J. Stepien, M. Renz, M. J. Grabowski, K. Kostka and R. Modranka



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Acta Cryst. (1994). C50, 286-289    [doi:10.1107/S0108270193006638]

Structure of 5-[(1-amidiniohydrazono)ethyl]-4-methyl-2-methylthio-3H+-pyrimidinium dichloride hydrate, C19H16N6S2+.2Cl-.H2O

A. Cousson, F. Nectoux, B. Bachet, B. Kokel and M. Hubert-Habart



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Acta Cryst. (1994). C50, 289-291    [doi:10.1107/S0108270193006626]

Structure of 2-methylthio-7,8-dihydroquinazolin-5(6H)-one amidinohydrazone hydrochloride, C10H15N6S+.Cl-

A. Cousson, F. Nectoux, B. Bachet, B. Kokel and M. Hubert-Habart



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Acta Cryst. (1994). C50, 291-294    [doi:10.1107/S0108270193008662]

Structure of a modified nucleoside, 3'[alpha]-diethylphosphono-3'[beta]-hydroxy-5'-O-tritylthymidine

M. A. Capron, W. L. McEldoon, N. C. Baenziger and D. F. Wiemer



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Acta Cryst. (1994). C50, 294-297    [doi:10.1107/S0108270193009047]

(E)-1,3-Dibenzoyl-2-trifluoromethylpropene and 3-benzoyl-6-phenyl-2,4-bis(trifluoromethyl)-2H-pyran-2-ol: novel products from the oxidation of 1-phenyl-4,4,4-trifluorobut-2-yn-1-ol with active manganese(IV) oxide

R. G. Pritchard, S. Tajammal and A. E. Tipping



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Acta Cryst. (1994). C50, 297-300    [doi:10.1107/S0108270193008467]

Structures of ap-8-bromo-1,4-dimethyl-9-(2-methylbenzyl)triptycene and sc*(9S*)-8-bromo-1,4-dimethyl-9-(2-methylbenzyl)triptycene

T. Nemoto, T. Ono, A. Uchida, Y. Ohashi and G. Yamamoto



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Acta Cryst. (1994). C50, 300-302    [doi:10.1107/S0108270193008029]

5,5-Diphenyl-1H,2H,5H-imidazo[1,2-a]imidazole-3,6-dione

J. Karolak-Wojciechowska and K. Kiec-Kononowicz



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Acta Cryst. (1994). C50, 302-304    [doi:10.1107/S0108270193007358]

Structure of OPC-21268

M. Kido, K. Kondo, H. Yamashita and H. Ogawa



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Acta Cryst. (1994). C50, 304-306    [doi:10.1107/S0108270193006225]

1,6-Diselenacyclodecane-3,4,8,9-tetraone tetrakis(O-methyloxime)

S. Shatzmiller, I. Goldberg, Z. Stein and V. I. Naddaka



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Acta Cryst. (1994). C50, 306-312    [doi:10.1107/S0108270193007139]

HBF4 and HBr salts of new chiral cyclens

K. Kobayashi, S. Tsuboyama, K. Tsuboyama and T. Sakurai



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Acta Cryst. (1994). C50, 312-314    [doi:10.1107/S0108270193007681]

17[alpha]-Benzyl-3[beta],17[beta]-dihydroxy-5-androstene

S. Stankovic, D. Miljkovic, L. Medic-Mijacevic, K. Gasi and C. Courseille



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Acta Cryst. (1994). C50, 314-317    [doi:10.1107/S0108270193007826]

3,12-Dinitro-5,10,15,20-tetraphenylporphyrin - an example of a twisted intramolecular charge-transfer system

S. Dahal, M. Nethaji and V. Krishnan



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Acta Cryst. (1994). C50, 317-324    [doi:10.1107/S0108270193007061]

The structures of endo-13-syn-methyltricyclo[8.2.1.02,9]trideca-5,11-dien-13-anti-ol, endo-13-syn-methyltricyclo[8.2.1.02,9]trideca-5,11-dien-13-anti-yl acetate and its corresponding endo-endo-anti Diels-Alder adducts with 1,2,3,4-tetrachloro-5,5-dimethoxy-1,3-cyclopentadiene and hexachlorocyclopentadiene

J. G. Garcia, G. Morales, F. R. Fronczek and M. L. McLaughlin



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Acta Cryst. (1994). C50, 324-326    [doi:10.1107/S0108270193007772]

2,2,4,4,6,6-Tris(2,3-naphthylenedioxy)cyclotriphosphazene

K. Kubono, N. Asaka, S. Isoda, T. Kobayashi and T. Taga


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