Acta Crystallographica Section C

Crystal Structure Communications

Volume 50, Part 5 (May 1994)


Cover illustration Cover illustration: Bis{[mu]-P,P'-imido-1:2[kappa]2N''-bis[P,P-diphenyl-N-(trimethylsilyl)phosphine imido](1-)-1[kappa]N,1[kappa]P:2[kappa]N',2[kappa]P'}dilithium(Li-Li), see Van der Maelen Uría, Pandey, Roesky & Sheldrick, pages 671-674.

inorganic compounds



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Acta Cryst. (1994). C50, 653-655    [doi:10.1107/S0108270193010182]

Refinement of the structure of hilgardite-1A

P. C. Burns and F. C. Hawthorne



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Acta Cryst. (1994). C50, 655-656    [doi:10.1107/S010827019300890X]

Li3NbO4

K. Ukei, H. Suzuki, T. Shishido and T. Fukuda



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Acta Cryst. (1994). C50, 656-659    [doi:10.1107/S0108270193011205]

Bi12(Bi0.5IIITl0.5III)O19.50

S. F. Radaev, M. Trömel, Y. F. Kargin, A. A. Marin, E. E. Rider and V. A. Sarin



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Acta Cryst. (1994). C50, 659-661    [doi:10.1107/S0108270193010534]

P2Se5

R. Blachnik, P. Lönnecke, K. Boldt and B. Engelen



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Acta Cryst. (1994). C50, 661-663    [doi:10.1107/S0108270193014453]

T-phase Al18Mg3Mn2

H.-K. Fun, H.-C. Lin, T.-J. Lee and B.-C. Yip



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Acta Cryst. (1994). C50, 663-666    [doi:10.1107/S0108270193010042]

Nd2(OH)2(CrO4)2 and [Tb2(CrO4)3(H2O)5].2H2O

J. Leppä-aho



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Acta Cryst. (1994). C50, 666-668    [doi:10.1107/S0108270193010789]

A copper monofluorophosphate, Cu(H2O)2(NH4)2(PO3F)2

M. Berraho, A. Vegas, M. Martínez-Ripoll and M. Rafiq



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Acta Cryst. (1994). C50, 668-669    [doi:10.1107/S0108270193010492]

A precise structure redetermination of nickel ammonium sulfate hexahydrate, Ni(H2O)6.2NH4.2SO4

T. H. Tahirov, T.-H. Lu, C.-C. Huang and C.-S. Chung


metal-organic compounds



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Acta Cryst. (1994). C50, 670-671    [doi:10.1107/S0108270193013046]

Bis(1-methylcytosinium) tetrachlorocobaltate(II), (C5H8N3O)2[CoCl4]

E. C. Hillgeris and B. Lippert



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Acta Cryst. (1994). C50, 671-674    [doi:10.1107/S0108270193010558]

[Li{N(Me3SiNPPh2)2}]2.2.5C7H8

J. F. Van der Maelen Uría, S. K. Pandey, H. W. Roesky and G. M. Sheldrick



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Acta Cryst. (1994). C50, 674-675    [doi:10.1107/S0108270193007206]

Lithium tris(trimethylsilyl)silylselenolate mono(1,2-dimethoxyethane)

K. E. Flick, P. J. Bonasia, D. E. Gindelberger, J. E. B. Katari and D. Schwartz



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Acta Cryst. (1994). C50, 676-678    [doi:10.1107/S0108270193013034]

cis-Tetracarbonylbis(triphenyl phosphite)molybdenum(0)

E. C. Alyea, G. Ferguson and M. Zwikker



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Acta Cryst. (1994). C50, 678-681    [doi:10.1107/S0108270194002180]

Hydrogen bonding in ferrocene derivatives: structure of the 1:1 adduct of ferrocenyl(diphenyl)methanol and dimethyl sulfoxide

C. Glidewell, C. M. Zakaria and G. Ferguson



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Acta Cryst. (1994). C50, 681-683    [doi:10.1107/S0108270193007693]

[Pd{P(C5H10N)Ph2}2Cl2]

R. A. Burrow, D. H. Farrar and C. H. Honeyman



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Acta Cryst. (1994). C50, 683-686    [doi:10.1107/S010827019301114X]

Pentaaqua(2-furancarboxylato)nickel(II) 2-furancarboxylate at 120 K

B. Paluchowska, T. Lis and J. Leciejewicz



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Acta Cryst. (1994). C50, 686-688    [doi:10.1107/S0108270193010522]

Polyol metal complexes. VI. Structure of lithium bis[methyl [alpha]-L-rhamnopyranosid(2,3)-ato(2-)]cuprate(II) tetrahydrate

M. Klaassen and P. Klüfers



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Acta Cryst. (1994). C50, 688-690    [doi:10.1107/S0108270193011072]

Bis(1,1,1,5,5,5-hexafluoro-2,4-pentanedionato)(1,4,10,13-tetraoxa-7,16-diazacyclooctadecane)barium

H. D. Inerowicz, M. A. Khan, G. Atkinson and R. L. White



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Acta Cryst. (1994). C50, 691-693    [doi:10.1107/S0108270193010935]

Tris([mu]-acetato)-[mu]-[(2-bromophenyl)(o-phenylene)phenylphosphine-C:P]tricyclohexylphosphinedirhodium(II)

S. García-Granda, M. R. Díaz, F. Gómez-Beltrán, E. Peris and P. Lahuerta



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Acta Cryst. (1994). C50, 693-695    [doi:10.1107/S0108270193010613]

Trichlorobis(tetrahydrofuran)indium(III)

B. R. Whittlesey and I. P. Ittycheriah



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Acta Cryst. (1994). C50, 695-697    [doi:10.1107/S0108270193008546]

(C18H36N2O6Na)2[Ta6Cl12(CH3O)6].6CH3OH with partial substitution of CH3O- by OH-

U. Beck, H. Borrmann and A. Simon



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Acta Cryst. (1994). C50, 697-700    [doi:10.1107/S010827019301162X]

Di-[mu]-chlorobis[hydrogen bis(diphenylphosphinito)(1-)-P,P']dipalladium, [Pd2Cl2{(C6H5)2PO...H...OP(C6H5)2}2\]

T. Ghaffar, A. Kieszkiewicz, S. C. Nyburg and A. W. Parkins



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Acta Cryst. (1994). C50, 700-702    [doi:10.1107/S0108270193010510]

[mu]3-(O,O'-Diethyl dithiophosphato-2[kappa]S,3:4[kappa]2S')-di-[mu]3-sulfido-1:2:3[kappa]3S;1:2:4[kappa]3S-[mu]-sulfido-1:3[kappa]2S-sulfido-1[kappa]S-tris(triphenylphosphine)-2[kappa]P;3[kappa]P;4[kappa]P-molybdenumtrisilver

S. Du and X. Wu



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Acta Cryst. (1994). C50, 702-704    [doi:10.1107/S0108270193010261]

Bis(2,6-di-tert-butylphenolato-[kappa]O)tin

D. M. Barnhart, D. L. Clark and J. G. Watkin



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Acta Cryst. (1994). C50, 704-706    [doi:10.1107/S0108270193010911]

[Au2(C6H5CS2)([mu]-dppm)2]Cl

J.-C. Wang and L.-K. Liu



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Acta Cryst. (1994). C50, 706-708    [doi:10.1107/S0108270193011187]

trans-Bis(2-hydroxyiminopropionato-N,O)dimethanolnickel(II) dimethanol solvate, [Ni{CH3C(NOH)COO}2(CH3OH)2].2CH3OH

R. D. Lampeka, N. M. Dudarenko and V. V. Skopenko



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Acta Cryst. (1994). C50, 708-710    [doi:10.1107/S0108270193010479]

A binuclear copper(II) complex of the deprotonated anion of N,N'-diglycylethylenediamine

T. H. Tahirov, T.-H. Lu, K. Shu and C.-S. Chung



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Acta Cryst. (1994). C50, 710-712    [doi:10.1107/S0108270193010480]

A copper(II) complex of the deprotonated anion of (2R,10R)-N,N'-dialanylpropylenediamine

T. H. Tahirov, T.-H. Lu, K. Shu and C.-S. Chung



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Acta Cryst. (1994). C50, 712-714    [doi:10.1107/S0108270193012247]

Trichloro(1,4,7-trithiacyclononane-S,S',S'')iron(III), [FeCl3(C6H12S3)]

J. Ballester, O. J. Parker and G. L. Breneman


organic compounds



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Acta Cryst. (1994). C50, 715-717    [doi:10.1107/S0108270193008066]

N,N'-Dicyano-4,7-indanquinone diimine

E. Tillmanns, F. Schwabenländer, S. Güssregen, S. Hünig and T. Metzenthin



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Acta Cryst. (1994). C50, 717-719    [doi:10.1107/S0108270193012284]

A cubic modification of (triphenylarsine)diiodine

S. Abbas, S. M. Godfrey, C. A. McAuliffe and R. G. Pritchard



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Acta Cryst. (1994). C50, 719-721    [doi:10.1107/S0108270193012296]

(2Z,4E,6E)-8-Ethyl-1,1,1-trifluoro-5-trifluoromethyl-3,4,8-triazadeca-2,4,6-triene-2-amine: formation of hydrogen-bonded pairs via an amine-diazine interaction

M. Abdul-Ghani, R. G. Pritchard and A. E. Tipping



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Acta Cryst. (1994). C50, 721-722    [doi:10.1107/S0108270193012326]

(Z,Z)-5-Chloro-1,1,1,6,6,6-hexafluoro-3,4-diaza-4-hexen-2-one oxime, formed by the action of hydroxylamine on 2,5-dichlorohexafluoro-3,4-diazahexa-2,4-diene

M. Abdul-Ghani, R. G. Pritchard and A. E. Tipping



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Acta Cryst. (1994). C50, 722-724    [doi:10.1107/S0108270193012909]

(Z,Z)-5-Chloro-1,1,1,6,6,6-hexafluoro-3,4-diazahexa-2,4-diene-2-amine, in which the amino group is conjugated with a chain double bond

M. Abdul-Ghani, R. G. Pritchard and A. E. Tipping



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Acta Cryst. (1994). C50, 724-726    [doi:10.1107/S0108270193011941]

Diethyl 5,6-dihydro-2H-1,3-dithiolo[4,5-b][1,4]dithiin-2-ylphosphonate, C9H15O3PS4

S. V. Kelkar, J. D. Kilburn and M. Webster



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Acta Cryst. (1994). C50, 726-727    [doi:10.1107/S0108270193012569]

A D-homotestosterone derivative

M. Noltemeyer, L. F. Tietze, J. Wölfling and G. Schneider



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Acta Cryst. (1994). C50, 728-729    [doi:10.1107/S0108270193011254]

2,3-Dihydro-2-methyl-2-indenylmethylammonium chloride

J. C. Barnes, J. D. Paton, D. Rae, J. Cairns and J. Redpath



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Acta Cryst. (1994). C50, 729-732    [doi:10.1107/S0108270193011837]

Dimethyl[3,3,4,4,5,5-hexamethyl-1(E),2(E)cyclopentandiylidene]diacetate, C17H26O4

L. B. Jerzykiewicz, T. Lis, J. Baran and D. Dziewonska-Baran



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Acta Cryst. (1994). C50, 732-734    [doi:10.1107/S010827019301008X]

Intermolecular hydrogen-bonded structure of (1R)-(+)-camphor semicarbazone

P. D. Robinson, C. Y. Meyers and V. M. Kolb



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Acta Cryst. (1994). C50, 734-736    [doi:10.1107/S0108270193011850]

3-[beta]-D-Ribofuranosyl-6,7-dihydro-9H-thiazolo[3,2-a]purin-9-one hydrate

Y.-C. Liaw, A. H.-J. Wang, G.-S. Lin and J.-W. Chern



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Acta Cryst. (1994). C50, 736-738    [doi:10.1107/S0108270193012193]

Absolute stereostructure of 13,17-epoxyalisol B 23-acetate isolated from Alisma orientale

K. Yamaguchi, Y. Ida, Y. Nakajima, Y. Satoh and J. Shoji



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Acta Cryst. (1994). C50, 738-740    [doi:10.1107/S010827019301220X]

A kaurane derivative isolated from Alisma orientale

K. Yamaguchi, Y. Ida, Y. Satoh, Y. Nakajima and J. Shoji



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Acta Cryst. (1994). C50, 740-742    [doi:10.1107/S0108270193011096]

Triphenylphosphoranylideneammonium azide, [Ph3P=NH2][N3]

W. Clegg and C. Bleasdale



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Acta Cryst. (1994). C50, 742-744    [doi:10.1107/S0108270193012041]

Low-temperature structure of bicyclohexylidene, C12H20

N. Veldman, A. L. Spek, F. J. Hoogesteger, J. W. Zwikker and L. W. Jenneskens



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Acta Cryst. (1994). C50, 744-746    [doi:10.1107/S010827019301203X]

trans-transoid-trans-transoid-trans-Tetracyclo[16.4.0.02,9.010,17]docosa-5,13-diene

A. L. Spek, P. J. J. A. Timmermans and A. Mackor



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Acta Cryst. (1994). C50, 746-749    [doi:10.1107/S0108270193012417]

1-Deoxynojirimycin hydrochloride

A. Linden, R. Hoos and A. Vasella



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Acta Cryst. (1994). C50, 749-753    [doi:10.1107/S0108270193011242]

Crystal studies of musk compounds. VII. Molecular structures of 1-tert-butyl-2,4,6-trimethyl-3,5-dinitrobenzene, C13H18N2O4 (2), and 1-bromo-3,5-dimethyl-2,4,6-trinitrobenzene, C8H6BrN3O6 (4)

D. J. A. De Ridder, J. Fraanje and H. Schenk



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Acta Cryst. (1994). C50, 753-755    [doi:10.1107/S0108270193012399]

Crystal studies of musk compounds. IX. 4-Acetyl-1,1,3,3,5,6-hexamethylindan

D. J. A. De Ridder, J. Fraanje and H. Schenk



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Acta Cryst. (1994). C50, 755-757    [doi:10.1107/S0108270193012405]

Crystal studies of musk compounds. X. 1,1,2,3,3-Pentamethyl-2,3,4,5,6,7-hexahydroinden-4-one

D. J. A. De Ridder, J. Fraanje and H. Schenk



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Acta Cryst. (1994). C50, 757-759    [doi:10.1107/S0108270193010832]

X-ray study of static disorder in N-methylacetamide

F. Hamzaoui and F. Baert



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Acta Cryst. (1994). C50, 759-761    [doi:10.1107/S0108270193014258]

1H-Benzimidazolium hydrogen L-tartrate dihydrate

C. B. Aakeröy and P. B. Hitchcock



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Acta Cryst. (1994). C50, 761-763    [doi:10.1107/S0108270193012375]

1-Methyl-5-nitro-2-phenylimidazole and 2-(p-aminophenyl)-1-methyl-5-nitroimidazole

T. A. Olszak, O. M. Peeters, N. M. Blaton and C. J. De Ranter



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Acta Cryst. (1994). C50, 763-765    [doi:10.1107/S0108270193012673]

Methyl DL-3-benzyl-2,2-dioxo-1,2,3-oxathiazolidine-4-carboxylate - an intermediate for amino acid synthesis

P. Gritsonie, M. Pilkington, J. D. Wallis and D. C. Povey



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Acta Cryst. (1994). C50, 765-767    [doi:10.1107/S0108270193010546]

3-Phenyl-1-(2,4,6-triphenylphenyl)propane-1,3-dione

S. Abram, U. Abram and T. Zimmermann



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Acta Cryst. (1994). C50, 767-769    [doi:10.1107/S0108270193008418]

Methyl 3-(1,3-benzothiazol-2-yldithio)propanoate, C11H11NO2S3

P. Krüger, M. Kustos and R. Steudel



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Acta Cryst. (1994). C50, 769-771    [doi:10.1107/S0108270193010625]

Molecular structure and absolute configuration of (P)-7-phenyldinaphtho[2,1-b;1',2'-d]phosphole

K. Tani, T. Yamagata and H. Tashiro



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Acta Cryst. (1994). C50, 771-773    [doi:10.1107/S0108270193010741]

5,6-Dihydroxy-7-methoxyflavone

M. Shoja



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Acta Cryst. (1994). C50, 773-775    [doi:10.1107/S0108270193011217]

3-Bromo-6-methylamino-2'-methoxybenzophenone

B. Berger and M. Bolte



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Acta Cryst. (1994). C50, 775-777    [doi:10.1107/S0108270193008844]

Ein Zwölfring mit Phosphor(V), Kohlenstoff und Dimethylhydrazin als Ringbausteinen und grossen endocyclischen Torsionswinkeln um die N-N-Bindungen

U. Engelhardt und M. Rosefid



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Acta Cryst. (1994). C50, 777-781    [doi:10.1107/S0108270193012685]

Structural investigations of a tetracyclic endo-norborenyl derivative

B. A. Lloyd, A. M. Arif, R. J. Coots and E. L. Allred



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Acta Cryst. (1994). C50, 781-784    [doi:10.1107/S0108270193007048]

Structural comparisons of a perpendicular diene with known derivatives

B. A. Lloyd, A. M. Arif and E. L. Allred



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Acta Cryst. (1994). C50, 784-787    [doi:10.1107/S0108270193009977]

2-[1-Phenylsulfonyl-2-(3,4,5-trimethoxyphenyl)vinyl]-3-(phenylthio)indole

J. Sivaraman, K. Subramanian, D. Velmurugan, E. Subramanian and E. V. Sadanandan



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Acta Cryst. (1994). C50, 787-789    [doi:10.1107/S0108270193008285]

[2-(3,4-Methylenedioxyphenyl)-1-(phenylsulfonyl)vinyl]-3-(phenylthio)indole

J. Sivaraman, K. Subramanian, D. Velmurugan, E. Subramanian and E. V. Sadanandan



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Acta Cryst. (1994). C50, 789-791    [doi:10.1107/S0108270193001817]

2-[2-(4-Methoxyphenyl)-1-(phenylsulfonyl)vinyl]-3-(phenylthio)indole

J. Sivaraman, K. Subramanian, D. Velmurugan, E. Subramanian and E. V. Sadanandan



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Acta Cryst. (1994). C50, 791-794    [doi:10.1107/S0108270193010285]

2-Benzoyl-3-(4-methoxyphenyl)-4-methyl-1-phenyl-2,3-dihydro-1H-pyrazolo[4,3-c][1,2]benzothiazine 5,5-dioxide

F. Theobald, N. Rodier, C. Aubry, K. Ciamala and Nguyan Dinh An



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Acta Cryst. (1994). C50, 794-797    [doi:10.1107/S0108270193011357]

A new quassinoid isolated from Picrolemma pseudocoffea

J. Zukerman-Schpector, E. E. Castellano, E. Rodrigues Fho and I. J. Cursino V.



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Acta Cryst. (1994). C50, 797-798    [doi:10.1107/S0108270193010194]

2-Acetoxy-7-methoxynaphthalene

P. Prince, F. R. Fronczek and R. D. Gandour



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Acta Cryst. (1994). C50, 798-801    [doi:10.1107/S0108270193006596]

11-Ketoprogesterone

V. K. Gupta, Rajnikant, K. N. Goswami, S. K. Mazumdar and K. K. Bhutani



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Acta Cryst. (1994). C50, 801-803    [doi:10.1107/S0108270193010303]

2-(2-Hydroxy-5-methylphenyl)-5-chlorobenzotriazole, C13H10ClN3O

A. Lewanowicz and F. Baert



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Acta Cryst. (1994). C50, 804-805    [doi:10.1107/S0108270193010947]

3-(4-Chlorophenyl)-1-(3-thienyl)-2-propen-1-one

Y. He, J. Shi and G. Su



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Acta Cryst. (1994). C50, 805-807    [doi:10.1107/S0108270193011540]

2-(p-Butoxyphenyl)-5-pentyl-1,3-dithiane, C19H30OS2

M. Miyake, Y. Haramoto and H. Kamogawa



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Acta Cryst. (1994). C50, 807-810    [doi:10.1107/S0108270193010583]

Anomalous products formed from N-(5,6-dihydrobenzo[h]quinazolin-4-yl)amidines and hydroxylamine hydrochloride

T. Hirota, K. Sasaki, H. Yamamoto, K. Mori and S. Kashino



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Acta Cryst. (1994). C50, 810-813    [doi:10.1107/S0108270193010327]

3-Sulfure de 3-mercapto-5,7-diméthyl-2-phényl-3H-[1,4,2]diazaphospholo[1,5-a]pyridinium

N. Rodier, J.-M. Cense, J.-M. Robert, S. Robert-Piessard, J. Courant et G. Le Baut



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Acta Cryst. (1994). C50, 813-816    [doi:10.1107/S010827019301087X]

3-(Benzoylamino)propanoic acid and 6-[(4-nitrobenzoyl)amino]hexanoic acid

N. Feeder and W. Jones



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Acta Cryst. (1994). C50, 816-820    [doi:10.1107/S0108270193010881]

6-Oxo-6-(phenylamino)hexanoic acid [two polymorphic forms, (I) and (II)] and 4-oxo-4-(N-methylphenylamino)butanoic acid (III)

N. Feeder and W. Jones



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Acta Cryst. (1994). C50, 820-823    [doi:10.1107/S010827019301090X]

2-Phthalimidoethanoic acid monohydrate (I) and 6-phthalimidohexanoic acid monohydrate (II)

N. Feeder and W. Jones



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Acta Cryst. (1994). C50, 824-827    [doi:10.1107/S0108270193010893]

Trimellitimide (C9H5NO4) and N-ethyltrimellitimide (C11H9NO4)

N. Feeder and W. Jones



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Acta Cryst. (1994). C50, 827-829    [doi:10.1107/S0108270193010856]

t-3-Isopropyl-r-2,c-7-diphenylhexahydro-1,4-diazepin-5-one, C20H24N2O

K. Ravikumar, S. S. Rajan, V. Parthasarathi, A. Thiruvalluvar, R. Jeyaraman and U. P. Senthilkumar



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Acta Cryst. (1994). C50, 830-833    [doi:10.1107/S0108270193011497]

Avarol, a sesquiterpenoid hydroquinone from Dysidea avara

R. Puliti, S. De Rosa and C. A. Mattia


addenda and errata



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Acta Cryst. (1994). C50, 834    [doi:10.1107/S0108270194003550]

Three substituted 3-amino-2-benzoylaminopropenoic acid derivatives. Erratum

K. Djinovic-Carugo, L. Golic, I. Leban, J. Svete, B. Stanovnik, M. Tisler and C. Tate



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Acta Cryst. (1994). C50, 834    [doi:10.1107/S0108270194099804]

3,3'-Dimethyl-4,4'-diphenyl-2,2',5,5'-tetrathiafulvalenium hexamolybdate, 2(C20H16S4+)[Mo6O19]2-. Erratum

S. Triki, L. Ouahab and J. M. Fabre


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