Acta Crystallographica Section C

Crystal Structure Communications

Volume 50, Part 6 (June 1994)

Cover illustration: Tris(dimethylphenylphosphine)-2P,3P,4P-3-iodo-2:43I-tri-3-selenido-1:2:33Se;1:2:43Se;1:3:43Se-selenido-1Se-trisilvertungsten, see Ansari, Bollinger, Christuk & Ibers, pages 868-871.

• inorganic compounds
• metal-organic compounds
• organic compounds
• addenda and errata

inorganic compounds

Acta Cryst. (1994). C50, 835-838    [doi:10.1107/S0108270193010066]

Sodium lanthanum(III) sulfate monohydrate, NaLa(SO₄)₂.H₂O

A. C. Blackburn and R. E. Gerkin

Acta Cryst. (1994). C50, 838-840    [doi:10.1107/S010827019300962X]

NaScSi₂O₆

H. Ohashi, T. Osawa and A. Sato

Acta Cryst. (1994). C50, 840-842    [doi:10.1107/S0108270193011011]

CdV₂(P₂O₇)₂

S. Boudin, A. Grandin, A. Leclaire, M. M. Borel and B. Raveau

Acta Cryst. (1994). C50, 842-843    [doi:10.1107/S0108270193011795]

Hydrazinium(1+) hexafluorotitanate(IV), 2N₂H₅⁺.TiF₆^2-

I. Leban, A. Jesih and A. Rahten

Acta Cryst. (1994). C50, 844-845    [doi:10.1107/S0108270193012570]

Struktur der hexagonalen Modifikation von Lanthan(III) trichlorid trihydrat

G. Reuter und G. Frenzen

Acta Cryst. (1994). C50, 845-847    [doi:10.1107/S0108270193011990]

Tetraammineplatinum(II) hexachlorostannate(IV), [Pt(NH₃)₄][SnCl₆]

E. Garnier, A. El Mouahid and J. Cernák

metal-organic compounds

Acta Cryst. (1994). C50, 848-850    [doi:10.1107/S0108270193011163]

Methylammonium tris(galliophosphate)hydroxide

F. P. Glasser, R. A. Howie and Q. Kan

Acta Cryst. (1994). C50, 850-852    [doi:10.1107/S0108270193006493]

Dipotassium bis(oxalato)oxotitanate(IV) dihydrate

A. Fester, W. Bensch and M. Trömel

Acta Cryst. (1994). C50, 852-854    [doi:10.1107/S0108270194000326]

Microcrystal structure determination of AlPO₄-CHA using synchrotron radiation

M. M. Harding and B. M. Kariuki

Acta Cryst. (1994). C50, 854-857    [doi:10.1107/S0108270194003197]

Tetracarbonyl[1-phenyl-N-(2-pyridylmethylidene)ethylamine-N,N']molybdenum(0)

E. C. Alyea, G. Ferguson and V. K. Jain

Acta Cryst. (1994). C50, 857-861    [doi:10.1107/S0108270193013654]

Hydrogen bonding in ferrocene derivatives: structures of 1-ferrocenyl-2,2-dimethylpropan-1-ol and 2,2'-(1,1'-ferrocenediyl)di(propan-2-ol)

Y. Li, G. Ferguson, C. Glidewell and C. M. Zakaria

Acta Cryst. (1994). C50, 861-862    [doi:10.1107/S0108270194000259]

(O-Ethyl dithiocarbonato-S)phenylmercury, [Hg(C₃H₅OS₂)(C₆H₅)]

E. R. T. Tiekink

Acta Cryst. (1994). C50, 862-864    [doi:10.1107/S0108270193004950]

Bis(4-aminopyridinium) hexabromodicuprate(II) diaquatetrabromodicopper(II)

H. Place and R. Willett

Acta Cryst. (1994). C50, 864-866    [doi:10.1107/S010827019301217X]

Di--chlorobis[chloro(4,7-diphenyl-1,10-phenanthroline)copper(II)]

A. M. Atria, R. F. Baggio, M. T. Garland and E. Spodine

Acta Cryst. (1994). C50, 867-869    [doi:10.1107/S0108270193012892]

cis-Diisothiocyanatobis(1,10-phenanthroline)manganese(II), [Mn(NCS)₂(C₁₂H₈N₂)₂]

S. R. Holleman, O. J. Parker and G. L. Breneman

Acta Cryst. (1994). C50, 869-871    [doi:10.1107/S0108270193012338]

Synthesis and structure of [(₃-I)(₃-WSe₄){Ag(PMe₂Ph)}₃]

M. A. Ansari, J. C. Bollinger, C. C. Christuk and J. A. Ibers

Acta Cryst. (1994). C50, 871-874    [doi:10.1107/S0108270193011588]

Lithium bis(tetramethyllammonium) hexanitrocobaltate(III) at 113 and 293 K

V. Adovasio, F. Lina, M. Nardelli and G. Pelizzi

Acta Cryst. (1994). C50, 874-876    [doi:10.1107/S0108270193013526]

Hexacarbonylcyclopentadienyl-bis--diphenylphosphanido-manganesetungsten, [MnW(C₁₂H₁₀P)₂(C₅H₅)(CO)₆]

U. Flörke and H.-J. Haupt

Acta Cryst. (1994). C50, 876-879    [doi:10.1107/S010827019300945X]

Effects of halogen substitution in nucleic acid components. Structure of sodium 5-bromocytidine 5'-phosphate hydrate

S. S. Mande, T. P. Seshadri and M. A. Viswamitra

Acta Cryst. (1994). C50, 879-882    [doi:10.1107/S0108270193010923]

[Ir(dppm)₂(O₂)](C₄N₃)

J.-C. Wang, L.-Y. Chou, W.-Y. Hsien and L.-K. Liu

Acta Cryst. (1994). C50, 882-884    [doi:10.1107/S0108270193011734]

(OC-6-14)-(7-Azaindole)dichloro(ethoxo)oxo(triphenylphosphine)rhenium(V)

A.-M. Lebuis and A. L. Beachamp

Acta Cryst. (1994). C50, 884-886    [doi:10.1107/S0108270193011618]

Tris(1,10-phenanthroline)iron(II) diperchlorate hemihydrate

L. L. Koh, Y. Xu, A. K. Hsieh, B. Song, F. Wu and L. Ji

Acta Cryst. (1994). C50, 887-889    [doi:10.1107/S0108270193011564]

catena-Poly[zinc(II)-bis{-(N-carbamoylglycinato)}-O:O'';O'':O], [Zn(C₃H₅N₂O₃)₂]

L. Menabue and M. Saladini

Acta Cryst. (1994). C50, 889-891    [doi:10.1107/S0108270193011813]

(Pyridine-2-thiolato-N,S)bis(triphenylphosphine)platinum(II) hexafluorophosphate chloroform solvate

S. Wang, R. J. Staples and J. P. Fackler Jnr

Acta Cryst. (1994). C50, 891-893    [doi:10.1107/S010827019301193X]

Tris(tert-butylcyclopentadienyl)neodymium--chloro-tris(tetrahydrofuran)lithium, [Nd(⁵-^tBuCp)₃(-Cl)Li(thf)₃]

J. Guan, Q. Shen, S. Jin and Y. Lin

Acta Cryst. (1994). C50, 893-895    [doi:10.1107/S0108270193011473]

A 1:2 addition compound of cadmium bromide with 3-methyl-4-nitropyridine N-oxide

S.-Z. Hu, D.-S. Shi, Y.-Q. Huang, S.-X. Li and Y.-C. Yang

Acta Cryst. (1994). C50, 896-898    [doi:10.1107/S0108270193011771]

A tetrahedral titanium(IV) amido aryloxide compound [Ti(OC₆H₃^tBu₂-2,6)₂(NMe₂)₂]

V. M. Visciglio, P. E. Fanwick and I. P. Rothwell

Acta Cryst. (1994). C50, 898-899    [doi:10.1107/S0108270193011746]

[Mo{P(Ph)₂OC₆H₃(Ph)(⁶-Ph)}(CO)₂]

D. Jaques, J. R. Clark, D. E. Chebi, P. E. Fanwick and I. P. Rothwell

Acta Cryst. (1994). C50, 900-902    [doi:10.1107/S010827019301176X]

A dinuclear niobium oxo compound [Nb(OC₆H₃ⁱPr₂-2,6)₃O]₂

V. M. Visciglio, P. E. Fanwick and I. P. Rothwell

Acta Cryst. (1994). C50, 902-904    [doi:10.1107/S0108270193011758]

[Nb(CH₂SiMe₃)(OC₆H₃Ph₂-2,6)(-CSiMe₃)]₂

E. Torrez, R. D. Profilet, P. E. Fanwick and I. P. Rothwell

organic compounds

Acta Cryst. (1994). C50, 905-907    [doi:10.1107/S0108270193011783]

Crystal and molecular structure of 1,12-dicarboxy-1,12-dicarba-closo-dodecaborane(12), C₄H₁₂B₁₀O₄

R. Centore, M. R. Ciajolo, A. Tuzi, L. G. Komarova, A. L. Rusanov and V. A. Vasnev

Acta Cryst. (1994). C50, 907-910    [doi:10.1107/S0108270193012922]

N-[2-(7-Methoxy-1-naphthyl)ethyl]acetamide, a potent melatonin analog

B. Tinant, J.-P. Declercq, J. H. Poupaert, S. Yous and D. Lesieur

Acta Cryst. (1994). C50, 910-913    [doi:10.1107/S0108270193010455]

2-Methyl-4-(4-pyridyl)-3-butyn-2-ol: a two-dimensional hydrogen-bond network

T. P. Pollagi, S. J. Geib and M. D. Hopkins

Acta Cryst. (1994). C50, 913-915    [doi:10.1107/S0108270193010777]

Structure of a Diels-Alder adduct at a 5,7-disubstituted thebaine derivative

R. H. Woudenberg, H. van Koningsveld and L. Maat

Acta Cryst. (1994). C50, 915-919    [doi:10.1107/S0108270193012910]

2,2',3,3'-Tetra-O-acetyl-6,6'-dichloro-4,4',6,6'-tetradeoxy-,-trehalose

C. K. Lee, L. L. Koh, Y. Xu and A. Linden

Acta Cryst. (1994). C50, 919-921    [doi:10.1107/S0108270193012521]

1-Methyl-2-methylthio-5-nitroimidazole, C₅H₇N₃O₂S

T. A. Olszak, O. M. Peeters, N. M. Blaton and C. J. De Ranter

Acta Cryst. (1994). C50, 921-922    [doi:10.1107/S0108270193012533]

2-(5-Nitro-2-styryl-1-imidazolyl)ethanol

T. A. Olszak, O. M. Peeters, N. M. Blaton and C. J. De Ranter

Acta Cryst. (1994). C50, 922-924    [doi:10.1107/S0108270193014003]

Isopropyl hydrogen 9,10-dihydro-9,10-ethenoanthracene-11,12-dicarboxylate

P. R. Pokkuluri, J. R. Scheffer and J. Trotter

Acta Cryst. (1994). C50, 924-928    [doi:10.1107/S0108270193014209]

Molecules isoelectronic with triphenylmethanol: diphenyl(4-pyridyl)methanol and triphenylmethylamine

C. Glidewell and G. Ferguson

Acta Cryst. (1994). C50, 928-931    [doi:10.1107/S0108270194002179]

2,2,2-Triphenylethanol: a hydrogen-bonded tetramer based upon a centrosymmetric R₄⁴(8) motif

G. Ferguson, C. Glidewell and C. M. Zakaria

Acta Cryst. (1994). C50, 931-933    [doi:10.1107/S0108270193010273]

2,6-Bis[(4-methyl-1-piperazinyl)methyl]-4-nitrophenol

D. Velmurugan, L. Govindasamy, E. Subramanian, T. M. Rajendran and M. Kandaswamy

Acta Cryst. (1994). C50, 933-935    [doi:10.1107/S0108270193011928]

(5-Chloro-1,3-benzoxazol-2-ylthio)acetonitrile

Ö. Ergin, R. Sillanpää, C. Safak and I. Calis

Acta Cryst. (1994). C50, 935-938    [doi:10.1107/S0108270193010790]

[2(2S,3S,4R,6R),3,5]-14-Hydroxy-19-oxo-3,2-[(tetrahydro-3,4-dihydroxy-6-methyl-2H-pyran-2,3-diyl)bis(oxy)]card-20(22)-enolide dihydrate (calactin), C₂₉H₃₉O₉.2H₂O, a cardenolide from Asclepias linaria

T. Hernández-Quiroz, M. Soriano-García, A. Rodríguez-Romero, C. Valencia, L. Hernandez and F. Aguirre-García

Acta Cryst. (1994). C50, 938-941    [doi:10.1107/S0108270193010212]

D-glycero-D-gulo-Heptono- (I) and 2,7-ditosyl-D-glycero-D-gulo-heptono-1,4-lactone (II)

I. Søtofte

Acta Cryst. (1994). C50, 941-945    [doi:10.1107/S0108270193010224]

2,6-Dimesyl-D-manno-hexono- (III), 2,6-dimesyl-D-allo-hexono- (IV) and 2,6-dimesyl-D-gulo-hexono-1,4-lactone (V)

I. Søtofte

Acta Cryst. (1994). C50, 945-946    [doi:10.1107/S0108270193011369]

Diethyl (2,3-dihydro-2-oxo-3-indolylidene)propanedioate

J. Zukerman-Schpector, A. DaC. Pinto, J. F. M. Da Silva, M. T. F. C. Barcellos, S. S. Pires and S. V. Fraiz Jnr

Acta Cryst. (1994). C50, 946-948    [doi:10.1107/S0108270193011849]

1,16-Hexadecanediol, C₁₆H₃₄O₂

N. Nakamura and T. Yamamoto

Acta Cryst. (1994). C50, 948-950    [doi:10.1107/S0108270194000119]

5-Nitro-2-furaldehyde semicarbazone

T. A. Olszak, O. M. Peeters, N. M. Blaton and C. J. De Ranter

Acta Cryst. (1994). C50, 950-952    [doi:10.1107/S0108270193014404]

An unusual C-4a hydroxylated decahydroquinolone

S. P. Joseph, D. L. Comins and P. Singh

Acta Cryst. (1994). C50, 952-954    [doi:10.1107/S0108270193011461]

2,3-Dihydro-6-hydroxy-1,3-dimethyl-7-propyl-9-(2-thienylmethyl)pyrimido[2,1-f]purine-4,8(1H,9H)-dione

A. K. Das, M. Datta, S. K. Mazumdar, G. Bhaumik, B. Mazumdar and S. K. Talapatra

Acta Cryst. (1994). C50, 954-955    [doi:10.1107/S0108270193011606]

A (2R,5S)-2-o-anisyl-3-oxa-1-aza-2-phosphabicyclo[3.3.0]octane-borane complex

J. M. Brunel, G. Buono, A. Baldy, J. Feneau-Dupont and J.-P. Declercq

Acta Cryst. (1994). C50, 955-957    [doi:10.1107/S0108270193010339]

4-(4,6-Diméthylpyrid-2-yl)-5-éthyl-3-phényl-4H-1,2,4-triazole

N. Rodier, S. Robert-Piessard, J.-M. Robert et G. Le Baut

Acta Cryst. (1994). C50, 957-960    [doi:10.1107/S0108270193012107]

N-(2,6-Diméthylphényl)-6-hydroxy-2,5,7,8-tétraméthyl-3,4-dihydro-2H-1-benzopyran-2-carboxamide

N. Rodier, J.-P. Babingui, M. Duflos et G. Le Baut

Acta Cryst. (1994). C50, 960-963    [doi:10.1107/S0108270193010352]

Structure du N-phényltroloxamide et du N-phényltroloxthioamide, inhibiteurs de leucotriènes

N. Rodier, J.-M. Cense, J.-P. Babingui, J. Courant et G. Le Baut

Acta Cryst. (1994). C50, 964-965    [doi:10.1107/S0108270193012557]

3-Methoxy-16,16-dimethyl-5-androstan-17-one

J. Wölfling, G. Schneider, M. Noltemeyer and L. F. Tietze

Acta Cryst. (1994). C50, 965-967    [doi:10.1107/S0108270194000041]

An enantiomerically pure 4-oxo--amino acid derivative

W. Clegg, R. F. W. Jackson, P. A. O'Neil and N. Wishart

Acta Cryst. (1994). C50, 967-971    [doi:10.1107/S010827019400003X]

p-Methyl-N-(pentafluorobenzylidene)aniline (1), 1,2,3,4-tetrafluoro-7-methoxyacridine (2), 1,2,3,4,7-pentafluoroacridine (3) and 3-(p-methylanilino)-1,2,4-trifluoro-7-methylacridine (4): four molecules representing key stages in the one-pot synthesis of 1,2,3,4-tetrafluoroacridines by treating pentafluorobenzaldehyde with para-substituted anilines

A. J. Adamson, Y. Archambeau, R. E. Banks, B. Beagley, M. Helliwell, R. G. Pritchard and A. E. Tipping

Acta Cryst. (1994). C50, 971-974    [doi:10.1107/S0108270193013927]

3-Selenocyanatopyridine

S. J. Dunne, L. A. Summers, E. I. von Nagy-Felsobuki and M. F. Mackay

Acta Cryst. (1994). C50, 974-976    [doi:10.1107/S010827019400048X]

A high-density thermally stable explosive: octahydro-2,5-bis(nitroimino)imidazo[4,5-d]imidazole

J. L. Flippen-Anderson, M. Kony and I. J. Dagley

Acta Cryst. (1994). C50, 976-977    [doi:10.1107/S0108270193014544]

2,2'-Dimethoxybibenzyl

J.-N. Ross, J. L. Wardell, G. Ferguson and J. N. Low

addenda and errata

Acta Cryst. (1994). C50, 978    [doi:10.1107/S0108270194004543]

Structure of a model for the aranorosin nucleus. Erratum

R. C. Haltiwanger, D. S. Eggleston, A. McKillop, R. J. K. Taylor, R. J. Watson and N. Lewis

Acta Cryst. (1994). C50, 978    [doi:10.1107/S0108270194004531]

Synthesis and structure of trans-1,2,3-tris(3-thenoyl)cyclopropane. Erratum

A. Saba

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