Acta Crystallographica Section C

Crystal Structure Communications

Volume 50, Part 7 (July 1994)


Cover illustration Cover illustration: Tetraethyl 2,3,3a,7b,9,10,10a,14b-hexahydro-1H,8H-3a,7b[1',2']-benzeno-10a,14b-ethenodibenzo[a,e]dicyclopenta[c,g]cyclooctene-2,2,9,9-tetracarboxylate, see Hua, Dantoing, Robinson, Qui & Meyers, pages 1090-1093.

inorganic compounds



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Acta Cryst. (1994). C50, 979-980    [doi:10.1107/S0108270193014337]

Refinement of the structure of synthetic sodium zinc monophosphate

J. Yamakawa, I. Watanabe and A. Kawahara



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Acta Cryst. (1994). C50, 981-984    [doi:10.1107/S0108270194001368]

Synthesis and structures of two isostructural phosphites, Fe11(HPO3)8(OH)6 and Mn11(HPO3)8(OH)6

M. P. Attfield, R. E. Morris and A. K. Cheetham



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Acta Cryst. (1994). C50, 984-986    [doi:10.1107/S0108270194002039]

Rietveld refinement of dry-synthesized Rb2ZnSi5O12 leucite by synchrotron X-ray powder diffraction

A. M. T. Bell and C. M. B. Henderson



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Acta Cryst. (1994). C50, 986-988    [doi:10.1107/S0108270193012004]

Un monophosphate de magnésium et de sodium

J. Yamakawa, T. Yamada et A. Kawahara



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Acta Cryst. (1994). C50, 988-991    [doi:10.1107/S0108270193008364]

SrZrSi2O7

M. E. Huntelaar, E. H. P. Cordfunke, P. van Vlaanderen and D. J. W. IJdo



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Acta Cryst. (1994). C50, 991-994    [doi:10.1107/S0108270193011278]

Cadmium selenite-water (4/3) and two polymorphic forms of cadmium selenite

J. Valkonen



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Acta Cryst. (1994). C50, 994-996    [doi:10.1107/S0108270193012090]

Tetraammineplatinum(II) aquapentachloroiridate(III) dihydrate, [Pt(NH3)4][IrCl5(H2O)].2H2O

E. Garnier and M. Bele



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Acta Cryst. (1994). C50, 996-997    [doi:10.1107/S0108270194001721]

A revised structure for [alpha]-dicalcium silicate hydrate

R. E. Marsh


metal-organic compounds



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Acta Cryst. (1994). C50, 998-1000    [doi:10.1107/S0108270193010650]

A cyclo-triarsenic complex of chromium

W. Chen, R. C. S. Wong and L. Y. Goh



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Acta Cryst. (1994). C50, 1000-1002    [doi:10.1107/S0108270193011448]

[mu]-[1,2-Bis(diethylphosphino)ethane]-P:P'-bis[bis(diethyldithiocarbamato-S,S')zinc(II)] ditoluene solvate

D. Zeng, M. J. Hampden-Smith and E. M. Larson



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Acta Cryst. (1994). C50, 1002-1003    [doi:10.1107/S0108270193013009]

Bis([eta]5-methylcyclopentadienyl)chromium, [Cr(C6H7)2]

F. Benetollo, A. Camporese and G. Rossetto



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Acta Cryst. (1994). C50, 1003-1005    [doi:10.1107/S0108270193013137]

(4,7-Dimethyl-4,7-diazadecanediamide)diisothiocyanatocopper(II)

J.-L. Lin, T.-H. Lu, T. H. Tahirov, Y.-L. Liu, T.-Y. Chi and C.-S. Chung



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Acta Cryst. (1994). C50, 1005-1007    [doi:10.1107/S0108270193012211]

Bis([mu]-4-methylphenoxido-1:2[kappa]2O)tris(triphenylphosphine)-1[kappa]2P,2[kappa]P-dicopper(I)

W. J. Evans, R. E. Golden and J. W. Ziller



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Acta Cryst. (1994). C50, 1008-1010    [doi:10.1107/S0108270193012934]

Terbium p-nitrobenzoate hydrate

J.-F. Ma, Z.-S. Jin and J.-Z. Ni



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Acta Cryst. (1994). C50, 1010-1012    [doi:10.1107/S0108270193012879]

Yttrium salicylate tetrahydrate

J.-F. Ma, Z.-S. Jin and J.-Z. Ni



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Acta Cryst. (1994). C50, 1012-1014    [doi:10.1107/S0108270193013411]

A mixed-ligand cadmium(II) complex of xanthic acid and N,N'-bis(4-methoxyphenyl)thiourea

Z.-F. Sun, C.-Y. Duan, X.-Z. You and X.-Y. Huang



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Acta Cryst. (1994). C50, 1014-1016    [doi:10.1107/S0108270193011102]

[meso-5,10,15,20-Tetrakis(4-methoxyphenyl)porphinato]bis(trimethyl phosphito)iron(II)

L. Toupet, N. Legrand, A. Bondon and G. Simonneaux



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Acta Cryst. (1994). C50, 1016-1019    [doi:10.1107/S0108270193014027]

1,4,7,10,13-Pentaoxacyclopentadecane (15-crown-5) sodium iodide complex, C10H20O5.NaI

G. W. Buchanan, M. Gerzain and C. Bensimon



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Acta Cryst. (1994). C50, 1019-1020    [doi:10.1107/S010827019201271X]

Di-[mu]-bromo-tetrabromotetrakis(trimethylphosphine)dirhodium(III)

S. E. Boyd, L. D. Field and T. W. Hambley



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Acta Cryst. (1994). C50, 1020-1023    [doi:10.1107/S0108270193013472]

Two crystalline polymorphs of chloro[tris(2-cyanoethyl)phosphine]gold(I), [AuCl(C9H12N3P)]

J. P. Fackler Jnr, R. J. Staples, M. N. I. Khan and R. E. P. Winpenny



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Acta Cryst. (1994). C50, 1023-1026    [doi:10.1107/S010827019301337X]

[mu]4-Oxo-hexakis([mu]-3,5-dimethylpyrazolato-N,N')tetracobalt(II)

M. K. Ehlert, S. J. Rettig, A. Storr, R. C. Thompson and J. Trotter



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Acta Cryst. (1994). C50, 1026-1028    [doi:10.1107/S0108270193013083]

Tetrakis[{[mu]3-ethoxy(N-methylimino)methanethiolato}copper(I)]

T. Kuroda-Sowa, M. Munakata, M. Miyazaki and M. Maekawa



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Acta Cryst. (1994). C50, 1028-1031    [doi:10.1107/S0108270193011989]

[{PtCl(dmso)}2([mu]-OH)2]

Z. Bugarcic, K. Lövqvist and Å. Oskarsson



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Acta Cryst. (1994). C50, 1031-1034    [doi:10.1107/S0108270193012831]

Hexakis(tert-butylammonium) heptamolybdate(VI)-water (1/7)

P. Román, A. San José, A. Luque and J. M. Gutiérrez-Zorrilla



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Acta Cryst. (1994). C50, 1034-1037    [doi:10.1107/S0108270193012363]

2,2'-Bipyrimidine (bpm)-bridged dinuclear complexes. 3. Structure of [mu]-(2,2'-bipyrimidine-N1,N1':N3,N3')bis(tetraaquazinc) disulfate dihydrate, [Zn2([mu]-bpm)(H2O)8\](SO4)2.2H2O

G. De Munno and M. Julve



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Acta Cryst. (1994). C50, 1037-1040    [doi:10.1107/S0108270193011151]

Yttrium(III) and lanthanum(III) complexes of a 15-membered macrocycle with three pendant carboxymethyl groups

M. B. Inoue, M. Inoue and Q. Fernando



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Acta Cryst. (1994). C50, 1040-1042    [doi:10.1107/S0108270193012648]

(Bipyridyl-N,N')diiodoplatinum(II)

W. B. Connick and H. B. Gray



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Acta Cryst. (1994). C50, 1043-1044    [doi:10.1107/S0108270193013757]

N,N'-Ethylenebis(4,6-dimethoxysalicylideneiminato)copper(II) monohydrate

E. Labisbal, J. Romero, J. A. García-Vázquez, A. Sousa, E. E. Castellano and J. Zukerman-Schpector



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Acta Cryst. (1994). C50, 1044-1046    [doi:10.1107/S0108270193013915]

Potassium (5-nitro-1,10-phenanthroline-N1,N10)oxodiperoxovanadate(V) dihydrate: an insulin-mimetic peroxovanadate

A. Shaver, J. B. Ng, R. C. Hynes and B. I. Posner



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Acta Cryst. (1994). C50, 1046-1049    [doi:10.1107/S0108270193011825]

Tetrakis[m-(trifluoromethyl)phenyl]tin(IV)

F. E. Smith, R. C. Hynes, Y. Z. Zhang, G. Eng and L. E. Khoo



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Acta Cryst. (1994). C50, 1049-1052    [doi:10.1107/S0108270194000089]

Oxobis(N-oxopyridine-2-thiolato-N,O)vanadium(IV)

F. J. Higes-Rolando, A. Perez-Florindo, C. Valenzuela-Calahorro, J. D. Martin-Ramos and J. Romero-Garzon



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Acta Cryst. (1994). C50, 1052-1054    [doi:10.1107/S0108270194000363]

Octadecacarbonylhexaosmium chloroform solvate

A. J. Blake, B. F. G. Johnson and J. G. M. Nairn



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Acta Cryst. (1994). C50, 1054-1057    [doi:10.1107/S0108270193013897]

Sodium cyclododecyl sulfate trihydrate, Na+.C12H23O4S-.3H2O

R. Rudert, D. Vollhardt and G. Czichocki



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Acta Cryst. (1994). C50, 1057-1059    [doi:10.1107/S0108270193013216]

A palladium-dithiooxamide complex

M. Abboudi and A. Mosset



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Acta Cryst. (1994). C50, 1059-1062    [doi:10.1107/S0108270193014088]

(Benzenethiolato-[kappa]S)triphenyltin(IV), [Sn(C6H5S)(C6H5)3] (I), and bis(benzenethiolato-[kappa]S)diphenyltin(IV), [Sn(C6H5S)2(C6H5)2] (II)

N. Speziali, B. G. Guimarães, R. M. Silva, P. H. Duarte and S. R. Aguiar



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Acta Cryst. (1994). C50, 1062-1064    [doi:10.1107/S0108270193013629]

[2,6-Bis(2-pyrimidinylthiomethyl)pyridine]dichlorocopper(II) methanol solvate

R. Sillanpää, R. Kivekäs, L. Escriche, J. Casabó and G. Sánchez-Castelló



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Acta Cryst. (1994). C50, 1064-1065    [doi:10.1107/S0108270194001083]

[RuCl2(PH2Cy)([eta]6-p-cymene)]

J. F. Van der Maelen Uría, S. García-Granda, J. A. Cabeza and I. del Río



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Acta Cryst. (1994). C50, 1066-1069    [doi:10.1107/S0108270193012181]

Dichloro- and dibromo[N-(2-pyridylmethylidene)-2-thienylmethylamine-N,N']copper(II) complexes, [CuCl2(C11H10N2S)] and [CuBr2(C11H10N2S)]

A. M. Atria, R. F. Baggio, N. Espinosa, M. T. Garland, J. Manzur, Y. Moreno and E. Spodine



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Acta Cryst. (1994). C50, 1069-1072    [doi:10.1107/S0108270194001095]

A tri-[mu]-chloro dirhodium (III) complex [Rh2([mu]-Cl)3(triphos)2](CF3SO3)3 [triphos = CH3C(CH2PPh2)3]

F. Bachechi



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Acta Cryst. (1994). C50, 1072-1074    [doi:10.1107/S0108270194000417]

Monochloroindium derivative of tmtaa (dibenzotetramethyltetraaza[14]annulene), [In(C22H22N4)Cl]

P. R. Phillips, A. McCamley, N. W. Alcock and M. G. H. Wallbridge



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Acta Cryst. (1994). C50, 1074-1076    [doi:10.1107/S0108270193012843]

Hexakis(difluorphenylphosphan)wolfram(0) hydrat, W(PF2Ph)6.H2O

W. Crump, T. Kruck, B. Siegers and K.-F. Tebbe



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Acta Cryst. (1994). C50, 1076-1079    [doi:10.1107/S0108270194001010]

Sodium galactarate and potassium galactarate

T. Taga, T. Shimada and N. Mimura



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Acta Cryst. (1994). C50, 1079-1084    [doi:10.1107/S0108270193012119]

Two 4-nitropyridine N-oxide adducts: (C5H4N2O3)2.AgNO3 and (C5H4N2O3)2.Co(NO3)2.4H2O

M. Bagieu-Beucher, Y. Le Fur, J.-P. Levy and J.-P. Pécaut



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Acta Cryst. (1994). C50, 1084-1087    [doi:10.1107/S0108270193014052]

cis-Tetracarbonylbis[tris(p-fluorophenyl)phosphine]molybdenum(0)

E. C. Alyea, G. Ferguson, J. F. Gallagher and S. Song



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Acta Cryst. (1994). C50, 1087-1089    [doi:10.1107/S0108270193013149]

(C24H20P)2[Mo6Cl14]

M. A. White, M. R. Pressprich and P. Coppens


organic compounds



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Acta Cryst. (1994). C50, 1090-1093    [doi:10.1107/S0108270193014064]

Photoisomerization of tetraethyl 6,8,15,17-tetrahydro-7H,16H-5,18[1',2']-benzeno-9,14-ethenodibenzo[a,h]cyclotetradecene-7,7,16,16-tetracarboxylate. Structure of tetraethyl 2,3,3a,7b,9,10,10a,14b-hexahydro-1H,8H-3a,7b[1',2']-benzeno-10a,14b-ethenodibenzo[a,e]dicyclopenta[c,g]cyclooctene-2,2,9,9-tetracarboxylate as its methylene chloride solvate

D. H. Hua, B. Dantoing, P. D. Robinson, T.-C. Qui and C. Y. Meyers



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Acta Cryst. (1994). C50, 1093-1095    [doi:10.1107/S0108270193014532]

(R)-(+)-2-Phenylpropyl p-toluenesulfonate, C16H18O3S

H. Gallardo, A. A. Merlo, I. Vencato and Y. P. Mascarenhas



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Acta Cryst. (1994). C50, 1095-1097    [doi:10.1107/S0108270193012387]

Methyl N,N-diallyl-O-tert-butyltyrosyl-[alpha]-aminoisobutyryl-[alpha]-aminoisobutyrate, C28H43N3O5

J. L. Flippen-Anderson, C. George and J. R. Deschamps



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Acta Cryst. (1994). C50, 1097-1099    [doi:10.1107/S010827019400017X]

Nitrilotriacetic acid, C6H9NO6

E. Skrzypczak-Jankun, D. A. Smith and H. Maluszynska



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Acta Cryst. (1994). C50, 1099-1101    [doi:10.1107/S010827019300770X]

Bis(5-acetylamino-1,3,4-thiadiazole-2-sulfon)amide dihydrate

M. Vinkovic, S. Mutak, A. Nagl and B. Kamenar



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Acta Cryst. (1994). C50, 1101-1104    [doi:10.1107/S0108270194001009]

2-Nitrobiphenyl and 2,2'-dinitrobiphenyl

A. Sekine, Y. Ohashi, K. Yoshimura, M. Yagi and J. Higuchi



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Acta Cryst. (1994). C50, 1104-1106    [doi:10.1107/S0108270193013770]

Ein gesättigter anorganischer Phosphor(V) Hydrazin-Schwefel(IV)-Sechsring mit Twist-Boot-Konformation

U. Engelhardt, B. Stromburg und A. Simon



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Acta Cryst. (1994). C50, 1106-1108    [doi:10.1107/S0108270193011084]

4,4'-Isopropylidenediphenyl bis(chloroformate)

G. L. Bryant Jnr and J. A. King Jnr



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Acta Cryst. (1994). C50, 1108-1112    [doi:10.1107/S010827019400082X]

2,2',3,3'-Tetra-O-acetyl-4,4',6,6'-tetradeoxy-[alpha],[alpha]-xylo-trehalose

A. Linden and C.-K. Lee



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Acta Cryst. (1994). C50, 1112-1114    [doi:10.1107/S0108270194000612]

Octabutyltetrasila[2.2]terthiophenophane

J. K. Herrema, J. Wildeman, F. van Bolhuis and G. Hadziioannou



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Acta Cryst. (1994). C50, 1114-1117    [doi:10.1107/S0108270193009291]

Structure of charge-transfer complexes. 3. 2,4,5,7-Tetranitro-9-fluorenone-2-ethylnaphthalene (1/1)

M. C. Shah and R. G. Baughman



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Acta Cryst. (1994). C50, 1117-1118    [doi:10.1107/S0108270193012867]

A 2,5-diketomorpholine

M. Bolte and E. Egert



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Acta Cryst. (1994). C50, 1118-1122    [doi:10.1107/S010827019301323X]

Four N-saccharinaliphatic acids

N. Feeder and W. Jones



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Acta Cryst. (1994). C50, 1122-1124    [doi:10.1107/S0108270193013903]

[1R,2R,5(1')S,9R,2'R,4'R,5'S]-2,10,10-Triméthyl-3-oxa-6-azatricyclo[7,1,1,02,7]undeca-5-spiro[1'(2',4',5'-triméthylcyclohexane)]-6-ène-4-one

A. Chiaroni, C. Riche, J.-P. Lavergne, M. Sadoune, P. Viallefont et Y. Vidal



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Acta Cryst. (1994). C50, 1124-1126    [doi:10.1107/S0108270193013666]

1-(2,4-Dimethoxy-1,3,5-triazin-6-yloxy)pyrrolidine-2,5-dione, C9H10N4O5

M. L. Glówka and A. W. Sobanska



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Acta Cryst. (1994). C50, 1126-1130    [doi:10.1107/S0108270193011576]

Geneserine hydrochloride

A. Bacchi, G. Pelizzi, E. Redenti, M. Delcanale, G. Amari and P. Ventura



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Acta Cryst. (1994). C50, 1130-1132    [doi:10.1107/S0108270193013289]

Hydrogen-bonded trimers of methyl 4-trifluoromethylpyrazole-3-carboxylate solvated by chloroform

B. Beagley, K. J. Farnworth, E. T. Moss, R. G. Pritchard, S. Tajammal and A. E. Tipping



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Acta Cryst. (1994). C50, 1132-1135    [doi:10.1107/S0108270193013642]

p-Hydroxyephedrinium dihydrogenphosphate

M. Datta, A. Podder and J. K. Dattagupta



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Acta Cryst. (1994). C50, 1135-1138    [doi:10.1107/S0108270193011862]

N-(N-Benzyloxycarbonyl-L-1,2,3,4-tetrahydroisoquinol-3-ylcarbonyl)-L-phenylalanine methyl ester, Z-L-Tic-L-Phe-OMe

L. Vitagliano, A. Zagart, S. Capasso, S. Salvadori and G. Baldoni



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Acta Cryst. (1994). C50, 1139-1141    [doi:10.1107/S0108270193011199]

1:2 complexes of (thio)morpholinium derivatives and the electron acceptor 7,7,8,8-tetracyano-p-quinodimethane. VII. Triclinic form of N,N-dimethylmorpholinium di-7,7,8,8-tetracyano-p-quinodimethanide, DMM(TCNQ)2 (II), at 294 K

R. J. J. Visser, J. L. de Boer and A. Vos



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Acta Cryst. (1994). C50, 1141-1143    [doi:10.1107/S0108270193012065]

Indan-2,2-dicarboxylic acid, C11H10O4

J. G. Garcia, J. D. Enas and F. R. Fronczek



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Acta Cryst. (1994). C50, 1143-1145    [doi:10.1107/S0108270193012089]

A chromotropic bi(benzofuranonyl)

Y. Mori, I. Kubota, Y. Watanabe and K. Maeda



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Acta Cryst. (1994). C50, 1145-1148    [doi:10.1107/S0108270193012478]

threo-3-Fluoro-2-hydroxy-1,3-diphenyl-1-propanone and (1RS,2RS,3RS)-3-fluoro-1,3-diphenyl-1,2-propanediol

R. Stomberg, S. Li and K. Lundquist



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Acta Cryst. (1994). C50, 1148-1149    [doi:10.1107/S010827019400096X]

Ammonium salt of nitroacetamide

O. Simonsen and P. N. Jørgensen



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Acta Cryst. (1994). C50, 1150-1152    [doi:10.1107/S0108270193013022]

A mesoionic pyridazinium sulfonate; an unexpected reaction product

O. Simonsen, E. Fanghänel, B. B. Iversen and F. K. Larsen



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Acta Cryst. (1994). C50, 1152-1154    [doi:10.1107/S0108270193012752]

3,5-Difluorophenol

M. Shibakami and A. Sekiya



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Acta Cryst. (1994). C50, 1154-1156    [doi:10.1107/S0108270193011503]

Three tetramethylketals of 2,5-distyryl-[1,4]benzoquinones

H. Irngartinger and J. Lichtenthäler



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Acta Cryst. (1994). C50, 1156-1159    [doi:10.1107/S0108270193012697]

A spiro-indole derivative, C16H10ClFN2O2S

V. Sehgal, P. Singh, A. Dandia and R. Bohra



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Acta Cryst. (1994). C50, 1159-1161    [doi:10.1107/S0108270193013150]

1-Acetyl-5-benzyl-2-methylthio-5H-imidazol-4-one

M. F. Mackay, G. J. Trantino, B. M. Duggan and J. F. K. Wilshire



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Acta Cryst. (1994). C50, 1161-1163    [doi:10.1107/S0108270193012272]

Guanidinium nitrate

A. Katrusiak and M. Szafranski



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Acta Cryst. (1994). C50, 1163-1165    [doi:10.1107/S0108270193013393]

N,N'-Bis(2-hydroxypropyl)dithiooxamide

Y. C. Jean



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Acta Cryst. (1994). C50, 1165-1169    [doi:10.1107/S0108270193013721]

Methyl (2-methoxycarbonylbenzoyl)triphenylphosphoranylideneacetate and its ethanolate complex

F. D. Rochon, R. Melanson and M. M. Kayser



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Acta Cryst. (1994). C50, 1169-1171    [doi:10.1107/S010827019301368X]

2,2'-Azinodimethyldiphenol, C14H12N2O2

X.-X. Xu, X.-Z. You, Z.-F. Sun, X. Wang and H.-X. Liu



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Acta Cryst. (1994). C50, 1171-1173    [doi:10.1107/S0108270193012120]

3,4-Diméthoxycarbonyl-5-éthoxycarbonyl-1-(2,2,2-trichloro-1-éthoxycarbonylaminoéthyl)pyrazole, C15H18Cl3N3O8

N. Rodier, A. Belaissaoui, C. Morpain et B. Laude



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Acta Cryst. (1994). C50, 1173-1176    [doi:10.1107/S0108270193012132]

Bis[2-(3-morpholinobenzofuranyl)]phénylméthane, C31H30N2O4

N. Rodier, M. M'Saddek, M. Rammah et K. Ciamala


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