Acta Crystallographica Section C

Crystal Structure Communications

Volume 50, Part 7 (July 1994)

Cover illustration: Tetraethyl 2,3,3a,7b,9,10,10a,14b-hexahydro-1H,8H-3a,7b[1',2']-benzeno-10a,14b-ethenodibenzo[a,e]dicyclopenta[c,g]cyclooctene-2,2,9,9-tetracarboxylate, see Hua, Dantoing, Robinson, Qui & Meyers, pages 1090-1093.

• inorganic compounds
• metal-organic compounds
• organic compounds

inorganic compounds

Acta Cryst. (1994). C50, 979-980    [doi:10.1107/S0108270193014337]

Refinement of the structure of synthetic sodium zinc monophosphate

J. Yamakawa, I. Watanabe and A. Kawahara

Acta Cryst. (1994). C50, 981-984    [doi:10.1107/S0108270194001368]

Synthesis and structures of two isostructural phosphites, Fe₁₁(HPO₃)₈(OH)₆ and Mn₁₁(HPO₃)₈(OH)₆

M. P. Attfield, R. E. Morris and A. K. Cheetham

Acta Cryst. (1994). C50, 984-986    [doi:10.1107/S0108270194002039]

Rietveld refinement of dry-synthesized Rb₂ZnSi₅O₁₂ leucite by synchrotron X-ray powder diffraction

A. M. T. Bell and C. M. B. Henderson

Acta Cryst. (1994). C50, 986-988    [doi:10.1107/S0108270193012004]

Un monophosphate de magnésium et de sodium

J. Yamakawa, T. Yamada et A. Kawahara

Acta Cryst. (1994). C50, 988-991    [doi:10.1107/S0108270193008364]

SrZrSi₂O₇

M. E. Huntelaar, E. H. P. Cordfunke, P. van Vlaanderen and D. J. W. IJdo

Acta Cryst. (1994). C50, 991-994    [doi:10.1107/S0108270193011278]

Cadmium selenite-water (4/3) and two polymorphic forms of cadmium selenite

J. Valkonen

Acta Cryst. (1994). C50, 994-996    [doi:10.1107/S0108270193012090]

Tetraammineplatinum(II) aquapentachloroiridate(III) dihydrate, [Pt(NH₃)₄][IrCl₅(H₂O)].2H₂O

E. Garnier and M. Bele

Acta Cryst. (1994). C50, 996-997    [doi:10.1107/S0108270194001721]

A revised structure for -dicalcium silicate hydrate

R. E. Marsh

metal-organic compounds

Acta Cryst. (1994). C50, 998-1000    [doi:10.1107/S0108270193010650]

A cyclo-triarsenic complex of chromium

W. Chen, R. C. S. Wong and L. Y. Goh

Acta Cryst. (1994). C50, 1000-1002    [doi:10.1107/S0108270193011448]

-[1,2-Bis(diethylphosphino)ethane]-P:P'-bis[bis(diethyldithiocarbamato-S,S')zinc(II)] ditoluene solvate

D. Zeng, M. J. Hampden-Smith and E. M. Larson

Acta Cryst. (1994). C50, 1002-1003    [doi:10.1107/S0108270193013009]

Bis(⁵-methylcyclopentadienyl)chromium, [Cr(C₆H₇)₂]

F. Benetollo, A. Camporese and G. Rossetto

Acta Cryst. (1994). C50, 1003-1005    [doi:10.1107/S0108270193013137]

(4,7-Dimethyl-4,7-diazadecanediamide)diisothiocyanatocopper(II)

J.-L. Lin, T.-H. Lu, T. H. Tahirov, Y.-L. Liu, T.-Y. Chi and C.-S. Chung

Acta Cryst. (1994). C50, 1005-1007    [doi:10.1107/S0108270193012211]

Bis(-4-methylphenoxido-1:2²O)tris(triphenylphosphine)-1²P,2P-dicopper(I)

W. J. Evans, R. E. Golden and J. W. Ziller

Acta Cryst. (1994). C50, 1008-1010    [doi:10.1107/S0108270193012934]

Terbium p-nitrobenzoate hydrate

J.-F. Ma, Z.-S. Jin and J.-Z. Ni

Acta Cryst. (1994). C50, 1010-1012    [doi:10.1107/S0108270193012879]

Yttrium salicylate tetrahydrate

J.-F. Ma, Z.-S. Jin and J.-Z. Ni

Acta Cryst. (1994). C50, 1012-1014    [doi:10.1107/S0108270193013411]

A mixed-ligand cadmium(II) complex of xanthic acid and N,N'-bis(4-methoxyphenyl)thiourea

Z.-F. Sun, C.-Y. Duan, X.-Z. You and X.-Y. Huang

Acta Cryst. (1994). C50, 1014-1016    [doi:10.1107/S0108270193011102]

[meso-5,10,15,20-Tetrakis(4-methoxyphenyl)porphinato]bis(trimethyl phosphito)iron(II)

L. Toupet, N. Legrand, A. Bondon and G. Simonneaux

Acta Cryst. (1994). C50, 1016-1019    [doi:10.1107/S0108270193014027]

1,4,7,10,13-Pentaoxacyclopentadecane (15-crown-5) sodium iodide complex, C₁₀H₂₀O₅.NaI

G. W. Buchanan, M. Gerzain and C. Bensimon

Acta Cryst. (1994). C50, 1019-1020    [doi:10.1107/S010827019201271X]

Di--bromo-tetrabromotetrakis(trimethylphosphine)dirhodium(III)

S. E. Boyd, L. D. Field and T. W. Hambley

Acta Cryst. (1994). C50, 1020-1023    [doi:10.1107/S0108270193013472]

Two crystalline polymorphs of chloro[tris(2-cyanoethyl)phosphine]gold(I), [AuCl(C₉H₁₂N₃P)]

J. P. Fackler Jnr, R. J. Staples, M. N. I. Khan and R. E. P. Winpenny

Acta Cryst. (1994). C50, 1023-1026    [doi:10.1107/S010827019301337X]

₄-Oxo-hexakis(-3,5-dimethylpyrazolato-N,N')tetracobalt(II)

M. K. Ehlert, S. J. Rettig, A. Storr, R. C. Thompson and J. Trotter

Acta Cryst. (1994). C50, 1026-1028    [doi:10.1107/S0108270193013083]

Tetrakis[{₃-ethoxy(N-methylimino)methanethiolato}copper(I)]

T. Kuroda-Sowa, M. Munakata, M. Miyazaki and M. Maekawa

Acta Cryst. (1994). C50, 1028-1031    [doi:10.1107/S0108270193011989]

[{PtCl(dmso)}₂(-OH)₂]

Z. Bugarcic, K. Lövqvist and Å. Oskarsson

Acta Cryst. (1994). C50, 1031-1034    [doi:10.1107/S0108270193012831]

Hexakis(tert-butylammonium) heptamolybdate(VI)-water (1/7)

P. Román, A. San José, A. Luque and J. M. Gutiérrez-Zorrilla

Acta Cryst. (1994). C50, 1034-1037    [doi:10.1107/S0108270193012363]

2,2'-Bipyrimidine (bpm)-bridged dinuclear complexes. 3. Structure of -(2,2'-bipyrimidine-N¹,N^1':N³,N^3')bis(tetraaquazinc) disulfate dihydrate, [Zn₂(-bpm)(H₂O)₈\](SO₄)₂.2H₂O

G. De Munno and M. Julve

Acta Cryst. (1994). C50, 1037-1040    [doi:10.1107/S0108270193011151]

Yttrium(III) and lanthanum(III) complexes of a 15-membered macrocycle with three pendant carboxymethyl groups

M. B. Inoue, M. Inoue and Q. Fernando

Acta Cryst. (1994). C50, 1040-1042    [doi:10.1107/S0108270193012648]

(Bipyridyl-N,N')diiodoplatinum(II)

W. B. Connick and H. B. Gray

Acta Cryst. (1994). C50, 1043-1044    [doi:10.1107/S0108270193013757]

N,N'-Ethylenebis(4,6-dimethoxysalicylideneiminato)copper(II) monohydrate

E. Labisbal, J. Romero, J. A. García-Vázquez, A. Sousa, E. E. Castellano and J. Zukerman-Schpector

Acta Cryst. (1994). C50, 1044-1046    [doi:10.1107/S0108270193013915]

Potassium (5-nitro-1,10-phenanthroline-N¹,N¹⁰)oxodiperoxovanadate(V) dihydrate: an insulin-mimetic peroxovanadate

A. Shaver, J. B. Ng, R. C. Hynes and B. I. Posner

Acta Cryst. (1994). C50, 1046-1049    [doi:10.1107/S0108270193011825]

Tetrakis[m-(trifluoromethyl)phenyl]tin(IV)

F. E. Smith, R. C. Hynes, Y. Z. Zhang, G. Eng and L. E. Khoo

Acta Cryst. (1994). C50, 1049-1052    [doi:10.1107/S0108270194000089]

Oxobis(N-oxopyridine-2-thiolato-N,O)vanadium(IV)

F. J. Higes-Rolando, A. Perez-Florindo, C. Valenzuela-Calahorro, J. D. Martin-Ramos and J. Romero-Garzon

Acta Cryst. (1994). C50, 1052-1054    [doi:10.1107/S0108270194000363]

Octadecacarbonylhexaosmium chloroform solvate

A. J. Blake, B. F. G. Johnson and J. G. M. Nairn

Acta Cryst. (1994). C50, 1054-1057    [doi:10.1107/S0108270193013897]

Sodium cyclododecyl sulfate trihydrate, Na⁺.C₁₂H₂₃O₄S^-.3H₂O

R. Rudert, D. Vollhardt and G. Czichocki

Acta Cryst. (1994). C50, 1057-1059    [doi:10.1107/S0108270193013216]

A palladium-dithiooxamide complex

M. Abboudi and A. Mosset

Acta Cryst. (1994). C50, 1059-1062    [doi:10.1107/S0108270193014088]

(Benzenethiolato-S)triphenyltin(IV), [Sn(C₆H₅S)(C₆H₅)₃] (I), and bis(benzenethiolato-S)diphenyltin(IV), [Sn(C₆H₅S)₂(C₆H₅)₂] (II)

N. Speziali, B. G. Guimarães, R. M. Silva, P. H. Duarte and S. R. Aguiar

Acta Cryst. (1994). C50, 1062-1064    [doi:10.1107/S0108270193013629]

[2,6-Bis(2-pyrimidinylthiomethyl)pyridine]dichlorocopper(II) methanol solvate

R. Sillanpää, R. Kivekäs, L. Escriche, J. Casabó and G. Sánchez-Castelló

Acta Cryst. (1994). C50, 1064-1065    [doi:10.1107/S0108270194001083]

[RuCl₂(PH₂Cy)(⁶-p-cymene)]

J. F. Van der Maelen Uría, S. García-Granda, J. A. Cabeza and I. del Río

Acta Cryst. (1994). C50, 1066-1069    [doi:10.1107/S0108270193012181]

Dichloro- and dibromo[N-(2-pyridylmethylidene)-2-thienylmethylamine-N,N']copper(II) complexes, [CuCl₂(C₁₁H₁₀N₂S)] and [CuBr₂(C₁₁H₁₀N₂S)]

A. M. Atria, R. F. Baggio, N. Espinosa, M. T. Garland, J. Manzur, Y. Moreno and E. Spodine

Acta Cryst. (1994). C50, 1069-1072    [doi:10.1107/S0108270194001095]

A tri--chloro dirhodium (III) complex [Rh₂(-Cl)₃(triphos)₂](CF₃SO₃)₃ [triphos = CH₃C(CH₂PPh₂)₃]

F. Bachechi

Acta Cryst. (1994). C50, 1072-1074    [doi:10.1107/S0108270194000417]

Monochloroindium derivative of tmtaa (dibenzotetramethyltetraaza[14]annulene), [In(C₂₂H₂₂N₄)Cl]

P. R. Phillips, A. McCamley, N. W. Alcock and M. G. H. Wallbridge

Acta Cryst. (1994). C50, 1074-1076    [doi:10.1107/S0108270193012843]

Hexakis(difluorphenylphosphan)wolfram(0) hydrat, W(PF₂Ph)₆.H₂O

W. Crump, T. Kruck, B. Siegers and K.-F. Tebbe

Acta Cryst. (1994). C50, 1076-1079    [doi:10.1107/S0108270194001010]

Sodium galactarate and potassium galactarate

T. Taga, T. Shimada and N. Mimura

Acta Cryst. (1994). C50, 1079-1084    [doi:10.1107/S0108270193012119]

Two 4-nitropyridine N-oxide adducts: (C₅H₄N₂O₃)₂.AgNO₃ and (C₅H₄N₂O₃)₂.Co(NO₃)₂.4H₂O

M. Bagieu-Beucher, Y. Le Fur, J.-P. Levy and J.-P. Pécaut

Acta Cryst. (1994). C50, 1084-1087    [doi:10.1107/S0108270193014052]

cis-Tetracarbonylbis[tris(p-fluorophenyl)phosphine]molybdenum(0)

E. C. Alyea, G. Ferguson, J. F. Gallagher and S. Song

Acta Cryst. (1994). C50, 1087-1089    [doi:10.1107/S0108270193013149]

(C₂₄H₂₀P)₂[Mo₆Cl₁₄]

M. A. White, M. R. Pressprich and P. Coppens

organic compounds

Acta Cryst. (1994). C50, 1090-1093    [doi:10.1107/S0108270193014064]

Photoisomerization of tetraethyl 6,8,15,17-tetrahydro-7H,16H-5,18[1',2']-benzeno-9,14-ethenodibenzo[a,h]cyclotetradecene-7,7,16,16-tetracarboxylate. Structure of tetraethyl 2,3,3a,7b,9,10,10a,14b-hexahydro-1H,8H-3a,7b[1',2']-benzeno-10a,14b-ethenodibenzo[a,e]dicyclopenta[c,g]cyclooctene-2,2,9,9-tetracarboxylate as its methylene chloride solvate

D. H. Hua, B. Dantoing, P. D. Robinson, T.-C. Qui and C. Y. Meyers

Acta Cryst. (1994). C50, 1093-1095    [doi:10.1107/S0108270193014532]

(R)-(+)-2-Phenylpropyl p-toluenesulfonate, C₁₆H₁₈O₃S

H. Gallardo, A. A. Merlo, I. Vencato and Y. P. Mascarenhas

Acta Cryst. (1994). C50, 1095-1097    [doi:10.1107/S0108270193012387]

Methyl N,N-diallyl-O-tert-butyltyrosyl--aminoisobutyryl--aminoisobutyrate, C₂₈H₄₃N₃O₅

J. L. Flippen-Anderson, C. George and J. R. Deschamps

Acta Cryst. (1994). C50, 1097-1099    [doi:10.1107/S010827019400017X]

Nitrilotriacetic acid, C₆H₉NO₆

E. Skrzypczak-Jankun, D. A. Smith and H. Maluszynska

Acta Cryst. (1994). C50, 1099-1101    [doi:10.1107/S010827019300770X]

Bis(5-acetylamino-1,3,4-thiadiazole-2-sulfon)amide dihydrate

M. Vinkovic, S. Mutak, A. Nagl and B. Kamenar

Acta Cryst. (1994). C50, 1101-1104    [doi:10.1107/S0108270194001009]

2-Nitrobiphenyl and 2,2'-dinitrobiphenyl

A. Sekine, Y. Ohashi, K. Yoshimura, M. Yagi and J. Higuchi

Acta Cryst. (1994). C50, 1104-1106    [doi:10.1107/S0108270193013770]

Ein gesättigter anorganischer Phosphor(V) Hydrazin-Schwefel(IV)-Sechsring mit Twist-Boot-Konformation

U. Engelhardt, B. Stromburg und A. Simon

Acta Cryst. (1994). C50, 1106-1108    [doi:10.1107/S0108270193011084]

4,4'-Isopropylidenediphenyl bis(chloroformate)

G. L. Bryant Jnr and J. A. King Jnr

Acta Cryst. (1994). C50, 1108-1112    [doi:10.1107/S010827019400082X]

2,2',3,3'-Tetra-O-acetyl-4,4',6,6'-tetradeoxy-,-xylo-trehalose

A. Linden and C.-K. Lee

Acta Cryst. (1994). C50, 1112-1114    [doi:10.1107/S0108270194000612]

Octabutyltetrasila[2.2]terthiophenophane

J. K. Herrema, J. Wildeman, F. van Bolhuis and G. Hadziioannou

Acta Cryst. (1994). C50, 1114-1117    [doi:10.1107/S0108270193009291]

Structure of charge-transfer complexes. 3. 2,4,5,7-Tetranitro-9-fluorenone-2-ethylnaphthalene (1/1)

M. C. Shah and R. G. Baughman

Acta Cryst. (1994). C50, 1117-1118    [doi:10.1107/S0108270193012867]

A 2,5-diketomorpholine

M. Bolte and E. Egert

Acta Cryst. (1994). C50, 1118-1122    [doi:10.1107/S010827019301323X]

Four N-saccharinaliphatic acids

N. Feeder and W. Jones

Acta Cryst. (1994). C50, 1122-1124    [doi:10.1107/S0108270193013903]

[1R,2R,5(1')S,9R,2'R,4'R,5'S]-2,10,10-Triméthyl-3-oxa-6-azatricyclo[7,1,1,0^2,7]undeca-5-spiro[1'(2',4',5'-triméthylcyclohexane)]-6-ène-4-one

A. Chiaroni, C. Riche, J.-P. Lavergne, M. Sadoune, P. Viallefont et Y. Vidal

Acta Cryst. (1994). C50, 1124-1126    [doi:10.1107/S0108270193013666]

1-(2,4-Dimethoxy-1,3,5-triazin-6-yloxy)pyrrolidine-2,5-dione, C₉H₁₀N₄O₅

M. L. Glówka and A. W. Sobanska

Acta Cryst. (1994). C50, 1126-1130    [doi:10.1107/S0108270193011576]

Geneserine hydrochloride

A. Bacchi, G. Pelizzi, E. Redenti, M. Delcanale, G. Amari and P. Ventura

Acta Cryst. (1994). C50, 1130-1132    [doi:10.1107/S0108270193013289]

Hydrogen-bonded trimers of methyl 4-trifluoromethylpyrazole-3-carboxylate solvated by chloroform

B. Beagley, K. J. Farnworth, E. T. Moss, R. G. Pritchard, S. Tajammal and A. E. Tipping

Acta Cryst. (1994). C50, 1132-1135    [doi:10.1107/S0108270193013642]

p-Hydroxyephedrinium dihydrogenphosphate

M. Datta, A. Podder and J. K. Dattagupta

Acta Cryst. (1994). C50, 1135-1138    [doi:10.1107/S0108270193011862]

N-(N-Benzyloxycarbonyl-L-1,2,3,4-tetrahydroisoquinol-3-ylcarbonyl)-L-phenylalanine methyl ester, Z-L-Tic-L-Phe-OMe

L. Vitagliano, A. Zagart, S. Capasso, S. Salvadori and G. Baldoni

Acta Cryst. (1994). C50, 1139-1141    [doi:10.1107/S0108270193011199]

1:2 complexes of (thio)morpholinium derivatives and the electron acceptor 7,7,8,8-tetracyano-p-quinodimethane. VII. Triclinic form of N,N-dimethylmorpholinium di-7,7,8,8-tetracyano-p-quinodimethanide, DMM(TCNQ)₂ (II), at 294 K

R. J. J. Visser, J. L. de Boer and A. Vos

Acta Cryst. (1994). C50, 1141-1143    [doi:10.1107/S0108270193012065]

Indan-2,2-dicarboxylic acid, C₁₁H₁₀O₄

J. G. Garcia, J. D. Enas and F. R. Fronczek

Acta Cryst. (1994). C50, 1143-1145    [doi:10.1107/S0108270193012089]

A chromotropic bi(benzofuranonyl)

Y. Mori, I. Kubota, Y. Watanabe and K. Maeda

Acta Cryst. (1994). C50, 1145-1148    [doi:10.1107/S0108270193012478]

threo-3-Fluoro-2-hydroxy-1,3-diphenyl-1-propanone and (1RS,2RS,3RS)-3-fluoro-1,3-diphenyl-1,2-propanediol

R. Stomberg, S. Li and K. Lundquist

Acta Cryst. (1994). C50, 1148-1149    [doi:10.1107/S010827019400096X]

Ammonium salt of nitroacetamide

O. Simonsen and P. N. Jørgensen

Acta Cryst. (1994). C50, 1150-1152    [doi:10.1107/S0108270193013022]

A mesoionic pyridazinium sulfonate; an unexpected reaction product

O. Simonsen, E. Fanghänel, B. B. Iversen and F. K. Larsen

Acta Cryst. (1994). C50, 1152-1154    [doi:10.1107/S0108270193012752]

3,5-Difluorophenol

M. Shibakami and A. Sekiya

Acta Cryst. (1994). C50, 1154-1156    [doi:10.1107/S0108270193011503]

Three tetramethylketals of 2,5-distyryl-[1,4]benzoquinones

H. Irngartinger and J. Lichtenthäler

Acta Cryst. (1994). C50, 1156-1159    [doi:10.1107/S0108270193012697]

A spiro-indole derivative, C₁₆H₁₀ClFN₂O₂S

V. Sehgal, P. Singh, A. Dandia and R. Bohra

Acta Cryst. (1994). C50, 1159-1161    [doi:10.1107/S0108270193013150]

1-Acetyl-5-benzyl-2-methylthio-5H-imidazol-4-one

M. F. Mackay, G. J. Trantino, B. M. Duggan and J. F. K. Wilshire

Acta Cryst. (1994). C50, 1161-1163    [doi:10.1107/S0108270193012272]

Guanidinium nitrate

A. Katrusiak and M. Szafranski

Acta Cryst. (1994). C50, 1163-1165    [doi:10.1107/S0108270193013393]

N,N'-Bis(2-hydroxypropyl)dithiooxamide

Y. C. Jean

Acta Cryst. (1994). C50, 1165-1169    [doi:10.1107/S0108270193013721]

Methyl (2-methoxycarbonylbenzoyl)triphenylphosphoranylideneacetate and its ethanolate complex

F. D. Rochon, R. Melanson and M. M. Kayser

Acta Cryst. (1994). C50, 1169-1171    [doi:10.1107/S010827019301368X]

2,2'-Azinodimethyldiphenol, C₁₄H₁₂N₂O₂

X.-X. Xu, X.-Z. You, Z.-F. Sun, X. Wang and H.-X. Liu

Acta Cryst. (1994). C50, 1171-1173    [doi:10.1107/S0108270193012120]

3,4-Diméthoxycarbonyl-5-éthoxycarbonyl-1-(2,2,2-trichloro-1-éthoxycarbonylaminoéthyl)pyrazole, C₁₅H₁₈Cl₃N₃O₈

N. Rodier, A. Belaissaoui, C. Morpain et B. Laude

Acta Cryst. (1994). C50, 1173-1176    [doi:10.1107/S0108270193012132]

Bis[2-(3-morpholinobenzofuranyl)]phénylméthane, C₃₁H₃₀N₂O₄

N. Rodier, M. M'Saddek, M. Rammah et K. Ciamala

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