Acta Crystallographica Section C

Crystal Structure Communications

Volume 50, Part 8 (August 1994)

Cover illustration: Spiro[3-germabicyclo[3.1.0]hexane-3,9'-[9]germafluorene], see Ogawa, Takeuchi, Manuel & Boukherroub, pages 1337-1339.

• inorganic compounds
• metal-organic compounds
• organic compounds
• addenda and errata

inorganic compounds

Acta Cryst. (1994). C50, 1177-1178    [doi:10.1107/S0108270193010996]

NbSb₂

A. Rehr and S. M. Kauzlarich

Acta Cryst. (1994). C50, 1178-1180    [doi:10.1107/S010827019400466X]

Cu₃Bi₄V₂O₁₄, a new compound

G. B. Deacon, B. M. Gatehouse and G. N. Ward

Acta Cryst. (1994). C50, 1180-1183    [doi:10.1107/S0108270193013630]

Li₃BS₃

P. Vinatier, P. Gravereau, M. Ménétrier, L. Trut and A. Levasseur

Acta Cryst. (1994). C50, 1183-1185    [doi:10.1107/S0108270194000624]

Redetermination of the structure of LaMo₅O₈ by single-crystal X-ray diffraction

P. Gall and P. Gougeon

Acta Cryst. (1994). C50, 1185-1188    [doi:10.1107/S0108270194002027]

A short dynamically symmetrical hydrogen bond in the structure of K[Mg(H_0.5SO₄)₂(H₂O)₂]

J. Macícek, S. Gradinarov, R. Bontchev and C. Balarew

metal-organic compounds

Acta Cryst. (1994). C50, 1189-1191    [doi:10.1107/S0108270193014519]

Bis(tert-butylammonium) molybdate(VI)

P. Román, A. San José, A. Luque, J. M. Gutiérrez-Zorrilla and M. Martínez-Ripoll

Acta Cryst. (1994). C50, 1191-1193    [doi:10.1107/S0108270193013678]

A pyridine-2-thiolato molybdenum complex

P. Yu, L. Huang and B. Zhuang

Acta Cryst. (1994). C50, 1193-1196    [doi:10.1107/S0108270194000272]

A pseudo-octahedral tungsten oxo compound, [WO(C₁₈H₁₂O)(C₁₃H₁₃P)₃].C₇H₈

J. L. Kerschner, C. E. Kriley, P. E. Fanwick and I. P. Rothwell

Acta Cryst. (1994). C50, 1196-1199    [doi:10.1107/S010827019301159X]

Tris(4,6-dimethylpyrimidine-2-thiolato-N,S)cobalt(III) monohydrate: a complex with three stable four-membered N,S-chelate rings

S. Seth

Acta Cryst. (1994). C50, 1199-1201    [doi:10.1107/S0108270193014192]

Ferrocenyltriphenylsilane

R. T. Palmer, L. J. Radonovich and F. B. McCormick

Acta Cryst. (1994). C50, 1201-1203    [doi:10.1107/S0108270194003057]

Isothiocyanatobis(1,10-phenanthroline)copper(II) perchlorate, [Cu(NCS)(phen)₂]ClO₄

O. J. Parker, J. L. Manson and G. L. Breneman

Acta Cryst. (1994). C50, 1204-1207    [doi:10.1107/S0108270194002209]

A mononuclear oxovanadium(IV) complex [VO(H₂L)(SO₄)].5H₂O derived from a potentially dinucleating tetraaminodiphenol macrocyclic ligand (H₂L)

S. Ghosh, M. Mukherjee, A. K. Mukherjee, S. Mohanta and M. Helliwell

Acta Cryst. (1994). C50, 1207-1209    [doi:10.1107/S0108270194003781]

Bis(o-methoxyphenyl)tin dibromide

J.-N. Ross, J. Wardell, G. Ferguson and J. N. Low

Acta Cryst. (1994). C50, 1209-1211    [doi:10.1107/S0108270194004257]

Chlorobis{2-[(dimethylamino)methyl]phenyl-C¹,N}(pyridine)vanadium(III)

A. L. Spek, J. J. H. Edema and S. Gambarotta

Acta Cryst. (1994). C50, 1211-1212    [doi:10.1107/S0108270194000600]

1,3,5,7-Tetraazabicyclo[3.3.1]nonane-3,7-bis(acetato)-N³,N⁷,O,O''}nickel(II)

Z. Trávnícek and J. Marek

Acta Cryst. (1994). C50, 1212-1214    [doi:10.1107/S0108270194001551]

Bis(tetrapropylammonium) hexachlorodicuprate(II)

G. Hu and E. M. Holt

Acta Cryst. (1994). C50, 1214-1217    [doi:10.1107/S0108270194001757]

cis-Ammine(benzoylhydrazine-N)dichloroplatinum(II)

J. Macícek, N. Dodoff and N. Spassovska

Acta Cryst. (1994). C50, 1217-1220    [doi:10.1107/S010827019301073X]

Platinum(II) triamine complexes: cis-[PtCl(NH₃)₂(C₁₀H₁₃N₅O₅)]NO₃.2H₂O and [PtCl(C₂H₈N₂)(C₄H₆N₂)\]NO₃

G. M. Arvanitis, D. Gibson, T. J. Emge and H. M. Berman

Acta Cryst. (1994). C50, 1221-1222    [doi:10.1107/S0108270193014222]

Bis(3-bromoimidazolium) tetrachloropalladate(II)

G. Valle and R. Ettorre

Acta Cryst. (1994). C50, 1222-1225    [doi:10.1107/S0108270194002520]

Triethylammonium hydrogen dichlorotris(diphenylphosphinito-P)rhodium(III) tetrahydrofuran (1/1)

D. J. Irvine, D. J. Cole-Hamilton, J. C. Barnes and R. A. Howie

Acta Cryst. (1994). C50, 1225-1227    [doi:10.1107/S010827019301426X]

cis-Bis[3-sulfido-1,3-bis(2-thienyl)prop-2-enone-O,S]palladium(II)

L. A. M. Baxter, A. J. Blake, F. J. J. Dijksma, R. O. Gould and G. A. Heath

Acta Cryst. (1994). C50, 1227-1231    [doi:10.1107/S0108270194000454]

Dichloro(1-trimethylsilyl-1,5-cyclooctadiene)palladium(II)

N. S. Begum, B. S. Bandodakar and G. Nagendrappa

Acta Cryst. (1994). C50, 1231-1233    [doi:10.1107/S0108270194003495]

Cyclopentadienyl(thioacetamide-S)bis(triphenylphosphine-P)ruthenium(II) tetrafluoroborate

C. D. Bryan, A. W. Cordes and M. Draganjac

Acta Cryst. (1994). C50, 1233-1235    [doi:10.1107/S0108270194000855]

A redetermination of the X-ray structure of the hexanuclear mixed-metal cluster [Ru₅Rh(₆-C)(CO)₁₃(-CO)(⁵-C₁₀H₁₅)]

T. Adatia, M. McPartlin, J. Morris, H. Curtis and J. Lewis

Acta Cryst. (1994). C50, 1236-1239    [doi:10.1107/S0108270193012995]

Silver 2-pyrimidinolate dihydrate, [Ag(C₄H₃N₂O)].2H₂O: a case of pseudosymmetry

M. Quirós

Acta Cryst. (1994). C50, 1239-1241    [doi:10.1107/S0108270194000107]

Bis(dimethylglyoximato-N,N')(ethyl)(triphenylphosphine)rhodium(III)

V. Kettmann, M. Dunaj-Jurco, D. Steinborn and M. Ludwig

Acta Cryst. (1994). C50, 1242-1244    [doi:10.1107/S0108270194000570]

[Au(ⁿBuPPh₂){(Ph₂PS)₃C}].CH₃CN: an irregular three-coordinate Au_I complex

R. J. Staples, S. Wang, J. P. Fackler Jnr, S. O. Grim and E. de Laubenfels

Acta Cryst. (1994). C50, 1244-1247    [doi:10.1107/S0108270193012053]

Co-crystallized bis(-tert-butylphosphido)bis(di-tert-butylgallium) and tetra-tert-butylcyclotetraphosphane

K. Kirschbaum and D. M. Giolando

Acta Cryst. (1994). C50, 1247-1249    [doi:10.1107/S010827019400226X]

The 18-crown-6 potassium salt of a Meissenheimer anion, [K(C₇H₃Cl₃N₃O₆)(C₁₂H₂₄O₆)]

J. C. Barnes, J. Main and J. D. Paton

Acta Cryst. (1994). C50, 1249-1252    [doi:10.1107/S0108270194000466]

(Nitrato-O)(triphenylphosphine-P){3,6,9-trithiabicyclo[9.4.0]pentadeca-1(11),12,14-triene-³S^3,6,9}mercury(II) nitrate hydrate hemiethanol solvate

R. Kivekäs, R. Sillanpää, L. Escriche, M. P. Almajano, F. Teixidor and J. Casabó

Acta Cryst. (1994). C50, 1252-1254    [doi:10.1107/S010827019301412X]

Benzyl(bromo)diphenyllead

U. Fahrenkampf, M. Schürmann and F. Huber

Acta Cryst. (1994). C50, 1254-1256    [doi:10.1107/S0108270194002532]

A hydrate of the sodium salt of a penem carboxylic acid

Y. Oyama, S. Imajo, R. Tanaka and M. Ishiguro

Acta Cryst. (1994). C50, 1256-1258    [doi:10.1107/S0108270194003409]

Di--chloro-bis[dichlorotris(2-propanol)cerium(III)] at 153 K

M. Schäfer, R. Herbst-Irmer, U. Groth and T. Köhler

organic compounds

Acta Cryst. (1994). C50, 1259-1262    [doi:10.1107/S0108270193012259]

3,5-Dimethoxybenzoic acid and the second polymorph of the 2:1 adduct of 3,5-dinitrobenzoic acid with ethylenediamine

D. E. Lynch, G. Smith, K. A. Byriel and C. H. L. Kennard

Acta Cryst. (1994). C50, 1262-1265    [doi:10.1107/S0108270193013381]

2',3'-Didehydro-2',3'-dideoxy-5-hydroxymethyluridine

U. Pugazhenthi, L. T. J. Delbaere, S. V. P. Kumar, A. L. Stuart and S. V. Gupta

Acta Cryst. (1994). C50, 1265-1267    [doi:10.1107/S0108270193012466]

Thiamin acetate, C₁₂H₁₇N₄OS⁺.C₂H₃O₂^-

J. S. Casas, A. Castiñeiras, M. D. Couce, J. Sordo and J. M. Varela

Acta Cryst. (1994). C50, 1267-1269    [doi:10.1107/S010827019301248X]

2-Thymin-1-ylethyl ester of N-tert-butoxycarbonyl-L-tryptophan, C₂₃H₂₈N₄O₆

K. Fukuyama and M. Irie-Fujii

Acta Cryst. (1994). C50, 1269-1271    [doi:10.1107/S0108270193013861]

An isocoumarin derivative from Paepalanthus bromelioides

K. Tomita and W. Vilegas

Acta Cryst. (1994). C50, 1271-1273    [doi:10.1107/S0108270193014131]

2(RS)-r-2-[(RS)-1-(4-Chlorobenzoyloxy)ethyl]-2-ethyl-1,3-dioxolan-c-4-ylmethyl-4-chlorobenzoate

U. Berens and G. Raabe

Acta Cryst. (1994). C50, 1274-1276    [doi:10.1107/S0108270193012740]

(±)-8-Phenyldinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepine

K. Tani, T. Yamagata and K. Nagata

Acta Cryst. (1994). C50, 1276-1279    [doi:10.1107/S0108270193012491]

Tris(2,6-dimethoxyphenyl)phosphine sulfide monohydrate

S. Hayase, T. Erabi and M. Wada

Acta Cryst. (1994). C50, 1279-1281    [doi:10.1107/S0108270194000120]

A dimeric (phenylsulfonyl)oxazolidine

J. Hirschler, B. Berger and M. Bolte

Acta Cryst. (1994). C50, 1281-1282    [doi:10.1107/S0108270194000818]

A -hydroxyvinylsulfoximine, C₂₃H₃₁NO₃S

B. Berger and M. Bolte

Acta Cryst. (1994). C50, 1283-1284    [doi:10.1107/S0108270193013733]

N-Chlorosulfonyl-L-proline benzyl ester

A. J. Ibbett, D. J. Watkin and J. H. Jones

Acta Cryst. (1994). C50, 1284-1286    [doi:10.1107/S0108270193013617]

2,6-Bis(p-nitrophenylthiomethyl)pyridine

R. Sillanpää, R. Kivekäs, L. Escriche, G. Sánchez-Castelló and F. Teixidor

Acta Cryst. (1994). C50, 1286-1288    [doi:10.1107/S0108270193010728]

2-(o-Methoxyphenoxy)-1-methylbenzimidazole, C₁₅H₁₄N₂O₂

K. T. Vasudevan, Puttaraja and M. V. Kulkarni

Acta Cryst. (1994). C50, 1289-1291    [doi:10.1107/S0108270193013253]

1:1 Molecular complex of trimethoprim and sulfametrole

G. Giuseppetti, C. Tadini and G. P. Bettinetti

Acta Cryst. (1994). C50, 1291-1294    [doi:10.1107/S0108270193012260]

Molecular co-crystals of carboxylic acids. 16. 1:1 Adduct of 3-nitrobenzoic acid with 3-amino-1H-1,2,4-triazole

D. E. Lynch, G. Smith, K. A. Byriel and C. H. L. Kennard

Acta Cryst. (1994). C50, 1294-1295    [doi:10.1107/S0108270193014477]

2-(3-Benzyloxy-4-nitrophenyl)oxirane, an intermediate in the synthesis of formoterol

K. Chandra Mohan, K. Ravikumar, T. V. S. K. Vittal and C. K. Gido

Acta Cryst. (1994). C50, 1296-1299    [doi:10.1107/S0108270193012077]

Monohydrates of two isomers of aminotoluenesulfonic acid

A. J. Shubnell and P. J. Squattrito

Acta Cryst. (1994). C50, 1299-1301    [doi:10.1107/S0108270194000673]

An m-carboranedicarboxylic acid dianilide

S. V. Lindeman, G. A. Kats and L. G. Komarova

Acta Cryst. (1994). C50, 1301-1303    [doi:10.1107/S010827019400140X]

Bis(triphenylphosphine)iminium hexafluorophosphate dichloromethane solvate (1/1)

A. J. Blake, G. Freeman, B. F. G. Johnson and G. S. McDougall

Acta Cryst. (1994). C50, 1303-1305    [doi:10.1107/S0108270193012636]

1,7,9-Trimethyl-2,6-purinedione monohydrate, C₈H₁₀N₄O₂.H₂O

M. Parvez and G. Ferguson

Acta Cryst. (1994). C50, 1305-1308    [doi:10.1107/S0108270193012582]

Fluorinated barbituric acid derivatives

D. D. DesMarteau, W. T. Pennington and G. Resnati

Acta Cryst. (1994). C50, 1308-1312    [doi:10.1107/S0108270193012235]

Substituted diphenyl oxalates

C. George, P. M. Lahti, D. A. Modarelli and A. Inceli

Acta Cryst. (1994). C50, 1312-1314    [doi:10.1107/S0108270194000594]

3-[5-(3-Nitrophenyl)furfurylidene]-2,4-pentanedione, C₁₆H₁₃NO₅

J. Lokaj, V. Vrábel, J. Sivý, D. Ilavský and A. Korenová

Acta Cryst. (1994). C50, 1314-1318    [doi:10.1107/S0108270194001423]

Synthèses et structures de deux acides 5,6-dihydro-6-[aryl]-4-{2-[aryl]-éthényl}-2-oxo-2H-pyrane-3-carboxylique

A. Valla, M. Giraud et D. Ginderow

Acta Cryst. (1994). C50, 1318-1320    [doi:10.1107/S0108270194001435]

2-Acetyl-1,8-dihydroxy-3,6-dimethylnaphthalene

G. Müller, M. Lutz and J. Lachmann

Acta Cryst. (1994). C50, 1320-1323    [doi:10.1107/S0108270194000958]

5,11,17,23-Tetra-tert-butyl-25,26,27,28-[(5-methylfurfuryl)oxycarbonylmethoxy]calix[4]arene

G. Ferguson, Y. Li, M. A. McKervey and E. Madigan

Acta Cryst. (1994). C50, 1323-1326    [doi:10.1107/S0108270194001617]

Structure of a triazaoxatricyclodecadiene derivative. Partial disorder and a packing energy study

G. Gelli, E. Cadoni, M. Pani, M. M. Carnasciali, A. Mugnoli and P. Beltrame

Acta Cryst. (1994). C50, 1326-1328    [doi:10.1107/S0108270193013228]

Roburic acid, a triterpene 3,4-seco acid

T.-T. Jong and C.-T. Chen

Acta Cryst. (1994). C50, 1328-1329    [doi:10.1107/S0108270194003793]

6-Amino-5-hydroxyiminomethyl-1,3-dimethyluracil

J. N. Low, G. Ferguson, M. N. Moreno-Carretero and F. Hueso-Ureña

Acta Cryst. (1994). C50, 1329-1333    [doi:10.1107/S0108270194000946]

4-Amino-2-methylthio-6-oxo-1,6-dihydropyrimidine and its 1-methyl derivative and 4-amino-2-methoxy-1-methyl-6-oxo-1,6-dihydropyrimidine and its 5-nitroso derivative

J. N. Low, S. N. Scrimgeour, C. Egglishaw, R. A. Howie, M. N. Moreno-Carretero and F. Hueso-Ureña

Acta Cryst. (1994). C50, 1333-1335    [doi:10.1107/S0108270194001952]

Acetamide hydrochloride

L.-K. Liu, F.-T. Luo and L.-C. Hsieh

Acta Cryst. (1994). C50, 1335-1337    [doi:10.1107/S0108270194001071]

2,3,4,5,6-Penta-O-acetyl-D-galactonic acid 1'-phenyl-2'-ethoxycarbonylvinyl ester

J. Kopf, D. Abeln, P. Köll, R. Meisel and K. Peseke

Acta Cryst. (1994). C50, 1337-1339    [doi:10.1107/S010827019400291X]

Spiro[3-germabicyclo[3.1.0]hexane-3,9'-[9]germafluorene]

K. Ogawa, Y. Takeuchi, G. Manuel and R. Boukherroub

Acta Cryst. (1994). C50, 1339-1342    [doi:10.1107/S0108270193013265]

1-(3-Benzoylphenyl)ethanone (I) and 3-benzoyl--methylbenzeneacetamide methylene chloride solvate (2/1) (II)

D. Matak, M. Vinkovic and M. Dumic

Acta Cryst. (1994). C50, 1343-1345    [doi:10.1107/S0108270194001575]

1-Tosyl-1H-pyrrolo[2,3-c]pyridine-5-carboxylic acid ethyl ester

A. Chiaroni, C. Riche, M. Dekhane and R. H. Dodd

Acta Cryst. (1994). C50, 1345-1347    [doi:10.1107/S0108270194001538]

Product of a Paterno-Büchi reaction of pentafluorobenzaldehyde and 4-tert-butyl-1-acetoxycyclohexene

C. P. Brock, M. A. Lloyd, S. Vasudevan, D. S. Watt and H. Morita

Acta Cryst. (1994). C50, 1347-1349    [doi:10.1107/S0108270194002040]

Two N-saccharin peracids

N. Feeder and W. Jones

Acta Cryst. (1994). C50, 1350-1352    [doi:10.1107/S0108270194002337]

2-(4-Cyanobenzoylaminomethyl)-1-methyl-5-(3-thienyl)-2,3-dihydro-1H-1,4-benzodiazepin-4-ium p-toluenesulfonate

O. M. Peeters, N. M. Blaton, R. L. Meurisse and C. J. De Ranter

Acta Cryst. (1994). C50, 1352-1354    [doi:10.1107/S0108270194002349]

5-(2,4-Dichlorophenyl)-2-[(3-furoyl)aminomethyl]-8-methoxy-1-methyl-2,3-dihydro-1H-1,4-benzodiazepin-4-ium p-toluenesulfonate

O. M. Peeters, N. M. Blaton, R. L. Meurisse and C. J. De Ranter

Acta Cryst. (1994). C50, 1354-1357    [doi:10.1107/S0108270194001940]

4-Hydroxyacetophenone oxime (I) and 4-hydroxy-3-methylacetophenone oxime (II)

J. K. Maurin

Acta Cryst. (1994). C50, 1357-1359    [doi:10.1107/S0108270194001113]

2'-Hydroxypropiophenone oxime

J. K. Maurin

Acta Cryst. (1994). C50, 1359-1362    [doi:10.1107/S0108270193012703]

(1S,2S,5R,6S)-(+)-6-Carbanilino-1,5-dimethyltricyclo[3.2.0.0^2,6]heptane

T.-T. Jong, M. Y. Jean and T. J. Lu

Acta Cryst. (1994). C50, 1362-1366    [doi:10.1107/S0108270194004439]

Molecules isoelectronic with 2,2,2-triphenylethanol: multiple hydrogen-bonding modes in the structures of O-tritylhydroxylamine, Ph₃CONH₂, and triphenylmethanesulfenamide, Ph₃CSNH₂

C. Glidewell and G. Ferguson

Acta Cryst. (1994). C50, 1366-1368    [doi:10.1107/S0108270194001824]

(2S,3R,4S,5R,6S,7R,8R,9S)-1,2,3,4,5,6,7,8,9-Nonaacetoxydecane

K. Lewinski, J. A. Marshall and S. Beaudoin

Acta Cryst. (1994). C50, 1368-1370    [doi:10.1107/S0108270193014507]

Refinement of a twinned structure with SHELXL93: meso-2,2'-[1,6-bis(methylamino)-3,4-dithia-1,6-hexanediyl]diphenol

M. Bolte

Acta Cryst. (1994). C50, 1370-1372    [doi:10.1107/S0108270194002799]

Configuration of (E)-2-(1-hydroxy-1-methyl-2-oxopropyl)-2-(methylthio)thiolane S-oxide

J.-S. Brunck, J. Voss, H. Viebrock and F. Olbrich

addenda and errata

Acta Cryst. (1994). C50, 1372    [doi:10.1107/S0108270194099798]

The structures of alkalides and electrides. II. Structure of caesium bis(15-crown-5) electride. Erratum

D. L. Ward, R. H. Huang, M. E. Kuchenmeister and J. L. Dye

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