Acta Crystallographica Section C

Crystal Structure Communications

Volume 51, Part 2 (February 1995)


Cover illustrationCover illustration: 2'-carbamate taxol, see Gao & Golik, pages 295--298. The displacement ellipsoids are shown at the 50% probability level.

inorganic compounds



Acta Cryst. (1995). C51, 175-177    [ doi:10.1107/S0108270194003203 ]

Hydroxylammonium Scandium Sulfate Sesquihydrate, Sc(NH3OH)(SO4)2.1.5H2O

A. Mirceva and L. Golic

Synopsis: The structure consists of chains of octahedrally and tetrahedrally arranged O atoms around Sc and S atoms, respectively. These chains are hydrogen bonded by the hydroxylammonium ions and the water molecules.

Formula: Sc(NH3OH)(SO4)2.1.5H2O



Acta Cryst. (1995). C51, 177-179    [ doi:10.1107/S0108270194009030 ]

FeAl3Si2

C. Gueneau, C. Servant, F. d'Yvoire and N. Rodier

Synopsis: FeAl3Si2 is isotypic with PdGa5, but presents a superstructure (space group Pbcn). The structure may be described by the idealized formula FeAl(1)Al(2)2Si2, in which Fe and Al(1) are tenfold and Al(2) and Si are ninefold coordinated.

Formula: FeAl2.7Si2.3



Acta Cryst. (1995). C51, 179-181    [ doi:10.1107/S0108270194010395 ]

KAlAs2O7

H. Boughzala and T. Jouini

Synopsis: KAlAs2O7 is isotypic with RbAlAs2O7. The structure consists of a covalent framework built up from corner-sharing AsO4 tetrahedra and AlO6 octahedra, and containing intersecting tunnels within which the K+ ions are located.

Formula: KAlAs2O7



Acta Cryst. (1995). C51, 181-183    [ doi:10.1107/S0108270194010061 ]

Lithium Berylloarsenate Hydrate, LiBeAsO4.H2O

W. T. A. Harrison, T. E. Gier and G. D. Stucky

Synopsis: LiBeAsO4.H2O is isostructural with other LiABO4.H2O Li-A-type molecular sieves. Geometrical parameters, derived from X-ray powder data, are typical for the ordered, alternating BeO4 and AsO4 groups in this phase.

Formula: LiBeAsO4.H2O



Acta Cryst. (1995). C51, 183-185    [ doi:10.1107/S0108270194010796 ]

Strontium Dibromide Hexahydrate

I. Abrahams and E. Vordemvenne

Synopsis: In SrBr2.6H2O, Sr has tricapped trigonal prismatic coordination geometry involving six bridging and three terminal water molecules, resulting in a linear polymeric cation of general formula [Sr(H2O)6]n2n+ with charges balanced by Br- ions.

Formula: SrBr2.6H2O


metal-organic compounds



Acta Cryst. (1995). C51, 186-188    [ doi:10.1107/S010827019400301X ]

Sodium Chloranilate Trihydrate

R. Benchekroun and J.-M. Savariault

Formula: 2Na+.C6Cl2O42-.3H2O



Acta Cryst. (1995). C51, 188-190    [ doi:10.1107/S0108270194008139 ]

Cs[CB10H13] at 293 K

C. R. Whitaker, A. Romerosa, F. Teixidor and J. Rius

Formula: Cs[CB10H13]



Acta Cryst. (1995). C51, 190-193    [ doi:10.1107/S0108270194006530 ]

Bis(hexadecylpyridinium) Bis(3,6-dichloro-4,5-dihydroxy-3,5-cyclohexadiene-1,2-dionato-[kappa]2O4,O5)beryllium

H. Burzlaff, J. Lange, R. Spengler, M. I. Karayannis and P. G. Veltsistas

Formula: 2C21H38N[Be(C6Cl2O4)2]



Acta Cryst. (1995). C51, 193-195    [ doi:10.1107/S0108270194007079 ]

([eta]5-Cyclopentadienyl)[2-(1,1-diphenylethyl-C2)phenyl-C1]oxo(trimethylsilylmethylthio)tungsten, [WO(C4H11SSi)(C5H5)(C20H16)]

N. Brunet, P. Legzdins, J. Trotter and V. C. Yee

Formula: [WO(C4H11SSi)(C5H5)(C20H16)]



Acta Cryst. (1995). C51, 195-197    [ doi:10.1107/S0108270194008553 ]

(Tetraphenylporphyrinato)zirconium(IV) Diacetate

J. L. Huhmann, J. Y. Corey and N. P. Rath

Formula: [Zr(C2H3O2)2(C44H28N4)].CH2Cl2



Acta Cryst. (1995). C51, 197-198    [ doi:10.1107/S0108270194007535 ]

Tetraphenylphosphonium cis-Tetrabromobis(pyridine)molybdate(III)

J. V. Brencic, B. Modec and Z. Yao

Formula: (C24H20P)[MoBr4(C5H5N)2]



Acta Cryst. (1995). C51, 198-200    [ doi:10.1107/S0108270194007882 ]

2,2-Bis[(diphenylphosphino)methyl]-1-phenyl-thiopropane-P,P',S}tricarbonyltungsten(0)

H.-E. Wang, M.-C. Cheng, S.-M. Peng and S.-T. Liu

Formula: [W(CO)3(C35H34P2S)]



Acta Cryst. (1995). C51, 201-203    [ doi:10.1107/S0108270194007420 ]

[ReCl3(C8H11P)2(C7H11N)2].C6H4Cl2

N. Masciocchi, M. Moret, G. A. Ardizzoia and G. La Monica

Formula: [ReCl3(C8H11P)2(C7H11N)2].C6H4Cl2



Acta Cryst. (1995). C51, 203-205    [ doi:10.1107/S0108270194007651 ]

[3,10-Diethyl-5,8-diazadodecane-3,10-dithiolato-(3-)-N,N',S,S']oxorhenium(IV) Chloroform Solvate

T. W. Hambley, R. K. Knott, T. W. Jackson, M. Kojima and R. M. Lambrecht

Formula: [Re(C14H29N2S2)O].CHCl3



Acta Cryst. (1995). C51, 206-207    [ doi:10.1107/S0108270194009091 ]

trans-[Co(salen)(py)2][BPh4]

X.-H. Shi, X.-Z. You, C. Li, B.-L. Song, T.-H. Li and X.-Y. Huang

Formula: [Co(C16H14N2O2)(C5H5N)2]C24H20B



Acta Cryst. (1995). C51, 208-210    [ doi:10.1107/S0108270194009042 ]

trans-Bromo(o-tolyl)bis(triphenylphosphine)palladium(II) Crystals With and Without Stacking Faults

R. J. Cross, A. R. Kennedy and K. W. Muir

Formula: [PdBr(C7H7)(C18H15P)2]



Acta Cryst. (1995). C51, 210-213    [ doi:10.1107/S010827019400586X ]

Bis(dimethylglyoximato)(phenylacetylido)(triphenylphosphine)rhodium(III) Dichloromethane, [Rh(C4H7N2O2)2(C8H5)(C18H15P)].CH2Cl2

M. Dunaj-Jurco, V. Kettmann, D. Steinborn and M. Ludwig

Formula: [Rh(C4H7N2O2)2(C8H5)(C18H15P)].CH2Cl2



Acta Cryst. (1995). C51, 213-215    [ doi:10.1107/S0108270194006086 ]

L'hydrogénocarbonate de Bis(N,N-diméthylbiguanide) Cuivre(II), [Cu(C4H11N5)2]2HCO3

B. Viossat, A. Tomas et N.-H. Dung

Formula: [Cu(C4H11N5)2]2HCO3



Acta Cryst. (1995). C51, 215-217    [ doi:10.1107/S0108270194008991 ]

(Nitrito-O,O')bis(triphenylphosphine)copper(I), (PPh3)2Cu(NO2-O,O')

J. A. Halfen and W. B. Tolman

Formula: [Cu(NO2)(C18H15P)2]



Acta Cryst. (1995). C51, 217-219    [ doi:10.1107/S010827019400569X ]

Bis(diphenylphosphino)methanetetradecacarbonylhexairidium Dichloromethane Solvate

M. Mazzanti, R. Roulet and K. J. Schenk

Formula: [Ir6(CO)14(C25H22P2)].CH2Cl2



Acta Cryst. (1995). C51, 220-222    [ doi:10.1107/S0108270194008152 ]

Tetraethylammonium Tetramethylammonium Tetrachlorozincate(II), [(C2H5)4N][(CH3)4N]ZnCl4

O. Caëtano, J. Lapasset and P. Saint Grégoire

Formula: [(C2H5)4N][(CH3)4N][ZnCl4]



Acta Cryst. (1995). C51, 222-224    [ doi:10.1107/S0108270194010036 ]

A Zinc(II) Complex of Creatinine

N. Okabe, Y. Kohyama and K. Ikeda

Formula: [ZnCl2(C4H7N3O)2]



Acta Cryst. (1995). C51, 224-226    [ doi:10.1107/S0108270194010048 ]

Dichlorobis(creatinine)cadmium(II)

N. Okabe, K. Ikeda, Y. Kohyama and Y. Sasaki

Formula: [CdCl2(C4H7N3O)2]



Acta Cryst. (1995). C51, 226-229    [ doi:10.1107/S0108270194005147 ]

Anhydrous 2,3,5,6-Tetramethylpyrazinium Tetraiodocadmate(II) and its Trihydrate, [C8H12N2(H)2][CdI4].xH2O (x = 0, 3)

R. D. Bailey and W. T. Pennington

Formula: (C8H14N2)[CdI4] and (C8H14N2)[CdI4].3H2O



Acta Cryst. (1995). C51, 229-232    [ doi:10.1107/S0108270194009492 ]

Two Forms of (5,5-Dimethyl-4,7-diazadecane-1,10-diamine)nickel(II) Diperchlorate

T. H. Tahirov, T.-H. Lu, K. Shu and C.-S. Chung

Formula: Two forms of [Ni(C10H26N4)](ClO4)2



Acta Cryst. (1995). C51, 232-233    [ doi:10.1107/S0108270194010255 ]

trans-Di-[mu]-chloro-bis[chloro(tributylphosphine)palladium]

P. A. Chaloner, S. Z. Dewa and P. B. Hitchcock

Formula: [Pd2Cl4(C12H27P)2]



Acta Cryst. (1995). C51, 234-235    [ doi:10.1107/S0108270194007249 ]

The Polymeric Structure of Aquacadmium Bisnicotinate

W. Clegg, J. T. Cressey, A. McCamley and B. P. Straughan

Formula: [Cd(C6H4NO2)2(H2O)]



Acta Cryst. (1995). C51, 236-238    [ doi:10.1107/S010827019400987X ]

Tris(4-tert-butylphenyl)chlorotin(IV)

I. Wharf, M. G. Simard and K. McGinn

Formula: [Sn(C10H13)3Cl]



Acta Cryst. (1995). C51, 238-242    [ doi:10.1107/S0108270194008887 ]

A Dinitrato(diphenylphenanthroline)palladium(II) Complex

K. W. Törnroos

Formula: [Pd(NO3)2(C24H16N2)].C2H6OS



Acta Cryst. (1995). C51, 242-244    [ doi:10.1107/S0108270194009583 ]

Hexakis(2-chloroethylammonium) Hexachloroplumbate(II) Chloride

M. Geselle and H. Fuess

Formula: 6(C2H7ClN)[PbCl6]2Cl



Acta Cryst. (1995). C51, 244-245    [ doi:10.1107/S0108270194009340 ]

Bis(L-prolinato-N,O)zinc(II)

C.-H. Ng, H.-K. Fun, S.-B. Teo, S.-G. Teoh and K. Chinnakali

Formula: [Zn(C5H7NO2)2]


organic compounds



Acta Cryst. (1995). C51, 246-249    [ doi:10.1107/S0108270194005846 ]

Conformational Study of 1,3,5-Tris(o-methoxyphenyl)-1,3,5-triazacyclohexane and 1,3,5-Tris(p-methoxyphenyl)-1,3,5-triazacyclohexane

D. Adam, P. H. McCabe, G. A. Sim and A. Bouchemma

Formula: Two isomers of C24H27N3O3



Acta Cryst. (1995). C51, 249-251    [ doi:10.1107/S0108270194008061 ]

Non-Sinusoidal Structure of the 1:1 Complex of Phenothiazine and 7,7,8,8-Tetracyanoquinodimethane

L. Toupet and N. Karl

Formula: C12H9NS.C12H4N4



Acta Cryst. (1995). C51, 251-253    [ doi:10.1107/S0108270194008607 ]

cis-6-Methoxycarbonyl-2,10-dioxa-1-phosphabicyclo[4.4.0]decane 1-Oxide

T. M. Lane, O. P. Rodriguez, A. G. Sommese, S. E. Cremer and D. W. Bennett

Formula: C9H15O5P



Acta Cryst. (1995). C51, 253-256    [ doi:10.1107/S010827019400764X ]

(S)-1-Phenylethylammonium (S)-Mandelate-Mandelic Acid (1/2), C8H12N+.C8H7O3-.2C8H8O3

H. Lopez de Diego

Formula: C8H12N+.C8H7O3-.2C8H8O3



Acta Cryst. (1995). C51, 256-260    [ doi:10.1107/S0108270194002957 ]

Three Polychloromononitrobenzenes: C6H3Cl2NO2, C6H2Cl3NO2 and C6HCl4NO2

A. Bhar, J. P. Aune, N. Benali-Cherif, L. Benmenni and M. Giorgi

Formula: C6H3Cl2NO2, C6H2Cl3NO2 and C6HCl4NO2



Acta Cryst. (1995). C51, 260-262    [ doi:10.1107/S010827019400836X ]

1,5-Di-tert-butyl-2,4-dinitrobenzene, C14H20N2O4

M. Numan, H. Schenk and D. Döpp

Formula: C14H20N2O4



Acta Cryst. (1995). C51, 262-265    [ doi:10.1107/S0108270194005676 ]

Novel N-Acyl [alpha]-Azidopyrrolidines (N-Acyliminium-Ion Precursors)

V. M. Lynch, C. Hulme, P. Magnus and B. E. Davis

Formula: C17H17N5O and C14H17N7O4



Acta Cryst. (1995). C51, 265-267    [ doi:10.1107/S0108270194007973 ]

4,6-Dimethyl-2-(4-nitrobenzylidene)-3(2H)-benzofuranone

B. S. Goud, K. Panneerselvam, D. E. Zacharias and G. R. Desiraju

Formula: C17H13NO4



Acta Cryst. (1995). C51, 267-268    [ doi:10.1107/S0108270194008565 ]

9(10H)-Acridone

G. D. Potts and W. Jones

Formula: C13H9NO



Acta Cryst. (1995). C51, 268-270    [ doi:10.1107/S0108270194008759 ]

(1[beta],5[alpha],6[beta])-10,10-(1,2-Ethylenedioxy)-1,5-dimethylbicyclo[4.4.0]decan-4-one

K. Park, D. C. Swenson, W. J. Scott and D. F. Wiemer

Formula: C14H22O3



Acta Cryst. (1995). C51, 270-272    [ doi:10.1107/S0108270194010930 ]

Oxime of 1-Methyl-3-trifluoroacetylpyrrolidin-2-one

B. Tinant, J.-P. Declercq and J.-P. Bouillon

Formula: C7H9F3N2O2



Acta Cryst. (1995). C51, 272-274    [ doi:10.1107/S0108270194010589 ]

Aversin

S. Chan and J. Trotter

Formula: C20H16O7



Acta Cryst. (1995). C51, 274-277    [ doi:10.1107/S0108270194009376 ]

Hexaethyl (3,5-Di-tert-butyl-4-hydroxyphenyl)methanetrisphosphonate at 173 K

M. Ramm, B. Costisella and H. Gross

Formula: C27H51O10P3



Acta Cryst. (1995). C51, 277-279    [ doi:10.1107/S0108270194009364 ]

(E,E)-4-[3-(3,5-Dichloro-2-hydroxyphenylazo)-2-morpholino-2-butenoyl]morpholine

M. Ramm, H. Baumann and K. Kirschke

Formula: C18H22Cl2N4O4



Acta Cryst. (1995). C51, 279-280    [ doi:10.1107/S0108270194008838 ]

cis-5-Methyl-4-phenyl-3-(4-toluenesulfonyl)-1,3-oxazin-2-one

E. M. Campi, G. D. Fallon, A. Holmes, P. Perlmutter and C. C. Teo

Formula: C18H19NO4S



Acta Cryst. (1995). C51, 280-282    [ doi:10.1107/S0108270194008632 ]

(±)-[6[alpha](H)]-7,7,9[beta]-Trimethyl-cis-tricyclo[6.3.1.01,6]dodecan-2-one

M. Mukherjee, A. K. Mukherjee, S. Das, D. Mukherjee and M. Helliwell

Formula: C15H24O



Acta Cryst. (1995). C51, 282-285    [ doi:10.1107/S0108270194010243 ]

Quitenine Ethyl Ester

K. Lewinski, W. Nitek, B. J. Oleksyn and B. Stec

Formula: C21H26N2O4



Acta Cryst. (1995). C51, 285-287    [ doi:10.1107/S0108270194006414 ]

3-(4-Pyridyl)-5,6,7,8-tetrahydro-9H-1,2,4-triazolo[4,3-a][1,3]diazepine Monohydrate

M. L. Glówka

Formula: C11H13N5.H2O



Acta Cryst. (1995). C51, 287-289    [ doi:10.1107/S0108270194009431 ]

trans-3-Hydroxy-N-methyl-L-proline Hydrochloride

G. P. Jones, L. G. Paleg, Y. Waisel, A. Solomon, S. Beer and E. R. T. Tiekink

Formula: C6H12NO3+.Cl-



Acta Cryst. (1995). C51, 289-291    [ doi:10.1107/S0108270194009443 ]

N-[gamma]-L-Glutamyl-[beta]-cyano-L-alanine, an Antinutritional Factor ex Vicia sativa L., as its Ammonium Salt

I. M. Delaere, M. E. Tate, G. P. Jones and E. R. T. Tiekink

Formula: NH4+.C9H12N3O5-



Acta Cryst. (1995). C51, 291-293    [ doi:10.1107/S0108270194009121 ]

Benzophenone O-(2,3,5,6-Tetrafluoro-4-pyridyl)oxime, Formed by 4-Substitution of Pentafluoropyridine by Benzophenone Oximate

R. E. Banks, W. J. Jondi, R. G. Pritchard and A. E. Tipping

Formula: C18H10F4N2O



Acta Cryst. (1995). C51, 293-295    [ doi:10.1107/S0108270194009133 ]

(E)-Acetophenone O-(3,4,5,6-Tetrafluoro-2-pyridyl)oxime, Formed by 2-Substitution of Pentafluoropyridine by (E)-Acetophenone Oximate

R. E. Banks, W. J. Jondi, R. G. Pritchard and A. E. Tipping

Formula: C13H8F4N2O



Acta Cryst. (1995). C51, 295-298    [ doi:10.1107/S0108270194005317 ]

2'-Carbamate Taxol

Q. Gao and J. Golik

Formula: C48H52N2O15



Acta Cryst. (1995). C51, 298-301    [ doi:10.1107/S0108270193012983 ]

2-Methyl-2H-1,2-benzisoselenazol-3-one

M. Piatek, B. Oleksyn and J. Sliwinski

Formula: C8H7NOSe



Acta Cryst. (1995). C51, 301-304    [ doi:10.1107/S0108270194005329 ]

5-Fluoro-1-indanone and 2,2-Dimethyl-5-fluoro-1-indanone

J. G. Garcia, J. D. Enas, H. F. VanBrocklin and F. R. Fronczek

Formula: C9H7FO and C11H11FO



Acta Cryst. (1995). C51, 304-306    [ doi:10.1107/S0108270194005457 ]

cis,trans-3,3'-Sulfinylbis(acrylic acid)

T. R. Webb, Z.-C. Ho and P. Livant

Formula: C6H6O5S



Acta Cryst. (1995). C51, 306-308    [ doi:10.1107/S0108270194006992 ]

Decahydro-6,6-dimethoxy-1,2,2,4-tetramethylquinolinium Picrate

O. Kasemann, P. Stanetty and K. Mereiter

Formula: C15H30NO2+.C6H2N3O7-



Acta Cryst. (1995). C51, 308-311    [ doi:10.1107/S0108270194004233 ]

Ergotamine Tartrate Bis(ethanol) Solvate

S. Pakhomova, J. Ondráucek, M. Huusák, B. Kratochvíl, A. Jegorov and J. Stuchlík

Formula: C33H36N5O5+.0.5C4H4O62-.2C2H6O



Acta Cryst. (1995). C51, 311-313    [ doi:10.1107/S0108270194008668 ]

2-Methoxy-5-(4-nitrostyryl)phenol

Z.-D. Li and G. Su

Formula: C15H13NO4



Acta Cryst. (1995). C51, 313-315    [ doi:10.1107/S0108270194006426 ]

2,4,7,9-Tetra-tert-butyl-1,3,7,9-decatetraene

J. S. Overby and T. P. Hanusa

Formula: C26H46



Acta Cryst. (1995). C51, 315-318    [ doi:10.1107/S0108270194003811 ]

Thiamin Thiothiazolone Acetone Solvate, C12H16N4OS2.0.5C3H6O

W. Shin and B. C. Lim

Formula: C12H16N4OS2.0.5C3H6O



Acta Cryst. (1995). C51, 318-322    [ doi:10.1107/S0108270194004166 ]

The Novel GABAA Receptor Ligand NNC 14-0764: 5-(3-Cyclopropyl-1,2,4-oxadiazol-5-yl)-2,3-dihydrodiimidazo[1,5-a:1',2'-c]quinazoline

R. A. Palmer, R. W. Janes, A. L. Corper, J. N. Lisgarten and H. C. Hansen

Formula: C17H14N6O



Acta Cryst. (1995). C51, 322-324    [ doi:10.1107/S0108270194006013 ]

Polymorph (II) of Methyl 3-(4-Ethoxy-[alpha]-hydroxyiminobenzyl)-1,2,2-trimethyl-cyclopentanecarboxylate

J. Nurit, J. Rambaud, B. Pauvert, A. Térol, P. Chevallet, O. Doumbia and J.-P. Declercq

Formula: C19H27NO4



Acta Cryst. (1995). C51, 324-326    [ doi:10.1107/S0108270194005949 ]

6'-Diethylamino-2'-nitrospiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one

X.-L. Liu, J.-L. Wang, J.-W. Liu and F.-M. Miao

Formula: C24H20N2O5



Acta Cryst. (1995). C51, 326-330    [ doi:10.1107/S0108270194003653 ]

Phenyl 2-Fluorobenzoate, Phenyl 4-Fluorobenzoate and Phenyl Benzoate

M. Shibakami and A. Sekiya

Formula: Two isomers of C13H9FO2 and C13H10O2



Acta Cryst. (1995). C51, 330-333    [ doi:10.1107/S0108270193014015 ]

3,4,5-Trimethoxybenzaldehyde Thiosemicarbazone Monohydrate

M. K. Kokila, Puttaraja. Puttaraja, M. V. Kulkarni and S. Thampi

Formula: C11H15N3O3S.H2O



Acta Cryst. (1995). C51, 333-336    [ doi:10.1107/S0108270193014180 ]

4-Amino-N-(2-pyrimidinyl)benzenesulfonamide

M. K. Kokila, Puttaraja. Puttaraja, M. V. Kulkarni and S. Thampi

Formula: C10H10N4O2S



Acta Cryst. (1995). C51, 336-339    [ doi:10.1107/S0108270194008577 ]

N-Acetylglycyl-L-alaninamide and N-Acetyl-L-alanyl-L-alaninamide

R. Puliti and C. A. Mattia

Formula: C7H13N3O3 and C8H15N3O3: Ca6Al5SiO16Cl3: C26H38O10


addenda and errata



Acta Cryst. (1995). C51, 340    [ doi:10.1107/S0108270195099781 ]

Comments on wadalite, Ca6Al5SiO16Cl3, and the structures of garnet, mayenite and calcium chlorosilicate. Addendum

F. P. Glasser

Synopsis: Addendum to Acta Cryst. (1993), C49, 205-207.



Acta Cryst. (1995). C51, 340    [ doi:10.1107/S010827019509977X ]

Functionalized hydrocarbons with condensed ring skeletons. XV. A (methoxymethoxymethyl)tricyclo[9.4.0.02,8]pentadec-9-ene. Erratum

A. G. Michel, D. G. Hall and M. Drouin

Synopsis: Erratum to Acta Cryst. (1993), C49, 1830-1833.


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