OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 2-EtH2-Cu.2H2O PAGE 1 H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S 1 0 0 103 106 0 4 4 0 5 5 0 -1 1 1 134 150 1 3 3 1 24 25 0 -10 6 1 8 -8 0 2 0 0 36 -36 0 5 4 0 14 13 0 0 1 1 19 18 0 4 3 1 22 -20 0 -9 6 1 16 -16 0 3 0 0 222 -238 1 6 4 0 17 -17 0 1 1 1 34 -34 0 5 3 1 22 -22 0 -8 6 1 10 -11 0 4 0 0 218 -227 1 7 4 0 13 -13 0 2 1 1 83 -82 0 6 3 1 26 -25 0 -7 6 1 17 16 0 5 0 0 6 -7 0 8 4 0 28 -27 0 3 1 1 20 19 0 7 3 1 31 -30 0 -6 6 1 36 34 0 6 0 0 131 128 0 9 4 0 30 30 0 4 1 1 14 14 0 8 3 1 39 39 0 -5 6 1 28 29 0 7 0 0 76 77 0 10 4 0 5 5 0 5 1 1 78 76 0 9 3 1 6 5 0 -4 6 1 9 -8 0 8 0 0 51 51 0 11 4 0 22 22 0 6 1 1 18 20 0 10 3 1 16 15 0 -3 6 1 48 -47 0 9 0 0 40 -38 0 12 4 0 3 3 0 7 1 1 5 5 0 11 3 1 1 0 -1 -2 6 1 29 -28 0 10 0 0 52 -51 0 1 5 0 60 59 1 8 1 1 16 -16 0 12 3 1 9 -10 0 -1 6 1 12 12 0 11 0 0 46 -48 0 2 5 0 49 48 0 9 1 1 18 -18 0 -12 4 1 5 6 0 0 6 1 63 62 0 12 0 0 2 0 -1 3 5 0 4 3 0 10 1 1 18 -19 0 -11 4 1 12 -13 0 1 6 1 62 61 1 13 0 0 13 14 0 4 5 0 36 -36 0 11 1 1 3 3 1 -10 4 1 7 -7 0 2 6 1 2 0 0 1 1 0 38 -37 0 5 5 0 51 -50 0 12 1 1 10 12 0 -9 4 1 5 5 0 3 6 1 34 -35 0 2 1 0 116 -117 0 6 5 0 26 -24 0 13 1 1 6 7 0 -8 4 1 21 -20 0 4 6 1 43 -43 0 3 1 0 49 -49 0 7 5 0 15 15 0 -13 2 1 11 -12 0 -7 4 1 7 7 0 5 6 1 32 -32 1 4 1 0 37 37 0 8 5 0 12 11 0 -12 2 1 3 -2 -1 -6 4 1 25 25 0 6 6 1 16 16 0 5 1 0 74 75 0 9 5 0 18 17 0 -11 2 1 20 20 0 -5 4 1 9 10 0 7 6 1 16 15 0 6 1 0 91 89 0 10 5 0 7 6 0 -10 2 1 34 34 0 -4 4 1 21 19 0 8 6 1 16 16 0 7 1 0 32 31 0 11 5 0 10 -10 0 -9 2 1 23 23 0 -3 4 1 20 -21 0 9 6 1 4 4 0 8 1 0 25 -25 0 0 6 0 70 71 0 -8 2 1 14 -13 0 -2 4 1 50 -48 0 -8 7 1 15 14 0 9 1 0 40 -40 0 1 6 0 27 26 0 -7 2 1 48 -47 0 -1 4 1 3 -3 0 -7 7 1 5 4 1 10 1 0 22 -22 0 2 6 0 18 -18 0 -6 2 1 48 -48 0 0 4 1 15 16 0 -6 7 1 18 -19 0 11 1 0 2 -2 -1 3 6 0 46 -46 0 -5 2 1 19 -19 0 1 4 1 23 23 0 -5 7 1 30 -30 1 12 1 0 19 19 0 4 6 0 46 -45 0 -4 2 1 12 13 0 2 4 1 7 7 1 -4 7 1 15 -15 0 13 1 0 16 18 0 5 6 0 4 4 0 -3 2 1 26 26 0 3 4 1 10 9 0 -3 7 1 5 5 0 0 2 0 47 -47 0 6 6 0 31 31 0 -2 2 1 8 -6 0 4 4 1 12 -12 0 -2 7 1 25 26 1 1 2 0 89 -87 1 7 6 0 33 33 1 -1 2 1 14 -14 0 5 4 1 19 -19 0 -1 7 1 40 41 0 2 2 0 11 12 0 8 6 0 7 7 0 0 2 1 66 -67 0 6 4 1 5 4 0 0 7 1 4 3 0 3 2 0 69 68 0 9 6 0 12 -11 0 1 2 1 39 -38 0 7 4 1 12 -11 0 1 7 1 9 -9 0 4 2 0 62 59 0 1 7 0 20 20 0 2 2 1 39 -38 0 8 4 1 10 10 0 2 7 1 31 -32 1 5 2 0 43 40 0 2 7 0 9 -11 0 3 2 1 16 16 0 9 4 1 20 20 0 3 7 1 20 -20 1 6 2 0 25 -25 0 3 7 0 2 1 0 4 2 1 56 56 0 10 4 1 8 -8 0 4 7 1 1 3 -1 7 2 0 43 -42 0 4 7 0 8 -8 0 5 2 1 48 48 0 11 4 1 4 -4 0 5 7 1 29 30 1 8 2 0 30 -29 0 5 7 0 10 -10 0 6 2 1 8 7 0 -11 5 1 1 0 -1 6 7 1 25 25 1 9 2 0 8 8 0 6 7 0 8 9 0 7 2 1 9 -10 0 -10 5 1 3 2 0 7 7 1 12 13 0 10 2 0 16 17 0 7 7 0 1 0 0 8 2 1 34 -33 0 -9 5 1 7 -7 0 -5 8 1 3 0 0 11 2 0 10 10 0 8 7 0 7 -7 0 9 2 1 5 5 0 -8 5 1 6 6 0 -4 8 1 15 15 0 12 2 0 2 -2 -1 0 8 0 9 9 0 10 2 1 15 15 0 -7 5 1 7 7 0 -3 8 1 28 29 0 13 2 0 4 -4 0 1 8 0 5 -5 0 11 2 1 19 19 0 -6 5 1 14 13 0 -2 8 1 3 3 0 1 3 0 10 8 0 2 8 0 15 16 0 12 2 1 13 13 0 -5 5 1 5 5 0 -1 8 1 12 -13 0 2 3 0 21 18 0 3 8 0 3 1 1 -12 3 1 9 8 0 -4 5 1 5 4 0 0 8 1 14 -14 0 3 3 0 9 8 0 4 8 0 2 2 -1 -11 3 1 14 14 0 -3 5 1 13 -12 0 1 8 1 27 -29 1 4 3 0 14 14 0 5 8 0 6 -6 0 -10 3 1 26 27 0 -2 5 1 11 9 0 2 8 1 2 0 -1 5 3 0 22 21 0 -13 1 1 2 2 -1 -9 3 1 28 -27 0 -1 5 1 27 -26 0 3 8 1 22 23 0 6 3 0 11 10 0 -12 1 1 22 -22 0 -8 3 1 23 -23 0 0 5 1 1 -1 0 4 8 1 19 20 1 7 3 0 2 1 0 -11 1 1 7 -6 0 -7 3 1 7 -2 1 1 5 1 11 -10 1 5 8 1 14 15 1 8 3 0 11 -11 0 -10 1 1 9 -9 0 -6 3 1 16 16 0 2 5 1 14 -12 0 -13 0 2 11 -12 0 9 3 0 8 -8 0 -9 1 1 2 -1 0 -5 3 1 40 41 0 3 5 1 26 25 0 -12 0 2 8 -8 0 10 3 0 11 11 0 -8 1 1 23 22 0 -4 3 1 43 43 0 4 5 1 2 1 0 -11 0 2 11 -9 0 11 3 0 9 9 0 -7 1 1 13 12 0 -3 3 1 43 -39 0 5 5 1 8 -9 0 -10 0 2 2 1 -1 12 3 0 5 5 0 -6 1 1 4 3 0 -2 3 1 12 7 0 6 5 1 3 -2 1 -9 0 2 30 29 0 0 4 0 29 -29 0 -5 1 1 68 -66 0 -1 3 1 40 -42 0 7 5 1 36 -36 0 -8 0 2 34 33 0 1 4 0 17 -17 0 -4 1 1 73 -72 0 0 3 1 13 -15 0 8 5 1 3 3 0 -7 0 2 24 21 0 2 4 0 33 -30 0 -3 1 1 3 -2 0 1 3 1 21 -18 0 9 5 1 2 -1 -1 -6 0 2 114 -112 0 3 4 0 29 29 0 -2 1 1 48 47 1 2 3 1 4 7 0 10 5 1 12 13 0 -5 0 2 78 -78 0 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 2-EtH2-Cu.2H2O PAGE 2 H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S -4 0 2 98 -99 0 0 2 2 12 -10 0 5 4 2 68 -67 0 -1 7 2 14 13 0 -3 2 3 55 -55 0 -3 0 2 32 33 0 1 2 2 43 43 0 6 4 2 45 -43 0 0 7 2 1 1 -1 -2 2 3 31 -33 0 -2 0 2 159 175 1 2 2 2 30 28 0 7 4 2 3 3 0 1 7 2 10 11 0 -1 2 3 112 -112 1 -1 0 2 23 23 0 3 2 2 37 -35 0 8 4 2 22 21 0 2 7 2 15 15 1 0 2 3 10 9 0 0 0 2 98 -103 0 4 2 2 22 -22 0 9 4 2 22 22 1 3 7 2 8 -8 0 1 2 3 8 10 0 1 0 2 45 -45 0 5 2 2 32 -30 0 10 4 2 6 6 0 4 7 2 2 2 -1 2 2 3 66 65 0 2 0 2 106 -106 0 6 2 2 14 13 0 11 4 2 7 -7 0 5 7 2 5 -6 0 3 2 3 3 0 0 3 0 2 57 55 0 7 2 2 33 32 0 -11 5 2 20 -20 0 6 7 2 7 -7 1 4 2 3 34 -34 0 4 0 2 138 138 1 8 2 2 22 21 0 -10 5 2 14 -13 0 7 7 2 9 10 0 5 2 3 59 -59 0 5 0 2 51 54 0 9 2 2 5 -5 0 -9 5 2 12 -11 0 -5 8 2 1 1 -1 6 2 3 38 -38 0 6 0 2 55 55 0 10 2 2 17 -17 0 -8 5 2 21 20 0 -4 8 2 8 8 0 7 2 3 8 -8 0 7 0 2 39 -38 0 11 2 2 5 -4 0 -7 5 2 45 45 0 -3 8 2 6 6 0 8 2 3 34 35 0 8 0 2 51 -51 0 12 2 2 9 -9 0 -6 5 2 18 18 0 -2 8 2 2 -1 -1 9 2 3 10 9 0 9 0 2 18 -18 0 -13 3 2 4 -5 0 -5 5 2 23 -22 0 -1 8 2 3 -3 1 10 2 3 24 25 0 10 0 2 8 7 0 -12 3 2 9 10 0 -4 5 2 59 -59 0 0 8 2 9 -10 0 11 2 3 5 -5 0 11 0 2 37 39 0 -11 3 2 17 17 0 -3 5 2 55 -53 1 1 8 2 3 -3 0 12 2 3 9 -8 0 12 0 2 14 13 0 -10 3 2 18 18 0 -2 5 2 19 19 0 2 8 2 2 1 -1 -13 3 3 17 16 0 -13 1 2 6 7 0 -9 3 2 2 2 -1 -1 5 2 74 74 1 3 8 2 6 6 0 -12 3 3 5 5 0 -12 1 2 16 16 0 -8 3 2 33 -32 0 0 5 2 78 78 0 4 8 2 9 10 0 -11 3 3 25 -24 0 -11 1 2 24 23 0 -7 3 2 13 -12 0 1 5 2 18 18 0 -14 1 3 2 1 -1 -10 3 3 49 -48 0 -10 1 2 9 9 0 -6 3 2 8 -7 0 2 5 2 23 -23 0 -13 1 3 2 -1 0 -9 3 3 5 5 0 -9 1 2 16 -15 0 -5 3 2 20 20 0 3 5 2 57 -56 0 -12 1 3 6 7 0 -8 3 3 11 11 0 -8 1 2 33 -32 0 -4 3 2 49 47 0 4 5 2 39 -38 0 -11 1 3 2 0 -1 -7 3 3 75 76 1 -7 1 2 8 4 0 -3 3 2 16 17 0 5 5 2 8 8 0 -10 1 3 16 15 0 -6 3 3 41 39 0 -6 1 2 9 7 0 -2 3 2 17 -15 0 6 5 2 26 26 0 -9 1 3 13 12 0 -5 3 3 29 -27 0 -5 1 2 48 47 0 -1 3 2 53 -51 1 7 5 2 30 30 1 -8 1 3 3 1 0 -4 3 3 59 -59 0 -4 1 2 16 16 0 0 3 2 75 -72 0 8 5 2 16 16 0 -7 1 3 37 -36 0 -3 3 3 74 -74 0 -3 1 2 68 -65 0 1 3 2 48 -46 0 9 5 2 18 -17 1 -6 1 3 39 -39 0 -2 3 3 16 14 0 -2 1 2 41 -40 0 2 3 2 2 -1 0 10 5 2 25 -24 0 -5 1 3 11 -11 0 -1 3 3 98 95 1 -1 1 2 36 -35 0 3 3 2 50 47 0 -10 6 2 13 14 0 -4 1 3 28 28 0 0 3 3 110 109 1 0 1 2 58 -59 1 4 3 2 24 23 0 -9 6 2 9 9 0 -3 1 3 12 -9 0 1 3 3 67 64 1 1 1 2 57 54 0 5 3 2 5 4 0 -8 6 2 18 18 0 -2 1 3 55 53 0 2 3 3 76 -72 0 2 1 2 19 19 0 6 3 2 11 -11 0 -7 6 2 2 0 -1 -1 1 3 127 -131 1 3 3 3 81 -79 1 3 1 2 8 10 0 7 3 2 25 -24 0 -6 6 2 33 -32 0 0 1 3 10 -11 0 4 3 3 71 -68 0 4 1 2 7 8 0 8 3 2 3 3 0 -5 6 2 23 -21 0 1 1 3 22 -21 0 5 3 3 4 4 0 5 1 2 54 -52 0 9 3 2 8 8 0 -4 6 2 20 -19 0 2 1 3 23 -21 0 6 3 3 51 49 0 6 1 2 35 -35 0 10 3 2 2 0 -1 -3 6 2 18 18 0 3 1 3 56 55 0 7 3 3 39 38 0 7 1 2 11 -11 0 11 3 2 12 12 0 -2 6 2 52 52 1 4 1 3 41 42 0 8 3 3 5 -5 0 8 1 2 16 16 0 12 3 2 4 5 0 -1 6 2 24 24 0 5 1 3 17 17 0 9 3 3 10 -10 0 9 1 2 34 33 0 -12 4 2 16 16 0 0 6 2 4 -2 0 6 1 3 8 6 0 10 3 3 30 -30 0 10 1 2 23 22 0 -11 4 2 3 2 1 1 6 2 38 -37 0 7 1 3 22 -22 0 11 3 3 11 -11 0 11 1 2 8 8 0 -10 4 2 12 -12 0 2 6 2 42 -43 1 8 1 3 26 -25 0 -12 4 3 3 -2 0 12 1 2 9 -9 0 -9 4 2 43 -44 1 3 6 2 7 -7 0 9 1 3 9 9 0 -11 4 3 1 0 -1 -13 2 2 2 1 -1 -8 4 2 5 5 0 4 6 2 25 25 0 10 1 3 20 21 0 -10 4 3 12 -11 0 -12 2 2 13 14 0 -7 4 2 16 15 0 5 6 2 31 30 1 11 1 3 11 11 0 -9 4 3 4 4 0 -11 2 2 7 7 0 -6 4 2 53 53 0 6 6 2 18 18 1 12 1 3 8 8 0 -8 4 3 20 20 1 -10 2 2 2 2 -1 -5 4 2 72 70 0 7 6 2 13 -13 0 -13 2 3 12 12 0 -7 4 3 2 2 0 -9 2 2 22 -22 0 -4 4 2 4 4 0 8 6 2 18 -18 0 -12 2 3 24 24 0 -6 4 3 6 6 0 -8 2 2 9 -9 0 -3 4 2 23 -24 0 9 6 2 13 -13 0 -11 2 3 10 10 0 -5 4 3 23 -23 0 -7 2 2 11 10 0 -2 4 2 58 -57 0 -8 7 2 11 -11 0 -10 2 3 5 5 0 -4 4 3 27 -26 0 -6 2 2 6 -6 0 -1 4 2 65 -63 0 -7 7 2 7 7 0 -9 2 3 42 -41 0 -3 4 3 11 11 0 -5 2 2 28 26 1 0 4 2 11 11 0 -6 7 2 15 16 1 -8 2 3 1 -1 -1 -2 4 3 12 12 0 -4 2 2 2 2 0 1 4 2 52 52 0 -5 7 2 7 7 0 -7 2 3 6 5 0 -1 4 3 19 20 0 -3 2 2 22 -21 0 2 4 2 72 70 1 -4 7 2 7 7 0 -6 2 3 50 51 0 0 4 3 9 8 0 -2 2 2 9 -10 0 3 4 2 8 9 0 -3 7 2 17 -18 0 -5 2 3 60 62 1 1 4 3 4 -4 0 -1 2 2 3 -4 0 4 4 2 33 -33 0 -2 7 2 9 -9 0 -4 2 3 33 34 0 2 4 3 16 -17 0 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 2-EtH2-Cu.2H2O PAGE 3 H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S 3 4 3 23 -22 0 -2 7 3 5 4 0 -4 1 4 20 -20 0 1 3 4 37 35 0 -9 6 4 7 8 0 4 4 3 6 -5 0 -1 7 3 22 -22 1 -3 1 4 19 -21 0 2 3 4 16 -14 0 -8 6 4 11 -11 0 5 4 3 8 8 0 0 7 3 26 -27 0 -2 1 4 100 -99 1 3 3 4 37 -35 0 -7 6 4 11 -11 0 6 4 3 21 21 0 1 7 3 29 -30 1 -1 1 4 48 45 0 4 3 4 44 -42 0 -6 6 4 9 -9 0 7 4 3 20 19 0 2 7 3 10 10 0 0 1 4 5 5 0 5 3 4 13 -12 0 -5 6 4 10 -10 0 8 4 3 10 -10 0 3 7 3 23 23 0 1 1 4 68 67 0 6 3 4 2 1 0 -4 6 4 27 28 0 9 4 3 16 -16 1 4 7 3 23 24 0 2 1 4 34 33 0 7 3 4 25 24 0 -3 6 4 14 14 0 10 4 3 9 -9 0 5 7 3 13 13 0 3 1 4 37 -36 0 8 3 4 9 -10 0 -2 6 4 5 5 0 11 4 3 1 -1 -1 6 7 3 15 -15 1 4 1 4 62 -62 0 9 3 4 10 10 0 -1 6 4 3 -1 1 -11 5 3 3 -3 0 -5 8 3 24 24 0 5 1 4 24 -24 0 10 3 4 9 -9 0 0 6 4 37 -38 0 -10 5 3 16 -17 0 -4 8 3 11 10 0 6 1 4 29 -27 0 11 3 4 7 -8 0 1 6 4 2 -1 -1 -9 5 3 13 13 0 -3 8 3 16 -16 0 7 1 4 32 31 0 -12 4 4 18 -19 1 2 6 4 3 3 0 -8 5 3 7 8 0 -2 8 3 22 -22 0 8 1 4 7 6 0 -11 4 4 32 -32 0 3 6 4 18 18 0 -7 5 3 10 11 0 -1 8 3 22 -22 0 9 1 4 9 9 0 -10 4 4 3 3 0 4 6 4 22 23 0 -6 5 3 4 4 0 0 8 3 2 -1 -1 10 1 4 6 -6 0 -9 4 4 10 10 0 5 6 4 12 -13 0 -5 5 3 7 7 0 1 8 3 30 31 0 11 1 4 9 -8 0 -8 4 4 28 28 0 6 6 4 9 -9 0 -4 5 3 5 -6 0 2 8 3 18 18 0 12 1 4 7 -6 0 -7 4 4 21 21 0 7 6 4 16 -15 0 -3 5 3 2 0 0 3 8 3 5 5 0 -13 2 4 4 4 0 -6 4 4 5 -5 0 8 6 4 1 -1 -1 -2 5 3 4 4 0 4 8 3 13 -13 1 -12 2 4 5 -4 0 -5 4 4 46 -45 0 -8 7 4 2 -1 -1 -1 5 3 2 -2 0 -14 0 4 8 -8 0 -11 2 4 18 -19 0 -4 4 4 22 -23 0 -7 7 4 5 -6 0 0 5 3 4 4 0 -13 0 4 2 1 -2 -10 2 4 10 10 0 -3 4 4 16 -16 0 -6 7 4 2 3 -1 1 5 3 28 27 0 -12 0 4 1 -1 -1 -9 2 4 7 7 0 -2 4 4 49 47 0 -5 7 4 6 -6 0 2 5 3 4 -4 0 -11 0 4 21 22 0 -8 2 4 5 4 0 -1 4 4 76 75 0 -4 7 4 2 0 -1 3 5 3 6 4 0 -10 0 4 32 33 0 -7 2 4 7 7 0 0 4 4 38 36 0 -3 7 4 3 -3 1 4 5 3 5 -5 0 -9 0 4 11 10 0 -6 2 4 6 5 0 1 4 4 5 -4 1 -2 7 4 4 -4 0 5 5 3 13 -13 0 -8 0 4 20 -20 0 -5 2 4 38 -37 0 2 4 4 48 -47 0 -1 7 4 3 -4 0 6 5 3 7 -7 0 -7 0 4 37 -37 0 -4 2 4 4 4 0 3 4 4 34 -33 0 0 7 4 16 16 0 7 5 3 11 11 0 -6 0 4 22 -20 0 -3 2 4 2 2 0 4 4 4 10 10 0 1 7 4 3 -2 1 8 5 3 11 -11 0 -5 0 4 7 8 0 -2 2 4 14 -13 0 5 4 4 30 30 0 2 7 4 1 0 -1 9 5 3 6 6 0 -4 0 4 52 51 0 -1 2 4 74 70 0 6 4 4 41 40 0 3 7 4 11 -12 0 10 5 3 3 -4 0 -3 0 4 36 35 0 0 2 4 2 -1 0 7 4 4 3 -2 1 4 7 4 1 2 -1 -10 6 3 9 -9 0 -2 0 4 30 -30 0 1 2 4 27 -24 0 8 4 4 14 -14 0 5 7 4 6 6 0 -9 6 3 18 19 1 -1 0 4 11 -12 0 2 2 4 29 -27 0 9 4 4 26 -27 0 6 7 4 17 18 0 -8 6 3 20 19 1 0 0 4 142 -148 0 3 2 4 4 -4 0 10 4 4 16 -17 1 -5 8 4 13 14 0 -7 6 3 11 10 0 1 0 4 57 -55 0 4 2 4 3 -2 0 -11 5 4 3 -3 -1 -4 8 4 14 14 0 -6 6 3 31 -32 0 2 0 4 40 -37 0 5 2 4 19 17 0 -10 5 4 22 22 0 -3 8 4 1 2 -1 -5 6 3 42 -42 0 3 0 4 46 46 0 6 2 4 4 4 0 -9 5 4 26 26 1 -2 8 4 25 -27 0 -4 6 3 27 -26 0 4 0 4 74 72 0 7 2 4 22 -21 0 -8 5 4 3 1 0 -1 8 4 21 -22 0 -3 6 3 11 11 0 5 0 4 16 13 0 8 2 4 6 7 1 -7 5 4 35 -35 0 0 8 4 20 -21 0 -2 6 3 43 43 0 6 0 4 31 -30 0 9 2 4 4 4 0 -6 5 4 41 -40 1 1 8 4 7 7 0 -1 6 3 54 54 0 7 0 4 42 -41 0 10 2 4 3 3 1 -5 5 4 32 -31 0 2 8 4 17 18 0 0 6 3 17 -16 0 8 0 4 12 -12 0 11 2 4 4 3 0 -4 5 4 21 21 0 3 8 4 15 16 0 1 6 3 3 -3 0 9 0 4 28 28 0 -13 3 4 8 9 0 -3 5 4 37 37 0 -14 1 5 3 4 1 2 6 3 34 -33 0 10 0 4 27 28 0 -12 3 4 4 5 0 -2 5 4 34 34 0 -13 1 5 5 5 0 3 6 3 18 -16 0 11 0 4 11 11 0 -11 3 4 2 2 -1 -1 5 4 16 -15 0 -12 1 5 20 20 0 4 6 3 23 23 0 12 0 4 1 0 -1 -10 3 4 27 -28 1 0 5 4 23 -23 0 -11 1 5 18 18 0 5 6 3 31 31 1 -14 1 4 5 6 0 -9 3 4 1 1 -1 1 5 4 37 -36 0 -10 1 5 10 -10 0 6 6 3 15 16 0 -13 1 4 15 16 0 -8 3 4 2 -1 0 2 5 4 13 -12 0 -9 1 5 32 -31 0 7 6 3 17 18 1 -12 1 4 3 -3 0 -7 3 4 13 13 0 3 5 4 20 20 0 -8 1 5 27 -26 0 8 6 3 25 -26 1 -11 1 4 7 -7 0 -6 3 4 42 42 0 4 5 4 46 45 0 -7 1 5 33 33 0 -8 7 3 15 -15 0 -10 1 4 26 -27 0 -5 3 4 24 24 0 5 5 4 23 23 0 -6 1 5 49 49 0 -7 7 3 23 -24 0 -9 1 4 8 -7 2 -4 3 4 20 -19 0 6 5 4 15 15 0 -5 1 5 69 67 0 -6 7 3 10 -9 0 -8 1 4 11 11 0 -3 3 4 14 11 0 7 5 4 29 -30 0 -4 1 5 17 16 0 -5 7 3 3 1 -1 -7 1 4 45 46 0 -2 3 4 59 -53 1 8 5 4 23 -23 0 -3 1 5 58 -55 0 -4 7 3 23 24 0 -6 1 4 52 52 0 -1 3 4 27 25 0 9 5 4 8 -8 0 -2 1 5 67 -67 0 -3 7 3 19 19 0 -5 1 4 30 30 0 0 3 4 36 34 0 -10 6 4 7 8 0 -1 1 5 43 -41 0 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 2-EtH2-Cu.2H2O PAGE 4 H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S 0 1 5 46 -43 0 6 3 5 13 12 0 -3 6 5 5 -6 0 10 0 6 9 -10 0 -9 3 6 4 -4 0 1 1 5 29 29 0 7 3 5 13 -12 0 -2 6 5 34 -34 0 11 0 6 20 -21 0 -8 3 6 31 31 0 2 1 5 70 68 0 8 3 5 35 -36 0 -1 6 5 9 -8 1 -14 1 6 2 2 -1 -7 3 6 6 -6 1 3 1 5 5 -4 1 9 3 5 13 -13 0 0 6 5 8 -7 0 -13 1 6 8 -8 0 -6 3 6 25 -24 0 4 1 5 8 -9 0 10 3 5 7 -8 0 1 6 5 16 -15 0 -12 1 6 15 -16 0 -5 3 6 29 -29 0 5 1 5 60 -58 0 -12 4 5 3 2 0 2 6 5 22 21 0 -11 1 6 33 -33 0 -4 3 6 28 -27 0 6 1 5 51 -50 0 -11 4 5 21 20 0 3 6 5 13 11 0 -10 1 6 4 4 0 -3 3 6 14 13 0 7 1 5 15 14 0 -10 4 5 16 15 0 4 6 5 4 4 0 -9 1 6 1 0 0 -2 3 6 91 86 0 8 1 5 27 27 0 -9 4 5 1 0 -1 5 6 5 18 18 0 -8 1 6 38 39 0 -1 3 6 32 30 0 9 1 5 26 27 0 -8 4 5 25 -24 1 6 6 5 21 -21 0 -7 1 6 23 23 0 0 3 6 22 21 0 10 1 5 5 5 0 -7 4 5 33 -33 0 7 6 5 7 -7 0 -6 1 6 4 -5 0 1 3 6 33 -31 0 11 1 5 9 -9 0 -6 4 5 9 -9 0 -8 7 5 7 -7 0 -5 1 6 38 -39 0 2 3 6 31 -30 0 -13 2 5 3 2 1 -5 4 5 22 21 0 -7 7 5 13 14 0 -4 1 6 34 -33 0 3 3 6 7 -6 0 -12 2 5 14 -15 0 -4 4 5 30 30 0 -6 7 5 16 16 0 -3 1 6 12 -10 0 4 3 6 13 13 0 -11 2 5 39 -39 0 -3 4 5 26 27 0 -5 7 5 20 21 0 -2 1 6 66 67 0 5 3 6 17 17 0 -10 2 5 30 -30 0 -2 4 5 2 -1 -1 -4 7 5 1 0 -1 -1 1 6 54 55 0 6 3 6 9 9 0 -9 2 5 14 13 0 -1 4 5 19 -19 0 -3 7 5 22 -22 0 0 1 6 57 54 0 7 3 6 2 0 -1 -8 2 5 27 28 0 0 4 5 19 -19 0 -2 7 5 29 -29 0 1 1 6 47 -47 0 8 3 6 1 0 -1 -7 2 5 83 83 0 1 4 5 25 -24 0 -1 7 5 20 -20 0 2 1 6 33 -34 0 9 3 6 15 -16 0 -6 2 5 38 37 0 2 4 5 1 0 -1 0 7 5 19 19 0 3 1 6 17 -17 0 10 3 6 4 -4 0 -5 2 5 40 -39 0 3 4 5 21 21 0 1 7 5 25 25 0 4 1 6 11 11 0 -12 4 6 3 3 0 -4 2 5 42 -45 0 4 4 5 27 26 0 2 7 5 22 22 0 5 1 6 47 46 0 -11 4 6 13 14 0 -3 2 5 86 -83 1 5 4 5 9 9 0 3 7 5 3 -4 0 6 1 6 24 23 0 -10 4 6 5 4 0 -2 2 5 32 31 0 6 4 5 15 -14 0 4 7 5 29 -30 0 7 1 6 11 -11 0 -9 4 6 4 4 0 -1 2 5 120 120 0 7 4 5 21 -21 0 5 7 5 26 -27 1 8 1 6 14 -14 1 -8 4 6 13 -13 0 0 2 5 95 95 0 8 4 5 8 -8 0 -4 8 5 21 -22 0 9 1 6 34 -34 0 -7 4 6 40 -40 0 1 2 5 38 36 0 9 4 5 10 10 0 -3 8 5 13 -13 0 10 1 6 9 -9 0 -6 4 6 31 -31 0 2 2 5 53 -52 0 10 4 5 11 11 0 -2 8 5 7 7 0 11 1 6 7 8 0 -5 4 6 15 -15 0 3 2 5 89 -89 0 -11 5 5 5 5 0 -1 8 5 31 32 0 -13 2 6 6 -5 0 -4 4 6 29 29 0 4 2 5 39 -39 0 -10 5 5 2 2 -1 0 8 5 24 25 0 -12 2 6 2 2 -1 -3 4 6 42 42 0 5 2 5 5 -4 0 -9 5 5 23 -23 0 1 8 5 9 -9 0 -11 2 6 3 2 0 -2 4 6 33 31 0 6 2 5 46 45 0 -8 5 5 20 -21 0 2 8 5 23 -24 0 -10 2 6 16 -17 0 -1 4 6 34 -33 0 7 2 5 16 15 0 -7 5 5 3 -1 0 -14 0 6 14 14 0 -9 2 6 17 17 0 0 4 6 52 -51 0 8 2 5 8 8 0 -6 5 5 4 -2 0 -13 0 6 18 18 0 -8 2 6 14 14 0 1 4 6 32 -33 0 9 2 5 20 -19 0 -5 5 5 31 30 0 -12 0 6 1 2 -1 -7 2 6 1 1 0 2 4 6 8 7 0 10 2 5 27 -27 0 -4 5 5 17 16 0 -11 0 6 13 -12 0 -6 2 6 13 12 0 3 4 6 43 42 0 11 2 5 11 -10 0 -3 5 5 12 -12 0 -10 0 6 42 -41 0 -5 2 6 32 -30 0 4 4 6 43 42 0 -13 3 5 27 -28 0 -2 5 5 10 -9 0 -9 0 6 1 0 -1 -4 2 6 12 -10 0 5 4 6 18 17 0 -12 3 5 24 -23 0 -1 5 5 22 -20 0 -8 0 6 30 31 0 -3 2 6 5 -3 0 6 4 6 8 -8 0 -11 3 5 5 -4 0 0 5 5 12 -12 0 -7 0 6 43 42 0 -2 2 6 6 6 0 7 4 6 13 -12 0 -10 3 5 21 21 0 1 5 5 17 17 0 -6 0 6 28 28 0 -1 2 6 21 -19 0 8 4 6 10 -10 0 -9 3 5 50 48 1 2 5 5 29 28 0 -5 0 6 19 -17 0 0 2 6 11 10 0 9 4 6 5 -5 0 -8 3 5 27 25 0 3 5 5 13 13 0 -4 0 6 7 2 0 1 2 6 37 33 0 -11 5 6 22 23 0 -7 3 5 20 -18 0 4 5 5 12 12 0 -3 0 6 23 18 0 2 2 6 2 2 0 -10 5 6 11 -11 0 -6 3 5 82 -80 1 5 5 5 6 -6 0 -2 0 6 38 35 0 3 2 6 15 14 0 -9 5 6 22 -23 1 -5 3 5 91 -91 1 6 5 5 15 -14 0 -1 0 6 25 27 0 4 2 6 17 -16 0 -8 5 6 23 -24 0 -4 3 5 24 -22 0 7 5 5 1 1 -1 0 0 6 54 -48 0 5 2 6 19 -19 0 -7 5 6 5 5 0 -3 3 5 86 83 0 8 5 5 3 2 0 1 0 6 8 9 0 6 2 6 1 0 -1 -6 5 6 28 28 1 -2 3 5 118 117 0 9 5 5 4 4 0 2 0 6 15 -15 0 7 2 6 9 9 0 -5 5 6 35 35 0 -1 3 5 90 87 1 -10 6 5 11 11 0 3 0 6 31 -32 0 8 2 6 5 -5 0 -4 5 6 8 8 0 0 3 5 50 -48 0 -9 6 5 7 -7 0 4 0 6 29 -29 0 9 2 6 1 -1 -1 -3 5 6 22 -21 0 1 3 5 111 -109 1 -8 6 5 14 -14 0 5 0 6 25 -25 0 10 2 6 1 1 -1 -2 5 6 41 -41 0 2 3 5 55 -53 0 -7 6 5 9 -9 0 6 0 6 7 -7 0 -13 3 6 10 -11 0 -1 5 6 26 -25 0 3 3 5 3 -1 0 -6 6 5 4 5 0 7 0 6 42 42 0 -12 3 6 8 -9 0 0 5 6 30 -30 0 4 3 5 85 82 0 -5 6 5 11 10 0 8 0 6 5 4 0 -11 3 6 9 -9 0 1 5 6 21 20 0 5 3 5 58 57 0 -4 6 5 9 8 0 9 0 6 5 -5 0 -10 3 6 13 13 0 2 5 6 29 28 0 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 2-EtH2-Cu.2H2O PAGE 5 H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S 3 5 6 22 22 0 -1 1 7 53 51 0 7 3 7 23 -24 0 4 6 7 9 -8 0 3 1 8 62 61 0 4 5 6 2 3 0 0 1 7 43 42 0 8 3 7 1 -2 -1 5 6 7 22 -22 0 4 1 8 43 43 0 5 5 6 23 -23 0 1 1 7 20 -19 0 9 3 7 26 27 1 6 6 7 4 -5 0 5 1 8 3 4 0 6 5 6 28 -28 0 2 1 7 27 -26 0 -12 4 7 3 2 0 -7 7 7 25 26 0 6 1 8 9 -9 0 7 5 6 1 1 -1 3 1 7 48 -47 0 -11 4 7 9 -8 0 -6 7 7 17 17 0 7 1 8 32 -33 0 8 5 6 12 13 0 4 1 7 15 -14 0 -10 4 7 17 -18 0 -5 7 7 23 -24 1 8 1 8 2 -1 -1 -10 6 6 13 -14 0 5 1 7 13 13 0 -9 4 7 11 -11 0 -4 7 7 35 -35 0 9 1 8 13 14 0 -9 6 6 3 -3 0 6 1 7 37 36 0 -8 4 7 23 23 0 -3 7 7 19 -19 0 -13 2 8 1 1 -1 -8 6 6 12 13 0 7 1 7 7 -7 0 -7 4 7 25 25 0 -2 7 7 10 10 0 -12 2 8 4 -4 0 -7 6 6 7 6 0 8 1 7 3 -3 1 -6 4 7 13 13 0 -1 7 7 36 36 0 -11 2 8 11 11 0 -6 6 6 16 16 1 9 1 7 21 -22 0 -5 4 7 2 0 0 0 7 7 33 33 0 -10 2 8 5 -5 0 -5 6 6 7 -7 0 10 1 7 9 -9 0 -4 4 7 49 -49 1 1 7 7 6 6 0 -9 2 8 15 -14 0 -4 6 6 17 -18 0 -13 2 7 11 -11 0 -3 4 7 27 -28 0 2 7 7 21 -22 0 -8 2 8 16 -16 0 -3 6 6 10 -10 0 -12 2 7 18 -18 0 -2 4 7 3 -3 0 3 7 7 28 -29 0 -7 2 8 2 2 -1 -2 6 6 11 -11 0 -11 2 7 17 17 0 -1 4 7 10 9 0 4 7 7 10 -9 0 -6 2 8 18 19 0 -1 6 6 12 12 0 -10 2 7 8 8 0 0 4 7 46 46 0 -14 0 8 15 -16 0 -5 2 8 42 40 0 0 6 6 17 16 0 -9 2 7 34 34 0 1 4 7 36 37 0 -13 0 8 20 -21 0 -4 2 8 6 5 0 1 6 6 8 8 0 -8 2 7 9 -8 0 2 4 7 5 -1 0 -12 0 8 35 -34 0 -3 2 8 24 -22 0 2 6 6 5 5 0 -7 2 7 55 -54 0 3 4 7 27 -27 0 -11 0 8 14 14 0 -2 2 8 29 -27 0 3 6 6 15 -15 0 -6 2 7 71 -72 0 4 4 7 39 -39 0 -10 0 8 45 45 0 -1 2 8 22 -21 0 4 6 6 16 -16 0 -5 2 7 30 -31 0 5 4 7 16 -16 0 -9 0 8 31 30 0 0 2 8 6 6 0 5 6 6 1 0 -1 -4 2 7 18 16 0 6 4 7 15 16 0 -8 0 8 7 -6 0 1 2 8 5 5 0 6 6 6 3 -3 0 -3 2 7 133 132 1 7 4 7 32 32 0 -7 0 8 47 -47 0 2 2 8 28 27 0 7 6 6 18 20 1 -2 2 7 44 45 0 8 4 7 14 14 0 -6 0 8 80 -81 0 3 2 8 7 7 0 -8 7 6 8 8 0 -1 2 7 17 13 2 -11 5 7 5 4 0 -5 0 8 6 2 0 4 2 8 6 5 0 -7 7 6 11 11 0 0 2 7 78 -77 0 -10 5 7 11 11 0 -4 0 8 34 33 0 5 2 8 3 -3 0 -6 7 6 2 1 -1 1 2 7 68 -68 0 -9 5 7 12 13 0 -3 0 8 89 88 0 6 2 8 24 -24 0 -5 7 6 8 -8 0 2 2 7 8 -8 0 -8 5 7 8 -8 0 -2 0 8 48 49 0 7 2 8 3 -3 0 -4 7 6 19 -21 0 3 2 7 62 61 0 -7 5 7 16 -17 1 -1 0 8 35 35 0 8 2 8 3 2 1 -3 7 6 2 -1 -1 4 2 7 65 64 0 -6 5 7 18 -18 0 0 0 8 14 -14 0 9 2 8 11 11 1 -2 7 6 5 4 0 5 2 7 49 49 0 -5 5 7 13 -14 0 1 0 8 68 -67 0 -13 3 8 1 1 -1 -1 7 6 18 19 0 6 2 7 17 -16 0 -4 5 7 10 10 0 2 0 8 4 -6 0 -12 3 8 2 1 1 0 7 6 9 -9 0 7 2 7 26 -26 0 -3 5 7 25 24 0 3 0 8 8 8 0 -11 3 8 4 4 0 1 7 6 12 -13 0 8 2 7 40 -40 0 -2 5 7 12 -12 0 4 0 8 15 15 0 -10 3 8 6 6 0 2 7 6 9 -10 0 9 2 7 3 -3 0 -1 5 7 12 12 0 5 0 8 58 58 0 -9 3 8 4 3 0 3 7 6 3 -4 0 10 2 7 10 10 0 0 5 7 27 -27 0 6 0 8 23 -23 0 -8 3 8 15 -15 0 4 7 6 5 6 0 -13 3 7 5 5 0 1 5 7 16 -16 0 7 0 8 5 -5 0 -7 3 8 16 -16 0 5 7 6 8 9 0 -12 3 7 10 10 0 2 5 7 2 1 -1 8 0 8 11 -10 0 -6 3 8 12 -13 0 -3 8 6 23 -24 0 -11 3 7 15 15 0 3 5 7 2 -1 -1 9 0 8 16 -16 0 -5 3 8 6 -5 0 -2 8 6 13 -13 0 -10 3 7 10 10 0 4 5 7 10 10 0 10 0 8 5 -5 0 -4 3 8 23 21 0 -1 8 6 14 15 0 -9 3 7 4 -4 0 5 5 7 13 13 0 -13 1 8 10 -10 0 -3 3 8 11 -10 0 0 8 6 27 28 0 -8 3 7 29 -28 0 6 5 7 1 0 -1 -12 1 8 9 8 0 -2 3 8 12 -10 0 1 8 6 17 18 0 -7 3 7 51 -51 0 7 5 7 2 3 1 -11 1 8 13 12 0 -1 3 8 15 -14 0 -14 1 7 4 4 0 -6 3 7 6 -5 0 -9 6 7 14 -14 0 -10 1 8 19 20 0 0 3 8 5 -5 0 -13 1 7 7 -8 0 -5 3 7 39 38 0 -8 6 7 2 2 -1 -9 1 8 10 10 0 1 3 8 10 9 0 -12 1 7 15 -16 0 -4 3 7 43 42 0 -7 6 7 10 9 0 -8 1 8 38 -38 0 2 3 8 21 20 0 -11 1 7 36 -36 0 -3 3 7 66 65 0 -6 6 7 24 24 0 -7 1 8 57 -56 0 3 3 8 8 8 0 -10 1 7 12 11 0 -2 3 7 77 -75 0 -5 6 7 11 10 0 -6 1 8 35 -35 0 4 3 8 17 16 0 -9 1 7 27 27 0 -1 3 7 77 -75 0 -4 6 7 7 7 0 -5 1 8 4 -3 0 5 3 8 1 1 -1 -8 1 7 37 37 0 0 3 7 57 -56 0 -3 6 7 7 -6 0 -4 1 8 74 72 0 6 3 8 4 0 0 -7 1 7 6 7 0 1 3 7 2 -1 -1 -2 6 7 11 -10 0 -3 1 8 64 63 0 7 3 8 11 -11 0 -6 1 7 17 -16 0 2 3 7 62 61 0 -1 6 7 39 -39 0 -2 1 8 11 10 0 8 3 8 4 -5 0 -5 1 7 44 -41 0 3 3 7 64 63 0 0 6 7 3 1 1 -1 1 8 61 -59 0 9 3 8 3 3 0 -4 1 7 1 -1 -1 4 3 7 15 14 0 1 6 7 1 -2 -1 0 1 8 64 -64 0 -12 4 8 18 18 0 -3 1 7 32 30 0 5 3 7 15 -14 0 2 6 7 17 17 0 1 1 8 36 -36 0 -11 4 8 14 14 0 -2 1 7 28 27 0 6 3 7 37 -37 0 3 6 7 13 14 0 2 1 8 20 21 0 -10 4 8 3 0 1 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 2-EtH2-Cu.2H2O PAGE 6 H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S -9 4 8 18 -18 0 -3 7 8 12 12 0 -8 3 9 13 14 0 -7 6 9 3 -2 0 1 1 10 51 49 0 -8 4 8 27 -28 0 -2 7 8 2 2 -1 -7 3 9 12 13 0 -6 6 9 20 -21 0 2 1 10 13 13 0 -7 4 8 5 5 0 -1 7 8 6 -7 0 -6 3 9 26 27 0 -5 6 9 19 -19 0 3 1 10 17 -17 0 -6 4 8 26 26 0 0 7 8 5 4 0 -5 3 9 30 30 0 -4 6 9 8 -7 0 4 1 10 36 -36 1 -5 4 8 31 32 0 1 7 8 5 -5 0 -4 3 9 12 -13 0 -3 6 9 15 16 0 5 1 10 35 -35 0 -4 4 8 22 22 0 2 7 8 5 -5 0 -3 3 9 32 -32 0 -2 6 9 36 36 0 6 1 10 8 8 0 -3 4 8 50 -50 0 3 7 8 8 9 0 -2 3 9 9 -8 0 -1 6 9 33 32 0 7 1 10 23 23 0 -2 4 8 50 -50 0 -13 1 9 7 -7 0 -1 3 9 35 -33 0 0 6 9 4 4 0 8 1 10 20 21 0 -1 4 8 35 -35 0 -12 1 9 4 -4 0 0 3 9 7 8 0 1 6 9 19 -19 0 -13 2 10 2 0 -1 0 4 8 8 8 0 -11 1 9 21 22 0 1 3 9 27 27 0 2 6 9 31 -31 0 -12 2 10 2 -2 1 1 4 8 30 30 0 -10 1 9 6 -6 0 2 3 9 4 4 0 3 6 9 15 -16 0 -11 2 10 16 -16 0 2 4 8 41 40 0 -9 1 9 2 1 -1 3 3 9 5 4 0 4 6 9 6 6 0 -10 2 10 4 -3 0 3 4 8 10 -10 0 -8 1 9 9 -10 0 4 3 9 25 -25 0 -6 7 9 26 -27 0 -9 2 10 5 6 1 4 4 8 23 -22 0 -7 1 9 27 -26 0 5 3 9 23 -24 0 -5 7 9 4 -3 0 -8 2 10 16 15 0 5 4 8 35 -35 0 -6 1 9 7 -4 1 6 3 9 4 -4 0 -4 7 9 21 22 0 -7 2 10 7 6 0 6 4 8 15 -14 0 -5 1 9 13 -13 0 7 3 9 13 13 0 -3 7 9 38 39 0 -6 2 10 11 -11 0 7 4 8 9 9 0 -4 1 9 2 1 -1 8 3 9 20 21 0 -2 7 9 21 22 0 -5 2 10 7 -7 0 8 4 8 28 31 0 -3 1 9 24 24 0 -12 4 9 11 -10 0 -1 7 9 11 -11 0 -4 2 10 14 -13 0 -11 5 8 22 -22 0 -2 1 9 15 15 0 -11 4 9 16 -15 0 0 7 9 34 -36 0 -3 2 10 13 13 0 -10 5 8 17 -17 0 -1 1 9 15 13 0 -10 4 9 2 2 -1 1 7 9 23 -24 0 -2 2 10 7 7 0 -9 5 8 5 6 0 0 1 9 21 -21 0 -9 4 9 4 4 0 -13 0 10 11 -10 0 -1 2 10 5 -4 0 -8 5 8 25 25 1 1 1 9 4 2 0 -8 4 9 17 16 0 -12 0 10 42 43 0 0 2 10 10 10 0 -7 5 8 30 30 0 2 1 9 5 5 0 -7 4 9 22 22 0 -11 0 10 6 6 0 1 2 10 3 1 0 -6 5 8 13 13 0 3 1 9 20 20 0 -6 4 9 11 -11 1 -10 0 10 25 25 0 2 2 10 5 -5 0 -5 5 8 14 -14 0 4 1 9 18 18 0 -5 4 9 19 -19 0 -9 0 10 23 -24 0 3 2 10 10 -9 0 -4 5 8 28 -27 0 5 1 9 1 0 -1 -4 4 9 13 -13 0 -8 0 10 56 -56 0 4 2 10 9 -8 0 -3 5 8 13 -11 0 6 1 9 6 -5 0 -3 4 9 24 -24 0 -7 0 10 47 -47 0 5 2 10 4 -5 0 -2 5 8 5 -5 0 7 1 9 1 2 -1 -2 4 9 29 29 0 -6 0 10 5 -5 0 6 2 10 17 18 0 -1 5 8 36 35 0 8 1 9 3 -2 1 -1 4 9 32 33 0 -5 0 10 29 29 0 7 2 10 10 10 0 0 5 8 36 35 0 9 1 9 6 -6 0 0 4 9 7 -6 0 -4 0 10 69 69 1 8 2 10 1 -1 -1 1 5 8 4 1 1 -13 2 9 2 2 0 1 4 9 11 -11 0 -3 0 10 17 18 0 -12 3 10 2 1 0 2 5 8 23 -22 0 -12 2 9 20 20 0 2 4 9 29 -29 0 -2 0 10 33 -34 0 -11 3 10 4 -3 0 3 5 8 37 -37 0 -11 2 9 19 20 0 3 4 9 7 -8 0 -1 0 10 100 -100 1 -10 3 10 7 -7 1 4 5 8 28 -28 0 -10 2 9 16 16 0 4 4 9 22 23 0 0 0 10 15 -16 0 -9 3 10 5 -5 0 5 5 8 14 14 0 -9 2 9 27 -28 0 5 4 9 19 19 0 1 0 10 11 11 0 -8 3 10 7 8 0 6 5 8 18 17 0 -8 2 9 39 -39 0 6 4 9 4 2 1 2 0 10 63 64 0 -7 3 10 17 18 0 7 5 8 15 15 0 -7 2 9 33 -33 0 7 4 9 13 -14 0 3 0 10 62 62 0 -6 3 10 7 6 0 -9 6 8 14 13 0 -6 2 9 5 6 0 -10 5 9 7 -7 0 4 0 10 11 10 0 -5 3 10 5 5 0 -8 6 8 1 1 -1 -5 2 9 46 46 0 -9 5 9 12 -13 0 5 0 10 29 -29 0 -4 3 10 17 -17 0 -7 6 8 6 -6 0 -4 2 9 33 34 0 -8 5 9 16 18 1 6 0 10 2 0 -2 -3 3 10 16 -15 0 -6 6 8 25 -25 0 -3 2 9 12 -11 0 -7 5 9 23 22 0 7 0 10 34 -35 0 -2 3 10 11 -10 0 -5 6 8 7 -6 0 -2 2 9 48 -48 0 -6 5 9 26 27 0 8 0 10 8 8 0 -1 3 10 16 -16 0 -4 6 8 9 9 0 -1 2 9 69 -68 0 -5 5 9 2 -1 -1 -13 1 10 15 15 0 0 3 10 8 -8 0 -3 6 8 20 20 0 0 2 9 23 -24 0 -4 5 9 30 -30 0 -12 1 10 22 23 0 1 3 10 4 4 0 -2 6 8 22 21 0 1 2 9 20 21 0 -3 5 9 36 -36 0 -11 1 10 15 15 0 2 3 10 12 11 0 -1 6 8 6 -7 0 2 2 9 43 43 0 -2 5 9 13 -12 0 -10 1 10 20 -20 0 3 3 10 8 8 0 0 6 8 12 -13 0 3 2 9 39 39 0 -1 5 9 11 11 0 -9 1 10 29 -28 0 4 3 10 4 -3 0 1 6 8 25 -26 0 4 2 9 5 -4 1 0 5 9 40 41 0 -8 1 10 17 -18 0 5 3 10 14 -14 0 2 6 8 6 -5 0 5 2 9 23 -23 0 1 5 9 20 19 0 -7 1 10 13 13 0 6 3 10 8 -9 0 3 6 8 9 9 0 6 2 9 23 -23 0 2 5 9 8 -8 0 -6 1 10 46 46 0 7 3 10 4 3 0 4 6 8 11 11 0 7 2 9 1 0 -1 3 5 9 24 -24 0 -5 1 10 34 33 0 -11 4 10 14 -13 1 5 6 8 15 16 0 8 2 9 21 21 0 4 5 9 39 -39 0 -4 1 10 21 -19 0 -10 4 10 8 -9 0 -7 7 8 1 -1 -1 -12 3 9 6 5 0 5 5 9 7 -6 0 -3 1 10 53 -53 0 -9 4 10 26 28 1 -6 7 8 11 -11 0 -11 3 9 2 -1 0 6 5 9 10 10 0 -2 1 10 50 -48 0 -8 4 10 36 35 0 -5 7 8 1 -1 -1 -10 3 9 10 -11 0 -9 6 9 24 24 0 -1 1 10 21 -20 0 -7 4 10 28 29 0 -4 7 8 6 6 0 -9 3 9 24 -25 0 -8 6 9 15 15 0 0 1 10 33 33 0 -6 4 10 6 -7 0 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 2-EtH2-Cu.2H2O PAGE 7 H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S H K L FO FC S -5 4 10 27 -27 0 -1 1 11 31 -30 0 -3 4 11 41 40 0 -8 1 12 48 49 0 -5 4 12 4 3 0 -4 4 10 54 -54 0 0 1 11 13 14 0 -2 4 11 3 -1 0 -7 1 12 12 12 0 -4 4 12 11 11 0 -3 4 10 17 18 0 1 1 11 26 25 0 -1 4 11 16 -15 0 -6 1 12 30 -29 0 -3 4 12 23 22 0 -2 4 10 10 10 0 2 1 11 21 20 0 0 4 11 34 -34 1 -5 1 12 56 -55 0 -2 4 12 27 27 0 -1 4 10 53 53 0 3 1 11 13 12 0 1 4 11 20 -20 0 -4 1 12 37 -37 0 -1 4 12 2 0 -1 0 4 10 31 30 0 4 1 11 26 -26 0 2 4 11 19 20 0 -3 1 12 15 15 0 0 4 12 17 -16 0 1 4 10 12 -12 0 5 1 11 4 5 0 3 4 11 19 20 0 -2 1 12 60 59 0 1 4 12 10 -9 0 2 4 10 35 -35 0 6 1 11 13 -13 0 4 4 11 10 10 0 -1 1 12 60 60 0 2 4 12 12 -13 0 3 4 10 35 -35 0 7 1 11 3 3 0 5 4 11 2 1 -1 0 1 12 8 8 0 3 4 12 19 20 0 4 4 10 22 -22 0 -12 2 11 3 2 0 -9 5 11 12 13 0 1 1 12 34 -33 0 4 4 12 16 16 0 5 4 10 16 16 0 -11 2 11 13 -14 0 -8 5 11 4 4 0 2 1 12 53 -54 0 -9 5 12 12 -11 0 6 4 10 18 19 0 -10 2 11 23 -23 0 -7 5 11 2 1 -1 3 1 12 39 -38 0 -8 5 12 29 -29 0 -10 5 10 22 21 0 -9 2 11 5 -5 0 -6 5 11 2 -2 0 4 1 12 13 13 0 -7 5 12 17 -16 0 -9 5 10 16 16 0 -8 2 11 25 25 0 -5 5 11 18 -19 0 5 1 12 26 26 0 -6 5 12 2 -1 -1 -8 5 10 3 2 1 -7 2 11 43 42 0 -4 5 11 11 11 0 6 1 12 21 21 0 -5 5 12 29 29 0 -7 5 10 27 -27 0 -6 2 11 30 29 0 -3 5 11 5 4 1 -12 2 12 5 5 0 -4 5 12 34 34 0 -6 5 10 39 -39 0 -5 2 11 2 -1 -1 -2 5 11 20 21 0 -11 2 12 17 19 0 -3 5 12 8 -8 0 -5 5 10 15 -14 0 -4 2 11 45 -43 0 -1 5 11 8 7 0 -10 2 12 12 12 0 -2 5 12 30 -30 0 -4 5 10 11 11 0 -3 2 11 41 -39 0 0 5 11 3 3 0 -9 2 12 14 -15 0 -1 5 12 30 -31 0 -3 5 10 51 51 0 -2 2 11 20 -19 0 1 5 11 16 -16 0 -8 2 12 13 -13 0 0 5 12 11 -11 0 -2 5 10 52 51 0 -1 2 11 16 16 0 2 5 11 8 -8 0 -7 2 12 15 -16 0 1 5 12 24 25 0 -1 5 10 5 -4 0 0 2 11 42 42 0 3 5 11 2 -1 -1 -6 2 12 4 -4 0 2 5 12 28 29 0 0 5 10 31 -30 0 1 2 11 27 26 0 4 5 11 8 9 0 -5 2 12 16 16 0 -6 6 12 23 23 0 1 5 10 38 -38 0 2 2 11 18 -18 0 -7 6 11 19 -19 0 -4 2 12 9 9 0 -5 6 12 8 8 0 2 5 10 14 -14 0 3 2 11 37 -37 0 -6 6 11 3 -4 0 -3 2 12 3 -3 1 -4 6 12 12 -11 0 3 5 10 25 26 0 4 2 11 43 -43 0 -5 6 11 6 6 0 -2 2 12 9 9 0 -3 6 12 30 -32 0 4 5 10 27 27 1 5 2 11 7 -7 0 -4 6 11 23 24 0 -1 2 12 8 8 0 -2 6 12 13 -14 0 5 5 10 13 13 1 6 2 11 18 19 0 -3 6 11 17 17 0 0 2 12 14 -13 0 -1 6 12 7 8 0 -8 6 10 22 -22 0 7 2 11 25 26 1 -2 6 11 4 -4 0 1 2 12 6 -5 0 0 6 12 17 18 0 -7 6 10 18 -18 0 -12 3 11 10 -10 0 -1 6 11 21 -22 0 2 2 12 13 -13 0 -12 1 13 5 5 0 -6 6 10 1 1 -1 -11 3 11 2 -1 -1 0 6 11 11 -12 0 3 2 12 5 -5 0 -11 1 13 17 -17 0 -5 6 10 27 28 0 -10 3 11 20 20 0 1 6 11 7 7 0 4 2 12 16 17 0 -10 1 13 7 -7 0 -4 6 10 25 25 0 -9 3 11 15 15 0 2 6 11 15 16 0 5 2 12 9 9 0 -9 1 13 14 13 0 -3 6 10 16 16 0 -8 3 11 4 -4 0 -12 0 12 4 -4 0 6 2 12 2 -2 -1 -8 1 13 21 22 0 -2 6 10 18 -19 0 -7 3 11 6 -7 0 -11 0 12 10 -12 0 -11 3 12 5 -5 0 -7 1 13 27 27 0 -1 6 10 32 -34 0 -6 3 11 17 -16 0 -10 0 12 42 -43 0 -10 3 12 3 2 0 -6 1 13 7 7 0 0 6 10 17 -17 0 -5 3 11 7 -6 0 -9 0 12 20 -20 0 -9 3 12 8 8 0 -5 1 13 30 -29 0 1 6 10 2 2 0 -4 3 11 36 36 0 -8 0 12 25 25 0 -8 3 12 2 1 1 -4 1 13 35 -35 0 2 6 10 20 21 0 -3 3 11 8 -7 0 -7 0 12 48 48 0 -7 3 12 5 5 0 -3 1 13 13 -13 0 3 6 10 23 24 0 -2 3 11 21 20 0 -6 0 12 76 76 0 -6 3 12 7 7 0 -2 1 13 27 27 0 -4 7 10 1 1 -1 -1 3 11 5 4 0 -5 0 12 11 11 0 -5 3 12 3 3 1 -1 1 13 20 20 0 -3 7 10 3 -2 0 0 3 11 1 0 -1 -4 0 12 67 -66 0 -4 3 12 16 16 1 0 1 13 15 15 0 -2 7 10 4 4 0 1 3 11 3 -1 0 -3 0 12 99 -98 0 -3 3 12 5 -5 0 1 1 13 12 -12 0 -1 7 10 3 -4 0 2 3 11 11 -10 0 -2 0 12 60 -60 0 -2 3 12 14 -15 0 2 1 13 30 -30 0 -13 1 11 20 21 0 3 3 11 18 -18 0 -1 0 12 22 21 0 -1 3 12 7 7 0 3 1 13 16 -16 0 -12 1 11 4 4 0 4 3 11 3 3 0 0 0 12 60 59 0 0 3 12 1 -1 -1 4 1 13 1 -2 -1 -11 1 11 9 9 0 5 3 11 8 7 0 1 0 12 64 63 0 1 3 12 3 4 1 5 1 13 2 -2 -1 -10 1 11 1 -1 -1 6 3 11 13 13 0 2 0 12 3 -1 -1 2 3 12 2 2 -1 -11 2 13 3 -3 0 -9 1 11 18 -18 0 -11 4 11 3 3 0 3 0 12 44 -44 0 3 3 12 16 -17 0 -10 2 13 22 22 0 -8 1 11 24 -25 0 -10 4 11 12 11 0 4 0 12 32 -33 0 4 3 12 5 -6 0 -9 2 13 22 23 0 -7 1 11 2 2 1 -9 4 11 17 18 0 5 0 12 32 -33 0 5 3 12 1 0 -1 -8 2 13 11 11 0 -6 1 11 4 3 0 -8 4 11 6 -5 0 6 0 12 16 16 0 -10 4 12 19 19 0 -7 2 13 10 -10 0 -5 1 11 39 38 0 -7 4 11 20 -20 0 -12 1 12 25 -24 0 -9 4 12 5 4 0 -6 2 13 27 -26 1 -4 1 11 7 7 0 -6 4 11 18 -18 0 -11 1 12 12 -13 0 -8 4 12 2 2 0 -5 2 13 18 -18 0 -3 1 11 24 -25 0 -5 4 11 14 -15 0 -10 1 12 6 6 0 -7 4 12 15 -16 0 -4 2 13 16 15 0 -2 1 11 50 -49 0 -4 4 11 33 33 0 -9 1 12 37 37 0 -6 4 12 22 -22 0 -3 2 13 18 18 0 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 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