SUBMISSION: DU1125 (JARDIN, GAO, GUERY & JACOBONI) OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 1 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 1 0 0 91 90 9 2 0 10 11 6 5 0 13 13 6 8 0 10 10 9 11 0 12 11 2 0 0 31 32 10 2 0 17 18 8 5 0 37 -37 7 8 0 17 17 11 11 0 6 -6 3 0 0 36 -43 11 2 0 9 8 9 5 0 30 -31 8 8 0 6 7 0 12 0 76 74 4 0 0 59 -64 12 2 0 8 -7 11 5 0 9 8 9 8 0 12 -12 1 12 0 21 22 5 0 0 53 -52 13 2 0 12 -12 12 5 0 6 6 10 8 0 16 -16 2 12 0 19 -17 6 0 0 27 29 14 2 0 4 -4 0 6 0 115 -121 13 8 0 9 9 3 12 0 36 -37 7 0 0 12 11 1 3 0 45 40 1 6 0 78 -74 14 8 0 5 4 4 12 0 11 -11 8 0 0 13 14 2 3 0 60 63 2 6 0 12 14 1 9 0 19 -18 5 12 0 14 -15 9 0 0 18 -19 3 3 0 10 -7 3 6 0 65 62 2 9 0 45 -43 6 12 0 21 21 10 0 0 18 -18 4 3 0 62 -62 4 6 0 16 18 3 9 0 9 -7 7 12 0 17 18 11 0 0 10 -10 5 3 0 28 -30 5 6 0 11 10 4 9 0 13 14 8 12 0 5 5 12 0 0 7 7 6 3 0 23 -22 6 6 0 22 -23 5 9 0 12 11 9 12 0 9 -9 13 0 0 9 9 8 3 0 21 21 7 6 0 33 -34 7 9 0 5 -4 10 12 0 9 -10 14 0 0 5 5 9 3 0 16 17 8 6 0 22 -23 8 9 0 19 -18 11 12 0 7 -7 1 1 0 109 -107 11 3 0 9 -8 9 6 0 17 17 9 9 0 15 -15 1 13 0 35 -33 2 1 0 115 -114 12 3 0 10 -9 10 6 0 17 18 11 9 0 10 10 2 13 0 20 -18 3 1 0 36 33 0 4 0 130 126 11 6 0 9 9 12 9 0 6 6 4 13 0 16 15 4 1 0 14 14 1 4 0 117 112 14 6 0 7 -6 0 10 0 82 -77 5 13 0 24 26 5 1 0 30 33 2 4 0 26 -29 1 7 0 44 42 1 10 0 81 -76 6 13 0 7 7 6 1 0 22 23 3 4 0 63 -65 2 7 0 54 58 2 10 0 17 18 7 13 0 5 -5 7 1 0 10 -12 4 4 0 21 -22 3 7 0 20 16 3 10 0 20 19 8 13 0 14 -14 8 1 0 21 -22 5 4 0 7 -8 4 7 0 40 -41 4 10 0 27 25 9 13 0 10 -10 9 1 0 20 -20 6 4 0 15 16 5 7 0 40 -40 5 10 0 8 7 12 13 0 6 5 11 1 0 16 16 7 4 0 36 38 6 7 0 19 -19 7 10 0 20 -21 0 14 0 52 -50 12 1 0 8 8 8 4 0 6 5 7 7 0 11 -13 9 10 0 12 12 1 14 0 20 -21 15 1 0 5 -4 9 4 0 9 -8 8 7 0 17 18 10 10 0 12 14 2 14 0 16 17 0 2 0 118 -113 10 4 0 20 -19 9 7 0 23 25 13 10 0 7 -8 3 14 0 15 14 1 2 0 53 -54 11 4 0 8 -8 11 7 0 11 -10 1 11 0 49 48 4 14 0 19 19 2 2 0 98 91 13 4 0 9 8 0 8 0 89 91 2 11 0 40 39 6 14 0 18 -18 3 2 0 13 12 1 5 0 45 -41 1 8 0 41 41 3 11 0 4 6 7 14 0 11 -11 4 2 0 53 54 2 5 0 19 -23 2 8 0 8 5 4 11 0 19 -19 10 14 0 10 10 5 2 0 7 -9 3 5 0 23 22 3 8 0 47 -47 5 11 0 10 -10 1 15 0 23 25 6 2 0 24 -25 4 5 0 52 53 4 8 0 34 -34 6 11 0 21 -21 2 15 0 7 7 7 2 0 24 -25 5 5 0 22 22 5 8 0 4 -4 8 11 0 15 16 3 15 0 6 -5 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 2 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 4 15 0 14 -14 2 21 0 6 -7 13 0 1 7 7 -2 2 1 30 30 10 3 1 10 -9 5 15 0 15 -15 0 22 0 9 -10 -13 1 1 7 -7 -1 2 1 93 -89 11 3 1 5 -5 7 15 0 6 6 1 22 0 6 -6 -12 1 1 16 -15 0 2 1 60 -52 13 3 1 6 5 8 15 0 8 8 2 22 0 5 5 -10 1 1 15 15 1 2 1 15 16 -14 4 1 8 8 9 15 0 9 9 0 24 0 9 8 -9 1 1 23 23 3 2 1 32 30 -13 4 1 10 9 0 16 0 34 33 3 24 0 6 -6 -8 1 1 16 15 4 2 1 29 28 -12 4 1 8 -7 1 16 0 9 10 2 25 0 5 -4 -7 1 1 4 -3 5 2 1 19 -19 -11 4 1 13 -13 2 16 0 18 -18 0 26 0 6 -5 -6 1 1 29 -31 6 2 1 47 -49 -10 4 1 12 -12 3 16 0 12 -13 -15 0 1 5 5 -5 1 1 35 -33 7 2 1 10 -10 -8 4 1 26 26 4 16 0 10 -10 -14 0 1 11 10 -4 1 1 17 -21 8 2 1 14 14 -7 4 1 27 27 6 16 0 7 8 -13 0 1 6 5 -3 1 1 56 55 9 2 1 16 16 -6 4 1 15 15 7 16 0 10 11 -11 0 1 26 -25 -2 1 1 37 36 10 2 1 10 10 -5 4 1 14 -15 10 16 0 8 -8 -10 0 1 17 -16 -1 1 1 44 39 12 2 1 10 -10 -4 4 1 92 -93 1 17 0 18 -17 -9 0 1 4 4 0 1 1 78 -75 -13 3 1 9 9 -3 4 1 55 -55 2 17 0 19 -17 -8 0 1 10 11 1 1 1 13 -10 -12 3 1 12 11 -2 4 1 19 15 4 17 0 9 9 -7 0 1 18 16 2 1 1 21 -17 -10 3 1 15 -16 -1 4 1 89 85 5 17 0 9 9 -6 0 1 22 22 3 1 1 18 -18 -9 3 1 16 -15 0 4 1 31 26 6 17 0 7 7 -5 0 1 88 -87 4 1 1 25 23 -8 3 1 25 -25 2 4 1 34 -32 8 17 0 8 -8 -4 0 1 6 0 5 1 1 51 51 -7 3 1 8 7 3 4 1 17 -19 9 17 0 7 -6 -3 0 1 41 -42 7 1 1 23 -23 -6 3 1 29 31 4 4 1 16 -15 0 18 0 28 -29 -2 0 1 42 37 8 1 1 26 -26 -5 3 1 72 70 5 4 1 19 18 1 18 0 19 -19 -1 0 1 167 165 10 1 1 12 12 -4 3 1 29 30 6 4 1 31 31 3 18 0 17 17 0 0 1 106 100 11 1 1 9 9 -3 3 1 53 -54 7 4 1 17 17 4 18 0 10 10 1 0 1 103 -108 14 1 1 6 -5 -2 3 1 117 -116 8 4 1 23 -23 7 18 0 8 -8 2 0 1 33 -30 -14 2 1 12 -11 -1 3 1 11 11 9 4 1 19 -19 1 19 0 9 9 3 0 1 53 -53 -13 2 1 11 -10 0 3 1 135 -137 10 4 1 9 -9 2 19 0 16 17 4 0 1 98 -96 -12 2 1 7 6 1 3 1 9 3 12 4 1 8 8 3 19 0 6 7 6 0 1 44 44 -11 2 1 19 19 2 3 1 10 -12 -12 5 1 7 -6 4 19 0 7 -7 7 0 1 5 5 -10 2 1 19 19 3 3 1 15 -15 -10 5 1 18 18 0 20 0 16 16 8 0 1 20 -22 -7 2 1 29 -28 4 3 1 36 -36 -9 5 1 29 28 1 20 0 11 11 9 0 1 21 -20 -6 2 1 9 -10 5 3 1 17 -18 -8 5 1 8 8 3 20 0 12 -12 10 0 1 12 -12 -5 2 1 52 47 7 3 1 31 31 -7 5 1 10 -10 4 20 0 5 -7 11 0 1 6 6 -4 2 1 80 78 8 3 1 15 15 -6 5 1 37 -38 1 21 0 7 -6 12 0 1 9 9 -3 2 1 22 20 9 3 1 7 7 -5 5 1 59 -60 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 3 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -4 5 1 76 -75 13 6 1 6 -5 2 8 1 30 -29 -3 10 1 24 23 -4 12 1 35 -34 -3 5 1 50 48 -12 7 1 7 7 3 8 1 23 -25 -2 10 1 40 -39 -3 12 1 28 -28 -2 5 1 74 69 -10 7 1 12 -11 4 8 1 10 -11 -1 10 1 72 -69 -2 12 1 12 14 -1 5 1 19 -21 -9 7 1 23 -24 5 8 1 18 18 0 10 1 34 -34 -1 12 1 47 46 0 5 1 21 -14 -6 7 1 28 28 6 8 1 19 19 1 10 1 6 7 0 12 1 31 30 2 5 1 8 7 -5 7 1 59 57 7 8 1 8 8 2 10 1 34 33 1 12 1 17 -15 3 5 1 44 41 -4 7 1 20 18 8 8 1 11 -10 3 10 1 24 24 2 12 1 17 -18 4 5 1 26 28 -3 7 1 73 -75 9 8 1 15 -15 4 10 1 21 22 3 12 1 11 -11 5 5 1 22 21 -2 7 1 66 -62 10 8 1 9 -8 5 10 1 6 6 4 12 1 12 -13 7 5 1 32 -32 -1 7 1 27 -23 -13 9 1 8 -8 6 10 1 22 -22 5 12 1 16 15 8 5 1 30 -30 0 7 1 40 35 -12 9 1 7 -7 8 10 1 11 11 6 12 1 30 30 10 5 1 11 11 1 7 1 7 -9 -11 9 1 7 -7 9 10 1 12 12 7 12 1 10 10 11 5 1 6 6 2 7 1 13 12 -10 9 1 10 10 -12 11 1 9 9 8 12 1 12 -11 -14 6 1 8 -8 3 7 1 27 -30 -9 9 1 16 16 -9 11 1 15 -16 9 12 1 12 -11 -11 6 1 14 14 4 7 1 39 -39 -8 9 1 18 18 -8 11 1 6 -5 10 12 1 8 -6 -10 6 1 16 16 5 7 1 18 -18 -5 9 1 49 -50 -6 11 1 15 17 -12 13 1 7 -6 -8 6 1 25 -24 6 7 1 8 8 -4 9 1 9 -9 -5 11 1 22 22 -10 13 1 10 10 -7 6 1 17 -18 7 7 1 10 10 -3 9 1 31 31 -4 11 1 13 12 -9 13 1 10 10 -6 6 1 8 -8 8 7 1 30 31 -2 9 1 42 43 -3 11 1 33 -33 -8 13 1 6 6 -5 6 1 21 21 10 7 1 9 -9 0 9 1 18 -18 -2 11 1 49 -48 -6 13 1 27 -27 -4 6 1 93 87 -14 8 1 11 9 1 9 1 24 -25 0 11 1 19 21 -5 13 1 20 -21 -3 6 1 78 72 -11 8 1 14 -14 2 9 1 15 -20 1 11 1 23 20 -4 13 1 7 -7 -2 6 1 44 -39 -10 8 1 13 -13 3 9 1 4 -4 3 11 1 11 -12 -3 13 1 23 21 -1 6 1 84 -81 -9 8 1 7 -6 4 9 1 28 27 4 11 1 13 -13 -2 13 1 21 20 0 6 1 34 -34 -8 8 1 7 7 6 9 1 6 7 5 11 1 19 -19 -1 13 1 13 15 1 6 1 51 51 -7 8 1 11 12 7 9 1 12 -11 6 11 1 6 -7 0 13 1 19 -19 2 6 1 39 38 -6 8 1 14 15 8 9 1 11 -12 7 11 1 21 21 1 13 1 6 -6 3 6 1 41 42 -5 8 1 28 -31 10 9 1 11 10 8 11 1 14 14 2 13 1 6 -6 5 6 1 17 -18 -4 8 1 59 -58 -14 10 1 8 -7 11 11 1 5 -6 3 13 1 11 10 6 6 1 41 -42 -3 8 1 52 -49 -13 10 1 8 -7 -13 12 1 5 5 4 13 1 15 15 7 6 1 18 -19 -2 8 1 55 52 -11 10 1 12 12 -11 12 1 12 -12 5 13 1 20 22 8 6 1 13 13 -1 8 1 63 63 -10 10 1 15 15 -8 12 1 10 11 6 13 1 7 -6 9 6 1 23 24 0 8 1 36 37 -7 10 1 22 -22 -7 12 1 11 12 7 13 1 16 -16 10 6 1 8 8 1 8 1 18 15 -4 10 1 36 37 -5 12 1 28 -26 8 13 1 11 -12 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 4 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 11 13 1 6 7 -4 16 1 18 -19 -9 19 1 6 -7 -12 0 2 11 -11 -2 1 2 43 -43 -11 14 1 9 9 -3 16 1 17 -17 -6 19 1 7 7 -11 0 2 16 -17 -1 1 2 66 -66 -8 14 1 7 -7 -1 16 1 24 23 -5 19 1 9 8 -10 0 2 5 -5 0 1 2 65 -64 -7 14 1 19 -18 0 16 1 12 13 -3 19 1 17 -17 -9 0 2 7 8 2 1 2 5 4 -6 14 1 13 -11 1 16 1 6 -6 -2 19 1 9 -9 -8 0 2 14 15 3 1 2 41 42 -5 14 1 21 20 2 16 1 6 -5 0 19 1 7 7 -7 0 2 43 43 4 1 2 58 58 -4 14 1 23 23 4 16 1 6 -6 1 19 1 12 11 -6 0 2 26 -24 5 1 2 17 17 -3 14 1 10 11 5 16 1 10 9 2 19 1 10 11 -5 0 2 47 -53 6 1 2 24 -24 -1 14 1 29 -28 6 16 1 16 16 4 19 1 8 -8 -4 0 2 12 16 7 1 2 7 -8 0 14 1 20 -19 7 16 1 6 6 5 19 1 4 -5 -3 0 2 40 39 9 1 2 7 7 1 14 1 14 12 9 16 1 6 -7 7 19 1 6 4 -1 0 2 95 95 10 1 2 7 8 3 14 1 15 14 -9 17 1 8 8 -5 20 1 5 -5 0 0 2 173 -177 13 1 2 7 -6 4 14 1 12 11 -6 17 1 7 -8 -4 20 1 12 -12 1 0 2 62 -64 -15 2 2 8 -8 5 14 1 15 -16 -5 17 1 12 -12 -3 20 1 6 -6 2 0 2 14 -17 -14 2 2 10 -9 6 14 1 18 -19 -3 17 1 17 16 -2 20 1 11 10 3 0 2 39 -43 -12 2 2 11 11 9 14 1 11 10 -2 17 1 17 17 -1 20 1 14 14 4 0 2 7 5 -11 2 2 13 13 10 14 1 6 7 0 17 1 10 -9 0 20 1 9 8 5 0 2 64 66 -10 2 2 7 8 -10 15 1 9 -9 1 17 1 8 -7 2 20 1 9 -8 6 0 2 10 9 -8 2 2 22 -22 -9 15 1 7 -7 3 17 1 5 5 3 20 1 10 -9 7 0 2 12 -12 -7 2 2 26 -28 -8 15 1 6 -5 4 17 1 10 10 6 20 1 6 5 8 0 2 18 -19 -6 2 2 26 28 -6 15 1 14 15 5 17 1 9 10 -5 21 1 7 -8 11 0 2 11 9 -5 2 2 86 86 -5 15 1 25 25 7 17 1 9 -10 -3 21 1 7 8 12 0 2 11 10 -4 2 2 26 -24 -3 15 1 4 -3 8 17 1 7 -7 -2 21 1 10 10 13 0 2 5 3 -3 2 2 50 -49 -2 15 1 21 -21 -8 18 1 6 -6 -4 22 1 9 9 -13 1 2 8 -8 -2 2 2 123 -121 -1 15 1 10 -9 -7 18 1 8 -8 -3 22 1 7 7 -12 1 2 8 -8 -1 2 2 86 -83 2 15 1 8 -9 -5 18 1 6 8 -1 22 1 10 -11 -11 1 2 8 8 0 2 2 48 -49 4 15 1 14 -14 -4 18 1 17 16 0 22 1 6 -5 -10 1 2 11 10 1 2 2 45 48 5 15 1 9 -10 -3 18 1 7 8 -5 23 1 7 6 -9 1 2 14 13 2 2 2 32 31 7 15 1 13 12 -2 18 1 16 -16 -2 23 1 6 -7 -8 1 2 8 10 3 2 2 37 39 8 15 1 8 9 -1 18 1 20 -21 -4 24 1 6 -7 -7 1 2 25 -29 4 2 2 20 -24 -11 16 1 7 -7 0 18 1 11 -11 -1 24 1 6 6 -6 1 2 55 -56 5 2 2 42 -44 -10 16 1 8 -7 2 18 1 14 14 2 24 1 5 -5 -5 1 2 6 7 6 2 2 21 -22 -7 16 1 9 9 3 18 1 13 14 -15 0 2 9 8 -4 1 2 28 28 7 2 2 15 14 -5 16 1 12 -12 6 18 1 11 -12 -14 0 2 7 7 -3 1 2 61 62 8 2 2 9 9 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 5 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 9 2 2 6 6 -1 4 2 12 -8 -10 6 2 5 5 5 7 2 11 11 -5 9 2 13 -15 11 2 2 7 -6 0 4 2 23 23 -9 6 2 18 -18 6 7 2 20 20 -4 9 2 19 19 12 2 2 7 -7 1 4 2 17 17 -8 6 2 16 -15 7 7 2 18 18 -3 9 2 14 17 -13 3 2 12 11 2 4 2 38 -39 -6 6 2 23 24 8 7 2 6 7 -2 9 2 19 -19 -10 3 2 11 -10 3 4 2 6 5 -5 6 2 40 40 9 7 2 11 -11 -1 9 2 25 -26 -9 3 2 23 -22 4 4 2 27 26 -4 6 2 42 42 10 7 2 7 -7 0 9 2 13 -13 -8 3 2 13 -13 5 4 2 40 42 -3 6 2 32 -33 13 7 2 6 4 1 9 2 59 -58 -7 3 2 40 39 6 4 2 25 26 -2 6 2 64 -62 -15 8 2 8 7 2 9 2 11 -11 -6 3 2 45 45 7 4 2 23 -23 0 6 2 10 -7 -14 8 2 8 7 3 9 2 39 39 -5 3 2 54 52 8 4 2 12 -13 1 6 2 19 19 -12 8 2 8 -8 4 9 2 36 35 -4 3 2 37 -37 9 4 2 10 -10 2 6 2 46 44 -11 8 2 11 -11 5 9 2 10 10 -3 3 2 4 1 11 4 2 7 6 3 6 2 13 13 -10 8 2 7 -7 7 9 2 8 -8 -2 3 2 22 22 12 4 2 7 7 4 6 2 28 -30 -8 8 2 23 23 9 9 2 6 5 -1 3 2 4 1 -10 5 2 10 10 5 6 2 51 -53 -7 8 2 10 9 -14 10 2 8 -8 0 3 2 14 -19 -9 5 2 8 7 6 6 2 16 -17 -6 8 2 11 -9 -12 10 2 11 10 1 3 2 55 54 -8 5 2 27 -27 7 6 2 11 11 -5 8 2 37 -38 -11 10 2 11 10 3 3 2 28 -32 -7 5 2 34 -34 8 6 2 22 22 -4 8 2 13 -12 -10 10 2 9 9 4 3 2 32 -33 -6 5 2 46 -47 9 6 2 8 9 -3 8 2 42 42 -8 10 2 23 -22 5 3 2 9 8 -5 5 2 37 -39 11 6 2 6 -6 -2 8 2 29 25 -7 10 2 9 -8 6 3 2 17 17 -4 5 2 32 33 -14 7 2 7 6 -1 8 2 33 35 -5 10 2 25 26 7 3 2 17 16 -3 5 2 59 59 -10 7 2 18 -18 0 8 2 22 17 -4 10 2 9 8 10 3 2 5 -5 -2 5 2 9 6 -9 7 2 10 -10 2 8 2 48 -49 -3 10 2 17 -15 -15 4 2 8 7 0 5 2 12 9 -7 7 2 11 9 3 8 2 31 -31 -2 10 2 42 -40 -14 4 2 11 10 1 5 2 11 -17 -6 7 2 37 36 4 8 2 24 23 1 10 2 39 36 -12 4 2 7 -7 2 5 2 6 -4 -5 7 2 7 7 5 8 2 32 34 2 10 2 33 31 -11 4 2 10 -10 3 5 2 53 51 -4 7 2 29 -28 6 8 2 7 7 3 10 2 30 30 -9 4 2 13 11 4 5 2 46 47 -3 7 2 21 -25 8 8 2 13 -13 4 10 2 11 -11 -8 4 2 31 32 6 5 2 18 -17 -2 7 2 14 14 9 8 2 8 -8 5 10 2 24 -24 -7 4 2 25 24 7 5 2 22 -23 -1 7 2 4 2 12 8 2 6 6 6 10 2 17 -17 -6 4 2 23 -23 8 5 2 4 -4 0 7 2 5 -8 -13 9 2 7 -7 7 10 2 10 10 -5 4 2 44 -47 9 5 2 12 12 1 7 2 15 16 -10 9 2 14 14 8 10 2 8 8 -4 4 2 68 -65 -15 6 2 8 -8 2 7 2 22 19 -9 9 2 9 9 11 10 2 5 -5 -3 4 2 12 14 -12 6 2 7 7 3 7 2 59 -59 -7 9 2 18 -19 12 10 2 7 -6 -2 4 2 17 18 -11 6 2 8 8 4 7 2 26 -26 -6 9 2 33 -32 -13 11 2 7 7 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 6 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -10 11 2 11 -11 6 12 2 10 11 8 14 2 7 7 -1 17 2 12 -10 2 20 2 14 -14 -9 11 2 11 -11 7 12 2 11 -11 9 14 2 6 6 0 17 2 7 -8 5 20 2 8 8 -7 11 2 17 17 8 12 2 11 -11 -10 15 2 7 -7 1 17 2 7 -7 -6 21 2 6 -6 -6 11 2 15 15 9 12 2 5 -4 -7 15 2 16 16 2 17 2 4 4 -3 21 2 7 8 -5 11 2 13 12 -11 13 2 6 5 -6 15 2 27 27 3 17 2 11 11 1 21 2 4 -5 -4 11 2 24 -22 -9 13 2 8 7 -5 15 2 9 9 4 17 2 12 12 3 21 2 6 6 -3 11 2 25 -25 -7 13 2 16 -16 -4 15 2 15 -15 6 17 2 7 -8 4 21 2 7 6 -2 11 2 6 5 -6 13 2 30 -31 -3 15 2 12 -10 7 17 2 7 -7 7 21 2 4 -4 -1 11 2 18 16 -4 13 2 20 20 -2 15 2 13 -13 -8 18 2 8 -8 -8 22 2 6 -5 0 11 2 15 13 -3 13 2 15 14 0 15 2 9 8 -6 18 2 6 6 -5 22 2 8 8 1 11 2 16 15 -1 13 2 9 -10 3 15 2 11 -11 -5 18 2 11 11 -4 22 2 5 5 2 11 2 8 -7 0 13 2 20 -21 4 15 2 13 -13 -4 18 2 8 8 -2 22 2 9 -9 3 11 2 22 -23 1 13 2 5 -5 6 15 2 10 10 -3 18 2 11 -12 5 22 2 6 -6 4 11 2 20 -21 2 13 2 8 8 -11 16 2 6 -6 -2 18 2 15 -15 -6 23 2 6 5 5 11 2 8 -9 3 13 2 22 21 -8 16 2 9 10 1 18 2 12 11 3 23 2 7 -6 6 11 2 17 17 4 13 2 22 22 -7 16 2 6 6 2 18 2 18 18 -15 0 3 5 5 7 11 2 13 13 6 13 2 14 -14 -6 16 2 8 -8 4 18 2 7 -7 -13 0 3 5 -5 9 11 2 5 -5 7 13 2 8 -9 -5 16 2 23 -22 5 18 2 11 -12 -12 0 3 19 -18 -12 12 2 8 -8 10 13 2 5 5 -4 16 2 11 -12 -7 19 2 7 6 -11 0 3 4 -4 -9 12 2 5 6 -11 14 2 6 5 -2 16 2 20 20 -6 19 2 7 7 -10 0 3 14 15 -8 12 2 11 11 -8 14 2 16 -16 -1 16 2 18 18 -4 19 2 10 -9 -9 0 3 14 14 -7 12 2 11 11 -7 14 2 18 -17 1 16 2 9 -9 -3 19 2 8 -8 -8 0 3 15 16 -6 12 2 28 -28 -6 14 2 14 15 2 16 2 6 -5 -2 19 2 7 8 -6 0 3 55 -56 -5 12 2 24 -23 -5 14 2 34 33 3 16 2 8 -8 -1 19 2 7 6 -5 0 3 37 40 -4 12 2 14 -15 -4 14 2 6 6 4 16 2 8 8 0 19 2 8 7 -4 0 3 6 8 -3 12 2 26 26 -2 14 2 12 -12 5 16 2 17 16 1 19 2 11 11 -3 0 3 8 -9 -2 12 2 33 31 -1 14 2 14 -13 6 16 2 7 7 3 19 2 15 -15 -2 0 3 44 45 -1 12 2 35 34 0 14 2 6 5 8 16 2 7 -6 4 19 2 8 -9 -1 0 3 5 -7 0 12 2 11 -8 1 14 2 18 18 -10 17 2 5 6 -5 20 2 7 -8 0 0 3 73 -69 1 12 2 15 -14 2 14 2 10 9 -9 17 2 6 5 -4 20 2 6 -5 1 0 3 52 -48 2 12 2 24 -24 3 14 2 10 9 -7 17 2 6 -6 -3 20 2 8 8 2 0 3 24 -23 3 12 2 6 -5 4 14 2 14 -14 -6 17 2 10 -10 -2 20 2 10 10 3 0 3 25 29 4 12 2 9 8 5 14 2 21 -23 -4 17 2 11 11 -1 20 2 5 6 4 0 3 48 51 5 12 2 32 33 7 14 2 7 6 -3 17 2 15 16 1 20 2 6 -6 5 0 3 24 24 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 7 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 6 0 3 24 -24 -9 2 3 21 -22 3 3 3 34 -34 -5 5 3 29 29 -10 7 3 20 -20 7 0 3 20 -21 -8 2 3 34 -33 4 3 3 11 12 -4 5 3 72 71 -8 7 3 17 17 10 0 3 10 9 -7 2 3 25 27 5 3 3 8 9 -3 5 3 28 28 -7 7 3 27 25 11 0 3 11 10 -6 2 3 48 48 6 3 3 9 10 -2 5 3 17 -19 -6 7 3 8 7 13 0 3 5 -4 -5 2 3 4 7 9 3 3 10 -11 -1 5 3 10 -10 -5 7 3 23 -21 -13 1 3 7 -7 -4 2 3 37 -38 12 3 3 6 6 0 5 3 11 -10 -4 7 3 15 -15 -12 1 3 9 9 -2 2 3 54 -53 -16 4 3 6 5 1 5 3 22 -26 -3 7 3 17 11 -11 1 3 17 17 -1 2 3 59 -59 -15 4 3 7 6 2 5 3 49 49 -2 7 3 32 33 -10 1 3 15 14 0 2 3 30 33 -13 4 3 9 -9 3 5 3 28 28 -1 7 3 25 21 -9 1 3 5 5 1 2 3 88 89 -12 4 3 8 -8 4 5 3 10 -10 0 7 3 21 23 -8 1 3 18 -16 2 2 3 37 40 -10 4 3 6 6 5 5 3 15 -16 1 7 3 13 10 -7 1 3 26 -26 3 2 3 12 -12 -9 4 3 38 38 6 5 3 9 -8 2 7 3 39 -42 -5 1 3 35 33 4 2 3 21 -21 -8 4 3 10 11 8 5 3 9 8 3 7 3 31 -34 -4 1 3 9 -7 5 2 3 7 -7 -7 4 3 33 -31 9 5 3 10 10 4 7 3 16 16 -3 1 3 12 -17 6 2 3 23 22 -6 4 3 51 -52 -10 6 3 11 -12 5 7 3 17 18 -2 1 3 15 19 7 2 3 19 19 -5 4 3 54 -52 -9 6 3 28 -27 7 7 3 7 7 -1 1 3 71 -67 8 2 3 9 9 -4 4 3 22 -21 -7 6 3 26 28 8 7 3 8 -9 0 1 3 63 -66 10 2 3 7 -6 -3 4 3 23 21 -6 6 3 32 34 9 7 3 12 -12 1 1 3 18 19 11 2 3 11 -10 -1 4 3 30 31 -5 6 3 25 26 -13 8 3 8 -7 2 1 3 38 42 -14 3 3 6 6 0 4 3 6 5 -4 6 3 23 -24 -12 8 3 7 -8 3 1 3 63 62 -12 3 3 7 -6 1 4 3 61 -60 -3 6 3 62 -59 -11 8 3 8 -8 4 1 3 16 17 -11 3 3 15 -15 3 4 3 25 27 -2 6 3 32 -32 -10 8 3 7 8 5 1 3 22 -23 -10 3 3 20 -19 4 4 3 35 36 -1 6 3 5 -5 -9 8 3 30 29 8 1 3 9 9 -9 3 3 9 -10 6 4 3 16 -15 0 6 3 16 20 -8 8 3 20 20 9 1 3 9 8 -8 3 3 30 30 7 4 3 22 -23 1 6 3 15 16 -7 8 3 15 -13 11 1 3 5 -5 -7 3 3 38 40 8 4 3 11 -11 2 6 3 14 15 -6 8 3 39 -39 12 1 3 8 -7 -6 3 3 7 7 10 4 3 5 5 3 6 3 37 -36 -5 8 3 17 -17 13 1 3 5 -5 -5 3 3 27 -26 11 4 3 10 10 4 6 3 29 -31 -4 8 3 11 11 -16 2 3 5 -5 -4 3 3 13 -14 -11 5 3 13 12 6 6 3 22 22 -3 8 3 31 29 -15 2 3 5 -5 -2 3 3 22 -22 -10 5 3 12 11 7 6 3 19 21 -2 8 3 23 22 -13 2 3 11 10 -1 3 3 4 0 -9 5 3 12 -13 8 6 3 16 16 -1 8 3 7 9 -12 2 3 10 10 0 3 3 66 67 -8 5 3 31 -32 10 6 3 7 -7 0 8 3 18 -18 -11 2 3 5 5 1 3 3 22 19 -7 5 3 30 -29 11 6 3 9 -8 1 8 3 52 -50 -10 2 3 15 -15 2 3 3 52 -54 -6 5 3 4 4 -11 7 3 14 -14 2 8 3 30 -31 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 8 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 3 8 3 21 21 2 10 3 17 16 4 12 3 22 21 7 14 3 9 9 -2 17 3 6 -6 4 8 3 24 24 3 10 3 12 -11 5 12 3 5 6 8 14 3 8 7 -1 17 3 13 -12 6 8 3 6 -8 4 10 3 19 -21 6 12 3 12 -14 -11 15 3 10 -9 0 17 3 12 -13 7 8 3 9 -9 5 10 3 11 -12 7 12 3 15 -15 -8 15 3 10 10 2 17 3 13 12 8 8 3 11 -11 6 10 3 8 8 8 12 3 6 -6 -7 15 3 17 18 3 17 3 11 11 10 8 3 8 8 7 10 3 11 10 11 12 3 7 7 -6 15 3 6 7 5 17 3 7 -7 -11 9 3 13 12 11 10 3 7 -6 -8 13 3 13 -12 -5 15 3 18 -17 -9 18 3 8 -9 -10 9 3 17 16 -11 11 3 10 -10 -7 13 3 22 -23 -4 15 3 10 -9 -7 18 3 6 7 -9 9 3 5 5 -10 11 3 16 -16 -5 13 3 16 16 -3 15 3 16 -16 -6 18 3 8 8 -8 9 3 22 -23 -8 11 3 10 9 -4 13 3 9 8 -2 15 3 6 -7 -3 18 3 13 -12 -7 9 3 21 -22 -7 11 3 16 15 -2 13 3 5 6 -1 15 3 11 10 -2 18 3 7 -6 -6 9 3 11 -10 -6 11 3 4 3 -1 13 3 19 -20 0 15 3 23 24 0 18 3 8 8 -5 9 3 28 26 -5 11 3 9 -9 0 13 3 18 -19 2 15 3 7 -8 1 18 3 18 17 -4 9 3 24 22 -4 11 3 17 -16 2 13 3 27 28 3 15 3 15 -15 2 18 3 6 7 -2 9 3 18 -20 -2 11 3 22 22 3 13 3 14 14 5 15 3 8 8 3 18 3 10 -10 -1 9 3 20 -22 -1 11 3 24 24 5 13 3 12 -13 -12 16 3 6 -5 4 18 3 9 -9 0 9 3 42 -38 0 11 3 30 30 6 13 3 7 -7 -10 16 3 8 8 5 18 3 5 -4 1 9 3 6 -6 2 11 3 29 -29 9 13 3 6 6 -9 16 3 9 10 7 18 3 6 6 2 9 3 39 41 3 11 3 17 -18 -12 14 3 6 5 -8 16 3 7 7 -7 19 3 6 7 3 9 3 41 42 5 11 3 8 7 -10 14 3 6 -6 -6 16 3 17 -17 -4 19 3 8 -8 9 9 3 5 7 6 11 3 11 11 -9 14 3 7 -9 -5 16 3 8 -9 -2 19 3 6 6 -13 10 3 10 9 -12 12 3 6 -7 -8 14 3 11 -11 -3 16 3 10 10 -1 19 3 7 7 -12 10 3 9 8 -9 12 3 18 19 -7 14 3 12 13 -2 16 3 22 22 0 19 3 10 10 -10 10 3 6 -6 -8 12 3 10 9 -6 14 3 33 33 -1 16 3 9 9 2 19 3 16 -17 -9 10 3 19 -19 -7 12 3 11 -9 -5 14 3 12 12 0 16 3 8 -9 3 19 3 10 -10 -8 10 3 19 -19 -6 12 3 24 -24 -3 14 3 8 7 1 16 3 15 -15 -9 20 3 9 8 -7 10 3 17 18 -4 12 3 13 12 -2 14 3 20 -21 2 16 3 9 -9 -6 20 3 7 -8 -6 10 3 19 18 -3 12 3 24 23 -1 14 3 18 -19 4 16 3 13 13 -3 20 3 10 10 -5 10 3 20 21 -2 12 3 24 23 0 14 3 15 14 6 16 3 7 -7 -2 20 3 6 6 -4 10 3 6 -8 -1 12 3 15 15 1 14 3 14 14 7 16 3 9 -9 0 20 3 6 -7 -3 10 3 22 -22 0 12 3 25 -24 2 14 3 5 7 -11 17 3 7 6 1 20 3 14 -13 -2 10 3 18 -18 1 12 3 28 -28 3 14 3 13 -12 -8 17 3 8 -8 2 20 3 5 -6 0 10 3 22 22 2 12 3 7 -8 4 14 3 20 -20 -7 17 3 7 -6 4 20 3 8 7 1 10 3 44 44 3 12 3 9 8 6 14 3 9 8 -4 17 3 10 11 -2 21 3 5 -5 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 9 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -1 21 3 7 -7 9 0 4 7 7 -6 2 4 23 24 5 3 4 11 12 -7 5 4 4 5 0 21 3 7 -7 10 0 4 11 10 -5 2 4 22 -19 6 3 4 14 14 -6 5 4 9 8 2 21 3 6 5 12 0 4 5 -4 -4 2 4 5 -8 8 3 4 13 -12 -5 5 4 27 25 3 21 3 7 7 13 0 4 6 -5 -3 2 4 49 -53 9 3 4 10 -11 -4 5 4 35 36 -8 22 3 6 -3 -14 1 4 7 -7 -2 2 4 32 -30 11 3 4 6 6 -3 5 4 25 -23 -6 22 3 6 6 -12 1 4 20 19 -1 2 4 19 22 -14 4 4 10 -10 -2 5 4 45 -43 -5 22 3 6 6 -11 1 4 22 22 0 2 4 74 77 -13 4 4 9 -9 -1 5 4 37 -36 -3 22 3 7 -6 -9 1 4 8 -7 1 2 4 14 -10 -12 4 4 6 -6 0 5 4 5 -4 -2 22 3 8 -8 -8 1 4 18 -18 2 2 4 43 -39 -11 4 4 7 7 1 5 4 30 31 1 22 3 7 6 -7 1 4 13 -14 3 2 4 27 -30 -10 4 4 22 20 2 5 4 24 25 4 22 3 5 -5 -6 1 4 23 24 4 2 4 10 -9 -9 4 4 13 14 3 5 4 17 -17 -6 24 3 6 -6 -4 1 4 51 -50 6 2 4 24 24 -8 4 4 32 -34 4 5 4 30 -31 -14 0 4 6 -6 -3 1 4 28 -28 7 2 4 20 20 -7 4 4 41 -41 5 5 4 15 -16 -13 0 4 17 -17 -2 1 4 87 -89 8 2 4 8 7 -6 4 4 22 -22 6 5 4 10 -10 -12 0 4 11 -11 -1 1 4 59 -57 9 2 4 8 -7 -5 4 4 15 -14 7 5 4 4 4 -11 0 4 13 14 0 1 4 42 38 10 2 4 14 -12 -4 4 4 48 50 8 5 4 15 15 -10 0 4 20 20 1 1 4 52 55 11 2 4 6 -5 -3 4 4 83 82 9 5 4 8 7 -9 0 4 5 7 2 1 4 31 30 13 2 4 4 3 -2 4 4 52 57 11 5 4 6 -6 -7 0 4 44 -44 4 1 4 15 -15 -14 3 4 7 7 -1 4 4 5 -4 -13 6 4 9 8 -6 0 4 11 -11 5 1 4 18 -20 -12 3 4 12 -12 0 4 4 38 -38 -11 6 4 5 -6 -5 0 4 22 24 6 1 4 10 -9 -11 3 4 16 -17 1 4 4 14 -15 -10 6 4 22 -22 -4 0 4 32 33 8 1 4 11 10 -9 3 4 25 25 2 4 4 52 53 -8 6 4 24 22 -3 0 4 20 28 9 1 4 8 7 -8 3 4 33 33 3 4 4 32 33 -7 6 4 22 22 -2 0 4 19 20 10 1 4 4 -4 -6 3 4 22 -24 4 4 4 9 9 -6 6 4 14 15 -1 0 4 92 -95 11 1 4 8 -8 -5 3 4 31 -32 6 4 4 28 -28 -5 6 4 20 19 0 0 4 58 -55 -16 2 4 6 -5 -4 3 4 15 -16 7 4 4 19 -20 -4 6 4 23 -23 1 0 4 27 29 -14 2 4 9 8 -3 3 4 14 16 8 4 4 9 -9 -3 6 4 57 -55 2 0 4 44 42 -13 2 4 14 13 -2 3 4 44 50 9 4 4 6 6 -2 6 4 17 -18 3 0 4 37 41 -12 2 4 6 6 -1 3 4 92 92 10 4 4 13 12 -1 6 4 19 22 4 0 4 33 33 -11 2 4 11 -11 0 3 4 13 12 -15 5 4 5 -5 0 6 4 22 26 5 0 4 12 -12 -10 2 4 27 -27 1 3 4 63 -66 -14 5 4 7 -6 2 6 4 37 -39 6 0 4 19 -18 -9 2 4 26 -26 2 3 4 30 -31 -12 5 4 11 10 3 6 4 35 -35 7 0 4 20 -20 -8 2 4 12 12 3 3 4 4 4 -11 5 4 15 14 5 6 4 22 22 8 0 4 5 -3 -7 2 4 39 43 4 3 4 11 11 -9 5 4 22 -20 6 6 4 23 23 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 10 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 7 6 4 21 22 1 8 4 16 -13 -8 10 4 14 13 -3 12 4 14 13 -2 14 4 28 -28 8 6 4 5 5 2 8 4 27 27 -7 10 4 14 14 -2 12 4 15 14 -1 14 4 8 7 9 6 4 9 -9 3 8 4 39 40 -6 10 4 15 16 -1 12 4 32 -31 0 14 4 21 20 10 6 4 11 -11 4 8 4 9 8 -4 10 4 17 -18 0 12 4 24 -25 1 14 4 6 -5 -12 7 4 7 -8 5 8 4 8 -8 -3 10 4 41 -41 1 12 4 6 -5 2 14 4 13 -14 -11 7 4 17 -16 6 8 4 9 -9 -2 10 4 15 -18 2 12 4 23 23 3 14 4 15 -14 -9 7 4 16 16 7 8 4 18 -18 -1 10 4 17 19 3 12 4 13 13 6 14 4 11 11 -8 7 4 13 13 8 8 4 8 -8 0 10 4 44 45 4 12 4 8 9 7 14 4 11 11 -5 7 4 7 -6 9 8 4 10 9 2 10 4 20 -19 5 12 4 8 -8 8 14 4 5 5 -3 7 4 16 18 10 8 4 7 7 3 10 4 29 -29 6 12 4 16 -16 10 14 4 7 -6 -2 7 4 62 64 -15 9 4 7 -6 4 10 4 12 -13 7 12 4 11 -11 -11 15 4 9 -9 -1 7 4 44 47 -12 9 4 11 11 6 10 4 15 14 10 12 4 8 8 -9 15 4 5 4 1 7 4 32 -34 -11 9 4 21 20 7 10 4 12 13 -12 13 4 7 8 -8 15 4 10 11 2 7 4 46 -47 -10 9 4 5 6 8 10 4 5 4 -11 13 4 6 6 -6 15 4 13 -14 3 7 4 9 11 -9 9 4 11 -11 -14 11 4 6 5 -9 13 4 10 -9 -5 15 4 19 -19 4 7 4 21 21 -8 9 4 14 -14 -12 11 4 11 -11 -8 13 4 11 -11 -2 15 4 22 21 5 7 4 6 5 -6 9 4 6 5 -11 11 4 11 -11 -6 13 4 17 18 -1 15 4 24 25 6 7 4 8 7 -5 9 4 12 9 -9 11 4 10 10 -5 13 4 10 10 1 15 4 12 -13 8 7 4 15 -15 -4 9 4 13 15 -8 11 4 11 11 -4 13 4 5 4 2 15 4 9 -8 9 7 4 6 -7 -3 9 4 8 -8 -5 11 4 8 -7 -2 13 4 14 -14 4 15 4 7 7 -14 8 4 10 -9 -2 9 4 38 -38 -3 11 4 28 28 -1 13 4 27 -27 5 15 4 7 7 -13 8 4 9 -8 -1 9 4 32 -31 -2 11 4 33 34 1 13 4 24 24 6 15 4 6 5 -12 8 4 6 -6 0 9 4 7 -8 -1 11 4 32 31 2 13 4 6 6 -11 16 4 7 6 -10 8 4 23 22 1 9 4 48 49 1 11 4 37 -37 4 13 4 11 -11 -10 16 4 11 10 -9 8 4 17 16 2 9 4 37 38 2 11 4 22 -22 5 13 4 9 -9 -9 16 4 7 7 -8 8 4 14 -14 4 9 4 11 -11 5 11 4 14 14 8 13 4 8 8 -7 16 4 14 -14 -7 8 4 22 -21 5 9 4 9 -9 11 11 4 5 5 -11 14 4 5 -6 -6 16 4 12 -12 -6 8 4 8 -9 6 9 4 13 -13 -13 12 4 9 -8 -10 14 4 7 -7 -4 16 4 11 10 -5 8 4 5 -3 8 9 4 7 8 -10 12 4 13 13 -8 14 4 8 9 -3 16 4 19 19 -4 8 4 17 18 -14 10 4 9 8 -9 12 4 9 9 -7 14 4 28 29 -2 16 4 10 9 -3 8 4 39 36 -13 10 4 11 11 -8 12 4 4 -4 -6 14 4 16 16 -1 16 4 12 -12 -2 8 4 31 34 -11 10 4 6 -6 -7 12 4 21 -20 -5 14 4 13 -12 0 16 4 17 -18 -1 8 4 29 -29 -10 10 4 19 -19 -6 12 4 5 -5 -4 14 4 8 -8 3 16 4 10 10 0 8 4 53 -54 -9 10 4 15 -15 -4 12 4 14 13 -3 14 4 27 -29 6 16 4 10 -11 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 11 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 7 16 4 7 -7 2 20 4 6 7 8 0 5 6 6 -2 2 5 34 33 -14 4 5 12 -11 -11 17 4 6 7 3 20 4 8 8 9 0 5 7 7 -1 2 5 77 79 -12 4 5 8 8 -9 17 4 7 -7 -2 21 4 10 -10 12 0 5 6 -5 0 2 5 20 18 -11 4 5 13 13 -8 17 4 7 -6 -1 21 4 7 -8 -15 1 5 5 -5 1 2 5 36 -36 -10 4 5 13 13 -5 17 4 8 8 1 21 4 7 6 -13 1 5 15 14 2 2 5 30 -32 -9 4 5 26 -26 -4 17 4 6 5 2 21 4 8 8 -12 1 5 20 20 3 2 5 26 -26 -8 4 5 43 -44 -3 17 4 8 -8 -6 22 4 6 6 -10 1 5 10 -11 4 2 5 15 -15 -7 4 5 26 -28 -2 17 4 14 -14 -3 22 4 9 -10 -8 1 5 22 -23 5 2 5 17 17 -6 4 5 10 -9 -1 17 4 11 -11 0 22 4 7 7 -6 1 5 34 34 6 2 5 25 26 -5 4 5 40 41 1 17 4 12 12 3 22 4 7 -7 -5 1 5 29 29 7 2 5 8 8 -4 4 5 112 111 2 17 4 10 10 -5 23 4 6 -5 -4 1 5 12 -10 8 2 5 6 -6 -3 4 5 49 50 5 17 4 6 -6 0 24 4 5 -4 -3 1 5 30 -29 9 2 5 10 -10 -2 4 5 7 -7 -10 18 4 7 -7 -1 25 4 5 -5 -2 1 5 68 -70 12 2 5 5 4 -1 4 5 42 -41 -9 18 4 6 -5 -15 0 5 5 -5 -1 1 5 29 26 -15 3 5 8 7 0 4 5 23 -21 -8 18 4 6 5 -14 0 5 9 -9 0 1 5 71 76 -13 3 5 9 -9 1 4 5 21 20 -7 18 4 7 7 -13 0 5 10 -10 1 1 5 42 41 -12 3 5 15 -15 2 4 5 15 17 -4 18 4 10 -11 -12 0 5 18 17 2 1 5 23 20 -10 3 5 16 16 3 4 5 17 16 -3 18 4 11 -11 -11 0 5 19 18 3 1 5 3 5 -9 3 5 25 26 5 4 5 20 -19 -1 18 4 8 8 -10 0 5 6 6 4 1 5 25 -26 -7 3 5 11 -11 6 4 5 26 -27 0 18 4 14 13 -8 0 5 14 -15 5 1 5 18 -18 -6 3 5 53 -53 7 4 5 9 -9 2 18 4 11 -11 -7 0 5 47 -49 7 1 5 12 12 -5 3 5 36 -36 8 4 5 6 6 3 18 4 9 -10 -6 0 5 9 -9 8 1 5 7 7 -4 3 5 5 -5 9 4 5 10 10 6 18 4 6 6 -5 0 5 28 24 9 1 5 4 -3 -3 3 5 74 74 -15 5 5 7 -7 7 18 4 6 6 -4 0 5 63 62 10 1 5 6 -6 -2 3 5 67 65 -13 5 5 8 8 -3 19 4 7 7 -3 0 5 64 65 -14 2 5 11 11 -1 3 5 21 22 -12 5 5 17 16 -2 19 4 8 8 -2 0 5 42 -46 -12 2 5 11 -10 0 3 5 60 -60 -11 5 5 6 6 -1 19 4 9 9 -1 0 5 61 -63 -11 2 5 22 -21 1 3 5 46 -45 -10 5 5 10 -10 1 19 4 12 -13 1 0 5 25 21 -10 2 5 10 -12 2 3 5 19 -18 -9 5 5 7 -7 2 19 4 11 -11 2 0 5 25 26 -8 2 5 42 42 4 3 5 9 9 -8 5 5 7 6 -10 20 4 8 7 3 0 5 31 29 -7 2 5 38 38 5 3 5 27 26 -7 5 5 10 12 -4 20 4 6 6 4 0 5 8 8 -6 2 5 20 20 7 3 5 13 -12 -6 5 5 32 33 -3 20 4 9 10 5 0 5 23 -22 -5 2 5 20 -21 8 3 5 11 -11 -5 5 5 48 51 -1 20 4 7 -7 6 0 5 23 -23 -4 2 5 59 -57 10 3 5 6 6 -4 5 5 13 -11 0 20 4 10 -10 7 0 5 5 -6 -3 2 5 55 -58 -15 4 5 5 -4 -3 5 5 60 -64 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 12 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -2 5 5 32 -32 -12 7 5 12 -12 3 8 5 22 24 -3 10 5 24 -24 -4 12 5 28 27 -1 5 5 8 10 -10 7 5 18 19 4 8 5 4 5 -2 10 5 24 24 -3 12 5 11 12 0 5 5 8 8 -9 7 5 11 12 6 8 5 20 -19 -1 10 5 32 31 -2 12 5 12 -12 1 5 5 29 30 -7 7 5 20 -20 7 8 5 10 -10 0 10 5 12 12 -1 12 5 29 -30 2 5 5 7 7 -6 7 5 27 -26 8 8 5 7 6 1 10 5 13 -13 1 12 5 16 15 3 5 5 6 -7 -5 7 5 40 -38 9 8 5 9 9 2 10 5 21 -20 2 12 5 12 14 4 5 5 15 -16 -4 7 5 6 4 -13 9 5 9 9 3 10 5 19 -20 3 12 5 12 12 5 5 5 15 -15 -3 7 5 45 49 -12 9 5 19 18 4 10 5 12 -12 5 12 5 12 -13 7 5 5 15 15 -2 7 5 32 29 -11 9 5 8 8 5 10 5 11 12 6 12 5 12 -12 8 5 5 10 10 -1 7 5 18 -17 -10 9 5 9 -8 6 10 5 17 18 9 12 5 6 5 10 5 5 6 -6 0 7 5 25 -23 -9 9 5 20 -21 7 10 5 6 6 -12 13 5 8 8 -14 6 5 8 8 1 7 5 35 -34 -6 9 5 19 18 -13 11 5 8 -9 -8 13 5 7 -8 -12 6 5 5 -5 2 7 5 19 -20 -5 9 5 19 22 -12 11 5 8 -8 -7 13 5 9 8 -11 6 5 16 -16 4 7 5 11 11 -4 9 5 11 -11 -10 11 5 8 8 -6 13 5 19 19 -10 6 5 10 -10 5 7 5 9 8 -3 9 5 49 -49 -9 11 5 10 11 -5 13 5 18 19 -9 6 5 17 17 6 7 5 7 7 -2 9 5 28 -28 -6 11 5 20 -19 -3 13 5 13 -14 -8 6 5 34 34 7 7 5 12 -12 0 9 5 36 35 -5 11 5 25 -25 -2 13 5 30 -31 -7 6 5 25 25 8 7 5 9 -9 1 9 5 29 30 -4 11 5 10 11 0 13 5 18 17 -6 6 5 22 25 -15 8 5 6 -6 2 9 5 15 18 -3 11 5 34 34 1 13 5 15 15 -5 6 5 21 -25 -14 8 5 8 -7 3 9 5 5 -6 -2 11 5 17 18 4 13 5 10 -10 -4 6 5 67 -67 -12 8 5 6 4 4 9 5 12 -12 0 11 5 28 -29 5 13 5 9 -8 -3 6 5 33 -31 -11 8 5 16 17 5 9 5 20 -21 1 11 5 27 -28 7 13 5 9 8 -2 6 5 28 26 -10 8 5 17 17 6 9 5 7 -7 2 11 5 10 -11 -11 14 5 9 -8 -1 6 5 22 24 -9 8 5 13 -15 7 9 5 8 8 4 11 5 12 11 -8 14 5 17 18 0 6 5 9 -8 -8 8 5 29 -28 8 9 5 9 9 5 11 5 14 14 -7 14 5 20 20 2 6 5 20 -20 -7 8 5 24 -25 -14 10 5 10 10 7 11 5 7 -7 -5 14 5 21 -20 3 6 5 17 -17 -5 8 5 21 23 -12 10 5 8 -7 -13 12 5 5 -5 -4 14 5 27 -28 5 6 5 18 18 -4 8 5 46 46 -11 10 5 17 -18 -12 12 5 7 6 -3 14 5 35 -35 6 6 5 19 19 -3 8 5 31 31 -10 10 5 11 -12 -11 12 5 6 6 -1 14 5 28 29 7 6 5 9 9 -2 8 5 37 -38 -8 10 5 27 26 -10 12 5 6 6 1 14 5 8 -8 8 6 5 9 -9 -1 8 5 40 -39 -7 10 5 23 23 -8 12 5 15 -15 2 14 5 7 -7 9 6 5 9 -9 0 8 5 9 -10 -6 10 5 15 16 -7 12 5 23 -23 3 14 5 9 -9 -16 7 5 7 7 1 8 5 11 12 -5 10 5 23 -23 -6 12 5 6 -8 5 14 5 9 10 -15 7 5 4 4 2 8 5 25 25 -4 10 5 45 -45 -5 12 5 7 7 6 14 5 12 13 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 13 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 9 14 5 5 -5 -3 17 5 13 -13 1 21 5 7 7 -12 1 6 8 8 -1 2 6 24 22 -12 15 5 7 -7 -2 17 5 11 -11 -11 22 5 5 -4 -11 1 6 13 -13 0 2 6 18 -14 -8 15 5 4 5 0 17 5 11 11 -8 22 5 6 6 -10 1 6 18 -18 1 2 6 18 -20 -7 15 5 6 -5 1 17 5 11 11 -7 22 5 5 6 -9 1 6 25 -25 2 2 6 35 -35 -6 15 5 20 -21 4 17 5 7 -7 -4 22 5 9 -9 -8 1 6 30 -31 3 2 6 24 -23 -5 15 5 11 -11 5 17 5 5 -5 -1 22 5 5 6 -7 1 6 31 32 4 2 6 10 10 -3 15 5 23 23 -11 18 5 5 -5 3 22 5 6 -6 -6 1 6 27 29 5 2 6 27 27 -2 15 5 26 27 -10 18 5 7 -5 -17 0 6 5 3 -5 1 6 17 -20 6 2 6 8 7 -1 15 5 7 6 -8 18 5 8 8 -15 0 6 7 -7 -4 1 6 21 -26 7 2 6 7 -7 0 15 5 17 -18 -5 18 5 6 -6 -14 0 6 10 -10 -3 1 6 18 -17 8 2 6 9 -8 1 15 5 9 -9 -4 18 5 16 -16 -13 0 6 9 9 -2 1 6 5 -4 9 2 6 5 -4 2 15 5 8 -7 -3 18 5 4 -5 -12 0 6 24 23 -1 1 6 21 21 -14 3 6 8 -8 4 15 5 8 9 -2 18 5 7 7 -11 0 6 16 16 0 1 6 18 21 -13 3 6 11 -11 5 15 5 7 8 -1 18 5 11 11 -10 0 6 4 4 1 1 6 25 24 -12 3 6 12 -11 7 15 5 6 -5 0 18 5 5 5 -8 0 6 56 -59 2 1 6 9 9 -11 3 6 10 11 8 15 5 5 -6 1 18 5 6 -6 -7 0 6 25 -26 3 1 6 21 -22 -10 3 6 18 20 -11 16 5 8 8 2 18 5 10 -10 -6 0 6 8 10 4 1 6 27 -27 -9 3 6 21 21 -8 16 5 10 -12 -5 19 5 6 -6 -5 0 6 39 40 6 1 6 12 12 -8 3 6 6 -5 -7 16 5 17 -17 -3 19 5 9 10 -3 0 6 8 5 7 1 6 6 7 -7 3 6 26 -27 -6 16 5 8 -8 -2 19 5 7 7 -2 0 6 34 -35 9 1 6 5 -4 -6 3 6 46 -47 -5 16 5 10 10 0 19 5 7 -8 -1 0 6 8 10 10 1 6 6 -4 -5 3 6 4 3 -4 16 5 19 20 1 19 5 10 -9 1 0 6 9 9 -15 2 6 8 9 -4 3 6 39 38 -3 16 5 16 17 -8 20 5 7 -8 2 0 6 25 28 -14 2 6 6 7 -3 3 6 34 35 -2 16 5 10 -11 -7 20 5 5 -6 3 0 6 24 24 -13 2 6 7 -7 -2 3 6 9 10 -1 16 5 17 -17 -4 20 5 11 12 4 0 6 22 -21 -12 2 6 16 -16 -1 3 6 13 -12 0 16 5 5 -5 -2 20 5 5 -6 5 0 6 19 -20 -11 2 6 11 -12 0 3 6 39 -37 1 16 5 5 5 -1 20 5 9 -9 6 0 6 5 -6 -9 2 6 35 35 1 3 6 18 -17 2 16 5 9 9 2 20 5 6 7 7 0 6 8 8 -8 2 6 49 50 3 3 6 17 18 3 16 5 11 11 3 20 5 6 6 8 0 6 7 6 -7 2 6 31 31 4 3 6 27 26 5 16 5 8 -8 -6 21 5 7 7 9 0 6 5 3 -6 2 6 18 -19 6 3 6 16 -16 6 16 5 9 -9 -5 21 5 6 7 11 0 6 5 -4 -5 2 6 29 -33 7 3 6 9 -9 -9 17 5 5 -5 -3 21 5 10 -10 -16 1 6 6 -6 -4 2 6 28 -29 9 3 6 6 5 -6 17 5 10 10 -2 21 5 6 -6 -14 1 6 7 7 -3 2 6 22 21 10 3 6 6 5 -5 17 5 15 16 0 21 5 5 5 -13 1 6 21 21 -2 2 6 34 34 -15 4 6 11 -10 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 14 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -13 4 6 6 6 -1 5 6 9 -5 -8 7 6 11 11 -12 9 6 7 7 3 10 6 11 -11 -12 4 6 11 11 0 5 6 14 14 -7 7 6 19 -17 -11 9 6 7 -7 4 10 6 9 9 -11 4 6 11 12 1 5 6 27 28 -6 7 6 33 -32 -10 9 6 19 -19 5 10 6 18 18 -9 4 6 36 -36 3 5 6 17 -18 -5 7 6 16 -16 -9 9 6 19 -20 -14 11 6 8 -7 -8 4 6 33 -34 4 5 6 14 -14 -4 7 6 31 31 -8 9 6 8 -7 -13 11 6 9 -9 -7 4 6 26 -27 6 5 6 13 13 -3 7 6 27 29 -7 9 6 9 10 -11 11 6 5 5 -6 4 6 18 19 7 5 6 9 9 -2 7 6 6 -7 -6 9 6 25 25 -10 11 6 11 10 -5 4 6 56 59 10 5 6 5 -5 -1 7 6 13 -14 -4 9 6 33 -32 -9 11 6 16 16 -4 4 6 43 42 -15 6 6 7 8 0 7 6 12 -12 -3 9 6 31 -32 -8 11 6 6 7 -3 4 6 26 -29 -14 6 6 8 7 1 7 6 27 -26 -2 9 6 7 7 -7 11 6 10 -10 -2 4 6 27 -29 -13 6 6 5 -4 3 7 6 20 21 -1 9 6 15 15 -6 11 6 28 -28 -1 4 6 24 -27 -12 6 6 6 -5 4 7 6 11 11 0 9 6 30 30 -4 11 6 23 24 0 4 6 9 -9 -11 6 6 13 -14 6 7 6 8 -7 1 9 6 21 21 -1 11 6 8 -8 1 4 6 8 9 -9 6 6 16 16 7 7 6 9 -9 3 9 6 19 -19 0 11 6 18 -19 2 4 6 22 23 -8 6 6 35 36 -15 8 6 9 -8 4 9 6 16 -16 1 11 6 12 -14 3 4 6 8 10 -7 6 6 21 23 -12 8 6 12 12 5 9 6 6 -5 3 11 6 11 11 4 4 6 16 -14 -6 6 6 6 -6 -11 8 6 14 15 6 9 6 10 10 4 11 6 17 17 5 4 6 26 -26 -5 6 6 57 -57 -9 8 6 22 -23 7 9 6 8 8 6 11 6 8 -7 7 4 6 9 8 -4 6 6 37 -39 -8 8 6 34 -35 -15 10 6 7 7 -14 12 6 6 -6 8 4 6 10 9 -3 6 6 14 13 -7 8 6 21 -22 -13 10 6 8 -7 -12 12 6 8 8 9 4 6 7 6 -2 6 6 27 26 -5 8 6 32 33 -12 10 6 12 -13 -11 12 6 7 7 11 4 6 5 -4 0 6 6 13 13 -4 8 6 27 28 -11 10 6 10 -11 -9 12 6 9 -10 -16 5 6 8 -7 1 6 6 9 -10 -3 8 6 15 -15 -9 10 6 18 19 -8 12 6 25 -26 -14 5 6 7 7 2 6 6 27 -26 -2 8 6 36 -38 -8 10 6 25 24 -7 12 6 14 -15 -13 5 6 11 12 3 6 6 9 -9 -1 8 6 7 -9 -7 10 6 26 26 -6 12 6 8 7 -12 5 6 7 8 4 6 6 18 19 1 8 6 16 17 -6 10 6 9 -8 -5 12 6 23 25 -10 5 6 15 -15 5 6 6 13 13 2 8 6 29 30 -5 10 6 27 -27 -4 12 6 11 11 -9 5 6 16 -17 7 6 6 8 -8 3 8 6 10 11 -4 10 6 17 -16 -2 12 6 15 -13 -8 5 6 8 -7 8 6 6 8 -8 4 8 6 13 -12 -3 10 6 25 24 1 12 6 12 12 -7 5 6 17 18 -16 7 6 9 7 5 8 6 15 -15 -2 10 6 22 22 2 12 6 11 12 -6 5 6 42 42 -13 7 6 12 -12 6 8 6 7 -8 -1 10 6 18 17 3 12 6 10 11 -4 5 6 64 -66 -12 7 6 9 -8 8 8 6 10 9 0 10 6 6 -5 4 12 6 8 -8 -3 5 6 37 -39 -10 7 6 16 16 -14 9 6 8 8 1 10 6 14 -13 5 12 6 12 -12 -2 5 6 13 -13 -9 7 6 15 16 -13 9 6 9 10 2 10 6 26 -26 7 12 6 6 6 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 15 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -13 13 6 10 10 -1 15 6 8 -8 -7 18 6 6 6 -6 0 7 18 15 -8 2 7 12 12 -10 13 6 9 -9 0 15 6 8 -9 -5 18 6 11 -11 -4 0 7 16 -14 -7 2 7 23 -23 -9 13 6 8 -9 1 15 6 8 -9 -2 18 6 6 7 -3 0 7 13 -15 -6 2 7 43 -44 -7 13 6 16 17 3 15 6 9 10 1 18 6 7 -7 -2 0 7 33 -31 -5 2 7 16 -18 -6 13 6 13 13 4 15 6 7 7 2 18 6 7 -7 0 0 7 13 14 -3 2 7 23 25 -4 13 6 17 -15 6 15 6 8 -7 5 18 6 7 6 1 0 7 38 39 -2 2 7 25 27 -3 13 6 13 -13 -12 16 6 7 7 -10 19 6 8 8 2 0 7 18 19 0 2 7 26 -26 -2 13 6 11 -11 -9 16 6 9 -10 -9 19 6 7 7 3 0 7 15 -14 1 2 7 31 -32 -1 13 6 9 8 -8 16 6 16 -17 -4 19 6 8 8 4 0 7 17 -18 2 2 7 18 -18 0 13 6 11 10 -7 16 6 8 -9 -1 19 6 6 -4 7 0 7 5 3 3 2 7 12 12 1 13 6 7 7 -6 16 6 11 11 0 19 6 6 -7 -14 1 7 11 11 4 2 7 20 21 3 13 6 7 -7 -5 16 6 18 18 1 19 6 6 -6 -13 1 7 13 13 5 2 7 8 7 4 13 6 10 -10 -4 16 6 9 10 -9 20 6 7 -7 -11 1 7 15 -15 7 2 7 5 -4 7 13 6 6 5 -3 16 6 6 -6 -8 20 6 8 -9 -10 1 7 18 -18 -15 3 7 5 -4 -12 14 6 9 -9 -2 16 6 11 -10 -5 20 6 9 8 -9 1 7 27 -26 -14 3 7 8 -9 -11 14 6 5 -6 -1 16 6 7 -7 -4 20 6 5 6 -8 1 7 17 15 -13 3 7 11 -12 -9 14 6 8 10 1 16 6 5 5 -2 20 6 9 -9 -7 1 7 35 37 -11 3 7 11 11 -8 14 6 20 21 2 16 6 12 13 1 20 6 7 6 -5 1 7 29 -29 -10 3 7 15 15 -7 14 6 6 6 3 16 6 7 7 2 20 6 8 8 -4 1 7 4 -4 -9 3 7 7 -7 -6 14 6 17 -17 4 16 6 6 -6 -6 21 6 7 7 -3 1 7 14 -16 -8 3 7 16 -16 -5 14 6 15 -15 5 16 6 10 -10 -4 21 6 7 -6 -2 1 7 6 6 -7 3 7 29 -29 -4 14 6 14 -14 -13 17 6 5 5 0 21 6 7 6 -1 1 7 30 30 -6 3 7 6 5 -2 14 6 21 20 -10 17 6 6 -6 1 21 6 6 6 0 1 7 35 33 -5 3 7 28 28 -1 14 6 11 12 -7 17 6 8 8 3 21 6 6 -6 2 1 7 18 -18 -4 3 7 30 30 2 14 6 8 -8 -6 17 6 12 13 -4 22 6 6 -5 3 1 7 17 -17 -3 3 7 6 6 4 14 6 6 7 -4 17 6 11 -11 -4 23 6 6 4 5 1 7 11 10 -2 3 7 6 6 5 14 6 12 12 -3 17 6 6 -7 -16 0 7 5 -4 6 1 7 7 8 -1 3 7 37 -38 -13 15 6 7 -7 0 17 6 8 8 -15 0 7 4 -4 9 1 7 5 -3 0 3 7 28 -28 -11 15 6 7 7 1 17 6 7 8 -13 0 7 18 19 -15 2 7 6 6 2 3 7 20 20 -7 15 6 15 -15 3 17 6 7 -7 -12 0 7 10 11 -13 2 7 9 -9 3 3 7 12 13 -6 15 6 16 -16 4 17 6 7 -7 -11 0 7 13 14 -12 2 7 14 -13 5 3 7 17 -16 -5 15 6 7 7 -11 18 6 8 -7 -9 0 7 26 -26 -11 2 7 5 -5 6 3 7 10 -10 -4 15 6 10 11 -9 18 6 7 7 -8 0 7 52 -53 -10 2 7 7 7 -15 4 7 7 -7 -3 15 6 17 17 -8 18 6 8 9 -7 0 7 21 19 -9 2 7 33 34 -13 4 7 6 6 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 16 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -12 4 7 11 11 5 5 7 11 11 2 7 7 21 20 2 9 7 19 -19 -12 12 7 6 6 -11 4 7 10 9 6 5 7 7 7 3 7 7 12 13 3 9 7 13 -13 -11 12 7 6 6 -10 4 7 9 -10 -16 6 7 7 8 4 7 7 6 -6 5 9 7 9 9 -10 12 7 6 -6 -9 4 7 28 -28 -15 6 7 7 6 6 7 7 9 -8 6 9 7 7 8 -9 12 7 16 -17 -7 4 7 17 16 -13 6 7 7 -7 -16 8 7 6 -5 -15 10 7 5 5 -8 12 7 14 -14 -6 4 7 38 38 -12 6 7 8 -8 -13 8 7 9 8 -14 10 7 6 -5 -7 12 7 12 12 -5 4 7 19 18 -11 6 7 10 -10 -12 8 7 13 13 -12 10 7 11 -12 -6 12 7 18 20 -4 4 7 12 -12 -10 6 7 11 11 -11 8 7 9 9 -9 10 7 23 23 -5 12 7 13 14 -3 4 7 27 -28 -9 6 7 21 21 -10 8 7 16 -16 -8 10 7 6 7 -2 12 7 16 -16 -2 4 7 24 -25 -8 6 7 9 9 -9 8 7 22 -23 -7 10 7 7 -7 -1 12 7 8 -8 -1 4 7 22 -24 -7 6 7 19 -20 -8 8 7 11 -10 -6 10 7 22 -21 0 12 7 9 9 0 4 7 17 16 -6 6 7 23 -23 -7 8 7 16 16 -4 10 7 11 12 1 12 7 16 16 1 4 7 27 29 -5 6 7 20 -21 -6 8 7 14 16 -3 10 7 20 19 2 12 7 6 6 2 4 7 16 16 -4 6 7 11 11 -5 8 7 14 14 -2 10 7 10 11 4 12 7 12 -12 3 4 7 13 -12 -3 6 7 17 16 -3 8 7 21 -22 -1 10 7 9 9 -14 13 7 6 6 4 4 7 19 -18 -2 6 7 21 20 -2 8 7 13 -14 0 10 7 18 -18 -13 13 7 8 7 7 4 7 5 5 -1 6 7 15 16 0 8 7 10 10 1 10 7 26 -27 -10 13 7 8 -7 8 4 7 7 6 0 6 7 8 7 1 8 7 30 30 2 10 7 13 -13 -8 13 7 11 11 -14 5 7 9 9 1 6 7 32 -33 2 8 7 16 16 3 10 7 9 9 -7 13 7 14 14 -13 5 7 7 7 2 6 7 14 -16 3 8 7 15 -14 4 10 7 15 15 -5 13 7 16 -16 -11 5 7 13 -13 3 6 7 13 13 4 8 7 13 -13 -14 11 7 10 -10 -4 13 7 12 -12 -10 5 7 16 -15 4 6 7 13 13 5 8 7 8 -7 -11 11 7 9 9 -3 13 7 14 -15 -8 5 7 15 15 -14 7 7 9 -9 -13 9 7 6 6 -10 11 7 14 14 -1 13 7 13 13 -7 5 7 18 17 -13 7 7 13 -12 -11 9 7 14 -13 -9 11 7 6 8 0 13 7 15 15 -5 5 7 36 -36 -12 7 7 5 -4 -10 9 7 18 -19 -8 11 7 8 -8 2 13 7 6 -6 -4 5 7 28 -28 -11 7 7 11 11 -9 9 7 5 3 -7 11 7 17 -18 3 13 7 6 -6 -3 5 7 8 -8 -10 7 7 13 13 -8 9 7 12 12 -5 11 7 17 18 5 13 7 5 6 -2 5 7 9 -10 -8 7 7 16 -17 -7 9 7 14 15 -4 11 7 6 7 -12 14 7 7 -7 -1 5 7 14 14 -7 7 7 10 -11 -5 9 7 16 -17 -2 11 7 6 6 -9 14 7 12 12 0 5 7 44 43 -5 7 7 15 16 -4 9 7 15 -15 -1 11 7 15 -15 -8 14 7 8 8 1 5 7 14 15 -4 7 7 18 19 -2 9 7 6 6 0 11 7 19 -19 -7 14 7 12 -12 2 5 7 14 -14 -3 7 7 10 11 -1 9 7 24 24 2 11 7 14 14 -6 14 7 14 -15 3 5 7 8 -7 0 7 7 28 -29 0 9 7 26 26 3 11 7 10 11 -3 14 7 17 17 4 5 7 7 8 1 7 7 7 -7 1 9 7 6 5 5 11 7 7 -8 -2 14 7 19 20 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 17 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 0 14 7 8 -8 -9 18 7 9 8 2 0 8 11 -11 -2 2 8 19 19 -5 4 8 5 -3 1 14 7 11 -11 -8 18 7 5 5 3 0 8 17 -17 -1 2 8 22 -22 -4 4 8 22 -23 2 14 7 6 -7 -3 18 7 6 6 4 0 8 4 -5 0 2 8 22 -24 -3 4 8 32 -30 4 14 7 9 8 -2 18 7 7 7 7 0 8 5 3 1 2 8 5 -3 -2 4 8 16 -18 -13 15 7 6 -5 0 18 7 5 -5 8 0 8 5 1 2 2 8 16 14 -1 4 8 19 20 -10 15 7 5 5 1 18 7 9 -9 -15 1 8 6 6 3 2 8 16 17 0 4 8 28 27 -8 15 7 10 -9 4 18 7 7 6 -14 1 8 12 11 4 2 8 8 9 1 4 8 8 7 -7 15 7 15 -15 -11 19 7 6 6 -12 1 8 17 -16 -15 3 8 7 -8 2 4 8 12 -12 -5 15 7 11 11 -4 19 7 5 5 -11 1 8 12 -13 -14 3 8 7 -7 3 4 8 12 -12 -4 15 7 13 13 -1 19 7 6 -6 -9 1 8 10 10 -12 3 8 14 13 -15 5 8 7 7 -3 15 7 8 8 2 19 7 4 4 -8 1 8 33 34 -11 3 8 10 10 -14 5 8 8 8 -1 15 7 13 -14 -9 20 7 6 -7 -7 1 8 6 6 -9 3 8 21 -22 -11 5 8 14 -15 0 15 7 11 -11 -3 20 7 7 -7 -5 1 8 6 -7 -6 3 8 26 28 -9 5 8 20 19 2 15 7 8 8 -2 20 7 5 -5 -4 1 8 17 -16 -5 3 8 27 27 -8 5 8 18 20 5 15 7 6 -6 1 20 7 8 8 -3 1 8 26 -27 -4 3 8 31 31 -7 5 8 7 8 -12 16 7 5 4 -7 21 7 5 4 -2 1 8 17 17 -3 3 8 11 11 -6 5 8 11 -11 -9 16 7 9 -9 -4 21 7 6 -5 -1 1 8 22 22 -2 3 8 11 -12 -5 5 8 28 -27 -8 16 7 6 -5 2 21 7 7 -6 1 1 8 24 -24 -1 3 8 30 -30 -4 5 8 18 -19 -7 16 7 10 10 -6 22 7 6 -6 2 1 8 9 -9 0 3 8 14 13 -3 5 8 10 -10 -6 16 7 19 19 -3 22 7 5 5 4 1 8 6 7 1 3 8 18 18 -2 5 8 11 11 -3 16 7 12 -12 -16 0 8 6 -5 5 1 8 7 7 2 3 8 7 6 -1 5 8 27 26 -2 16 7 10 -11 -14 0 8 9 9 6 1 8 5 5 4 3 8 9 -9 1 5 8 18 -17 -1 16 7 5 -4 -13 0 8 17 16 8 1 8 5 -4 5 3 8 11 -11 3 5 8 7 7 0 16 7 7 7 -11 0 8 12 -12 -14 2 8 8 -8 8 3 8 7 6 4 5 8 6 7 1 16 7 11 11 -10 0 8 23 -24 -13 2 8 13 -13 -16 4 8 7 -6 8 5 8 7 -6 2 16 7 7 7 -9 0 8 30 -31 -11 2 8 11 11 -14 4 8 6 6 -13 6 8 9 -8 3 16 7 7 -7 -7 0 8 18 20 -10 2 8 21 21 -13 4 8 6 6 -12 6 8 10 -10 4 16 7 8 -8 -5 0 8 4 3 -9 2 8 8 8 -12 4 8 7 8 -10 6 8 21 22 -7 17 7 8 8 -4 0 8 10 10 -8 2 8 14 -15 -11 4 8 10 -9 -9 6 8 14 14 -5 17 7 11 -11 -3 0 8 29 -30 -7 2 8 21 -22 -10 4 8 23 -23 -8 6 8 13 -14 -4 17 7 8 -7 -2 0 8 11 -13 -6 2 8 7 -6 -9 4 8 6 -7 -7 6 8 19 -20 -1 17 7 7 8 -1 0 8 20 19 -5 2 8 7 -5 -8 4 8 17 16 -6 6 8 14 -16 0 17 7 9 9 0 0 8 35 33 -4 2 8 10 10 -7 4 8 16 16 -5 6 8 6 -6 2 17 7 7 -7 1 0 8 12 11 -3 2 8 33 33 -6 4 8 12 13 -4 6 8 18 20 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 18 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -3 6 8 29 31 0 8 8 20 19 -11 11 8 9 9 1 13 8 7 -7 -5 17 8 7 -7 -2 6 8 13 13 1 8 8 6 6 -9 11 8 11 -10 5 13 8 4 4 -4 17 8 5 -7 -1 6 8 6 -4 2 8 8 12 -13 -8 11 8 13 -14 -13 14 8 7 -7 -1 17 8 8 8 0 6 8 21 -22 3 8 8 13 -13 -7 11 8 8 -9 -10 14 8 7 8 1 17 8 5 -6 1 6 8 9 -10 7 8 8 6 5 -6 11 8 10 9 -9 14 8 5 4 -10 18 8 9 9 2 6 8 13 12 -12 9 8 12 -12 -5 11 8 14 13 -8 14 8 7 -7 -6 18 8 7 -7 3 6 8 11 11 -11 9 8 12 -12 -4 11 8 10 10 -7 14 8 13 -12 -3 18 8 7 7 -14 7 8 10 -9 -9 9 8 17 16 -3 11 8 10 10 -4 14 8 8 7 -2 18 8 5 4 -12 7 8 7 7 -8 9 8 12 13 -2 11 8 6 -6 -3 14 8 17 18 0 18 8 8 -8 -11 7 8 17 16 -7 9 8 8 8 -1 11 8 17 -17 -2 14 8 8 7 -9 19 8 6 -6 -9 7 8 14 -13 -6 9 8 8 -8 1 11 8 14 15 -1 14 8 10 -10 -8 19 8 5 -6 -8 7 8 19 -20 -5 9 8 13 -13 2 11 8 5 5 0 14 8 12 -12 -5 19 8 7 7 -6 7 8 6 6 -4 9 8 15 -16 4 11 8 5 -5 3 14 8 7 6 -1 19 8 5 -5 -5 7 8 29 29 -2 9 8 12 12 -13 12 8 8 7 -12 15 8 7 6 1 19 8 6 5 -4 7 8 26 26 -1 9 8 14 14 -10 12 8 11 -11 -9 15 8 7 -7 -10 20 8 7 -7 -3 7 8 8 8 0 9 8 9 -8 -9 12 8 9 -10 -8 15 8 8 -9 -7 20 8 6 4 -2 7 8 14 -14 1 9 8 18 -17 -8 12 8 6 7 -6 15 8 11 11 -3 20 8 6 -5 -1 7 8 12 -11 2 9 8 11 -10 -7 12 8 13 13 -5 15 8 7 7 0 20 8 6 6 0 7 8 5 -4 5 9 8 7 7 -6 12 8 11 11 -4 15 8 11 12 -5 21 8 5 -5 1 7 8 18 18 -14 10 8 6 -6 -3 12 8 17 -17 -2 15 8 9 -9 -7 22 8 5 -5 2 7 8 7 7 -11 10 8 8 8 -2 12 8 13 -14 -1 15 8 9 -10 2 22 8 5 3 3 7 8 7 -8 -10 10 8 18 20 -1 12 8 8 7 1 15 8 8 7 -17 0 9 5 -4 6 7 8 7 -6 -9 10 8 11 11 0 12 8 15 15 2 15 8 6 5 -14 0 9 15 14 -13 8 8 11 11 -8 10 8 5 -4 3 12 8 8 -8 4 15 8 5 -4 -13 0 9 5 5 -11 8 8 7 -7 -7 10 8 13 -13 4 12 8 5 -5 -8 16 8 7 7 -12 0 9 9 -9 -10 8 8 22 -22 -6 10 8 10 -10 -11 13 8 7 -6 -7 16 8 11 12 -11 0 9 17 -17 -9 8 8 9 -9 -4 10 8 10 11 -9 13 8 6 6 -4 16 8 6 -6 -10 0 9 13 -15 -8 8 8 10 11 -3 10 8 11 11 -8 13 8 13 13 -3 16 8 11 -11 -9 0 9 6 -6 -7 8 8 15 14 -2 10 8 6 6 -6 13 8 6 -6 -2 16 8 5 -7 -8 0 9 34 34 -6 8 8 9 10 -1 10 8 19 -19 -5 13 8 11 -12 -1 16 8 6 6 -7 0 9 21 22 -5 8 8 7 8 0 10 8 22 -22 -4 13 8 13 -14 0 16 8 10 10 -6 0 9 11 12 -4 8 8 19 -18 2 10 8 11 11 -3 13 8 11 -11 3 16 8 7 -7 -4 0 9 14 -14 -3 8 8 27 -27 3 10 8 11 11 -2 13 8 11 12 -8 17 8 6 7 -3 0 9 5 -5 -1 8 8 16 16 4 10 8 6 7 -1 13 8 12 13 -6 17 8 6 -6 -2 0 9 41 41 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 19 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -1 0 9 30 31 -5 2 9 13 14 0 4 9 7 6 -15 7 9 5 -5 -7 9 9 4 4 0 0 9 11 10 -4 2 9 28 27 2 4 9 9 -9 -13 7 9 10 10 -6 9 9 8 -9 1 0 9 9 -9 -2 2 9 35 -36 3 4 9 10 -10 -12 7 9 9 10 -5 9 9 14 -15 2 0 9 12 -11 -1 2 9 31 -32 5 4 9 7 6 -10 7 9 11 -11 -3 9 9 15 15 3 0 9 12 -13 1 2 9 7 7 -16 5 9 7 7 -9 7 9 9 -10 -2 9 9 8 8 4 0 9 7 -6 2 2 9 10 11 -15 5 9 7 7 -6 7 9 15 14 -1 9 9 9 -10 6 0 9 9 8 3 2 9 12 12 -12 5 9 8 -8 -5 7 9 29 28 0 9 9 16 -16 9 0 9 4 -3 5 2 9 8 -7 -10 5 9 14 14 -3 7 9 23 -23 1 9 9 10 -10 -16 1 9 5 4 6 2 9 8 -7 -9 5 9 14 14 -2 7 9 15 -15 4 9 9 8 8 -15 1 9 7 7 9 2 9 4 4 -6 5 9 23 -23 0 7 9 10 10 5 9 9 7 6 -13 1 9 14 -13 -15 3 9 6 -7 -5 5 9 25 -24 1 7 9 11 10 -12 10 9 7 6 -12 1 9 10 -11 -13 3 9 6 7 -3 5 9 18 19 3 7 9 5 -5 -11 10 9 12 12 -10 1 9 13 12 -12 3 9 11 12 -2 5 9 19 19 4 7 9 6 -5 -10 10 9 9 10 -9 1 9 22 22 -10 3 9 12 -12 0 5 9 16 -16 5 7 9 8 -8 -9 10 9 6 -6 -8 1 9 19 20 -9 3 9 8 -8 1 5 9 9 -9 -14 8 9 7 7 -8 10 9 7 -7 -7 1 9 10 -10 -6 3 9 27 27 5 5 9 6 6 -12 8 9 8 -7 -7 10 9 13 -13 -6 1 9 21 -21 -5 3 9 20 20 7 5 9 7 -7 -11 8 9 13 -13 -6 10 9 6 -6 -5 1 9 21 -21 -4 3 9 7 -6 -15 6 9 7 -6 -10 8 9 6 -7 -5 10 9 5 5 -4 1 9 6 -5 -3 3 9 25 -24 -14 6 9 10 -10 -9 8 9 6 5 -4 10 9 12 13 -3 1 9 18 20 -2 3 9 23 -21 -11 6 9 13 14 -8 8 9 6 5 -2 10 9 18 -18 -2 1 9 18 17 -1 3 9 9 9 -10 6 9 7 8 -6 8 9 10 9 -1 10 9 24 -23 -1 1 9 11 -11 0 3 9 18 18 -9 6 9 6 -6 -5 8 9 8 -8 1 10 9 8 7 0 1 9 21 -21 4 3 9 12 -12 -8 6 9 15 -16 -4 8 9 25 -25 2 10 9 11 11 1 1 9 7 -8 5 3 9 7 -7 -7 6 9 10 -8 -2 8 9 27 27 3 10 9 9 9 4 1 9 9 9 7 3 9 8 7 -6 6 9 13 -14 -1 8 9 21 20 6 10 9 5 -4 5 1 9 11 10 -14 4 9 8 8 -5 6 9 11 12 0 8 9 8 8 -13 11 9 6 5 7 1 9 6 -6 -11 4 9 14 -14 -4 6 9 27 27 2 8 9 13 -13 -12 11 9 8 8 -14 2 9 11 -11 -9 4 9 11 11 -3 6 9 8 8 3 8 9 8 -8 -10 11 9 8 -9 -13 2 9 9 -9 -8 4 9 9 9 -2 6 9 24 -24 6 8 9 7 7 -9 11 9 12 -12 -12 2 9 9 9 -7 4 9 12 13 -1 6 9 23 -23 -13 9 9 6 -6 -8 11 9 7 -8 -11 2 9 14 13 -5 4 9 17 -16 0 6 9 15 -15 -12 9 9 6 -7 -6 11 9 17 16 -10 2 9 11 12 -4 4 9 28 -28 2 6 9 10 10 -10 9 9 13 13 -5 11 9 11 11 -8 2 9 10 -10 -2 4 9 28 28 3 6 9 8 8 -9 9 9 10 10 -3 11 9 10 -8 -7 2 9 15 -13 -1 4 9 34 34 6 6 9 8 -7 -8 9 9 8 8 -2 11 9 15 -14 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 20 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC 0 11 9 14 14 -9 15 9 7 -6 -9 0 10 12 12 -12 2 10 16 16 5 3 10 5 4 1 11 9 6 5 -7 15 9 8 8 -8 0 10 29 28 -11 2 10 10 10 6 3 10 6 6 4 11 9 7 -7 -6 15 9 8 9 -7 0 10 6 5 -10 2 10 6 5 -16 4 10 6 5 -14 12 9 9 9 -5 15 9 9 8 -6 0 10 14 -14 -8 2 10 16 -16 -15 4 10 9 9 -11 12 9 11 -11 -3 15 9 11 -11 -5 0 10 28 -27 -7 2 10 7 -7 -14 4 10 5 5 -8 12 9 11 11 -2 15 9 8 -8 -4 0 10 20 -18 -6 2 10 18 18 -12 4 10 11 -11 -7 12 9 9 8 0 15 9 6 6 -3 0 10 13 13 -5 2 10 27 28 -11 4 10 11 -11 -5 12 9 11 -11 -14 16 9 5 4 -2 0 10 21 23 -4 2 10 8 9 -9 4 10 11 10 -4 12 9 13 -13 -7 16 9 5 6 -1 0 10 10 10 -3 2 10 20 -19 -8 4 10 12 12 -3 12 9 7 -7 -5 16 9 7 -7 1 0 10 11 -11 -2 2 10 24 -24 -7 4 10 7 7 -2 12 9 14 14 -4 16 9 10 -10 2 0 10 17 -17 -1 2 10 9 -9 -6 4 10 22 -23 -1 12 9 18 18 -2 16 9 10 9 3 0 10 9 -8 1 2 10 7 6 -5 4 10 30 -30 3 12 9 8 -8 -1 16 9 11 11 4 0 10 5 4 2 2 10 15 15 -4 4 10 8 -8 -13 13 9 7 -7 -12 17 9 6 -5 5 0 10 9 9 3 2 10 7 7 -3 4 10 16 17 -12 13 9 7 -6 -9 17 9 6 7 -14 1 10 10 -9 4 2 10 8 -8 -2 4 10 20 20 -9 13 9 10 9 -6 17 9 7 -8 -13 1 10 9 -10 5 2 10 8 -8 -1 4 10 10 10 -8 13 9 8 7 -5 17 9 5 -6 -12 1 10 5 4 -16 3 10 5 -5 2 4 10 14 -13 -7 13 9 5 -4 -3 17 9 7 6 -11 1 10 10 10 -14 3 10 7 6 4 4 10 8 7 -6 13 9 12 -12 -2 17 9 7 7 -10 1 10 16 16 -13 3 10 7 8 5 4 10 7 6 -5 13 9 11 -11 0 17 9 7 -6 -9 1 10 21 21 -11 3 10 10 -11 -16 5 10 7 6 -3 13 9 14 13 -7 18 9 6 -6 -7 1 10 27 -27 -10 3 10 13 -13 -13 5 10 6 -6 -2 13 9 11 12 -4 18 9 6 6 -6 1 10 26 -27 -9 3 10 11 -10 -12 5 10 5 -5 0 13 9 7 -8 -2 18 9 8 -7 -4 1 10 16 17 -8 3 10 6 -6 -11 5 10 9 9 7 13 9 5 -3 -1 18 9 9 -8 -3 1 10 22 21 -7 3 10 22 22 -10 5 10 15 15 -14 14 9 7 -6 -5 19 9 7 7 -2 1 10 5 4 -6 3 10 22 23 -9 5 10 9 8 -13 14 9 5 -4 -3 19 9 4 -4 -1 1 10 7 -6 -5 3 10 6 -6 -8 5 10 9 -9 -11 14 9 6 6 -2 20 9 5 5 0 1 10 11 -12 -4 3 10 25 -25 -7 5 10 25 -26 -10 14 9 5 4 -16 0 10 6 5 1 1 10 9 -8 -3 3 10 16 -17 -6 5 10 28 -27 -8 14 9 9 -10 -15 0 10 9 8 3 1 10 10 10 -2 3 10 7 -6 -4 5 10 23 23 -7 14 9 8 -8 -14 0 10 5 6 4 1 10 10 9 -1 3 10 8 7 -3 5 10 20 19 -5 14 9 7 7 -13 0 10 11 -11 6 1 10 7 -7 0 3 10 6 5 -2 5 10 7 7 -4 14 9 14 14 -12 0 10 16 -15 -15 2 10 9 -8 1 3 10 8 7 0 5 10 9 -9 -2 14 9 15 -15 -11 0 10 13 -12 -14 2 10 5 -5 3 3 10 9 -9 1 5 10 8 -8 -1 14 9 14 -13 -10 0 10 9 -8 -13 2 10 8 7 4 3 10 8 -8 3 5 10 7 7 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 21 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -15 6 10 9 -9 -7 8 10 6 5 -6 11 10 15 16 -3 14 10 8 -8 -1 0 11 6 7 -12 6 10 13 12 -6 8 10 10 -10 -4 11 10 10 -10 -2 14 10 11 -10 0 0 11 8 -9 -11 6 10 17 17 -5 8 10 25 -26 -3 11 10 13 -12 2 14 10 7 6 1 0 11 13 -14 -9 6 10 12 -13 -3 8 10 21 21 -2 11 10 5 -6 -9 15 10 6 -5 2 0 11 5 -4 -8 6 10 13 -13 -2 8 10 12 13 -1 11 10 5 5 -7 15 10 11 11 3 0 11 8 8 -6 6 10 19 19 -1 8 10 5 5 0 11 10 6 6 -4 15 10 9 -9 4 0 11 10 9 -5 6 10 34 33 2 8 10 12 -12 3 11 10 6 -6 -3 15 10 9 -9 5 0 11 5 4 -4 6 10 11 11 -13 9 10 6 -7 4 11 10 5 -6 4 15 10 6 -3 -14 1 11 11 -11 -3 6 10 17 -18 -11 9 10 8 8 -12 12 10 9 -9 -8 16 10 6 5 -13 1 11 6 -5 -2 6 10 18 -17 -10 9 10 15 14 -11 12 10 10 -9 -6 16 10 6 -7 -12 1 11 5 6 -1 6 10 12 -12 -9 9 10 11 10 -9 12 10 7 6 -5 16 10 9 -9 -11 1 11 12 12 0 6 10 7 -7 -7 9 10 18 -18 -8 12 10 11 11 -2 16 10 9 9 -10 1 11 18 18 1 6 10 7 7 -6 9 10 18 -18 -6 12 10 13 -12 -1 16 10 6 5 -8 1 11 25 -25 2 6 10 12 12 -4 9 10 15 16 -5 12 10 16 -16 -10 17 10 6 6 -7 1 11 20 -21 4 6 10 5 -3 -3 9 10 7 7 -4 12 10 7 -7 -7 17 10 7 -7 -5 1 11 6 7 5 6 10 6 -6 0 9 10 6 -6 -3 12 10 7 8 -6 17 10 7 -7 -4 1 11 9 9 -14 7 10 8 7 1 9 10 6 -6 -2 12 10 14 15 -3 17 10 7 7 -3 1 11 8 8 -13 7 10 9 9 3 9 10 7 7 -1 12 10 9 10 -11 18 10 5 5 -1 1 11 10 -10 -11 7 10 8 -9 4 9 10 7 6 2 12 10 8 -8 -5 18 10 8 8 0 1 11 12 -11 -10 7 10 18 -18 -15 10 10 6 -6 -10 13 10 5 6 -6 19 10 8 8 2 1 11 12 11 -9 7 10 13 -13 -12 10 10 10 10 -9 13 10 10 10 -3 20 10 5 4 3 1 11 9 9 -7 7 10 18 18 -11 10 10 11 10 -7 13 10 13 -13 -16 0 11 7 6 -16 2 11 7 -7 -6 7 10 22 23 -9 10 10 9 -9 -6 13 10 14 -14 -15 0 11 9 9 -15 2 11 7 -7 -4 7 10 25 -25 -8 10 10 13 -13 -4 13 10 11 11 -13 0 11 13 -13 -13 2 11 11 11 -3 7 10 16 -16 -6 10 10 12 12 -3 13 10 13 13 -12 0 11 15 -14 -12 2 11 13 13 0 7 10 9 9 -5 10 10 17 17 0 13 10 6 -6 -11 0 11 8 -7 -11 2 11 7 6 1 7 10 9 9 -3 10 10 10 -10 1 13 10 5 -5 -10 0 11 9 9 -10 2 11 7 -7 3 7 10 6 -6 -2 10 10 13 -13 3 13 10 5 5 -9 0 11 27 26 -9 2 11 19 -19 4 7 10 6 -6 1 10 10 7 7 -14 14 10 5 -4 -8 0 11 8 8 -8 2 11 12 -13 -15 8 10 6 6 2 10 10 10 10 -12 14 10 6 5 -7 0 11 15 -16 -7 2 11 12 12 -12 8 10 12 -12 -11 11 10 7 -7 -8 14 10 9 -9 -6 0 11 16 -16 -6 2 11 15 16 -11 8 10 13 -13 -10 11 10 11 -11 -6 14 10 8 8 -5 0 11 8 -8 -4 2 11 8 -7 -9 8 10 10 10 -9 11 10 12 -11 -5 14 10 14 14 -3 0 11 10 11 -3 2 11 9 -10 -8 8 10 14 13 -7 11 10 17 17 -4 14 10 6 6 -2 0 11 10 10 -2 2 11 11 -12 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 22 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -1 2 11 6 -6 -13 5 11 8 -8 -5 7 11 10 -11 -9 10 11 10 -10 -4 13 11 7 7 1 2 11 13 12 -11 5 11 10 11 -4 7 11 13 -13 -8 10 11 8 -7 0 13 11 6 -6 2 2 11 5 4 -10 5 11 11 11 -1 7 11 8 8 -7 10 11 7 6 2 13 11 6 5 3 2 11 9 -8 -8 5 11 17 -17 0 7 11 14 13 -6 10 11 12 11 -9 14 11 8 -7 4 2 11 9 -8 -7 5 11 18 -19 2 7 11 10 -9 -5 10 11 5 5 -7 14 11 8 8 -14 3 11 9 9 -5 5 11 13 12 -13 8 11 6 -6 -2 10 11 8 -7 -6 14 11 9 9 -13 3 11 8 7 -4 5 11 15 14 -12 8 11 9 -9 0 10 11 4 5 -3 14 11 6 -5 -11 3 11 10 -10 -3 5 11 11 10 -11 8 11 7 -6 1 10 11 8 9 -8 15 11 8 9 -10 3 11 10 -10 -1 5 11 10 -10 -10 8 11 7 7 3 10 11 5 -6 -4 15 11 5 -5 -8 3 11 17 18 0 5 11 12 -11 -9 8 11 14 14 4 10 11 7 -6 -9 16 11 6 6 -7 3 11 23 23 2 5 11 10 9 -8 8 11 10 9 -14 11 11 6 5 -3 16 11 5 5 -5 3 11 9 -10 3 5 11 7 7 -7 8 11 4 -3 -11 11 11 9 -10 -7 17 11 7 -7 -3 3 11 7 -7 -16 6 11 9 -8 -6 8 11 14 -13 -10 11 11 10 -9 -6 18 11 7 7 -1 3 11 9 9 -12 6 11 14 13 -5 8 11 10 -10 -8 11 11 11 11 -7 19 11 7 7 0 3 11 11 10 -11 6 11 9 9 -4 8 11 7 7 -7 11 11 13 14 -14 0 12 5 -5 2 3 11 10 -9 -10 6 11 8 -8 -3 8 11 7 8 -3 11 11 8 -8 -13 0 12 9 -9 3 3 11 8 -8 -9 6 11 15 -15 -2 8 11 5 5 -1 11 11 8 8 -11 0 12 6 5 -16 4 11 11 9 -7 6 11 9 8 -1 8 11 6 6 0 11 11 6 5 -10 0 12 18 17 -15 4 11 7 7 -6 6 11 18 19 1 8 11 13 -12 2 11 11 6 -6 -9 0 12 8 9 -12 4 11 15 -14 -5 6 11 10 11 3 8 11 7 7 -13 12 11 7 -6 -8 0 12 8 -8 -11 4 11 8 -7 -4 6 11 7 -7 4 8 11 6 6 -12 12 11 10 -9 -7 0 12 13 -14 -9 4 11 13 12 -3 6 11 15 -15 -14 9 11 7 -6 -10 12 11 5 5 -6 0 12 11 -11 -8 4 11 7 7 -2 6 11 13 -12 -11 9 11 6 7 -9 12 11 12 12 -5 0 12 8 -7 -7 4 11 10 -11 -1 6 11 10 -10 -10 9 11 9 9 -8 12 11 6 5 -4 0 12 7 7 -6 4 11 19 -20 0 6 11 6 6 -8 9 11 13 -13 -6 12 11 13 -12 -3 0 12 14 14 -5 4 11 6 -5 1 6 11 12 13 -7 9 11 17 -17 -3 12 11 8 8 -2 0 12 6 6 -4 4 11 5 6 3 6 11 8 -7 -4 9 11 6 5 -2 12 11 8 9 -1 0 12 11 -10 -3 4 11 9 10 4 6 11 7 -6 -3 9 11 4 4 0 12 11 5 -5 0 0 12 13 -13 -2 4 11 13 13 -14 7 11 6 7 -1 9 11 5 -5 2 12 11 5 -4 2 0 12 5 5 -1 4 11 6 6 -11 7 11 10 -10 0 9 11 8 -7 3 12 11 5 4 3 0 12 5 4 1 4 11 12 -12 -10 7 11 16 -14 2 9 11 9 9 -14 13 11 7 -7 -15 1 12 5 -5 3 4 11 8 8 -8 7 11 13 14 3 9 11 6 6 -10 13 11 7 6 -14 1 12 5 -4 4 4 11 8 7 -7 7 11 16 16 -12 10 11 10 10 -8 13 11 12 -12 -13 1 12 4 3 -14 5 11 7 -8 -6 7 11 8 7 -11 10 11 6 6 -7 13 11 12 -11 -12 1 12 8 8 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 23 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -11 1 12 10 10 -12 4 12 9 -8 -11 7 12 9 -9 -1 11 12 8 7 -1 0 13 8 -7 -10 1 12 4 4 -11 4 12 7 6 -9 7 12 14 13 -11 12 12 7 6 -15 1 13 6 -6 -9 1 12 14 -15 -10 4 12 8 8 -8 7 12 9 8 -10 12 12 9 9 -14 1 13 4 2 -8 1 12 15 -16 -8 4 12 6 -7 -5 7 12 9 -9 -7 12 12 10 -9 -13 1 13 10 9 -5 1 12 9 9 -7 4 12 12 -12 -4 7 12 7 -7 -6 12 12 6 -6 -12 1 13 6 6 -4 1 12 13 13 -6 4 12 9 -8 -2 7 12 8 8 -3 12 12 9 9 -10 1 13 6 -7 -2 1 12 12 -13 -3 4 12 14 13 -1 7 12 12 12 0 12 12 7 -7 -9 1 13 10 -11 -1 1 12 13 -12 -2 4 12 8 7 1 7 12 9 -9 -11 13 12 5 4 -8 1 13 7 -6 1 1 12 11 10 -1 4 12 7 -7 -13 8 12 7 -7 -9 13 12 7 -7 -5 1 13 9 8 2 1 12 7 6 0 4 12 10 -10 -10 8 12 12 12 -8 13 12 9 -8 -3 1 13 13 -12 3 1 12 4 2 1 4 12 6 -4 -7 8 12 9 -8 -4 13 12 5 6 -2 1 13 10 -9 -16 2 12 6 -5 -14 5 12 6 -5 -6 8 12 9 -9 -2 13 12 7 -7 0 1 13 6 6 -14 2 12 4 4 -12 5 12 8 9 0 8 12 11 -11 -1 13 12 7 -7 4 1 13 5 -3 -13 2 12 9 8 -11 5 12 11 11 -12 9 12 6 7 1 13 12 6 4 -14 2 13 8 8 -11 2 12 5 -5 -9 5 12 10 -11 -11 9 12 9 9 -7 14 12 6 7 -12 2 13 6 -6 -10 2 12 12 -12 -8 5 12 6 -7 -9 9 12 8 -8 -3 14 12 8 -6 -11 2 13 11 -10 -9 2 12 9 -9 -6 5 12 6 7 -8 9 12 10 -10 -9 15 12 5 4 -10 2 13 5 -6 -7 2 12 13 14 -5 5 12 9 10 -4 9 12 6 6 -8 15 12 6 6 -8 2 13 7 7 -6 2 12 10 9 -4 5 12 12 11 -2 9 12 6 -6 -2 15 12 6 5 -7 2 13 9 9 -5 2 12 5 4 -2 5 12 12 -12 -1 9 12 7 -7 1 15 12 5 -3 -6 2 13 6 6 -3 2 12 13 -12 -1 5 12 13 -12 1 9 12 8 7 -4 16 12 4 3 -4 2 13 11 -11 -1 2 12 8 8 1 5 12 7 7 -13 10 12 7 7 -2 17 12 5 -5 -3 2 13 6 -6 0 2 12 12 12 -16 6 12 6 -5 -11 10 12 7 -6 -15 0 13 5 -5 -2 2 13 6 6 3 2 12 5 -4 -13 6 12 8 8 -10 10 12 10 -10 -14 0 13 8 -7 -1 2 13 6 5 -12 3 12 7 -7 -11 6 12 9 -8 -7 10 12 8 8 -12 0 13 10 9 -13 3 13 7 -7 -11 3 12 10 -10 -10 6 12 15 -15 -6 10 12 7 6 -11 0 13 10 10 -12 3 13 9 -9 -8 3 12 14 14 -8 6 12 8 8 -3 10 12 8 -8 -10 0 13 7 6 -9 3 13 9 9 -5 3 12 7 -7 -7 6 12 9 8 0 10 12 8 7 -9 0 13 6 -6 -8 3 13 8 8 -4 3 12 10 -9 -6 6 12 9 9 -12 11 12 7 -8 -8 0 13 7 -6 -5 3 13 6 -6 -2 3 12 12 13 -4 6 12 9 -9 -11 11 12 7 -7 -7 0 13 10 -9 -3 3 13 12 11 -1 3 12 11 10 -3 6 12 11 -12 -9 11 12 8 8 -6 0 13 6 -6 -2 3 13 10 9 1 3 12 9 -8 -2 6 12 7 -7 -8 11 12 11 10 -4 0 13 14 14 -14 4 13 7 -7 2 3 12 5 -5 0 6 12 13 12 -4 11 12 7 -7 -3 0 13 5 5 -13 4 13 6 -6 -13 4 12 9 -9 -12 7 12 8 -8 -2 11 12 9 10 -2 0 13 6 -5 -11 4 13 11 11 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 24 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -7 4 13 9 -8 -5 8 13 7 6 -13 1 14 7 6 -6 6 14 9 -8 -9 2 15 13 12 -5 4 13 7 6 -4 8 13 10 9 -10 1 14 6 -6 -5 6 14 13 -12 -8 2 15 5 5 -4 4 13 13 13 -13 9 13 6 5 -9 1 14 5 -4 -7 7 14 7 -7 -7 2 15 6 -5 -3 4 13 7 7 -12 9 13 7 8 -7 1 14 11 10 -6 7 14 8 -7 -6 2 15 10 -9 -13 5 13 6 6 -11 9 13 5 4 -6 1 14 8 7 -4 7 14 8 8 -5 2 15 4 -4 -12 5 13 10 10 -9 9 13 8 -7 -4 1 14 10 -10 -1 7 14 4 -3 -14 3 15 7 -6 -11 5 13 5 3 -8 9 13 8 -7 -3 1 14 5 -5 -8 8 14 6 -6 -11 3 15 8 6 -9 5 13 6 -6 -5 9 13 6 6 -1 1 14 5 5 -6 8 14 6 6 -10 3 15 8 8 -8 5 13 6 -5 -3 9 13 8 -7 0 1 14 5 4 -5 8 14 10 10 -8 3 15 11 -9 -6 5 13 6 6 -2 9 13 6 -6 -15 2 14 5 4 -6 9 14 7 6 -7 3 15 6 -6 -5 5 13 8 7 -12 10 13 5 -4 -12 2 14 5 -5 -12 10 14 5 -5 -4 3 15 6 5 -3 5 13 14 -14 -11 10 13 10 -9 -9 2 14 7 7 -8 10 14 7 7 -3 3 15 5 3 -2 5 13 10 -9 -8 10 13 6 5 -8 2 14 12 11 -5 10 14 9 -8 0 3 15 4 -4 0 5 13 5 4 -7 10 13 7 7 -6 2 14 9 -8 -7 11 14 6 -6 -10 4 15 7 -6 -14 6 13 5 5 -4 10 13 8 -8 -5 2 14 12 -11 -5 12 14 7 7 -9 4 15 11 -11 -11 6 13 10 -10 -13 11 13 6 -5 -4 2 14 5 -4 -4 13 14 6 -5 -7 4 15 6 5 -7 6 13 9 9 -9 11 13 7 7 -2 2 14 5 4 -8 16 14 5 -4 -6 4 15 9 8 -6 6 13 5 5 -8 11 13 5 6 -9 3 14 9 8 -13 0 15 5 5 -2 4 15 5 -3 -5 6 13 8 -8 -3 11 13 9 8 -7 3 14 9 -9 -10 0 15 9 -8 1 4 15 5 4 -4 6 13 14 -13 -2 11 13 6 6 -6 3 14 7 -7 -9 0 15 11 -10 -11 5 15 7 -7 -2 6 13 6 5 -7 12 13 7 -6 -4 3 14 8 8 -8 0 15 6 -6 -10 5 15 7 -6 -1 6 13 7 7 -4 12 13 8 8 -3 3 14 7 7 -7 0 15 5 5 -8 5 15 7 7 -12 7 13 6 -7 -3 13 13 7 -6 -12 4 14 6 6 -6 0 15 9 9 -5 5 15 5 -6 -10 7 13 7 7 -4 14 13 7 -6 -8 4 14 9 -8 1 0 15 5 4 -2 5 15 6 1 -9 7 13 8 8 -12 15 13 5 -4 -6 4 14 9 9 -11 1 15 6 -6 -12 6 15 5 -5 -6 7 13 6 -7 -15 0 14 6 -5 -5 4 14 13 11 -10 1 15 9 -8 -10 6 15 8 7 -5 7 13 8 -8 -12 0 14 6 6 -2 4 14 5 -4 -8 1 15 8 8 -9 6 15 8 7 -3 7 13 10 10 -11 0 14 4 4 -13 5 14 6 7 -7 1 15 7 7 -7 6 15 5 -5 -2 7 13 8 7 -9 0 14 8 -8 -7 5 14 8 7 -5 1 15 5 -5 -6 6 15 9 -8 0 7 13 6 -5 -8 0 14 10 -9 -6 5 14 6 6 -4 1 15 5 -4 -11 7 15 7 7 -14 8 13 5 -4 -6 0 14 11 9 -4 5 14 11 -10 -1 1 15 5 4 -10 7 15 7 6 -11 8 13 9 9 -5 0 14 14 13 -3 5 14 7 -6 0 1 15 5 3 -8 7 15 7 -6 -10 8 13 6 7 -3 0 14 6 -5 -12 6 14 6 -5 -13 2 15 5 -4 -7 7 15 6 -6 -7 8 13 9 -8 -14 1 14 6 6 -8 6 14 5 5 -10 2 15 8 7 -10 8 15 9 -8 OBSERVED AND CALCULATED STRUCTURE FACTORS FOR 11ZR(DPM)3CL P21/M PAGE 25 H K L FO FC H K L FO FC H K L FO FC H K L FO FC H K L FO FC -9 8 15 9 -9 -7 0 16 5 5 -2 1 16 5 5 -13 4 16 6 6 -8 0 17 4 2 -6 8 15 8 8 -2 0 16 5 -2 -13 2 16 7 -6 -11 5 16 7 -6 -7 0 17 5 4 -11 9 15 7 -7 -1 0 16 5 3 -11 2 16 5 4 -4 5 16 5 -2 -5 0 17 5 -3 -8 9 15 7 7 -12 1 16 5 -5 -10 2 16 8 7 -10 8 16 6 -5 -4 0 17 4 -4 -7 9 15 6 6 -11 1 16 8 -7 -3 2 16 5 5 -7 8 16 5 4 -6 1 17 5 -4 -9 10 15 9 9 -9 1 16 5 5 -12 3 16 3 5 -11 9 16 5 -5 -5 1 17 6 -5 -8 11 15 6 -6 -8 1 16 5 5 -4 3 16 5 4 -8 9 16 5 4 -11 2 17 5 4 -9 12 15 6 -6 -5 1 16 4 -2 -2 3 16 5 -5 -9 10 16 5 3 -4 2 17 6 5 -10 0 16 9 -8 -4 1 16 5 -3 -1 3 16 5 -4 -11 0 17 4 -4 -5 3 17 6 5 11ZR(DPM)3CL P21/M DEVIATIONS GREATER THAN 2 SIGMA H K L FO FC D/SIGMA 3 0 0 36.40 43.06 5.94 4 0 0 59.28 63.83 4.05 3 1 0 36.13 33.37 2.46 5 1 0 30.20 32.99 2.49 0 2 0 117.57 113.42 3.70 2 2 0 98.38 91.01 6.57 1 3 0 44.56 40.41 3.69 2 3 0 59.82 62.51 2.40 3 3 0 9.56 7.16 2.14 0 4 0 129.95 125.78 3.72 1 4 0 117.24 111.62 5.01 2 4 0 25.95 28.60 2.37 1 5 0 44.80 41.39 3.05 2 5 0 19.01 22.85 3.43 0 6 0 115.24 120.98 5.11 1 6 0 77.65 74.27 3.01 3 6 0 65.42 62.22 2.85 2 7 0 53.93 58.11 3.73 3 7 0 20.48 15.59 4.36 2 8 0 8.01 5.35 2.36 0 10 0 82.42 76.56 5.22 1 10 0 80.51 76.20 3.84 0 14 0 52.18 49.87 2.06 -4 0 1 6.32 1.22 4.54 -2 0 1 41.54 37.44 3.65 0 0 1 105.63 99.92 5.08 1 0 1 103.34 107.73 3.91 2 0 1 33.37 30.36 2.68 -5 1 1 35.43 33.00 2.17 -4 1 1 17.04 20.61 3.18 -1 1 1 43.73 38.91 4.30 0 1 1 77.91 75.31 2.31 1 1 1 13.29 9.83 3.08 2 1 1 21.19 17.24 3.52 -5 2 1 52.40 46.79 5.00 -1 2 1 92.58 88.72 3.44 0 2 1 60.16 52.22 7.07 1 3 1 9.25 3.05 5.53 2 3 1 9.62 11.93 2.06 -2 4 1 18.90 15.03 3.45 -1 4 1 89.00 84.99 3.58 0 4 1 30.66 26.30 3.88 -2 5 1 73.61 69.31 3.83 0 5 1 21.24 14.37 6.12 3 5 1 43.53 40.87 2.38 -4 6 1 92.53 87.11 4.83 -3 6 1 77.74 71.81 5.28 -2 6 1 43.94 38.91 4.48 -1 6 1 84.17 80.71 3.08 -2 7 1 66.39 62.40 3.56 -1 7 1 26.60 22.85 3.34 0 7 1 40.48 35.20 4.71 3 7 1 27.38 29.63 2.01 -5 8 1 28.32 31.47 2.81 -3 8 1 52.41 48.87 3.15 -2 8 1 55.15 52.43 2.42 2 9 1 15.48 19.75 3.80 -1 10 1 72.21 69.20 2.68 1 11 1 23.37 20.41 2.64 -2 12 1 12.16 14.44 2.03 -5 0 2 46.97 53.07 5.43 -4 0 2 11.77 15.69 3.49 0 0 2 172.99 176.50 3.13 2 0 2 13.52 17.14 3.23 3 0 2 39.17 43.10 3.50 -7 1 2 24.52 28.97 3.97 -1 2 2 86.06 82.82 2.89 1 2 2 44.72 48.42 3.29 4 2 2 20.33 23.73 3.03 -3 3 2 3.94 1.45 2.22 -1 3 2 4.14 1.14 2.67 0 3 2 13.76 18.59 4.30 3 3 2 28.00 31.88 3.46 -5 4 2 44.35 47.36 2.68 -4 4 2 68.14 65.32 2.51 -1 4 2 12.01 7.87 3.69 -2 5 2 9.37 5.63 3.34 0 5 2 11.98 8.59 3.02 1 5 2 11.22 17.34 5.45 2 5 2 6.04 3.60 2.17 -2 6 2 63.82 61.53 2.04 0 6 2 9.91 6.62 2.93 -3 7 2 20.66 25.17 4.02 0 7 2 5.22 7.66 2.18 2 7 2 21.87 18.90 2.65 -6 8 2 11.33 9.04 2.04 -2 8 2 28.53 25.44 2.75 0 8 2 21.73 17.41 3.85 -3 9 2 14.05 16.77 2.42 -1 11 2 18.48 16.17 2.06 -5 0 3 36.84 39.69 2.55 0 0 3 72.77 69.48 2.94 1 0 3 52.19 47.88 3.84 3 0 3 24.82 29.00 3.72 4 0 3 47.69 51.44 3.34 -5 1 3 34.79 32.55 2.00 -3 1 3 12.38 17.05 4.16 -2 1 3 15.12 18.97 3.43 -1 1 3 71.42 66.83 4.09 0 1 3 62.56 65.94 3.01 2 1 3 38.47 42.15 3.28 -5 2 3 4.19 7.02 2.52 0 2 3 30.05 32.53 2.21 2 2 3 36.65 40.09 3.07 -1 3 3 4.13 0.82 2.95 1 3 3 22.16 19.09 2.74 1 5 3 22.26 25.61 2.98 -3 6 3 61.64 58.78 2.55 0 6 3 16.13 20.17 3.60 -3 7 3 16.55 10.67 5.24 -1 7 3 24.67 21.21 3.08 1 7 3 13.09 10.05 2.70 2 7 3 39.32 41.88 2.28 3 7 3 31.39 33.80 2.15 -3 8 3 31.30 29.00 2.05 -5 9 3 27.83 25.56 2.02 0 9 3 41.63 38.05 3.19 -8 22 3 5.71 3.42 2.04 -9 0 4 4.68 7.46 2.48 -3 0 4 20.35 27.62 6.48 -1 0 4 91.78 94.54 2.46 0 0 4 58.50 55.23 2.91 3 0 4 36.66 40.99 3.86 0 1 4 42.04 37.69 3.87 1 1 4 52.12 55.21 2.75 -7 2 4 39.43 43.22 3.38 -5 2 4 21.64 18.61 2.71 -4 2 4 5.29 7.94 2.36 -3 2 4 49.48 52.61 2.79 -1 2 4 19.48 22.18 2.41 0 2 4 74.46 76.77 2.06 1 2 4 14.41 10.08 3.86 2 2 4 42.92 38.98 3.52 3 2 4 27.23 30.45 2.87 -2 3 4 43.79 50.24 5.75 1 3 4 63.11 66.16 2.72 -2 4 4 52.30 56.99 4.18 -5 5 4 27.29 24.94 2.10 -3 5 4 24.97 22.56 2.14 -1 6 4 18.61 22.46 3.43 0 6 4 22.01 26.05 3.61 -3 8 4 38.68 36.26 2.16 -2 8 4 30.96 34.36 3.03 1 8 4 16.01 12.73 2.93 -5 9 4 11.70 9.42 2.03 -2 10 4 15.00 17.57 2.29 -5 0 5 28.06 24.15 3.48 -2 0 5 41.80 45.56 3.35 1 0 5 24.73 21.34 3.03 -1 1 5 28.54 26.09 2.19 0 1 5 70.75 75.59 4.31 2 1 5 23.39 20.36 2.70 -3 2 5 54.60 57.70 2.77 -1 2 5 76.77 79.09 2.07 0 2 5 20.30 17.84 2.19 -2 3 5 67.17 64.79 2.12 -7 5 5 9.73 12.04 2.06 -5 5 5 47.85 50.52 2.38 -3 5 5 60.46 63.81 2.99 -6 6 5 22.10 24.52 2.15 -5 6 5 21.07 24.91 3.42 -3 7 5 44.64 49.35 4.20 -2 7 5 31.85 29.50 2.09 -5 9 5 19.39 22.00 2.33 -17 0 6 5.42 2.86 2.29 -8 0 6 56.42 58.83 2.15 -3 0 6 8.18 4.91 2.92 2 0 6 24.70 28.26 3.17 -5 1 6 16.81 20.05 2.89 -4 1 6 20.61 25.86 4.68 0 1 6 17.87 21.26 3.03 -5 2 6 29.11 32.58 3.09 -1 2 6 24.24 21.74 2.23 0 2 6 18.19 14.32 3.44 -3 4 6 25.67 28.56 2.58 -1 4 6 24.04 27.15 2.77 -1 5 6 8.58 5.05 3.14 -4 6 6 37.19 39.47 2.03 -6 0 7 17.70 14.61 2.75 -7 0 8 17.95 20.30 2.09 -2 0 8 10.83 13.45 2.33 8 0 8 4.53 1.11 3.04 0 2 8 21.65 23.94 2.04 -3 6 8 28.73 31.00 2.03 4 15 10 5.75 2.81 2.62 -11 5 13 4.99 2.70 2.04 -2 5 15 5.59 1.05 4.04 -2 0 16 4.65 1.88 2.46